DTA measure 1pb4prog Test Date: 20231011:1524 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1274.32 s Mass = 1452.300 mg data_number = 1578 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1500 -2.0417 235.9200 237.9617 265.4397 1.9718 -2.0423 236.0506 238.0929 265.4685 2.7318 -2.0418 236.1825 238.2243 265.5090 3.5850 -2.0385 236.3259 238.3644 265.5343 4.3460 -2.0380 236.4415 238.4795 265.5726 5.1680 -2.0396 236.5564 238.5960 265.6236 5.9898 -2.0389 236.7012 238.7401 265.6692 6.7523 -2.0402 236.8183 238.8584 265.7224 7.6035 -2.0387 236.9411 238.9798 265.7648 8.3680 -2.0357 237.0580 239.0937 265.8203 9.1943 -2.0335 237.1978 239.2314 265.8872 9.9853 -2.0349 237.3118 239.3467 265.9476 10.7798 -2.0355 237.4375 239.4730 266.0228 11.6053 -2.0344 237.5623 239.5967 266.1238 12.4898 -2.0353 237.6991 239.7344 266.2236 13.2555 -2.0350 237.8242 239.8592 266.2833 14.0865 -2.0345 237.9493 239.9837 266.3709 14.8555 -2.0331 238.0697 240.1028 266.4643 15.6798 -2.0343 238.2013 240.2356 266.5772 16.4768 -2.0361 238.3232 240.3593 266.6831 17.2670 -2.0366 238.4373 240.4739 266.8007 18.1168 -2.0360 238.5830 240.6191 266.9281 18.8763 -2.0365 238.7081 240.7446 267.0491 19.6975 -2.0379 238.8282 240.8661 267.1752 20.4895 -2.0370 238.9483 240.9853 267.2833 21.2820 -2.0350 239.0677 241.1027 267.4076 22.1035 -2.0352 239.1993 241.2345 267.5375 22.8950 -2.0313 239.3323 241.3636 267.6895 23.7158 -2.0315 239.4631 241.4946 267.8177 24.5080 -2.0321 239.5700 241.6022 267.9484 25.3000 -2.0307 239.6885 241.7192 268.0940 26.1220 -2.0287 239.8167 241.8454 268.2465 26.8860 -2.0266 239.9441 241.9707 268.3872 27.7380 -2.0290 240.0639 242.0929 268.5445 28.5000 -2.0265 240.1892 242.2157 268.6822 29.3215 -2.0265 240.3215 242.3480 268.8444 30.1428 -2.0307 240.4541 242.4848 269.0023 30.9033 -2.0349 240.5647 242.5996 269.1396 31.7588 -2.0339 240.7044 242.7383 269.2965 32.6148 -2.0333 240.8212 242.8545 269.4567 33.5948 -2.0331 240.9712 243.0043 269.6350 34.3583 -2.0325 241.0901 243.1226 269.7698 35.1905 -2.0322 241.2188 243.2510 269.9199 35.9833 -2.0341 241.3584 243.3925 270.0735 36.7753 -2.0349 241.4979 243.5328 270.1845 37.6003 -2.0341 241.6136 243.6477 270.3298 38.3693 -2.0332 241.7246 243.7577 270.4605 39.2213 -2.0351 241.8542 243.8893 270.6124 39.9835 -2.0362 241.9679 244.0041 270.7384 40.8088 -2.0357 242.1026 244.1383 270.8852 41.6048 -2.0350 242.2371 244.2721 271.0145 42.5195 -2.0357 242.3780 244.4137 271.1445 43.2835 -2.0363 242.4860 244.5224 271.2624 44.1078 -2.0364 242.6179 244.6543 271.3896 44.9060 -2.0361 242.7412 244.7773 271.4964 45.7305 -2.0369 242.8578 244.8947 271.6204 46.5533 -2.0392 242.9827 245.0219 271.7233 47.3440 -2.0392 243.1237 245.1629 271.8292 48.1355 -2.0409 243.2583 245.2992 271.9417 48.9575 -2.0422 243.3717 245.4139 272.0462 49.7193 -2.0425 243.4969 245.5393 272.1499 50.5733 -2.0419 243.6269 245.6688 272.2662 51.3365 -2.0425 243.7298 245.7724 272.3599 52.2180 -2.0404 243.8680 245.9084 272.4852 53.1318 -2.0423 244.0038 246.0461 272.5918 53.9000 -2.0435 244.1284 246.1719 272.6843 54.7270 -2.0426 244.2609 246.3035 272.7869 55.5213 -2.0429 244.3712 246.4141 272.8903 56.3190 -2.0436 244.4944 246.5380 272.9888 57.1468 -2.0443 244.6402 246.6845 273.0790 57.9113 -2.0445 244.7561 246.8006 273.1871 58.7660 -2.0439 244.8920 246.9359 273.2726 59.5293 -2.0407 245.0142 247.0549 273.3627 60.3508 -2.0434 245.1338 247.1772 273.4650 61.1808 -2.0416 245.2499 247.2915 273.5550 61.9455 -2.0441 245.3660 247.4101 273.6489 62.8063 -2.0455 245.5133 247.5588 273.7426 63.6008 -2.0444 245.6409 247.6853 273.8199 64.4835 -2.0416 245.7497 247.7913 273.9346 65.2515 -2.0425 245.8714 247.9139 274.0204 66.0900 -2.0429 246.0104 248.0534 274.0968 66.8523 -2.0422 246.1251 248.1674 274.1923 67.7045 -2.0435 246.2528 248.2963 274.2817 68.4973 -2.0417 246.3665 248.4082 274.3671 69.2945 -2.0421 246.4952 248.5373 274.4606 70.0860 -2.0434 246.6150 248.6585 274.5597 70.8830 -2.0413 246.7359 248.7772 274.6461 71.7105 -2.0408 246.8565 248.8973 274.7185 72.4763 -2.0427 246.9677 249.0105 274.8010 73.3338 -2.0406 247.1247 249.1653 274.8908 74.0985 -2.0398 247.2312 249.2710 274.9742 74.9225 -2.0388 247.3472 249.3860 275.0720 75.7588 -2.0411 247.4584 249.4995 275.1615 76.5533 -2.0409 247.5828 249.6238 275.2349 77.4385 -2.0422 247.7266 249.7689 275.3397 78.4768 -2.0425 247.8795 249.9219 275.4704 79.2998 -2.0418 248.0214 250.0632 275.5568 80.0653 -2.0427 248.1380 250.1806 275.6374 80.9263 -2.0420 248.2648 250.3068 275.7481 81.6615 -2.0405 248.3710 250.4115 275.8275 82.5160 -2.0428 248.4992 250.5421 275.9215 83.3085 -2.0414 248.6205 250.6619 276.0177 84.0998 -2.0413 248.7410 250.7823 276.1174 84.9220 -2.0411 248.8646 250.9057 276.2129 85.7765 -2.0402 249.0046 251.0449 276.3218 86.5693 -2.0393 249.1244 251.1637 276.4144 87.3938 -2.0396 249.2447 251.2843 276.5111 88.1880 -2.0400 249.3575 251.3975 276.6214 88.9820 -2.0399 249.4922 251.5321 276.7154 89.8040 -2.0400 249.6093 251.6492 276.8243 90.5670 -2.0407 249.7116 251.7523 276.9268 91.4165 -2.0383 249.8426 251.8809 277.0449 92.2085 -2.0411 249.9462 251.9873 277.1491 93.0003 -2.0391 250.0655 252.1045 277.2548 93.8525 -2.0392 250.2060 252.2452 277.3856 94.6128 -2.0377 250.3190 252.3567 277.4923 95.4350 -2.0403 250.4335 252.4738 277.5960 96.2305 -2.0415 250.5557 252.5972 277.7135 97.0265 -2.0400 250.6725 252.7126 277.8242 97.8495 -2.0394 250.7984 252.8377 277.9420 98.6098 -2.0406 250.9012 252.9418 278.0606 99.4645 -2.0416 251.0497 253.0913 278.1748 100.2253 -2.0400 251.1645 253.2045 278.3081 101.0483 -2.0385 251.2861 253.3246 278.4228 101.8695 -2.0380 251.3980 253.4360 278.5512 102.6305 -2.0403 251.4996 253.5399 278.6494 103.4858 -2.0417 251.6356 253.6772 278.7876 104.2485 -2.0409 251.7626 253.8035 278.9192 105.0753 -2.0411 251.8898 253.9309 279.0454 105.8680 -2.0401 252.0025 254.0426 279.1588 106.6635 -2.0402 252.1125 254.1528 279.2774 107.4878 -2.0420 252.2298 254.2718 279.3870 108.2508 -2.0422 252.3546 254.3969 279.5058 109.1020 -2.0428 252.4769 254.5197 279.6408 109.8918 -2.0415 252.6052 254.6468 279.7431 110.6818 -2.0424 252.7263 254.7687 279.8510 111.5008 -2.0421 252.8509 254.8929 279.9650 112.2920 -2.0432 252.9762 255.0195 280.0927 113.1135 -2.0421 253.0814 255.1235 280.2166 113.9080 -2.0419 253.1927 255.2346 280.3259 114.6988 -2.0445 253.3100 255.3545 280.4490 115.5195 -2.0484 253.4439 255.4922 280.5564 116.2810 -2.0494 253.5597 255.6091 280.6666 117.1328 -2.0462 253.6656 255.7118 280.7681 117.9223 -2.0447 253.7822 255.8269 280.8579 118.7125 -2.0463 253.9073 255.9536 280.9764 119.5363 -2.0470 254.0346 256.0816 281.1029 120.3013 -2.0480 254.1576 256.2056 281.1869 121.1543 -2.0472 254.2829 256.3301 281.3164 121.9198 -2.0478 254.3742 256.4219 281.4136 122.7405 -2.0467 254.4927 256.5394 281.5116 123.5320 -2.0462 254.6158 256.6620 281.6245 124.3235 -2.0447 254.7292 256.7739 281.7109 125.1790 -2.0473 254.8538 256.9011 281.8241 126.0013 -2.0498 254.9833 257.0331 281.9244 126.7638 -2.0510 255.0994 257.1504 282.0237 127.6210 -2.0512 255.2162 257.2674 282.1409 128.3873 -2.0515 255.3341 257.3856 282.2320 129.2103 -2.0504 255.4656 257.5160 282.3293 130.0025 -2.0490 255.5906 257.6396 282.4144 130.7990 -2.0499 255.6883 257.7382 282.5106 131.6248 -2.0474 255.8111 257.8585 282.6362 132.3888 -2.0483 255.9251 257.9734 282.7281 133.2480 -2.0493 256.0592 258.1085 282.8488 134.0073 -2.0478 256.1724 258.2202 282.9320 134.8310 -2.0489 256.2916 258.3405 283.0203 135.6238 -2.0490 256.3992 258.4483 283.1154 136.4155 -2.0497 256.5257 258.5753 283.1921 137.2360 -2.0483 256.6416 258.6900 283.2998 138.0273 -2.0485 256.7680 258.8165 283.4020 138.8478 -2.0476 256.8973 258.9449 283.5044 139.6398 -2.0462 256.9996 259.0458 283.6031 140.4330 -2.0461 257.1160 259.1622 283.6891 141.2593 -2.0465 257.2373 259.2838 283.7982 142.0233 -2.0472 257.3577 259.4049 283.9022 142.8775 -2.0470 257.4868 259.5337 284.0035 143.6405 -2.0494 257.5938 259.6433 284.0781 144.4618 -2.0482 257.7152 259.7634 284.1910 145.2520 -2.0467 257.8416 259.8883 284.2931 146.0433 -2.0466 257.9547 260.0013 284.3934 146.9013 -2.0468 258.0828 260.1296 284.4881 147.6493 -2.0454 258.1828 260.2282 284.5841 148.5045 -2.0471 258.3142 260.3613 284.6695 149.2648 -2.0477 258.4282 260.4759 284.7766 150.0865 -2.0474 258.5391 260.5865 284.8798 150.8790 -2.0497 258.6398 260.6895 284.9737 151.6725 -2.0486 258.7471 260.7957 285.0778 152.4958 -2.0480 258.8852 260.9331 285.1864 153.2595 -2.0468 259.0081 261.0550 285.2901 154.1123 -2.0461 259.1191 261.1653 285.4371 154.9043 -2.0446 259.2386 261.2831 285.5277 155.6955 -2.0448 259.3536 261.3984 285.6327 156.5175 -2.0420 259.4823 261.5243 285.7509 157.2785 -2.0410 259.6088 261.6498 285.8576 158.1415 -2.0399 259.7090 261.7489 285.9674 158.9055 -2.0408 259.8297 261.8705 286.0708 159.7273 -2.0413 259.9547 261.9960 286.2037 160.5193 -2.0413 260.0503 262.0916 286.3080 161.3100 -2.0349 260.1711 262.2060 286.4303 162.1315 -2.0262 260.2904 262.3166 286.5372 162.8933 -2.0385 260.4093 262.4478 286.6337 163.7468 -2.0391 260.5212 262.5603 286.7466 164.5118 -2.0409 260.6395 262.6804 286.8680 165.3348 -2.0439 260.7704 262.8143 286.9917 166.1570 -2.0429 260.8967 262.9396 287.1146 166.9185 -2.0413 261.0036 263.0449 287.2272 167.7708 -2.0415 261.1188 263.1603 287.3559 168.5318 -2.0437 261.2381 263.2817 287.4636 169.3535 -2.0452 261.3507 263.3959 287.5751 170.1448 -2.0445 261.4783 263.5229 287.6972 170.9365 -2.0449 261.5833 263.6282 287.8073 171.7888 -2.0395 261.7023 263.7418 287.9268 172.5505 -2.0433 261.8049 263.8482 288.0421 173.3718 -2.0242 261.9154 263.9396 288.1595 174.1635 -2.0297 262.0456 264.0752 288.2570 174.9558 -2.0453 262.1586 264.2039 288.3716 175.7775 -2.0425 262.2785 264.3210 288.4870 176.5695 -2.0439 262.3982 264.4420 288.5930 177.3918 -2.0510 262.5197 264.5706 288.6918 178.1828 -2.0513 262.6508 264.7021 288.8141 178.9745 -2.0536 262.7529 264.8065 288.9233 179.7960 -2.0550 262.8823 264.9373 289.0230 180.5575 -2.0515 262.9914 265.0429 289.1215 181.4088 -2.0552 263.0981 265.1533 289.2255 182.1718 -2.0581 263.2204 265.2785 289.3363 182.9975 -2.0581 263.3250 265.3831 289.4238 183.8195 -2.0558 263.4243 265.4801 289.5254 184.5808 -2.0591 263.5373 265.5964 289.6252 185.4320 -2.0591 263.6803 265.7393 289.7267 186.1943 -2.0578 263.8052 265.8630 289.8125 187.0160 -2.0593 263.9028 265.9622 289.9156 187.8093 -2.0609 264.0020 266.0628 290.0032 188.6380 -2.0623 264.1323 266.1946 290.0921 189.7010 -2.0576 264.2842 266.3418 290.2244 190.4618 -2.0598 264.4024 266.4622 290.3253 191.2830 -2.0630 264.5309 266.5939 290.4101 192.1038 -2.0664 264.6333 266.6997 290.4953 192.8650 -2.0685 264.7404 266.8089 290.5917 193.7165 -2.0672 264.8758 266.9430 290.6704 194.5068 -2.0680 265.0052 267.0732 290.7696 195.2983 -2.0647 265.1106 267.1753 290.8754 196.1208 -2.0684 265.2157 267.2841 290.9773 196.8825 -2.0699 265.3277 267.3976 291.0694 197.7338 -2.0710 265.4541 267.5252 291.1608 198.4945 -2.0722 265.5656 267.6378 291.2576 199.3163 -2.0727 265.6768 267.7495 291.3629 200.1378 -2.0724 265.7965 267.8689 291.4632 200.8988 -2.0733 265.9144 267.9877 291.5427 201.7485 -2.0741 266.0378 268.1120 291.6466 202.5385 -2.0711 266.1503 268.2214 291.7475 203.3303 -2.0727 266.2674 268.3402 291.8361 204.1515 -2.0737 266.3982 268.4719 291.9435 204.9128 -2.0734 266.4910 268.5644 292.0513 205.7635 -2.0719 266.6118 268.6838 292.1488 206.5545 -2.0742 266.7278 268.8020 292.2405 207.3463 -2.0744 266.8334 268.9079 292.3418 208.1668 -2.0761 266.9624 269.0385 292.4491 208.9388 -2.0768 267.0659 269.1427 292.5498 209.7645 -2.0784 267.1985 269.2769 292.6612 210.5548 -2.0795 267.3119 269.3914 292.7634 211.3760 -2.0797 267.4154 269.4951 292.8594 212.1665 -2.0781 267.5295 269.6076 292.9725 212.9563 -2.0778 267.6525 269.7303 293.0790 213.7780 -2.0778 267.7682 269.8460 293.1819 214.5693 -2.0777 267.8805 269.9582 293.2892 215.3908 -2.0778 267.9853 270.0631 293.3847 216.1820 -2.0801 268.0982 270.1783 293.4995 216.9723 -2.0811 268.2327 270.3138 293.5952 217.7938 -2.0784 268.3298 270.4082 293.7003 218.5840 -2.0797 268.4574 270.5370 293.8046 219.4053 -2.0837 268.5626 270.6463 293.9424 220.1955 -2.0814 268.6785 270.7599 294.0415 220.9868 -2.0809 268.7934 270.8744 294.1434 221.8075 -2.0841 268.9163 271.0004 294.2496 222.5990 -2.0864 269.0193 271.1057 294.3869 223.4205 -2.0854 269.1308 271.2163 294.4955 224.2110 -2.0861 269.2530 271.3391 294.6100 225.0013 -2.0868 269.3815 271.4683 294.7184 225.8525 -2.0872 269.4977 271.5849 294.8549 226.6138 -2.0890 269.6021 271.6911 294.9652 227.4355 -2.0881 269.7085 271.7965 295.0852 228.2270 -2.0858 269.8154 271.9012 295.2086 229.0178 -2.0851 269.9322 272.0173 295.3268 229.8685 -2.0878 270.0599 272.1477 295.4477 230.6298 -2.0898 270.1768 272.2665 295.5742 231.4500 -2.0903 270.2977 272.3880 295.6729 232.2405 -2.0923 270.4119 272.5042 295.7841 233.0318 -2.0960 270.5178 272.6137 295.9140 233.8845 -2.0974 270.6529 272.7503 296.0435 234.6515 -2.0977 270.7535 272.8512 296.1533 235.4755 -2.1000 270.8815 272.9815 296.2506 236.2693 -2.1008 270.9874 273.0882 296.3599 237.0605 -2.1004 271.0803 273.1807 296.4740 237.8823 -2.0997 271.2036 273.3033 296.5852 238.6445 -2.1032 271.3142 273.4174 296.6882 239.4960 -2.1044 271.4431 273.5475 296.8166 240.2603 -2.1050 271.5666 273.6715 296.9204 241.0880 -2.1032 271.6765 273.7797 297.0159 241.8845 -2.1054 271.7885 273.8939 297.1331 242.6763 -2.1085 271.9048 274.0134 297.2344 243.4973 -2.1086 272.0217 274.1303 297.3568 244.2590 -2.1091 272.1303 274.2394 297.4435 245.1130 -2.1103 272.2575 274.3678 297.5634 245.9035 -2.1126 272.3740 274.4866 297.6545 246.6973 -2.1148 272.4823 274.5971 297.7655 247.5218 -2.1135 272.5685 274.6820 297.8824 248.2850 -2.1148 272.6823 274.7971 297.9637 249.1363 -2.1192 272.8268 274.9460 298.0839 249.8965 -2.1210 272.9302 275.0512 298.1831 250.7175 -2.1220 273.0338 275.1559 298.2792 251.5095 -2.1230 273.1545 275.2775 298.3916 252.3010 -2.1212 273.2815 275.4027 298.4891 253.1523 -2.1242 273.3956 275.5197 298.6045 253.9135 -2.1267 273.4964 275.6231 298.6990 254.7350 -2.1274 273.6109 275.7383 298.7964 255.5265 -2.1263 273.7281 275.8543 298.8770 256.3193 -2.1273 273.8512 275.9785 298.9814 257.1405 -2.1265 273.9636 276.0901 299.0959 257.9308 -2.1300 274.0773 276.2074 299.1959 258.7518 -2.1281 274.1952 276.3232 299.2990 259.5435 -2.1305 274.3146 276.4451 299.3830 260.3358 -2.1326 274.4213 276.5540 299.4832 261.1580 -2.1333 274.5305 276.6638 299.5988 261.9195 -2.1365 274.6478 276.7843 299.6863 262.7710 -2.1386 274.7662 276.9047 299.7679 263.5325 -2.1363 274.8737 277.0100 299.8551 264.3543 -2.1368 274.9765 277.1133 299.9619 265.1763 -2.1404 275.0999 277.2402 300.0770 265.9368 -2.1424 275.2093 277.3516 300.1782 266.7873 -2.1443 275.3385 277.4829 300.2624 267.5470 -2.1446 275.4401 277.5847 300.3547 268.3680 -2.1437 275.5492 277.6929 300.4526 269.1883 -2.1482 275.6620 277.8102 300.5385 269.9565 -2.1473 275.7752 277.9225 300.6360 270.7960 -2.1473 275.8968 278.0442 300.7443 271.5560 -2.1470 276.0013 278.1483 300.8252 272.4078 -2.1465 276.1258 278.2723 300.9139 273.1685 -2.1481 276.2344 278.3825 301.0320 273.9888 -2.1485 276.3515 278.5000 301.1589 274.7813 -2.1493 276.4616 278.6109 301.2381 275.5738 -2.1525 276.5655 278.7181 301.3233 276.4263 -2.1520 276.7039 278.8559 301.4419 277.1878 -2.1541 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