DTA measure 2fázisátalakulás 1.2 Date: 2024116:1015 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1536.12 s Mass = 100.000 mg data_number = 1904 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1885 -4.0767 407.8139 411.8906 410.8865 1.9808 -4.0750 407.8521 411.9270 410.8936 2.7725 -4.0684 407.8938 411.9622 410.8985 3.5945 -4.0738 407.9178 411.9916 410.9018 4.3865 -4.0783 407.9475 412.0258 410.9182 5.2098 -4.0691 407.9809 412.0499 410.9133 6.0045 -4.0544 408.0207 412.0751 410.8892 6.7965 -3.9072 408.0642 411.9714 410.8925 7.6185 -3.8955 408.0821 411.9776 410.8712 8.3805 -3.9143 408.1232 412.0374 410.8736 9.2325 -3.9610 408.1443 412.1053 410.8451 10.0245 -3.9702 408.1848 412.1549 410.8213 10.8165 -3.9785 408.2177 412.1962 410.7830 11.6385 -4.0007 408.2465 412.2472 410.7412 12.4000 -3.9775 408.2899 412.2674 410.6893 13.2520 -3.9779 408.3106 412.2885 410.6359 14.0443 -3.9516 408.3259 412.2775 410.5891 14.8368 -3.9858 408.3662 412.3520 410.5208 15.6590 -3.9409 408.3818 412.3227 410.4604 16.4205 -4.0097 408.4047 412.4144 410.3995 17.2730 -3.1748 408.4396 411.6144 410.3288 18.0703 -3.4784 408.4830 411.9614 410.2560 18.8685 -3.5852 408.5039 412.0891 410.1722 19.6913 -3.7614 408.5280 412.2895 410.0712 20.4535 -3.7856 408.5527 412.3383 409.9752 21.3060 -3.7251 408.5790 412.3041 409.8968 22.0678 -3.7387 408.5967 412.3354 409.7976 22.8898 -3.7502 408.6075 412.3577 409.6950 23.7120 -3.7569 408.6417 412.3987 409.5944 24.4730 -3.7903 408.6776 412.4680 409.4978 25.3210 -3.4651 408.7060 412.1711 409.3828 26.0793 -3.6789 408.7179 412.3968 409.2662 26.8980 -3.8438 408.7346 412.5785 409.1551 27.6868 -3.8139 408.7504 412.5642 409.0360 28.4760 -3.8003 408.7735 412.5738 408.9250 29.3243 -3.6955 408.8143 412.5098 408.7959 30.0823 -3.6642 408.8303 412.4945 408.6917 30.9000 -3.2457 408.8433 412.0890 408.5815 31.7190 -1.5918 408.8885 410.4803 408.4523 32.4770 -2.7909 408.8944 411.6853 408.3503 33.3260 -3.5441 408.8939 412.4379 408.2087 34.0843 -3.7101 408.9041 412.6143 408.0880 34.9038 -3.7607 408.9358 412.6965 407.9717 35.7223 -3.7139 408.9569 412.6708 407.8332 36.4820 -3.7166 408.9748 412.6914 407.6990 37.3318 -3.7128 408.9669 412.6797 407.5925 38.0923 -3.7068 408.9802 412.6870 407.4779 38.9120 -3.6712 409.0047 412.6758 407.3439 39.7310 -3.6803 409.0145 412.6948 407.2088 40.4910 -3.7113 409.0263 412.7376 407.0794 41.3418 -3.7362 409.0584 412.7946 406.9533 42.1328 -3.6732 409.0557 412.7290 406.8327 42.9240 -3.6478 409.0705 412.7183 406.7030 43.7448 -3.7178 409.0909 412.8087 406.5782 44.5065 -3.6699 409.1032 412.7731 406.4724 45.3590 -3.6432 409.1215 412.7646 406.3527 46.1505 -3.7303 409.1248 412.8551 406.2364 46.9425 -3.7529 409.1346 412.8875 406.1087 47.7645 -3.7596 409.1281 412.8877 405.9676 48.5265 -3.7445 409.1187 412.8631 405.8672 49.3785 -3.7342 409.1444 412.8786 405.7782 50.1705 -2.0535 409.1677 411.2212 405.6730 50.9625 -0.9855 409.1762 410.1618 405.5586 51.7845 -1.1338 409.1912 410.3250 405.4322 52.5465 -1.2078 409.1969 410.4046 405.3345 53.3985 -2.9457 409.1538 412.0995 405.2108 54.1905 -3.5043 409.1675 412.6718 405.1050 54.9825 -3.5980 409.1669 412.7649 405.0136 55.8045 -3.5133 409.1768 412.6901 404.9134 56.5665 -3.5706 409.1809 412.7515 404.8098 57.4185 -3.6360 409.1690 412.8050 404.7200 58.2105 -2.4434 409.1939 411.6373 404.6183 59.0095 -3.2090 409.1683 412.3773 404.5334 59.8085 -3.5525 409.1612 412.7137 404.4155 60.6005 -3.6955 409.1760 412.8716 404.3116 61.4220 -3.7239 409.1732 412.8971 404.2108 62.2140 -3.6097 409.1805 412.7901 404.1373 63.0358 -2.5934 409.2070 411.8004 404.0465 63.8283 -3.4368 409.1663 412.6032 403.9385 64.6198 -3.6965 409.1698 412.8662 403.8433 65.4420 -3.6826 409.1670 412.8496 403.7573 66.2340 -3.6567 409.1590 412.8157 403.6605 67.0568 -3.6814 409.1434 412.8249 403.5548 67.8490 -3.6361 409.1350 412.7711 403.4701 68.7010 -3.5469 409.1221 412.6690 403.3624 69.4925 -3.5899 409.1137 412.7036 403.2755 70.3150 -3.6350 409.1226 412.7576 403.1832 71.0765 -3.4460 409.1264 412.5724 403.1069 71.9295 -2.6328 409.1103 411.7430 403.0384 72.7220 -3.4022 409.0935 412.4956 402.9418 73.5145 -3.5588 409.0908 412.6497 402.8655 74.3370 -3.4949 409.0847 412.5795 402.7699 75.0995 -3.5291 409.0794 412.6085 402.6890 75.9518 -3.5051 409.0515 412.5566 402.6007 76.7438 -3.4451 409.0370 412.4822 402.5242 77.5355 -3.5031 409.0314 412.5344 402.4470 78.3575 -3.4864 409.0187 412.5051 402.3543 79.1195 -3.4858 409.0169 412.5028 402.2735 79.9715 -3.5024 408.9941 412.4965 402.1845 80.7635 -3.4986 408.9824 412.4810 402.0933 81.5555 -3.4964 408.9723 412.4687 401.9940 82.3775 -3.4783 408.9713 412.4495 401.9201 83.1395 -3.5044 408.9510 412.4554 401.8227 83.9920 -3.5052 408.9304 412.4355 401.7349 84.7545 -3.4809 408.9151 412.3960 401.6506 85.5773 -3.4993 408.8939 412.3931 401.5598 86.3995 -3.3955 408.8967 412.2922 401.4574 87.1615 -3.4002 408.8888 412.2890 401.3886 88.0133 -3.3323 408.8596 412.1919 401.3018 88.7725 -3.3722 408.8462 412.2185 401.2183 89.5970 -3.3518 408.8219 412.1737 401.1346 90.3700 -3.2842 408.8005 412.0848 401.0172 91.1905 -3.2459 408.7706 412.0165 400.9274 92.0085 -3.2821 408.7598 412.0419 400.8405 92.7665 -3.3338 408.7566 412.0905 400.7474 93.6148 -3.4293 408.7263 412.1557 400.6535 94.3715 -3.4829 408.7116 412.1946 400.5450 95.1903 -3.4676 408.6722 412.1398 400.4650 96.0093 -3.4877 408.6571 412.1449 400.3797 96.7675 -3.5264 408.6435 412.1698 400.2728 97.6160 -3.4758 408.6170 412.0928 400.1775 98.4038 -3.4310 408.5963 412.0274 400.0941 99.1930 -3.4054 408.5743 411.9797 400.0070 100.0110 -3.3597 408.5302 411.8899 399.9163 100.7998 -3.3403 408.5348 411.8752 399.8069 101.6173 -3.3477 408.5036 411.8513 399.7055 102.4063 -3.3478 408.4772 411.8249 399.6164 103.1963 -3.3568 408.4583 411.8151 399.5280 104.0150 -3.3833 408.4388 411.8221 399.4272 104.8045 -3.3200 408.4168 411.7368 399.3382 105.6253 -3.2700 408.3721 411.6421 399.2354 106.4160 -3.3095 408.3613 411.6708 399.1344 107.2070 -3.2976 408.3419 411.6394 399.0464 108.0295 -3.2397 408.3019 411.5416 398.9334 108.7908 -3.2886 408.2905 411.5791 398.8470 109.6440 -3.3188 408.2520 411.5708 398.7666 110.4360 -3.2802 408.2132 411.4934 398.6782 111.2275 -3.3005 408.1962 411.4967 398.5651 112.0500 -3.4227 408.1605 411.5832 398.4680 112.8115 -3.4088 408.1309 411.5397 398.3812 113.6640 -3.4576 408.1052 411.5629 398.2635 114.4258 -3.4333 408.0641 411.4973 398.1713 115.2478 -3.4644 408.0288 411.4932 398.0755 116.0408 -3.4939 408.0018 411.4957 397.9770 116.8345 -3.4822 407.9824 411.4646 397.8614 117.6870 -3.4625 407.9444 411.4068 397.7532 118.4488 -3.4793 407.9129 411.3922 397.6605 119.2708 -3.3927 407.8911 411.2838 397.5553 120.1230 -3.0626 407.8672 410.9298 397.4488 120.9148 -3.2856 407.8388 411.1244 397.3635 121.7065 -2.9087 407.8039 410.7126 397.2539 122.5290 -2.2698 407.7729 410.0427 397.1331 123.3205 -2.9625 407.7187 410.6812 397.0308 124.1428 -3.2645 407.6722 410.9367 396.9338 124.9348 -3.3439 407.6455 410.9894 396.8107 125.7265 -3.3671 407.5968 410.9640 396.7240 126.5488 -3.3858 407.5715 410.9573 396.6354 127.3405 -3.3615 407.5556 410.9171 396.5158 128.1625 -3.3712 407.5155 410.8866 396.4075 128.9545 -3.3788 407.4935 410.8723 396.3088 129.7473 -3.3741 407.4492 410.8233 396.1996 130.5695 -3.3594 407.4003 410.7597 396.1046 131.3615 -3.2465 407.3475 410.5939 395.9982 132.1835 -3.2674 407.3049 410.5723 395.8927 132.9755 -3.2595 407.2714 410.5309 395.7917 133.7675 -3.2041 407.2399 410.4440 395.6968 134.6195 -3.1469 407.1934 410.3403 395.5691 135.3815 -3.0946 407.1729 410.2675 395.4773 136.2035 -3.0337 407.1453 410.1790 395.3827 136.9955 -2.9750 407.0889 410.0639 395.3056 137.7875 -2.9815 407.0330 410.0145 395.1965 138.6395 -3.0509 406.9994 410.0503 395.0779 139.4013 -3.0515 406.9653 410.0168 394.9906 140.2233 -3.0579 406.9254 409.9833 394.8768 141.0150 -3.0034 406.8728 409.8761 394.7851 141.8075 -3.0565 406.8332 409.8897 394.6904 142.6600 -3.1444 406.8107 409.9552 394.5761 143.4218 -3.1124 406.7488 409.8613 394.4823 144.2438 -2.9657 406.7155 409.6812 394.3720 145.0663 -2.9451 406.6705 409.6156 394.2959 145.8285 -2.9498 406.6159 409.5656 394.1968 146.6815 -2.7895 406.5749 409.3644 394.0871 147.4438 -2.7705 406.5378 409.3083 394.0160 148.2658 -2.7801 406.4986 409.2787 393.9081 149.0883 -2.4478 406.4409 408.8887 393.8091 149.8505 -2.8700 406.3971 409.2671 393.7235 150.7028 -3.0744 406.3624 409.4368 393.6014 151.4690 -3.0606 406.3274 409.3880 393.5138 152.2935 -2.8926 406.2740 409.1665 393.4178 153.0855 -2.9938 406.2168 409.2106 393.3331 153.8750 -2.9959 406.1710 409.1669 393.2434 154.7230 -3.0406 406.1266 409.1672 393.1456 155.4810 -3.1484 406.0813 409.2297 393.0549 156.2990 -3.1199 406.0326 409.1525 392.9590 157.0870 -3.1107 405.9894 409.1001 392.8419 157.8750 -3.0968 405.9326 409.0294 392.7585 158.7230 -3.1598 405.8888 409.0486 392.6533 159.4810 -3.1744 405.8350 409.0094 392.5625 160.3000 -3.1060 405.7761 408.8821 392.4729 161.0880 -3.0001 405.7257 408.7258 392.3819 161.8760 -3.0944 405.6719 408.7663 392.2835 162.7245 -2.9948 405.6124 408.6072 392.1596 163.4830 -3.0258 405.5609 408.5868 392.0706 164.3018 -3.1425 405.5243 408.6668 391.9692 165.1203 -2.8300 405.4785 408.3085 391.8675 165.8800 -3.0390 405.4260 408.4650 391.7821 166.7295 -3.1110 405.3783 408.4893 391.6695 167.5180 -3.0823 405.3279 408.4102 391.5868 168.3078 -2.9788 405.2810 408.2598 391.4744 169.1278 -2.9277 405.2159 408.1436 391.3767 169.8880 -2.8598 405.1667 408.0265 391.2761 170.7385 -2.9573 405.1118 408.0690 391.1963 171.5305 -3.0208 405.0709 408.0916 391.0826 172.3225 -3.0827 405.0085 408.0912 390.9945 173.1445 -3.0819 404.9480 408.0299 390.8846 173.9065 -3.1236 404.8926 408.0162 390.7923 174.7585 -3.1938 404.8567 408.0505 390.6943 175.5240 -3.2394 404.7934 408.0328 390.6051 176.3465 -3.2465 404.7385 407.9851 390.4955 177.1385 -3.2390 404.6812 407.9202 390.3969 177.9305 -3.2418 404.6131 407.8549 390.3023 178.7825 -3.2495 404.5657 407.8152 390.2007 179.5445 -3.2513 404.5259 407.7772 390.1134 180.3665 -3.2493 404.4707 407.7200 390.0240 181.1585 -3.2452 404.4109 407.6561 389.9111 181.9505 -3.2416 404.3559 407.5976 389.8317 182.8025 -3.2369 404.2757 407.5126 389.7161 183.5645 -3.2334 404.2380 407.4714 389.6053 184.3865 -3.2317 404.1749 407.4066 389.5101 185.1785 -3.2260 404.1301 407.3560 389.4205 185.9705 -3.2246 404.0822 407.3068 389.3192 186.8223 -3.2193 404.0229 407.2422 389.2102 187.5843 -3.2182 403.9549 407.1731 389.1340 188.4058 -3.2188 403.8954 407.1143 389.0158 189.2285 -3.2161 403.8149 407.0310 388.9070 189.9898 -3.2110 403.7548 406.9658 388.8041 190.8420 -3.2122 403.7012 406.9135 388.7066 191.6038 -3.2139 403.6480 406.8619 388.6064 192.4258 -3.2169 403.6037 406.8206 388.4906 193.2480 -3.2156 403.5216 406.7372 388.3771 194.0095 -3.2165 403.4602 406.6767 388.2774 194.8620 -3.2119 403.3936 406.6055 388.1699 195.6238 -3.2058 403.3268 406.5326 388.0747 196.4458 -3.2032 403.2672 406.4705 387.9766 197.2680 -3.2004 403.2318 406.4322 387.8734 198.0295 -3.1983 403.1654 406.3636 387.7623 198.8820 -3.1944 403.1077 406.3021 387.6571 199.6438 -3.1910 403.0499 406.2408 387.5330 200.4658 -3.1905 402.9705 406.1611 387.4319 201.2878 -3.1864 402.9214 406.1078 387.3362 202.0495 -3.1854 402.8558 406.0413 387.2525 202.9023 -3.1793 402.7827 405.9620 387.1339 203.6645 -3.1796 402.7384 405.9180 387.0242 204.4868 -3.1778 402.6737 405.8515 386.9117 205.3090 -3.1690 402.6023 405.7714 386.7916 206.0715 -3.1684 402.5391 405.7074 386.7124 206.9240 -3.1711 402.4748 405.6459 386.5988 207.6865 -3.1629 402.4065 405.5694 386.4963 208.5085 -3.1336 402.3349 405.4685 386.4074 209.3005 -3.1215 402.2872 405.4087 386.2889 210.0925 -3.1149 402.2350 405.3499 386.1828 210.9445 -3.1113 402.1603 405.2716 386.0842 211.7065 -3.1062 402.0840 405.1903 385.9795 212.5295 -3.1073 402.0246 405.1318 385.8754 213.3215 -3.1010 401.9454 405.0464 385.7651 214.1135 -3.0941 401.8662 404.9603 385.6730 214.9660 -3.0913 401.8081 404.8994 385.5704 215.7285 -3.0887 401.7450 404.8337 385.4717 216.5508 -3.0866 401.6750 404.7616 385.3586 217.3430 -3.0886 401.6112 404.6999 385.2625 218.1310 -3.0894 401.5641 404.6534 385.1604 218.9498 -3.0891 401.5103 404.5994 385.0559 219.7070 -3.0853 401.4440 404.5293 384.9605 220.5540 -3.0827 401.3584 404.4410 384.8479 221.3438 -3.0769 401.2914 404.3682 384.7776 222.1323 -3.0755 401.2443 404.3198 384.6721 222.9510 -3.0758 401.1578 404.2336 384.5464 223.7093 -3.0719 401.0888 404.1607 384.4567 224.5583 -3.0707 401.0180 404.0887 384.3587 225.3468 -3.0677 400.9688 404.0364 384.2562 226.1345 -3.0649 400.8880 403.9529 384.1660 226.9528 -3.0593 400.8056 403.8648 384.0633 227.7110 -3.0557 400.7404 403.7961 383.9764 228.5598 -3.0517 400.6572 403.7089 383.8595 229.3488 -3.0502 400.5893 403.6395 383.7654 230.1373 -3.0486 400.5285 403.5771 383.6954 230.9558 -3.0404 400.4562 403.4965 383.5909 231.7443 -3.0373 400.3930 403.4304 383.5083 232.5643 -3.0377 400.3200 403.3577 383.3940 233.3143 -3.0342 400.2533 403.2875 383.3057 234.1728 -3.0307 400.1914 403.2220 383.1954 234.9633 -3.0294 400.1102 403.1396 383.1053 235.7523 -3.0266 400.0449 403.0715 383.0266 236.5740 -3.0274 399.9558 402.9832 382.9320 237.3355 -3.0269 399.8970 402.9238 382.8225 238.1880 -3.0222 399.8261 402.8484 382.7199 238.9498 -3.0167 399.7569 402.7736 382.6439 239.7718 -3.0120 399.6864 402.6984 382.5383 240.5940 -3.0093 399.6148 402.6240 382.4350 241.3555 -3.0094 399.5596 402.5690 382.3451 242.2080 -3.0054 399.4748 402.4803 382.2571 242.9698 -3.0034 399.4039 402.4073 382.1645 243.7918 -2.9955 399.3179 402.3134 382.0737 244.6140 -2.9927 399.2648 402.2574 381.9625 245.3755 -2.9911 399.2016 402.1927 381.8569 246.2280 -2.9881 399.1042 402.0923 381.7535 246.9898 -2.9876 399.0622 402.0498 381.6630 247.8118 -2.9832 398.9662 401.9494 381.5750 248.6038 -2.9800 398.8986 401.8787 381.4590 249.3955 -2.9701 398.8281 401.7981 381.3628 250.2478 -2.9583 398.7517 401.7099 381.2379 251.0095 -2.9585 398.6815 401.6400 381.1414 251.8318 -2.9659 398.5894 401.5554 381.0494 252.6238 -2.9659 398.5166 401.4825 380.9374 253.4155 -2.9667 398.4452 401.4120 380.8551 254.2675 -2.9534 398.3718 401.3253 380.7444 255.0295 -2.9503 398.3024 401.2527 380.6653 255.8515 -2.9471 398.2032 401.1503 380.5666 256.6435 -2.9438 398.1381 401.0819 380.4706 257.4355 -2.9379 398.0606 400.9985 380.3517 258.2875 -2.9333 397.9862 400.9195 380.2553 259.0495 -2.9308 397.9268 400.8576 380.1589 259.8715 -2.9287 397.8532 400.7819 380.0582 260.6935 -2.9242 397.7606 400.6848 379.9621 261.4555 -2.9217 397.7069 400.6286 379.8688 262.3075 -2.9226 397.6220 400.5446 379.7639 263.0695 -2.9272 397.5611 400.4883 379.6555 263.8915 -2.9298 397.4651 400.3949 379.5508 264.7138 -2.9271 397.3771 400.3042 379.4499 265.4760 -2.9257 397.3119 400.2376 379.3521 266.3285 -2.9204 397.2439 400.1644 379.2566 267.0905 -2.9168 397.1859 400.1027 379.1692 267.9118 -2.9130 397.0913 400.0043 379.0600 268.7343 -2.9107 397.0097 399.9205 378.9727 269.4965 -2.9116 396.9344 399.8459 378.8797 270.3493 -2.9034 396.8620 399.7654 378.7719 271.1420 -2.9004 396.7809 399.6813 378.6842 271.9345 -2.9012 396.7128 399.6140 378.5897 272.7570 -2.8973 396.6322 399.5295 378.4702 273.5185 -2.8952 396.5625 399.4577 378.3804 274.3710 -2.8940 396.4729 399.3668 378.2703 275.1630 -2.8891 396.3938 399.2829 378.1948 275.9565 -2.8869 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