DTA measure 1pb3 Date: 202458:1316 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1018.95 s Mass = 1122.600 mg data_number = 1269 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1595 -1.4068 243.7036 245.1105 263.2799 1.9190 -1.4033 243.7868 245.1901 263.2687 2.7708 -1.3957 243.8902 245.2859 263.3028 3.5613 -1.3943 243.9822 245.3765 263.2990 4.3510 -1.3912 244.1021 245.4933 263.3014 5.1715 -1.3905 244.1972 245.5877 263.2978 5.9310 -1.3863 244.2647 245.6509 263.3077 6.7823 -1.3796 244.3785 245.7581 263.3463 7.5718 -1.3733 244.4770 245.8503 263.3492 8.3628 -1.3726 244.5701 245.9426 263.3563 9.1835 -1.3714 244.6756 246.0470 263.3711 9.9450 -1.3723 244.7589 246.1311 263.3810 10.7963 -1.3683 244.8518 246.2201 263.3961 11.5858 -1.3643 244.9541 246.3184 263.4169 12.3760 -1.3662 245.0547 246.4209 263.4748 13.1965 -1.3718 245.1609 246.5328 263.5013 13.9570 -1.3671 245.2453 246.6124 263.5531 14.8083 -1.3592 245.3262 246.6854 263.6059 15.5998 -1.3516 245.4209 246.7725 263.6311 16.3913 -1.3502 245.5223 246.8725 263.6855 17.2125 -1.3457 245.6206 246.9663 263.7586 17.9728 -1.3428 245.7003 247.0430 263.8282 18.8228 -1.3402 245.7946 247.1348 263.8920 19.5840 -1.3465 245.8795 247.2261 263.9572 20.4055 -1.3582 245.9817 247.3399 264.0310 21.1975 -1.3628 246.0623 247.4251 264.1144 21.9945 -1.3581 246.1619 247.5200 264.2051 22.8223 -1.3520 246.2455 247.5975 264.3058 23.5825 -1.3548 246.3311 247.6859 264.3947 24.4348 -1.3534 246.4442 247.7977 264.5069 25.2260 -1.3514 246.5192 247.8706 264.6143 26.0163 -1.3505 246.5808 247.9313 264.7233 26.8380 -1.3473 246.6792 248.0266 264.8339 27.5990 -1.3324 246.7601 248.0925 264.9490 28.4508 -1.3239 246.8689 248.1928 265.0661 29.2118 -1.3237 246.9562 248.2799 265.1920 30.0333 -1.3209 247.0337 248.3545 265.3245 30.8540 -1.3217 247.1275 248.4492 265.4681 31.6145 -1.3191 247.2226 248.5417 265.5804 32.4655 -1.3144 247.3146 248.6290 265.7630 33.2248 -1.3162 247.3877 248.7039 265.9043 34.0463 -1.3168 247.4830 248.7998 266.0548 34.8665 -1.3162 247.5874 248.9036 266.2321 35.6273 -1.3122 247.6609 248.9731 266.3799 36.4778 -1.3107 247.7417 249.0524 266.5454 37.2388 -1.3134 247.8182 249.1316 266.7117 38.0590 -1.3132 247.9295 249.2428 266.8707 38.8795 -1.3169 248.0083 249.3252 267.0434 39.6400 -1.3235 248.0946 249.4180 267.2040 40.4905 -1.3193 248.1791 249.4984 267.3903 41.2525 -1.3153 248.2535 249.5688 267.5363 42.0733 -1.3143 248.3456 249.6599 267.6987 42.8945 -1.3179 248.4268 249.7447 267.8807 43.6548 -1.3240 248.5007 249.8247 268.0439 44.5065 -1.3223 248.5968 249.9191 268.2173 45.2685 -1.3188 248.6986 250.0174 268.4001 46.0900 -1.3177 248.7877 250.1054 268.5621 46.9115 -1.3185 248.8597 250.1782 268.7349 47.6705 -1.3177 248.9309 250.2486 268.8862 48.5210 -1.3162 248.9998 250.3160 269.0460 49.2810 -1.3201 249.0928 250.4129 269.2154 50.1023 -1.3214 249.2048 250.5263 269.3793 50.9230 -1.3216 249.2904 250.6120 269.5586 51.6833 -1.3209 249.3678 250.6886 269.7159 52.5353 -1.3200 249.4444 250.7644 269.8695 53.2963 -1.3221 249.5330 250.8551 270.0430 54.1170 -1.3246 249.6200 250.9446 270.1903 54.9370 -1.3246 249.7302 251.0549 270.3463 55.6970 -1.3290 249.7995 251.1285 270.4903 56.5480 -1.3266 249.8976 251.2242 270.6429 57.3373 -1.3268 249.9680 251.2948 270.7951 58.1275 -1.3284 250.0525 251.3808 270.9414 58.9475 -1.3322 250.1272 251.4595 271.0765 59.7090 -1.3440 250.2164 251.5604 271.2251 60.5603 -1.3522 250.3044 251.6566 271.3809 61.3498 -1.3541 250.4012 251.7554 271.5236 62.1413 -1.3560 250.4836 251.8395 271.6768 62.9625 -1.3598 250.5742 251.9340 271.8151 63.7528 -1.3636 250.6472 252.0108 271.9404 64.5745 -1.3714 250.7583 252.1296 272.0748 65.3663 -1.3711 250.8256 252.1966 272.1999 66.1560 -1.3763 250.9225 252.2989 272.3167 66.9765 -1.3754 251.0166 252.3920 272.4594 67.7380 -1.3747 251.1075 252.4822 272.5903 68.5893 -1.3822 251.1932 252.5754 272.6861 69.3795 -1.3866 251.2673 252.6539 272.8079 70.1713 -1.3890 251.3498 252.7387 272.9350 70.9935 -1.3948 251.4404 252.8352 273.0603 71.7555 -1.3993 251.4997 252.8990 273.1842 72.6075 -1.3907 251.6118 253.0024 273.3038 73.3695 -1.3920 251.6887 253.0807 273.4032 74.1903 -1.3993 251.7678 253.1671 273.5150 75.0103 -1.4058 251.8728 253.2786 273.6147 75.7698 -1.4045 251.9505 253.3551 273.7126 76.6208 -1.3973 252.0358 253.4331 273.8322 77.3808 -1.3918 252.1297 253.5215 273.9378 78.2035 -1.3873 252.2180 253.6053 274.0504 79.0250 -1.3901 252.2958 253.6860 274.1830 79.7865 -1.3946 252.3809 253.7756 274.2659 80.6390 -1.3924 252.4816 253.8740 274.3786 81.4008 -1.3950 252.5681 253.9631 274.4753 82.2220 -1.3997 252.6467 254.0464 274.5915 83.0435 -1.4021 252.7220 254.1241 274.7085 83.8098 -1.4047 252.8127 254.2174 274.8194 84.6620 -1.4062 252.9202 254.3264 274.9531 85.4235 -1.4079 253.0003 254.4083 275.0541 86.2448 -1.4085 253.1000 254.5085 275.1521 87.0355 -1.4083 253.1848 254.5931 275.2622 87.8268 -1.4117 253.2442 254.6560 275.3820 88.6783 -1.4236 253.3654 254.7890 275.4868 89.4385 -1.4322 253.4264 254.8586 275.6041 90.2598 -1.4351 253.5056 254.9407 275.7250 91.0795 -1.4265 253.6141 255.0406 275.8448 91.8398 -1.4215 253.6732 255.0947 275.9607 92.6915 -1.4220 253.7784 255.2004 276.0735 93.4525 -1.4246 253.8669 255.2915 276.2003 94.2738 -1.4283 253.9484 255.3768 276.3161 95.0945 -1.4327 254.0421 255.4748 276.4399 95.8543 -1.4331 254.1113 255.5444 276.5397 96.7043 -1.4360 254.1998 255.6358 276.6646 97.4645 -1.4373 254.2913 255.7286 276.7950 98.2855 -1.4397 254.3847 255.8245 276.9217 99.1073 -1.4418 254.4706 255.9124 277.0512 99.8675 -1.4451 254.5496 255.9947 277.1519 100.7190 -1.4487 254.6411 256.0898 277.2725 101.4793 -1.4528 254.7322 256.1850 277.3923 102.3000 -1.4512 254.8104 256.2616 277.5384 103.1193 -1.4533 254.8948 256.3481 277.6679 103.8790 -1.4551 254.9783 256.4334 277.8011 104.7308 -1.4580 255.0859 256.5438 277.9444 105.5210 -1.4603 255.1637 256.6240 278.0636 106.3113 -1.4626 255.2863 256.7488 278.1911 107.1330 -1.4656 255.3645 256.8301 278.3071 107.8923 -1.4673 255.4350 256.9024 278.4209 108.7438 -1.4691 255.5320 257.0012 278.5505 109.5340 -1.4723 255.6031 257.0754 278.6883 110.3245 -1.4731 255.7023 257.1753 278.8272 111.1458 -1.4751 255.8032 257.2783 278.9522 111.9068 -1.4819 255.8839 257.3658 279.0657 112.7583 -1.4854 255.9834 257.4688 279.2158 113.5495 -1.4850 256.0667 257.5517 279.3536 114.3400 -1.4882 256.1375 257.6258 279.4729 115.1605 -1.4900 256.2340 257.7240 279.6013 115.9203 -1.4916 256.3121 257.8037 279.7134 116.7713 -1.4933 256.4153 257.9086 279.8458 117.5613 -1.4924 256.5160 258.0084 279.9961 118.3513 -1.4976 256.6020 258.0995 280.1392 119.1725 -1.4992 256.6986 258.1977 280.2684 119.9328 -1.5018 256.7820 258.2838 280.3829 120.7843 -1.5077 256.8779 258.3856 280.5345 121.5745 -1.5169 256.9445 258.4614 280.6599 122.3650 -1.5193 257.0357 258.5550 280.7802 123.1855 -1.5218 257.1364 258.6583 280.9143 123.9460 -1.5281 257.2316 258.7597 281.0578 124.7975 -1.5293 257.3416 258.8709 281.2162 125.5873 -1.5296 257.4180 258.9476 281.3448 126.3773 -1.5308 257.5084 259.0392 281.5005 127.1980 -1.5338 257.5903 259.1241 281.6489 127.9575 -1.5387 257.6740 259.2127 281.7752 128.8090 -1.5414 257.7749 259.3163 281.9207 129.5698 -1.5432 257.8645 259.4076 282.0500 130.3910 -1.5433 257.9565 259.4998 282.1923 131.2120 -1.5472 258.0401 259.5873 282.3580 131.9713 -1.5476 258.1249 259.6725 282.5164 132.8218 -1.5454 258.2276 259.7731 282.6486 133.5828 -1.5551 258.3067 259.8619 282.7876 134.4040 -1.5638 258.4187 259.9824 282.9318 135.2245 -1.5650 258.5043 260.0693 283.0660 135.9843 -1.5655 258.6014 260.1670 283.2179 136.8358 -1.5676 258.7037 260.2713 283.3824 137.5963 -1.5648 258.7827 260.3475 283.5142 138.4175 -1.5644 258.8700 260.4344 283.6439 139.2395 -1.5645 258.9748 260.5393 283.7695 140.0015 -1.5711 259.0601 260.6311 283.8961 140.8535 -1.5776 259.1577 260.7353 284.0496 141.6155 -1.5807 259.2491 260.8298 284.1842 142.4373 -1.5829 259.3535 260.9364 284.3007 143.2285 -1.5870 259.4333 261.0203 284.4463 144.0205 -1.5943 259.5220 261.1163 284.5798 144.8725 -1.5991 259.6334 261.2325 284.7069 145.6345 -1.6040 259.7236 261.3276 284.8168 146.4563 -1.6062 259.8070 261.4132 284.9376 147.2475 -1.6075 259.8964 261.5038 285.0645 148.0383 -1.6091 259.9982 261.6073 285.1788 148.8595 -1.6145 260.0774 261.6920 285.2937 149.6495 -1.6213 260.1656 261.7869 285.4248 150.4698 -1.6275 260.2760 261.9035 285.5747 151.2600 -1.6295 260.3873 262.0168 285.6921 152.0495 -1.6312 260.4711 262.1023 285.8058 152.9008 -1.6394 260.5823 262.2217 285.9359 153.6618 -1.6447 260.6654 262.3101 286.0158 154.4833 -1.6467 260.7726 262.4193 286.1427 155.2750 -1.6495 260.8569 262.5064 286.2719 156.0660 -1.6535 260.9477 262.6012 286.3936 156.8880 -1.6580 261.0737 262.7316 286.5115 157.6780 -1.6538 261.1682 262.8219 286.6355 158.4993 -1.6551 261.2669 262.9220 286.7402 159.2900 -1.6585 261.3585 263.0170 286.8691 160.0810 -1.6676 261.4583 263.1260 286.9792 160.9030 -1.6704 261.5486 263.2190 287.1034 161.6930 -1.6727 261.6408 263.3135 287.2250 162.5143 -1.6770 261.7297 263.4067 287.3498 163.3050 -1.6823 261.8265 263.5089 287.4868 164.0960 -1.6859 261.9311 263.6170 287.6097 164.9175 -1.6876 262.0135 263.7010 287.7279 165.7075 -1.6877 262.1120 263.7997 287.8416 166.5278 -1.6929 262.2094 263.9023 287.9624 167.3175 -1.6944 262.3063 264.0007 288.0955 168.1083 -1.6953 262.4093 264.1046 288.2311 168.9595 -1.6974 262.5267 264.2241 288.3582 169.7205 -1.7001 262.6118 264.3119 288.5031 170.5423 -1.7014 262.7055 264.4070 288.6254 171.3325 -1.7056 262.7951 264.5007 288.7485 172.1238 -1.7109 262.8843 264.5951 288.8883 172.9755 -1.7133 262.9978 264.7111 289.0204 173.7358 -1.7187 263.0936 264.8123 289.1492 174.5568 -1.7295 263.2086 264.9381 289.2732 175.3465 -1.7379 263.2933 265.0312 289.3974 176.1370 -1.7453 263.3977 265.1429 289.5261 176.9880 -1.7494 263.4921 265.2415 289.6649 177.7473 -1.7520 263.5853 265.3373 289.7944 178.5680 -1.7605 263.6961 265.4566 289.9382 179.3595 -1.7625 263.8004 265.5629 290.0581 180.1493 -1.7624 263.9118 265.6742 290.1765 180.9998 -1.7651 263.9981 265.7633 290.3275 181.7598 -1.7678 264.0897 265.8575 290.4348 182.5810 -1.7721 264.2032 265.9753 290.5844 183.4020 -1.7723 264.3027 266.0751 290.7100 184.1625 -1.7826 264.3945 266.1771 290.8470 185.0150 -1.7913 264.4937 266.2850 290.9854 185.7750 -1.7896 264.5920 266.3817 291.1109 186.5965 -1.7847 264.7150 266.4997 291.2356 187.4188 -1.7814 264.8056 266.5871 291.3615 188.1783 -1.7843 264.8999 266.6842 291.5058 189.0295 -1.7895 264.9974 266.7870 291.6288 189.7900 -1.7964 265.0968 266.8932 291.7516 190.6108 -1.8016 265.2112 267.0128 291.8750 191.4308 -1.8008 265.3021 267.1029 292.0335 192.1903 -1.8074 265.4088 267.2162 292.1522 193.0415 -1.8104 265.5063 267.3167 292.2793 193.8325 -1.8107 265.6134 267.4241 292.4058 194.6238 -1.8126 265.6972 267.5098 292.5185 195.4445 -1.8180 265.8084 267.6264 292.6568 196.2055 -1.8184 265.9101 267.7285 292.7797 197.0553 -1.8215 266.0143 267.8358 292.9176 197.8443 -1.8244 266.1091 267.9335 293.0387 198.6343 -1.8270 266.2140 268.0409 293.1661 199.4548 -1.8320 266.3149 268.1470 293.3045 200.2448 -1.8350 266.4123 268.2473 293.4076 201.0660 -1.8398 266.5234 268.3631 293.5620 201.8565 -1.8397 266.6204 268.4601 293.6810 202.6470 -1.8452 266.7260 268.5712 293.7880 203.4673 -1.8441 266.8303 268.6744 293.9297 204.2575 -1.8483 266.9434 268.7917 294.0557 205.0783 -1.8495 267.0506 268.9000 294.1859 205.8690 -1.8552 267.1561 269.0113 294.3227 206.6590 -1.8600 267.2600 269.1199 294.4488 207.4800 -1.8696 267.3607 269.2303 294.6000 208.2408 -1.8764 267.4491 269.3256 294.7152 209.0928 -1.8766 267.5651 269.4417 294.8790 209.8830 -1.8714 267.6690 269.5404 294.9940 210.6738 -1.8723 267.7677 269.6401 295.1184 211.4955 -1.8783 267.8843 269.7626 295.2662 212.2565 -1.8794 267.9674 269.8468 295.4089 213.1088 -1.8837 268.0954 269.9791 295.5200 213.8688 -1.8859 268.1836 270.0695 295.6546 214.6898 -1.8868 268.3011 270.1879 295.8023 215.5110 -1.8885 268.3712 270.2597 295.9637 216.2718 -1.8935 268.4896 270.3831 296.1001 217.1233 -1.8980 268.6175 270.5155 296.2507 217.8845 -1.9010 268.7151 270.6161 296.3619 218.7063 -1.9074 268.8260 270.7335 296.5110 219.5275 -1.9098 268.9436 270.8534 296.6346 220.2873 -1.9081 269.0343 270.9424 296.7803 221.1383 -1.9065 269.1498 271.0562 296.9494 221.8983 -1.9115 269.2346 271.1461 297.0549 222.7188 -1.9125 269.3498 271.2622 297.1970 223.5385 -1.9190 269.4751 271.3941 297.3360 224.2990 -1.9290 269.5824 271.5115 297.4816 225.1503 -1.9295 269.6770 271.6065 297.6147 225.9105 -1.9398 269.7771 271.7169 297.7334 226.7323 -1.9461 269.8766 271.8227 297.8925 227.5525 -1.9436 269.9854 271.9289 298.0464 228.3135 -1.9479 270.0997 272.0476 298.1745 229.1650 -1.9473 270.2250 272.1723 298.3361 229.9265 -1.9507 270.3226 272.2733 298.4809 230.7483 -1.9602 270.4319 272.3922 298.6026 231.5403 -1.9646 270.5354 272.5001 298.7492 232.3303 -1.9638 270.6443 272.6080 298.8756 233.1520 -1.9705 270.7746 272.7451 299.0058 233.9420 -1.9753 270.8628 272.8382 299.1436 234.7623 -1.9746 270.9528 272.9275 299.2741 235.5530 -1.9779 271.0567 273.0345 299.4212 236.3433 -1.9819 271.1865 273.1684 299.5430 237.1650 -1.9834 271.3189 273.3023 299.6551 237.9550 -1.9878 271.4169 273.4047 299.8086 238.7768 -1.9922 271.5077 273.4998 299.9366 239.5678 -1.9947 271.6240 273.6187 300.0594 240.3588 -1.9942 271.7268 273.7210 300.1898 241.1798 -1.9951 271.8299 273.8249 300.3138 241.9708 -1.9960 271.9681 273.9641 300.4368 242.7923 -1.9950 272.0673 274.0624 300.5588 243.5825 -2.0021 272.1882 274.1902 300.6726 244.3743 -2.0071 272.2730 274.2801 300.7782 245.1955 -2.0128 272.3745 274.3873 300.9199 245.9868 -2.0201 272.4979 274.5180 301.0462 246.8085 -2.0221 272.6131 274.6352 301.1504 247.6003 -2.0307 272.7335 274.7642 301.2934 248.3915 -2.0376 272.8362 274.8737 301.4089 249.2135 -2.0388 272.9427 274.9814 301.4983 249.9748 -2.0348 273.0578 275.0926 301.6106 250.8255 -2.0366 273.1819 275.2184 301.7512 251.6165 -2.0365 273.2899 275.3264 301.8664 252.4083 -2.0380 273.4070 275.4451 301.9901 253.2295 -2.0411 273.5133 275.5545 302.1147 253.9915 -2.0461 273.5984 275.6446 302.2332 254.8433 -2.0497 273.7287 275.7784 302.3710 255.6043 -2.0477 273.8292 275.8769 302.4789 256.4250 -2.0526 273.9361 275.9887 302.6085 257.2453 -2.0574 274.0706 276.1281 302.7554 258.0065 -2.0566 274.1871 276.2437 302.8796 258.8578 -2.0547 274.2985 276.3531 303.0147 259.6178 -2.0589 274.4153 276.4741 303.1154 260.4395 -2.0599 274.5114 276.5713 303.2505 261.2610 -2.0653 274.6322 276.6975 303.3682 262.0220 -2.0686 274.7430 276.8117 303.4874 262.8738 -2.0683 274.8877 276.9560 303.6159 263.6638 -2.0731 274.9684 277.0416 303.7375 264.4540 -2.0794 275.0628 277.1421 303.8612 265.2753 -2.0817 275.1846 277.2663 303.9956 266.0353 -2.0818 275.2987 277.3805 304.1142 266.8863 -2.0705 275.4280 277.4985 304.2654 267.6770 -2.0682 275.5435 277.6117 304.3773 268.4685 -2.0703 275.6539 277.7242 304.5145 269.2905 -2.0687 275.7667 277.8355 304.6422 270.0525 -2.0671 275.8650 277.9321 304.7782 270.9043 -2.0551 275.9841 278.0392 304.9143 271.6655 -2.0570 276.1013 278.1583 305.0224 272.4875 -2.0629 276.2096 278.2725 305.1429 273.3095 -2.0756 276.3199 278.3955 305.2864 274.0700 -2.0798 276.4549 278.5347 305.3995 274.9213 -2.0805 276.5717 278.6522 305.5320 275.6825 -2.0825 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