DTA measure 1pb3prog Test Date: 20231011:1425 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1018.94 s Mass = 1452.300 mg data_number = 1269 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2240 0.1976 268.8862 268.6886 267.8002 1.9853 0.1966 268.8925 268.6959 267.8095 2.8365 0.1975 268.8934 268.6959 267.8086 3.6260 0.1963 268.8945 268.6981 267.8031 4.4168 0.1964 268.8906 268.6941 267.8035 5.2388 0.1956 268.8981 268.7025 267.8115 5.9995 0.1962 268.8977 268.7015 267.8116 6.8515 0.1988 268.9056 268.7068 267.8084 7.6410 0.1989 268.9041 268.7053 267.8130 8.4313 0.1969 268.8937 268.6967 267.8212 9.2528 0.1945 268.8909 268.6964 267.8334 10.0135 0.1952 268.8908 268.6956 267.8477 10.8653 0.1962 268.8929 268.6967 267.8746 11.6565 0.1952 268.9001 268.7050 267.9100 12.4485 0.1941 268.8974 268.7033 267.9376 13.2705 0.1957 268.8970 268.7013 267.9796 14.0325 0.1934 268.8845 268.6911 268.0301 14.8843 0.1926 268.8981 268.7055 268.0664 15.6755 0.1900 268.8936 268.7035 268.1239 16.4680 0.1896 268.8770 268.6874 268.1899 17.2910 0.1896 268.8913 268.7018 268.2481 18.0520 0.1904 268.9092 268.7189 268.3178 18.9033 0.1902 268.8986 268.7084 268.4016 19.6635 0.1855 268.8898 268.7042 268.4897 20.4848 0.1850 268.8899 268.7049 268.5795 21.3055 0.1854 268.9056 268.7201 268.6762 22.0663 0.1840 268.9112 268.7272 268.7929 22.9165 0.1864 268.9033 268.7170 268.8853 23.7058 0.1839 268.9010 268.7171 269.0042 24.4968 0.1824 268.8970 268.7146 269.1246 25.3173 0.1828 268.9107 268.7279 269.2546 26.0770 0.1816 268.9014 268.7198 269.3816 26.9288 0.1779 268.9088 268.7309 269.5304 27.7200 0.1749 268.8983 268.7234 269.6584 28.5103 0.1736 268.9118 268.7382 269.8211 29.3308 0.1703 268.9204 268.7501 269.9779 30.1205 0.1692 268.9269 268.7577 270.1089 30.9418 0.1682 268.9345 268.7663 270.2706 31.7325 0.1689 268.9342 268.7653 270.4502 32.5233 0.1644 268.9348 268.7704 270.5851 33.3448 0.1640 268.9472 268.7831 270.7640 34.1343 0.1671 268.9507 268.7836 270.9354 34.9555 0.1618 268.9574 268.7956 271.1110 35.7460 0.1539 268.9766 268.8227 271.2673 36.5373 0.1477 268.9673 268.8196 271.4431 37.3570 0.1457 268.9704 268.8247 271.6317 38.1185 0.1428 268.9662 268.8234 271.7900 38.9695 0.1389 268.9960 268.8571 271.9781 39.7598 0.1369 269.0016 268.8647 272.1592 40.5518 0.1299 269.0085 268.8786 272.3324 41.3735 0.1265 269.0142 268.8877 272.5174 42.1355 0.1252 269.0304 268.9052 272.6788 42.9868 0.1172 269.0433 268.9260 272.8589 43.7478 0.1106 269.0638 268.9533 273.0325 44.5688 0.1096 269.0572 268.9476 273.1990 45.3895 0.1031 269.0767 268.9736 273.3717 46.1513 0.0989 269.0778 268.9789 273.5251 47.0023 0.0972 269.0915 268.9943 273.7068 47.7625 0.0902 269.1190 269.0288 273.8739 48.5838 0.0774 269.1261 269.0487 274.0445 49.3733 0.0662 269.1147 269.0485 274.1853 50.1638 0.0595 269.1341 269.0746 274.3434 51.0145 0.0538 269.1435 269.0897 274.5032 51.7758 0.0477 269.1759 269.1282 274.6543 52.5950 0.0436 269.1889 269.1453 274.8116 53.3850 0.0405 269.2196 269.1792 274.9406 54.1753 0.0351 269.2382 269.2032 275.1013 55.0268 0.0253 269.2523 269.2271 275.2411 55.7885 0.0186 269.2753 269.2567 275.3799 56.6090 0.0155 269.2984 269.2829 275.5002 57.4028 0.0083 269.3063 269.2980 275.6327 58.1983 0.0020 269.3084 269.3064 275.7581 59.0198 -0.0006 269.3331 269.3337 275.8727 59.7810 -0.0089 269.3589 269.3678 276.0107 60.6328 -0.0138 269.3793 269.3931 276.1491 61.4243 -0.0199 269.3928 269.4127 276.2553 62.2165 -0.0260 269.4175 269.4435 276.3604 63.0375 -0.0309 269.4559 269.4868 276.4773 63.7990 -0.0406 269.4588 269.4995 276.5919 64.6503 -0.0467 269.4700 269.5166 276.7095 65.4108 -0.0530 269.4939 269.5469 276.8093 66.2310 -0.0594 269.5279 269.5873 276.9302 67.0525 -0.0620 269.5534 269.6154 277.0336 67.8153 -0.0709 269.5619 269.6328 277.1163 68.6735 -0.0789 269.5715 269.6504 277.2289 69.4350 -0.0850 269.6019 269.6869 277.3274 70.2553 -0.0866 269.6288 269.7154 277.4445 71.0465 -0.0881 269.6537 269.7418 277.5486 71.8370 -0.1036 269.6808 269.7845 277.6391 72.6865 -0.1068 269.7047 269.8115 277.7357 73.4460 -0.1050 269.7226 269.8276 277.8356 74.2665 -0.1094 269.7612 269.8705 277.9287 75.0575 -0.1209 269.7804 269.9013 278.0450 75.8485 -0.1337 269.8201 269.9538 278.1325 76.6988 -0.1433 269.8168 269.9601 278.2512 77.4595 -0.1521 269.8638 270.0158 278.3553 78.2808 -0.1602 269.8893 270.0495 278.4328 79.0725 -0.1665 269.9101 270.0766 278.5215 79.8620 -0.1713 269.9333 270.1046 278.6518 80.7128 -0.1789 269.9581 270.1370 278.7601 81.4738 -0.1831 269.9852 270.1683 278.8704 82.2953 -0.1888 270.0229 270.2117 278.9803 83.0860 -0.1937 270.0411 270.2348 279.0916 83.8760 -0.2032 270.0735 270.2767 279.1935 84.7268 -0.2073 270.0987 270.3059 279.3112 85.4885 -0.2112 270.1433 270.3545 279.4161 86.3103 -0.2187 270.1524 270.3710 279.5312 87.1008 -0.2245 270.1891 270.4135 279.6422 87.8920 -0.2304 270.2214 270.4519 279.7662 88.7138 -0.2369 270.2520 270.4889 279.9057 89.5055 -0.2429 270.2778 270.5207 280.0316 90.3270 -0.2497 270.3233 270.5730 280.1455 91.1185 -0.2566 270.3423 270.5989 280.2886 91.9100 -0.2648 270.3868 270.6516 280.3851 92.7315 -0.2718 270.4032 270.6750 280.5257 93.4913 -0.2792 270.4145 270.6937 280.6569 94.3423 -0.2852 270.4618 270.7469 280.8034 95.1325 -0.2913 270.5085 270.7998 280.9496 95.9235 -0.2966 270.5454 270.8421 281.0662 96.7445 -0.3031 270.5885 270.8917 281.2131 97.5048 -0.3087 270.6344 270.9431 281.3423 98.3563 -0.3156 270.6545 270.9700 281.4857 99.1458 -0.3236 270.6850 271.0086 281.6423 99.9373 -0.3299 270.7351 271.0650 281.7614 100.7585 -0.3374 270.7548 271.0922 281.9203 101.5483 -0.3438 270.7903 271.1341 282.0666 102.3690 -0.3526 270.8358 271.1883 282.1910 103.1605 -0.3593 270.8774 271.2367 282.3291 103.9525 -0.3661 270.9106 271.2767 282.4804 104.7733 -0.3736 270.9318 271.3054 282.6310 105.5638 -0.3801 270.9700 271.3501 282.7600 106.3843 -0.3882 271.0278 271.4160 282.9196 107.1750 -0.3959 271.0632 271.4591 283.0816 107.9663 -0.4025 271.1064 271.5088 283.2187 108.7883 -0.4104 271.1501 271.5605 283.3603 109.5773 -0.4172 271.1907 271.6080 283.4922 110.3988 -0.4259 271.2399 271.6658 283.6433 111.1900 -0.4300 271.2686 271.6985 283.7740 111.9803 -0.4388 271.3094 271.7483 283.9290 112.8018 -0.4471 271.3432 271.7904 284.0628 113.5913 -0.4529 271.3940 271.8469 284.1983 114.4128 -0.4624 271.4426 271.9050 284.3571 115.2043 -0.4682 271.4769 271.9451 284.4941 115.9953 -0.4750 271.5343 272.0094 284.6329 116.8165 -0.4837 271.5591 272.0427 284.7759 117.6085 -0.4911 271.6069 272.0981 284.9215 118.4308 -0.4979 271.6663 272.1642 285.0661 119.2218 -0.5078 271.7066 272.2144 285.2017 120.0135 -0.5154 271.7484 272.2638 285.3435 120.8355 -0.5236 271.7857 272.3094 285.4800 121.6260 -0.5299 271.8437 272.3736 285.6077 122.4473 -0.5386 271.8943 272.4329 285.7474 123.2375 -0.5445 271.9448 272.4894 285.8661 124.0293 -0.5526 271.9771 272.5297 286.0044 124.8505 -0.5617 272.0425 272.6042 286.1159 125.6410 -0.5708 272.0905 272.6613 286.2447 126.4618 -0.5788 272.1433 272.7221 286.3838 127.2525 -0.5867 272.1799 272.7666 286.5030 128.0435 -0.5909 272.2349 272.8259 286.6180 128.8943 -0.6020 272.2900 272.8920 286.7436 129.6588 -0.6063 272.3483 272.9546 286.8672 130.4805 -0.6129 272.4118 273.0247 286.9808 131.2725 -0.6227 272.4371 273.0598 287.0947 132.0620 -0.6321 272.4954 273.1275 287.2354 132.9130 -0.6383 272.5471 273.1854 287.3506 133.6730 -0.6426 272.6067 273.2493 287.4427 134.4945 -0.6520 272.6546 273.3066 287.5636 135.2855 -0.6604 272.7052 273.3655 287.6842 136.0753 -0.6684 272.7337 273.4021 287.7982 136.9268 -0.6760 272.8190 273.4951 287.9202 137.6885 -0.6817 272.8638 273.5456 288.0151 138.5108 -0.6878 272.9248 273.6125 288.1301 139.3018 -0.6957 272.9817 273.6774 288.2689 140.0928 -0.7030 273.0391 273.7421 288.3683 140.9438 -0.7114 273.0975 273.8089 288.4864 141.7043 -0.7169 273.1455 273.8624 288.5883 142.5258 -0.7219 273.1994 273.9213 288.7063 143.3175 -0.7319 273.2490 273.9809 288.8356 144.1080 -0.7431 273.3073 274.0504 288.9675 144.9583 -0.7496 273.4010 274.1507 289.0874 145.7190 -0.7555 273.4206 274.1761 289.1922 146.5405 -0.7631 273.4813 274.2444 289.3060 147.3315 -0.7713 273.5247 274.2960 289.4240 148.1233 -0.7792 273.6029 274.3821 289.5412 148.9745 -0.7846 273.6605 274.4450 289.6702 149.7100 -0.7906 273.7159 274.5065 289.7881 150.5705 -0.7903 273.8527 274.6430 289.9927 151.3598 -0.7942 273.9277 274.7219 290.1414 152.1513 -0.7988 273.9781 274.7768 290.2637 152.9725 -0.8023 274.0484 274.8507 290.3813 153.7340 -0.8083 274.1082 274.9165 290.5153 154.5853 -0.8175 274.1670 274.9846 290.6555 155.3748 -0.8278 274.2099 275.0376 290.7667 156.1653 -0.8387 274.2355 275.0742 290.8781 156.9865 -0.8497 274.2822 275.1320 290.9814 157.7470 -0.8599 274.3264 275.1863 291.1009 158.5970 -0.8643 274.3920 275.2562 291.2323 159.3863 -0.8725 274.4478 275.3204 291.3451 160.1773 -0.8812 274.5057 275.3869 291.4868 160.9983 -0.8908 274.5772 275.4680 291.6260 161.7593 -0.8960 274.6406 275.5367 291.7511 162.6108 -0.9051 274.6971 275.6022 291.9016 163.4000 -0.9109 274.7514 275.6623 292.0412 164.1915 -0.9178 274.8279 275.7457 292.1642 165.0130 -0.9264 274.8771 275.8035 292.3022 165.7745 -0.9353 274.9451 275.8804 292.4125 166.6268 -0.9398 275.0183 275.9581 292.5519 167.3868 -0.9482 275.0890 276.0372 292.6803 168.2080 -0.9540 275.1407 276.0948 292.8315 169.0288 -0.9598 275.2068 276.1666 292.9860 169.7900 -0.9676 275.2840 276.2517 293.1106 170.6415 -0.9742 275.3484 276.3226 293.2495 171.4030 -0.9812 275.3984 276.3796 293.3650 172.2240 -0.9903 275.4687 276.4591 293.5038 173.0155 -0.9974 275.5455 276.5429 293.6588 173.8060 -1.0042 275.6283 276.6325 293.7863 174.6565 -1.0111 275.6915 276.7027 293.9327 175.4173 -1.0163 275.7609 276.7772 294.0652 176.2385 -1.0235 275.8310 276.8544 294.2028 177.0295 -1.0319 275.9023 276.9341 294.3384 177.8203 -1.0380 275.9755 277.0135 294.4696 178.6713 -1.0445 276.0271 277.0717 294.6104 179.4303 -1.0530 276.0991 277.1521 294.7524 180.2505 -1.0605 276.1659 277.2264 294.9118 181.0413 -1.0662 276.2393 277.3055 295.0376 181.8310 -1.0726 276.3169 277.3895 295.1584 182.6813 -1.0813 276.3994 277.4807 295.2881 183.4418 -1.0868 276.4718 277.5587 295.4165 184.2623 -1.0928 276.5324 277.6252 295.5660 185.0530 -1.1021 276.6101 277.7122 295.6937 185.8430 -1.1075 276.6884 277.7959 295.8223 186.6653 -1.1155 276.7698 277.8853 295.9719 187.4548 -1.1235 276.8411 277.9646 296.1042 188.2753 -1.1317 276.9096 278.0414 296.2399 189.0665 -1.1388 276.9746 278.1134 296.3634 189.8565 -1.1438 277.0466 278.1903 296.4985 190.6778 -1.1492 277.1190 278.2682 296.6333 191.4683 -1.1564 277.2070 278.3634 296.7527 192.2888 -1.1620 277.2892 278.4512 296.8921 193.0790 -1.1667 277.3495 278.5163 297.0272 193.8698 -1.1732 277.4248 278.5979 297.1505 194.6908 -1.1820 277.5082 278.6902 297.2965 195.4803 -1.1895 277.5785 278.7679 297.4260 196.3015 -1.1943 277.6549 278.8492 297.5549 197.0928 -1.2016 277.7378 278.9394 297.6801 197.8843 -1.2081 277.8275 279.0356 297.7971 198.7055 -1.2170 277.9014 279.1184 297.9267 199.4670 -1.2237 277.9692 279.1929 298.0521 200.3183 -1.2284 278.0499 279.2783 298.2078 201.1078 -1.2349 278.1258 279.3608 298.3288 201.8980 -1.2418 278.2247 279.4665 298.4459 202.7175 -1.2498 278.2927 279.5425 298.5794 203.4790 -1.2560 278.3634 279.6194 298.7051 204.3303 -1.2631 278.4659 279.7290 298.8369 205.1208 -1.2691 278.5487 279.8178 298.9644 205.9113 -1.2762 278.6158 279.8919 299.0904 206.7325 -1.2849 278.6889 279.9738 299.2086 207.4928 -1.2906 278.7594 280.0500 299.3319 208.3443 -1.2980 278.8552 280.1532 299.4682 209.1048 -1.3045 278.9356 280.2401 299.5920 209.9255 -1.3107 279.0053 280.3159 299.7069 210.7465 -1.3144 279.0814 280.3958 299.8404 211.5068 -1.3190 279.1639 280.4828 299.9527 212.3560 -1.3276 279.2605 280.5881 300.0937 213.1453 -1.3357 279.3596 280.6952 300.2055 213.9365 -1.3400 279.4246 280.7647 300.3209 214.7590 -1.3483 279.5159 280.8642 300.4412 215.5205 -1.3556 279.6151 280.9708 300.5578 216.3725 -1.3593 279.6950 281.0542 300.6891 217.1328 -1.3648 279.7737 281.1385 300.8001 217.9548 -1.3717 279.8484 281.2202 300.9287 218.7468 -1.3776 279.9321 281.3097 301.0423 219.5378 -1.3853 280.0128 281.3981 301.1640 220.3893 -1.3922 280.1060 281.4982 301.2956 221.1488 -1.3976 280.1792 281.5768 301.4149 221.9703 -1.4039 280.2574 281.6613 301.5343 222.7615 -1.4119 280.3611 281.7730 301.6676 223.5528 -1.4168 280.4596 281.8764 301.7988 224.4043 -1.4220 280.5379 281.9599 301.9449 225.1648 -1.4263 280.6128 282.0392 302.0580 225.9863 -1.4331 280.7013 282.1344 302.1882 226.7775 -1.4368 280.7995 282.2364 302.3287 227.5688 -1.4463 280.8845 282.3308 302.4423 228.4203 -1.4550 280.9971 282.4522 302.5811 229.1815 -1.4600 281.0678 282.5278 302.7104 230.0033 -1.4657 281.1546 282.6203 302.8393 230.7935 -1.4705 281.2350 282.7055 302.9730 231.5843 -1.4777 281.3172 282.7949 303.0920 232.4353 -1.4841 281.4212 282.9054 303.2469 233.1965 -1.4890 281.5126 283.0016 303.3614 234.0168 -1.4950 281.5883 283.0834 303.4934 234.8365 -1.5025 281.6896 283.1921 303.6309 235.5965 -1.5072 281.7644 283.2716 303.7615 236.4475 -1.5104 281.8591 283.3695 303.9100 237.2088 -1.5163 281.9537 283.4700 304.0225 238.0288 -1.5232 282.0423 283.5655 304.1682 238.8493 -1.5295 282.1223 283.6518 304.3065 239.6093 -1.5374 282.2295 283.7670 304.4423 240.4608 -1.5429 282.3413 283.8842 304.5753 241.2215 -1.5494 282.4412 283.9906 304.6997 242.0433 -1.5542 282.5270 284.0813 304.8218 242.8648 -1.5598 282.6121 284.1718 304.9724 243.6263 -1.5656 282.6845 284.2501 305.1027 244.4778 -1.5714 282.7796 284.3510 305.2322 245.2375 -1.5785 282.8785 284.4570 305.3540 246.0590 -1.5844 282.9662 284.5505 305.4818 246.8798 -1.5900 283.0627 284.6527 305.6299 247.6398 -1.5964 283.1353 284.7317 305.7438 248.4913 -1.6033 283.2499 284.8531 305.8776 249.2810 -1.6092 283.3425 284.9517 306.0244 250.0718 -1.6160 283.4323 285.0484 306.1405 250.8925 -1.6193 283.5411 285.1604 306.2637 251.6535 -1.6271 283.6226 285.2497 306.3830 252.5053 -1.6318 283.7260 285.3578 306.5333 253.2958 -1.6363 283.8157 285.4520 306.6666 254.0875 -1.6450 283.8970 285.5420 306.7890 254.9095 -1.6491 284.0020 285.6511 306.9270 255.6705 -1.6562 284.0857 285.7420 307.0447 256.5223 -1.6619 284.1961 285.8579 307.1807 257.3118 -1.6655 284.2751 285.9406 307.3033 258.1035 -1.6725 284.3835 286.0560 307.4447 258.9255 -1.6811 284.4774 286.1586 307.5923 259.6865 -1.6842 284.5684 286.2526 307.7065 260.5383 -1.6913 284.6731 286.3644 307.8200 261.3295 -1.6971 284.7724 286.4695 307.9450 262.1205 -1.7020 284.8536 286.5556 308.0781 262.9415 -1.7068 284.9688 286.6756 308.2084 263.7025 -1.7115 285.0682 286.7797 308.3315 264.5538 -1.7196 285.1613 286.8808 308.4650 265.3453 -1.7241 285.2594 286.9835 308.5808 266.1360 -1.7308 285.3508 287.0816 308.7210 266.9580 -1.7362 285.4522 287.1884 308.8537 267.7478 -1.7402 285.5444 287.2846 308.9896 268.5688 -1.7456 285.6547 287.4003 309.1271 269.3605 -1.7531 285.7516 287.5047 309.2535 270.1508 -1.7590 285.8489 287.6080 309.3970 270.9728 -1.7621 285.9530 287.7151 309.5124 271.7635 -1.7660 286.0523 287.8183 309.6476 272.5853 -1.7713 286.1461 287.9174 309.7931 273.3765 -1.7756 286.2529 288.0285 309.9324 274.1680 -1.7830 286.3447 288.1277 310.0631 275.0198 -1.7875 286.4489 288.2364 310.1990 275.7805 -1.7948 286.5512 288.3460 310.3209 276.6018 -1.7988 286.6681 288.4670 310.4716 277.3925 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