DTA measure 1pb4 Date: 202458:1413 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.12 s Mass = 1122.600 mg data_number = 1587 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2303 -1.5978 233.3244 234.9222 261.8399 2.0815 -1.5950 233.4354 235.0304 261.8106 2.8425 -1.5948 233.5357 235.1305 261.7852 3.6638 -1.5920 233.6533 235.2453 261.7749 4.4845 -1.5916 233.7476 235.3393 261.7546 5.2460 -1.5936 233.8422 235.4358 261.7619 6.0975 -1.5866 233.9732 235.5598 261.7621 6.8578 -1.5870 234.0699 235.6569 261.7693 7.6793 -1.5832 234.1697 235.7529 261.7820 8.4705 -1.5817 234.2828 235.8645 261.7853 9.2633 -1.5774 234.3931 235.9705 261.8304 10.1148 -1.5815 234.4974 236.0789 261.8461 10.8740 -1.5809 234.5979 236.1788 261.8669 11.6950 -1.5720 234.7058 236.2779 261.9010 12.4860 -1.5712 234.8108 236.3820 261.9222 13.2763 -1.5663 234.9101 236.4764 261.9692 14.1278 -1.5583 235.0316 236.5899 262.0331 14.8888 -1.5568 235.1319 236.6887 262.0759 15.7108 -1.5629 235.2361 236.7990 262.1334 16.5028 -1.5664 235.3145 236.8809 262.2049 17.2945 -1.5682 235.4226 236.9908 262.2950 18.1168 -1.5733 235.5437 237.1169 262.3666 18.9070 -1.5601 235.6543 237.2144 262.4629 19.7278 -1.5477 235.7487 237.2964 262.5558 20.5170 -1.5454 235.8446 237.3900 262.6471 21.3073 -1.5440 235.9473 237.4913 262.7496 22.1583 -1.5406 236.0689 237.6095 262.8670 22.9188 -1.5422 236.1452 237.6873 262.9931 23.7405 -1.5426 236.2677 237.8102 263.1039 24.5325 -1.5429 236.3943 237.9372 263.2355 25.3233 -1.5422 236.4893 238.0314 263.3388 26.1445 -1.5415 236.5842 238.1257 263.4786 26.9065 -1.5463 236.6784 238.2247 263.6062 27.7583 -1.5483 236.7863 238.3347 263.7638 28.5485 -1.5469 236.9025 238.4494 263.8964 29.3395 -1.5435 237.0091 238.5526 264.0260 30.1605 -1.5482 237.1231 238.6714 264.1888 30.9208 -1.5507 237.2229 238.7736 264.3244 31.7723 -1.5486 237.3354 238.8840 264.4761 32.5633 -1.5505 237.4173 238.9678 264.6279 33.3545 -1.5524 237.5293 239.0818 264.7982 34.1760 -1.5514 237.6322 239.1835 264.9488 34.9363 -1.5505 237.7238 239.2743 265.1019 35.7878 -1.5501 237.8541 239.4043 265.2689 36.5490 -1.5497 237.9516 239.5013 265.4405 37.3705 -1.5481 238.0421 239.5902 265.5722 38.1620 -1.5536 238.1474 239.7010 265.7138 38.9530 -1.5538 238.2629 239.8167 265.8746 39.8093 -1.5539 238.3729 239.9267 266.0537 40.5720 -1.5566 238.4833 240.0399 266.2037 41.3938 -1.5589 238.5842 240.1430 266.3499 42.1850 -1.5633 238.6911 240.2544 266.5057 42.9760 -1.5680 238.7807 240.3486 266.6604 43.7980 -1.5691 238.8886 240.4577 266.8063 44.5878 -1.5700 238.9878 240.5578 266.9446 45.4093 -1.5705 239.1045 240.6750 267.0976 46.1998 -1.5720 239.2240 240.7960 267.2281 46.9898 -1.5721 239.3163 240.8884 267.3648 47.8115 -1.5710 239.4421 241.0131 267.5055 48.6028 -1.5773 239.5385 241.1158 267.6413 49.4245 -1.5886 239.6489 241.2375 267.7772 50.1903 -1.5918 239.7454 241.3372 267.9029 51.0143 -1.5867 239.8491 241.4358 268.0522 51.8350 -1.5855 239.9555 241.5410 268.1841 52.5965 -1.5920 240.0547 241.6468 268.2816 53.4485 -1.5923 240.1589 241.7513 268.4101 54.2105 -1.5947 240.2808 241.8755 268.5353 55.0325 -1.6022 240.4043 242.0065 268.6681 55.8235 -1.6034 240.5031 242.1064 268.7903 56.6143 -1.6005 240.5966 242.1971 268.8870 57.4655 -1.6009 240.6976 242.2984 268.9901 58.2268 -1.6013 240.8049 242.4062 269.1021 59.0483 -1.6030 240.9185 242.5215 269.2111 59.8393 -1.6057 241.0267 242.6325 269.3130 60.6303 -1.6069 241.1308 242.7376 269.4040 61.4520 -1.6057 241.2392 242.8448 269.5147 62.2420 -1.6108 241.3497 242.9605 269.6073 63.0638 -1.6130 241.4583 243.0713 269.7116 63.8550 -1.6136 241.5665 243.1801 269.8136 64.6460 -1.6156 241.6822 243.2978 269.8964 65.4680 -1.6158 241.7839 243.3997 269.9918 66.2590 -1.6182 241.8995 243.5177 270.0723 67.0805 -1.6179 242.0007 243.6186 270.1565 67.8715 -1.6209 242.1024 243.7232 270.2371 68.6618 -1.6215 242.2125 243.8340 270.3434 69.4830 -1.6207 242.3320 243.9527 270.4268 70.2453 -1.6121 242.4260 244.0381 270.5070 71.1065 -1.6077 242.5287 244.1363 270.5800 71.8668 -1.6075 242.6387 244.2461 270.6757 72.6878 -1.6081 242.7452 244.3533 270.7536 73.5085 -1.6091 242.8569 244.4659 270.8208 74.2683 -1.6072 242.9695 244.5767 270.8957 75.1195 -1.6083 243.0812 244.6895 271.0003 75.8815 -1.6139 243.1956 244.8095 271.0738 76.7030 -1.6171 243.2999 244.9170 271.1399 77.4945 -1.6246 243.4036 245.0282 271.2213 78.2860 -1.6299 243.4991 245.1290 271.3213 79.1378 -1.6278 243.6165 245.2443 271.4205 79.8988 -1.6276 243.7375 245.3651 271.4887 80.7198 -1.6286 243.8398 245.4684 271.5684 81.5105 -1.6322 243.9489 245.5811 271.6479 82.3013 -1.6372 244.0634 245.7006 271.7523 83.1515 -1.6345 244.2026 245.8371 271.8468 83.9135 -1.6288 244.2777 245.9065 271.9162 84.7345 -1.6262 244.3697 245.9959 271.9995 85.5255 -1.6257 244.4611 246.0869 272.0933 86.3160 -1.6272 244.5803 246.2075 272.1903 87.1680 -1.6277 244.7004 246.3281 272.2969 87.9300 -1.6309 244.7990 246.4299 272.3782 88.7518 -1.6282 244.8985 246.5267 272.4909 89.5440 -1.6246 245.0284 246.6530 272.5670 90.3355 -1.6259 245.1300 246.7560 272.6675 91.1878 -1.6284 245.2405 246.8689 272.7563 91.9470 -1.6391 245.3198 246.9588 272.8592 92.7688 -1.6462 245.4673 247.1134 272.9582 93.5610 -1.6483 245.5555 247.2037 273.0539 94.3513 -1.6507 245.6733 247.3240 273.1656 95.2030 -1.6512 245.7670 247.4183 273.2752 95.9648 -1.6559 245.8653 247.5212 273.3770 96.7860 -1.6544 245.9700 247.6245 273.4821 97.5765 -1.6536 246.0629 247.7165 273.5884 98.3678 -1.6572 246.1686 247.8258 273.6676 99.1895 -1.6552 246.2801 247.9353 273.8113 99.9815 -1.6545 246.3956 248.0501 273.9170 100.8030 -1.6574 246.5043 248.1617 274.0096 101.5933 -1.6571 246.6171 248.2742 274.1092 102.3838 -1.6527 246.7213 248.3740 274.2258 103.2055 -1.6607 246.8489 248.5097 274.3380 103.9968 -1.6636 246.9403 248.6040 274.4487 104.8185 -1.6663 247.0458 248.7122 274.5594 105.6095 -1.6667 247.1507 248.8174 274.6581 106.4008 -1.6637 247.2578 248.9215 274.7915 107.2225 -1.6573 247.3680 249.0253 274.9020 107.9835 -1.6569 247.4700 249.1268 274.9927 108.8353 -1.6563 247.5832 249.2395 275.1138 109.6265 -1.6567 247.7012 249.3580 275.2094 110.4175 -1.6612 247.8165 249.4778 275.3103 111.2393 -1.6686 247.9242 249.5928 275.4431 112.0000 -1.6735 247.9942 249.6677 275.5453 112.8520 -1.6782 248.1087 249.7870 275.6531 113.6138 -1.6773 248.2287 249.9060 275.7554 114.4350 -1.6752 248.3192 249.9944 275.8719 115.2560 -1.6751 248.4208 250.0958 275.9866 116.0170 -1.6796 248.5434 250.2229 276.0998 116.8688 -1.6778 248.6517 250.3295 276.2134 117.6298 -1.6841 248.7532 250.4373 276.3244 118.4513 -1.6865 248.8725 250.5590 276.4449 119.2420 -1.6856 248.9843 250.6699 276.5464 120.0328 -1.6842 249.1147 250.7989 276.6496 120.8548 -1.6844 249.2031 250.8876 276.7803 121.6448 -1.6811 249.3114 250.9925 276.8874 122.4660 -1.6889 249.4168 251.1057 276.9784 123.2575 -1.6961 249.5126 251.2087 277.0907 124.0490 -1.6955 249.6071 251.3026 277.2095 124.8718 -1.6961 249.7404 251.4365 277.3352 125.6328 -1.6953 249.8411 251.5364 277.4183 126.4845 -1.7007 249.9549 251.6555 277.5294 127.2465 -1.6996 250.0606 251.7602 277.6420 128.0680 -1.7010 250.1721 251.8731 277.7414 128.8888 -1.7034 250.2654 251.9688 277.8735 129.6505 -1.7060 250.3700 252.0760 277.9674 130.5023 -1.7018 250.5030 252.2048 278.0656 131.2635 -1.7047 250.6069 252.3116 278.1785 132.0893 -1.7077 250.7328 252.4405 278.3136 132.8800 -1.7080 250.8248 252.5328 278.4016 133.6710 -1.7115 250.9265 252.6380 278.5160 134.5223 -1.7120 251.0246 252.7366 278.6333 135.2835 -1.7125 251.1298 252.8424 278.7333 136.1048 -1.7153 251.2542 252.9695 278.8516 136.8938 -1.7143 251.3551 253.0694 278.9716 137.6845 -1.7166 251.4726 253.1892 279.0715 138.5360 -1.7212 251.5742 253.2954 279.1694 139.2978 -1.7227 251.6794 253.4021 279.2846 140.1193 -1.7215 251.7768 253.4982 279.3833 140.9110 -1.7281 251.8857 253.6138 279.4967 141.7013 -1.7314 251.9870 253.7184 279.6036 142.5230 -1.7276 252.1089 253.8365 279.7067 143.3140 -1.7309 252.2061 253.9370 279.8074 144.1353 -1.7371 252.3165 254.0536 279.9325 144.9270 -1.7367 252.4195 254.1561 280.0375 145.7175 -1.7301 252.5002 254.2304 280.1407 146.5388 -1.7315 252.6247 254.3562 280.2466 147.2995 -1.7412 252.7273 254.4685 280.3454 148.1515 -1.7424 252.8390 254.5814 280.4654 148.9415 -1.7426 252.9602 254.7028 280.5834 149.7328 -1.7448 253.0680 254.8128 280.6811 150.5545 -1.7469 253.1667 254.9136 280.7790 151.3155 -1.7558 253.2903 255.0461 280.8980 152.1675 -1.7545 253.4009 255.1554 281.0072 152.9585 -1.7494 253.5005 255.2499 281.1154 153.7498 -1.7522 253.6116 255.3637 281.2163 154.5715 -1.7503 253.7268 255.4770 281.3202 155.3318 -1.7522 253.8284 255.5806 281.4163 156.1833 -1.7561 253.9303 255.6864 281.5306 156.9728 -1.7564 254.0395 255.7959 281.6364 157.7643 -1.7552 254.1361 255.8913 281.7326 158.5855 -1.7531 254.2425 255.9956 281.8403 159.3468 -1.7575 254.3630 256.1205 281.9455 160.1985 -1.7587 254.4780 256.2366 282.0500 160.9895 -1.7594 254.5729 256.3323 282.1680 161.7798 -1.7591 254.6789 256.4380 282.2725 162.6010 -1.7640 254.8126 256.5766 282.3645 163.3613 -1.7642 254.9156 256.6797 282.4564 164.2130 -1.7688 255.0182 256.7870 282.5701 165.0035 -1.7704 255.1237 256.8942 282.6724 165.7943 -1.7695 255.2326 257.0021 282.7712 166.6160 -1.7628 255.3371 257.0999 282.8799 167.3775 -1.7609 255.4434 257.2043 282.9773 168.2303 -1.7651 255.5555 257.3206 283.0845 169.0220 -1.7644 255.6484 257.4129 283.1941 169.8130 -1.7633 255.7739 257.5371 283.3041 170.6343 -1.7637 255.9018 257.6655 283.4010 171.3943 -1.7665 255.9963 257.7628 283.4990 172.2448 -1.7713 256.0913 257.8626 283.6015 173.0355 -1.7742 256.1811 257.9553 283.6943 173.8268 -1.7752 256.2900 258.0652 283.8075 174.6485 -1.7760 256.4047 258.1807 283.9027 175.4105 -1.7757 256.5135 258.2891 284.0055 176.2625 -1.7782 256.6297 258.4079 284.1258 177.0245 -1.7818 256.7264 258.5081 284.2285 177.8458 -1.7824 256.8577 258.6402 284.3213 178.6665 -1.7828 256.9633 258.7461 284.4221 179.4285 -1.7850 257.0700 258.8550 284.5214 180.2805 -1.7841 257.1733 258.9574 284.6294 181.0418 -1.7844 257.2674 259.0517 284.7365 181.8628 -1.7803 257.3691 259.1493 284.8259 182.6843 -1.7837 257.4994 259.2831 284.9191 183.4458 -1.7845 257.6004 259.3849 285.0324 184.2975 -1.7888 257.7235 259.5123 285.1596 185.0583 -1.7906 257.8364 259.6270 285.2456 185.8788 -1.7914 257.9272 259.7186 285.3426 186.6990 -1.7897 258.0355 259.8252 285.4518 187.4600 -1.7947 258.1577 259.9524 285.5558 188.3110 -1.7962 258.2667 260.0629 285.6356 189.0713 -1.7974 258.3656 260.1630 285.7375 189.8923 -1.7982 258.4548 260.2530 285.8646 190.6830 -1.8012 258.5596 260.3608 285.9580 191.4738 -1.8018 258.6879 260.4897 286.0548 192.3240 -1.8049 258.7773 260.5822 286.1671 193.0848 -1.8073 258.8991 260.7064 286.2602 193.9058 -1.8051 259.0100 260.8151 286.3835 194.6980 -1.8088 259.1209 260.9297 286.4626 195.4895 -1.8107 259.2168 261.0275 286.5586 196.3418 -1.8115 259.3327 261.1442 286.6739 197.1015 -1.8117 259.4484 261.2601 286.7606 197.9228 -1.8281 259.5514 261.3795 286.8724 198.7148 -1.8402 259.6598 261.5000 286.9655 199.5058 -1.8426 259.7652 261.6078 287.0551 200.3258 -1.8472 259.8825 261.7297 287.1522 201.1168 -1.8516 259.9941 261.8457 287.2544 201.9385 -1.8513 260.0973 261.9487 287.3574 202.7295 -1.8555 260.1900 262.0455 287.4663 203.5213 -1.8538 260.2889 262.1427 287.5553 204.3415 -1.8540 260.4269 262.2809 287.6696 205.1028 -1.8541 260.5272 262.3813 287.7624 205.9545 -1.8537 260.6518 262.5055 287.8604 206.7455 -1.8578 260.7629 262.6207 287.9567 207.5373 -1.8623 260.8606 262.7228 288.0615 208.3578 -1.8605 260.9712 262.8317 288.1662 209.1183 -1.8627 261.0651 262.9278 288.2548 209.9695 -1.8663 261.1844 263.0507 288.3779 210.7605 -1.8693 261.2803 263.1496 288.4763 211.5523 -1.8745 261.3987 263.2732 288.5732 212.3733 -1.8772 261.4993 263.3765 288.6786 213.1340 -1.8789 261.6190 263.4978 288.7732 213.9850 -1.8745 261.7229 263.5974 288.8904 214.7463 -1.8760 261.8433 263.7193 288.9939 215.5670 -1.8743 261.9556 263.8299 289.1074 216.3875 -1.8756 262.0483 263.9239 289.2342 217.1475 -1.8790 262.1612 264.0402 289.3594 218.0000 -1.8880 262.2809 264.1689 289.4751 218.7608 -1.8866 262.3741 264.2608 289.5618 219.5813 -1.8869 262.4797 264.3666 289.6771 220.3730 -1.8884 262.5932 264.4816 289.7917 221.1633 -1.8920 262.7015 264.5936 289.8967 222.0148 -1.8861 262.8226 264.7087 290.0313 222.7758 -1.8892 262.9374 264.8266 290.1354 223.5978 -1.8912 263.0388 264.9300 290.2663 224.3878 -1.8892 263.1398 265.0290 290.3813 225.1773 -1.8924 263.2266 265.1190 290.5076 226.0288 -1.8964 263.3424 265.2388 290.6205 226.7905 -1.8965 263.4520 265.3485 290.7192 227.6123 -1.8985 263.5615 265.4601 290.8484 228.4035 -1.8998 263.6718 265.5716 290.9701 229.1955 -1.9057 263.7751 265.6808 291.0994 230.0175 -1.9071 263.8913 265.7984 291.2106 230.7785 -1.9073 263.9997 265.9070 291.3345 231.6303 -1.9050 264.1209 266.0259 291.4630 232.4205 -1.9120 264.2269 266.1388 291.5824 233.2125 -1.9195 264.3334 266.2528 291.6806 234.0340 -1.9223 264.4370 266.3593 291.7944 234.7938 -1.9242 264.5323 266.4566 291.8949 235.6453 -1.9292 264.6616 266.5908 292.0331 236.4355 -1.9290 264.7830 266.7120 292.1410 237.2265 -1.9354 264.8928 266.8283 292.2348 238.0485 -1.9355 264.9905 266.9260 292.3371 238.8105 -1.9353 265.0947 267.0300 292.4232 239.6618 -1.9348 265.2096 267.1444 292.5286 240.4523 -1.9380 265.3121 267.2501 292.6432 241.2428 -1.9378 265.3948 267.3326 292.7465 242.0628 -1.9346 265.5178 267.4524 292.8536 242.8228 -1.9339 265.6511 267.5849 292.9812 243.6748 -1.9321 265.7612 267.6934 293.0778 244.4650 -1.9386 265.8668 267.8055 293.1631 245.2558 -1.9482 265.9705 267.9187 293.2497 246.0775 -1.9484 266.0763 268.0246 293.3561 246.8368 -1.9486 266.1908 268.1395 293.4442 247.6890 -1.9536 266.2922 268.2458 293.5348 248.4800 -1.9576 266.4007 268.3583 293.6250 249.2708 -1.9581 266.5149 268.4730 293.7132 250.0920 -1.9541 266.6264 268.5805 293.8198 250.8518 -1.9524 266.7339 268.6863 293.9103 251.7035 -1.9509 266.8603 268.8112 293.9976 252.4945 -1.9535 266.9506 268.9041 294.0973 253.2858 -1.9635 267.0678 269.0313 294.1828 254.1075 -1.9632 267.1674 269.1306 294.2804 254.8690 -1.9668 267.2741 269.2409 294.3655 255.7215 -1.9666 267.3772 269.3438 294.4615 256.4825 -1.9713 267.4834 269.4547 294.5437 257.3035 -1.9757 267.6010 269.5766 294.6394 258.1248 -1.9759 267.7053 269.6812 294.7350 258.8868 -1.9804 267.8048 269.7852 294.8281 259.7385 -1.9774 267.9269 269.9043 294.9316 260.4995 -1.9780 268.0316 270.0096 295.0082 261.3208 -1.9799 268.1515 270.1314 295.1117 262.1415 -1.9800 268.2704 270.2503 295.2087 262.9030 -1.9812 268.3645 270.3458 295.3183 263.7543 -1.9816 268.4907 270.4723 295.4083 264.5145 -1.9836 268.5891 270.5727 295.5045 265.3350 -1.9868 268.7123 270.6990 295.6033 266.1560 -1.9864 268.8263 270.8127 295.7160 266.9160 -1.9861 268.9278 270.9139 295.8167 267.7668 -1.9897 269.0396 271.0293 295.9212 268.5565 -1.9947 269.1462 271.1409 296.0218 269.3463 -1.9987 269.2429 271.2416 296.1426 270.1680 -1.9975 269.3679 271.3654 296.2210 270.9295 -1.9988 269.4672 271.4659 296.3135 271.7820 -1.9968 269.5852 271.5820 296.4450 272.5438 -2.0018 269.6788 271.6807 296.5406 273.3650 -2.0069 269.7955 271.8024 296.6397 274.1860 -2.0106 269.8863 271.8969 296.7497 274.9475 -2.0155 269.9998 272.0153 296.8709 275.7995 -2.0134 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