DTA measure 16.első Date: 202435:1110 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1018.90 s Mass = 1145.300 mg data_number = 1262 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0550 -2.1545 200.3395 202.4940 260.2886 1.8795 -2.1487 200.6136 202.7623 260.2995 2.6708 -2.1445 200.8524 202.9969 260.3143 3.4610 -2.1401 201.1179 203.2581 260.3404 4.2885 -2.1335 201.3652 203.4987 260.3398 5.0515 -2.1279 201.5960 203.7239 260.3655 5.9033 -2.1290 201.8588 203.9878 260.4030 6.6638 -2.1257 202.1105 204.2362 260.4168 7.4855 -2.1201 202.3629 204.4830 260.4592 8.3065 -2.1157 202.6170 204.7327 260.4965 9.0678 -2.1126 202.8398 204.9524 260.5508 9.9188 -2.1029 203.0993 205.2021 260.6247 10.6803 -2.1002 203.3272 205.4274 260.6901 11.5010 -2.0947 203.5637 205.6584 260.7548 12.3210 -2.0869 203.8644 205.9512 260.8506 13.0818 -2.0835 204.0711 206.1546 260.9170 13.9330 -2.0766 204.3235 206.4001 261.0393 14.6940 -2.0693 204.5334 206.6027 261.1051 15.5153 -2.0630 204.8008 206.8638 261.2073 16.3060 -2.0589 205.0555 207.1144 261.3158 17.0960 -2.0552 205.2897 207.3450 261.4360 17.9463 -2.0529 205.5357 207.5886 261.5400 18.7068 -2.0467 205.7565 207.8032 261.6886 19.5270 -2.0423 205.9897 208.0321 261.8076 20.3468 -2.0374 206.2424 208.2797 261.9350 21.1085 -2.0304 206.4745 208.5049 262.0919 21.9603 -2.0285 206.7207 208.7493 262.2482 22.7215 -2.0269 206.9556 208.9826 262.4026 23.5433 -2.0205 207.1946 209.2150 262.5738 24.3775 -2.0161 207.4575 209.4736 262.7386 25.3335 -2.0139 207.7337 209.7476 262.9401 26.1553 -2.0059 207.9715 209.9774 263.1278 26.9455 -2.0054 208.1959 210.2014 263.3073 27.7373 -2.0028 208.4063 210.4091 263.4905 28.5585 -1.9985 208.6376 210.6361 263.6778 29.3505 -1.9996 208.8872 210.8868 263.8552 30.1725 -1.9985 209.1300 211.1285 264.0634 30.9645 -1.9945 209.3600 211.3545 264.2283 31.7558 -1.9901 209.6013 211.5914 264.4231 32.5775 -1.9873 209.8583 211.8456 264.6090 33.3385 -1.9858 210.0585 212.0444 264.7876 34.1905 -1.9869 210.2865 212.2733 265.0115 34.9510 -1.9845 210.5015 212.4860 265.2001 35.7715 -1.9823 210.7309 212.7132 265.3820 36.5673 -1.9785 210.9727 212.9512 265.5586 37.3598 -1.9752 211.1843 213.1595 265.7698 38.1820 -1.9755 211.4298 213.4053 265.9631 38.9715 -1.9756 211.6610 213.6366 266.1300 39.7928 -1.9720 211.9066 213.8787 266.3196 40.5843 -1.9683 212.1202 214.0885 266.5071 41.3745 -1.9669 212.3294 214.2964 266.6785 42.1960 -1.9649 212.5693 214.5343 266.8777 42.9863 -1.9636 212.7986 214.7622 267.0278 43.8075 -1.9610 213.0254 214.9864 267.2103 44.5983 -1.9602 213.2455 215.2058 267.3880 45.5958 -1.9543 213.5182 215.4725 267.5551 46.4165 -1.9553 213.7549 215.7103 267.7293 47.1785 -1.9567 213.9636 215.9203 267.8796 48.0295 -1.9488 214.2027 216.1515 268.0444 48.7898 -1.9464 214.4238 216.3702 268.2016 49.6110 -1.9458 214.6680 216.6138 268.3679 50.4308 -1.9421 214.8865 216.8286 268.5219 51.1913 -1.9392 215.0972 217.0364 268.6553 52.0423 -1.9377 215.3449 217.2826 268.8173 52.8035 -1.9409 215.5365 217.4774 268.9411 53.6248 -1.9376 215.7567 217.6944 269.1045 54.4455 -1.9358 215.9890 217.9248 269.2395 55.2073 -1.9346 216.1994 218.1339 269.3389 56.0578 -1.9339 216.4374 218.3713 269.4717 56.8185 -1.9355 216.6429 218.5785 269.6191 57.6403 -1.9330 216.8663 218.7992 269.7535 58.4313 -1.9291 217.0842 219.0133 269.8819 59.2240 -1.9284 217.2847 219.2131 270.0219 60.0745 -1.9267 217.5345 219.4612 270.1255 60.8355 -1.9279 217.7308 219.6587 270.2263 61.6563 -1.9254 217.9807 219.9060 270.3576 62.4470 -1.9298 218.1776 220.1073 270.4754 63.2380 -1.9333 218.3875 220.3208 270.5868 64.0600 -1.9312 218.6237 220.5549 270.6720 64.8510 -1.9329 218.8428 220.7757 270.7881 65.6728 -1.9267 219.0577 220.9844 270.9123 66.4635 -1.9250 219.2615 221.1864 271.0282 67.2528 -1.9239 219.4705 221.3944 271.1087 68.0750 -1.9216 219.7018 221.6234 271.2204 68.8368 -1.9214 219.9105 221.8319 271.3202 69.6890 -1.9187 220.1127 222.0313 271.4421 70.4803 -1.9157 220.3352 222.2510 271.5423 71.2708 -1.9168 220.5514 222.4681 271.6364 72.0915 -1.9160 220.7741 222.6901 271.7580 72.8535 -1.9151 220.9636 222.8787 271.8602 73.7053 -1.9139 221.1958 223.1097 271.9796 74.4658 -1.9147 221.3902 223.3048 272.0843 75.2873 -1.9073 221.6015 223.5088 272.2028 76.0848 -1.9048 221.8048 223.7096 272.3017 76.8788 -1.9019 222.0151 223.9170 272.3998 77.7303 -1.8982 222.2466 224.1448 272.5240 78.4905 -1.9033 222.4480 224.3512 272.6138 79.3125 -1.8992 222.6754 224.5746 272.7422 80.1035 -1.9054 222.8719 224.7773 272.8277 80.8945 -1.9506 223.0721 225.0227 272.9752 81.7155 -1.9663 223.2909 225.2572 273.1133 82.5065 -2.0032 223.4909 225.4941 273.2293 83.3283 -2.0298 223.7052 225.7350 273.3447 84.1195 -2.0272 223.9067 225.9339 273.4709 84.9105 -2.0209 224.1106 226.1314 273.5943 85.7315 -2.0267 224.3356 226.3623 273.7333 86.5215 -2.0020 224.5432 226.5452 273.8612 87.3433 -1.9701 224.7533 226.7234 273.9895 88.1353 -1.9622 224.9437 226.9060 274.1215 88.9263 -1.9614 225.1505 227.1119 274.2412 89.7483 -1.9930 225.3867 227.3797 274.3752 90.5383 -2.0077 225.5687 227.5764 274.5052 91.3595 -1.9917 225.7866 227.7782 274.6725 92.1810 -1.9567 225.9654 227.9221 274.7880 93.0628 -1.9478 226.2003 228.1481 274.9609 93.8840 -1.9396 226.4168 228.3563 275.0872 94.6445 -1.9367 226.6238 228.5605 275.2066 95.4968 -1.9386 226.8433 228.7819 275.3659 96.2478 -1.9369 227.0180 228.9549 275.4932 97.0920 -1.9296 227.2101 229.1397 275.6384 97.8828 -1.9369 227.4061 229.3430 275.7685 98.7043 -1.9422 227.6382 229.5804 275.9154 99.4955 -1.9411 227.8302 229.7713 276.0569 100.2875 -1.9435 228.0225 229.9660 276.1937 101.1395 -1.9411 228.2444 230.1855 276.3465 101.9010 -1.9462 228.4314 230.3775 276.4666 102.7225 -1.9429 228.6094 230.5523 276.6137 103.5145 -1.9211 228.7934 230.7145 276.7653 104.3065 -1.9108 229.0045 230.9153 276.8935 105.1285 -1.9085 229.2315 231.1399 277.0459 105.8895 -1.9519 229.4207 231.3726 277.1898 106.8315 -1.9644 229.6204 231.5848 277.3676 107.5923 -1.9516 229.8416 231.7932 277.4894 108.4435 -1.9356 230.0438 231.9793 277.6353 109.2345 -1.9292 230.2240 232.1532 277.7681 110.0265 -1.9236 230.4338 232.3573 277.9224 110.8485 -1.9248 230.6399 232.5648 278.0727 111.6088 -1.9273 230.8252 232.7525 278.2164 112.4603 -1.9269 231.0310 232.9580 278.3593 113.2215 -1.9646 231.2135 233.1780 278.4935 114.0428 -1.9664 231.4240 233.3905 278.6209 114.8930 -1.9621 231.6303 233.5924 278.7816 115.6840 -1.9256 231.8091 233.7347 278.9128 116.4743 -1.9007 232.0049 233.9056 279.0526 117.2983 -1.9002 232.2153 234.1155 279.2124 118.0893 -1.9031 232.3928 234.2960 279.3574 118.9105 -1.9049 232.5960 234.5009 279.4798 119.7010 -1.9005 232.7733 234.6738 279.6173 120.4923 -1.9412 232.9838 234.9249 279.7542 121.3140 -1.9693 233.1916 235.1610 279.8824 122.1053 -1.9817 233.3797 235.3613 280.0103 122.9263 -1.9881 233.5772 235.5652 280.1501 123.7178 -1.9891 233.7583 235.7474 280.2948 124.5095 -1.9867 233.9393 235.9260 280.4341 125.3315 -1.9883 234.1466 236.1349 280.5648 126.0928 -1.9953 234.3400 236.3354 280.7051 127.0573 -2.0041 234.5639 236.5681 280.8790 127.9155 -2.0097 234.7746 236.7842 281.0036 128.6760 -2.0213 234.9315 236.9528 281.1502 129.5275 -2.0147 235.1531 237.1677 281.3032 130.3195 -2.0138 235.3446 237.3583 281.4360 131.1115 -2.0139 235.5497 237.5636 281.5607 131.9335 -1.9918 235.7181 237.7100 281.6959 132.6940 -1.9536 235.8926 237.8462 281.8249 133.5455 -1.9394 236.0932 238.0325 281.9741 134.3075 -1.9209 236.2752 238.1961 282.0872 135.1295 -1.9269 236.4683 238.3952 282.2198 135.9515 -1.9573 236.6535 238.6108 282.3462 136.8015 -1.9158 236.8542 238.7700 282.4826 137.7538 -1.8514 237.1027 238.9541 282.6482 138.6050 -1.8419 237.2910 239.1329 282.7823 139.3973 -1.8401 237.4740 239.3141 282.9289 140.1880 -1.8395 237.6520 239.4915 283.0662 141.0103 -1.8386 237.8527 239.6913 283.1943 141.7700 -1.8402 238.0354 239.8756 283.3204 142.6220 -1.8440 238.2179 240.0620 283.4392 143.4130 -1.8402 238.3982 240.2384 283.5701 144.2038 -1.8413 238.5891 240.4305 283.7061 145.0245 -1.8431 238.7521 240.5952 283.8358 145.7858 -1.8436 238.9393 240.7829 283.9635 146.6378 -1.8429 239.1643 241.0072 284.1116 147.3995 -1.8441 239.3460 241.1901 284.2374 148.2205 -1.8449 239.5197 241.3646 284.3514 149.0418 -1.8443 239.7099 241.5542 284.4776 149.8030 -1.8434 239.8918 241.7352 284.6037 150.6538 -1.8413 240.1073 241.9487 284.7479 151.4153 -1.8415 240.2674 242.1089 284.8786 152.2360 -1.8489 240.4372 242.2861 284.9889 153.0275 -1.8556 240.6351 242.4906 285.1218 153.8193 -1.8554 240.8217 242.6771 285.2633 154.6705 -1.8534 240.9998 242.8532 285.3815 155.4325 -1.8484 241.1710 243.0194 285.5101 156.2538 -1.8414 241.3665 243.2079 285.6175 157.0445 -1.8440 241.5425 243.3865 285.7539 157.8353 -1.8414 241.7252 243.5666 285.9037 158.6565 -1.8449 241.9204 243.7653 286.0419 159.4468 -1.8374 242.1057 243.9430 286.1597 160.2678 -1.8238 242.2837 244.1075 286.2922 161.0585 -1.8231 242.4563 244.2794 286.4027 161.8500 -1.8234 242.6282 244.4516 286.5233 162.6710 -1.8226 242.8136 244.6362 286.6643 163.4615 -1.8249 243.0049 244.8298 286.7862 164.2823 -1.8225 243.1916 245.0141 286.9098 165.0745 -1.8213 243.3746 245.1959 287.0388 165.8645 -1.8260 243.5468 245.3728 287.1460 166.6855 -1.8225 243.7262 245.5487 287.3057 167.4758 -1.8243 243.8934 245.7177 287.4294 168.4700 -1.8289 244.1426 245.9715 287.5735 169.2920 -1.8268 244.3216 246.1484 287.7063 170.0830 -1.8251 244.4772 246.3023 287.8274 170.9048 -1.8267 244.6634 246.4901 287.9447 171.6963 -1.8279 244.8463 246.6742 288.0817 172.4870 -1.8353 245.0210 246.8563 288.2079 173.3090 -1.8354 245.1985 247.0339 288.3481 174.0995 -1.8380 245.3889 247.2269 288.4634 174.9210 -1.8349 245.5756 247.4105 288.5891 175.7120 -1.8286 245.7467 247.5753 288.7497 176.5035 -1.8129 245.9213 247.7341 288.8488 177.3248 -1.8282 246.0951 247.9233 288.9612 178.1143 -1.8342 246.2757 248.1099 289.0945 178.9355 -1.8371 246.4863 248.3234 289.2268 179.7258 -1.8406 246.6428 248.4834 289.3558 180.5163 -1.8432 246.8040 248.6473 289.4691 181.3673 -1.8386 246.9823 248.8210 289.6273 182.1275 -1.8399 247.1533 248.9932 289.7230 182.9490 -1.8434 247.3299 249.1733 289.8445 183.7405 -1.8445 247.4979 249.3424 289.9653 184.5318 -1.8486 247.6514 249.5000 290.0967 185.3833 -1.8449 247.8496 249.6945 290.2319 186.1445 -1.8516 248.0257 249.8772 290.3379 186.9665 -1.8588 248.2243 250.0831 290.4667 187.7575 -1.8584 248.4028 250.2612 290.5496 188.5488 -1.8573 248.5503 250.4076 290.7110 189.3995 -1.8639 248.7412 250.6050 290.8330 190.1605 -1.8711 248.9036 250.7748 290.9657 190.9813 -1.8721 249.0916 250.9638 291.0923 191.7725 -1.8679 249.2555 251.1234 291.2236 192.5625 -1.8693 249.4469 251.3162 291.3344 193.4138 -1.8710 249.6120 251.4831 291.4759 194.1740 -1.8723 249.7777 251.6499 291.6093 194.9950 -1.8750 249.9632 251.8382 291.7384 195.8160 -1.8758 250.0972 251.9731 291.8582 196.5753 -1.8722 250.2647 252.1369 292.0028 197.4268 -1.8754 250.4529 252.3283 292.1636 198.1878 -1.8813 250.6277 252.5089 292.2730 199.1898 -1.8821 250.8269 252.7090 292.4554 200.0418 -1.8842 251.0164 252.9006 292.5881 200.8020 -1.8879 251.1951 253.0830 292.7424 201.6230 -1.8869 251.3730 253.2599 292.8823 202.4438 -1.8739 251.5405 253.4145 293.0166 203.2055 -1.8707 251.7116 253.5823 293.1472 204.0573 -1.8871 251.8867 253.7738 293.2927 204.8185 -1.8871 252.0494 253.9365 293.4332 205.6400 -1.8692 252.2278 254.0970 293.5864 206.4615 -1.8675 252.4128 254.2802 293.7448 207.2213 -1.8760 252.5817 254.4577 293.8916 208.0723 -1.8762 252.7645 254.6406 294.0318 208.8625 -1.8794 252.9179 254.7973 294.1671 209.6530 -1.8769 253.1002 254.9771 294.3137 210.4735 -1.8764 253.2387 255.1151 294.4573 211.2343 -1.8742 253.4071 255.2814 294.5905 212.0853 -1.8770 253.6036 255.4807 294.7541 212.8765 -1.8856 253.7685 255.6541 294.9068 213.6683 -1.8909 253.9177 255.8086 295.0511 214.4895 -1.8900 254.0989 255.9889 295.1910 215.2515 -1.8920 254.2441 256.1362 295.3180 216.1028 -1.8920 254.4304 256.3225 295.4669 216.8933 -1.8911 254.6102 256.5012 295.6193 217.6845 -1.8978 254.7903 256.6881 295.7662 218.5063 -1.8987 254.9469 256.8456 295.9106 219.2665 -1.9003 255.1159 257.0162 296.0448 220.1188 -1.9008 255.2853 257.1862 296.1849 220.8790 -1.9003 255.4519 257.3522 296.3054 221.7005 -1.9002 255.6121 257.5123 296.4494 222.5220 -1.9017 255.7683 257.6700 296.5883 223.2830 -1.9057 255.9411 257.8468 296.7167 224.1345 -1.9048 256.1068 258.0116 296.8685 224.8958 -1.9078 256.2639 258.1717 296.9949 225.7175 -1.9082 256.4560 258.3642 297.1086 226.5420 -1.9058 256.6342 258.5401 297.2498 227.3038 -1.9087 256.7844 258.6931 297.3866 228.1558 -1.9123 256.9651 258.8774 297.4982 228.9175 -1.9180 257.1370 259.0550 297.6255 229.9090 -1.9212 257.3232 259.2444 297.7866 230.7603 -1.9278 257.4901 259.4179 297.9139 231.5500 -1.9247 257.6823 259.6070 298.0234 232.3393 -1.9265 257.8472 259.7738 298.1734 233.1600 -1.9255 258.0061 259.9316 298.3078 233.9205 -1.9265 258.1539 260.0804 298.4320 234.7723 -1.9257 258.3302 260.2559 298.5400 235.5625 -1.9313 258.4960 260.4273 298.6587 236.3533 -1.9279 258.6559 260.5838 298.7815 237.1745 -1.9243 258.8473 260.7716 298.9064 237.9350 -1.9176 258.9996 260.9172 299.0330 238.7865 -1.9166 259.1529 261.0695 299.1672 239.5775 -1.9231 259.3131 261.2362 299.2954 240.3685 -1.9226 259.4870 261.4096 299.4319 241.1893 -1.9199 259.6740 261.5939 299.5536 241.9513 -1.9254 259.8503 261.7756 299.6695 242.8030 -1.9231 259.9857 261.9088 299.7786 243.5640 -1.9282 260.1542 262.0824 299.9148 244.3853 -1.9355 260.3250 262.2605 300.0172 245.2060 -1.9372 260.4862 262.4234 300.1397 245.9668 -1.9412 260.6554 262.5966 300.2489 246.8180 -1.9396 260.8295 262.7692 300.3901 247.5790 -1.9425 260.9830 262.9254 300.5116 248.4008 -1.9425 261.1600 263.1025 300.6333 249.1920 -1.9407 261.2979 263.2386 300.7402 249.9823 -1.9432 261.4713 263.4146 300.8723 250.8340 -1.9397 261.6364 263.5761 301.0024 251.5943 -1.9350 261.7907 263.7257 301.1213 252.4143 -1.9307 261.9489 263.8796 301.2608 253.2045 -1.9378 262.1192 264.0570 301.3948 253.9950 -1.9401 262.2797 264.2198 301.5235 254.8455 -1.9347 262.4315 264.3662 301.6449 255.6068 -1.9385 262.5896 264.5281 301.7754 256.4280 -1.9395 262.7771 264.7166 301.9148 257.2183 -1.9401 262.9376 264.8777 302.0532 258.0080 -1.9419 263.0730 265.0149 302.1796 258.8585 -1.9455 263.2450 265.1905 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