DTA measure 16.második Date: 202435:1228 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.27 s Mass = 1145.300 mg data_number = 1583 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1505 -1.4407 227.1186 228.5593 261.4123 2.0028 -1.4381 227.2663 228.7044 261.3721 2.7615 -1.4348 227.3896 228.8244 261.3526 3.5828 -1.4245 227.5124 228.9368 261.3406 4.3740 -1.4147 227.6567 229.0714 261.3359 5.1643 -1.4255 227.7911 229.2166 261.3473 6.0160 -1.4364 227.9399 229.3764 261.3543 6.7778 -1.4372 228.0462 229.4834 261.3467 7.5995 -1.4267 228.1733 229.6000 261.3383 8.3895 -1.4207 228.2910 229.7117 261.3761 9.1805 -1.4274 228.4158 229.8432 261.4167 10.0020 -1.4271 228.5634 229.9905 261.4365 10.7935 -1.4249 228.6785 230.1034 261.4786 11.6155 -1.4191 228.8177 230.2368 261.5338 12.4065 -1.4177 228.9649 230.3826 261.5704 13.1985 -1.4176 229.0726 230.4902 261.6151 14.0205 -1.4166 229.1891 230.6057 261.6956 14.8003 -1.4145 229.3188 230.7333 261.7519 15.6140 -1.4134 229.4681 230.8815 261.8147 16.4058 -1.4146 229.6040 231.0186 261.8851 17.2565 -1.4060 229.7097 231.1158 261.9944 18.0168 -1.3972 229.8303 231.2274 262.0879 18.8380 -1.4026 229.9629 231.3654 262.1813 19.6293 -1.4046 230.1070 231.5117 262.2616 20.4195 -1.4075 230.2410 231.6485 262.3569 21.2703 -1.4090 230.3716 231.7806 262.4716 22.0295 -1.4058 230.4886 231.8944 262.5779 22.8488 -1.4012 230.6176 232.0188 262.6963 23.6395 -1.3949 230.7615 232.1564 262.8179 24.4298 -1.3959 230.8709 232.2668 262.9246 25.2808 -1.3979 230.9948 232.3927 263.0747 26.0420 -1.3931 231.1170 232.5101 263.1912 26.8630 -1.3887 231.2542 232.6428 263.3389 27.6530 -1.3990 231.3671 232.7661 263.4876 28.4443 -1.4062 231.5030 232.9092 263.6393 29.2958 -1.3901 231.6126 233.0027 263.7842 30.0560 -1.3901 231.7436 233.1338 263.9288 30.8800 -1.3912 231.8969 233.2881 264.0872 31.6743 -1.3788 232.0297 233.4086 264.2420 32.4648 -1.3785 232.1377 233.5162 264.4147 33.2860 -1.3896 232.2612 233.6508 264.5565 34.0755 -1.3971 232.3905 233.7876 264.7013 34.8965 -1.3944 232.5224 233.9169 264.8540 35.7033 -1.3949 232.6465 234.0415 265.0196 36.5238 -1.4025 232.7749 234.1775 265.1796 37.3143 -1.4021 232.9080 234.3101 265.3283 38.1045 -1.4032 233.0272 234.4304 265.4927 38.9553 -1.4057 233.1615 234.5673 265.6714 39.7143 -1.4099 233.2734 234.6833 265.8090 40.5358 -1.4059 233.3955 234.8014 265.9581 41.3275 -1.4060 233.5350 234.9410 266.0934 42.1188 -1.4059 233.6736 235.0795 266.2374 42.9695 -1.4080 233.7991 235.2072 266.4318 43.7315 -1.4063 233.9207 235.3270 266.5420 44.5528 -1.4088 234.0458 235.4545 266.6968 45.3425 -1.4053 234.1796 235.5848 266.8310 46.1345 -1.4049 234.2900 235.6949 266.9556 46.9565 -1.4103 234.4039 235.8142 267.0956 47.7463 -1.4119 234.5327 235.9446 267.2389 48.5665 -1.4124 234.6580 236.0704 267.3708 49.3598 -1.4134 234.8141 236.2274 267.4813 50.1525 -1.4056 234.9374 236.3430 267.6220 50.9758 -1.4144 235.0592 236.4735 267.7593 51.7375 -1.4116 235.1600 236.5716 267.8893 52.5893 -1.4115 235.2956 236.7071 268.0006 53.3490 -1.4612 235.4289 236.8901 268.1034 54.1700 -1.4669 235.5531 237.0200 268.2275 54.9900 -1.4621 235.6891 237.1512 268.3327 55.7555 -1.4637 235.8011 237.2648 268.4389 56.5980 -1.4756 235.9342 237.4098 268.5555 57.3570 -1.4678 236.0547 237.5224 268.6457 58.2078 -1.4702 236.1923 237.6624 268.7720 58.9680 -1.4639 236.3174 237.7814 268.8654 59.7888 -1.4600 236.4422 237.9022 268.9735 60.6088 -1.4633 236.5662 238.0295 269.0759 61.3690 -1.4675 236.6855 238.1531 269.1709 62.2203 -1.4728 236.8238 238.2966 269.2681 62.9798 -1.4735 236.9263 238.3997 269.3497 63.8008 -1.4779 237.0768 238.5547 269.4463 64.6215 -1.4796 237.2101 238.6898 269.5504 65.3815 -1.4792 237.3268 238.8060 269.6304 66.2323 -1.4794 237.4477 238.9271 269.7097 66.9915 -1.4868 237.5603 239.0472 269.7883 67.8113 -1.4945 237.6853 239.1798 269.8799 68.6315 -1.5007 237.8261 239.3267 269.9877 69.3920 -1.4990 237.9392 239.4382 270.0706 70.2433 -1.4807 238.0849 239.5656 270.1477 71.0330 -1.4829 238.2068 239.6896 270.2311 71.8250 -1.4841 238.3385 239.8227 270.3226 72.6455 -1.4830 238.4506 239.9335 270.3880 73.4070 -1.4715 238.5735 240.0449 270.4579 74.2583 -1.4729 238.6949 240.1679 270.5570 75.0193 -1.4723 238.8094 240.2816 270.6393 75.8410 -1.4676 238.9442 240.4118 270.7262 76.6095 -1.4573 239.0655 240.5227 270.7955 77.4728 -1.4812 239.2098 240.6909 270.8653 78.2320 -1.4866 239.3341 240.8206 270.9593 79.0548 -1.4793 239.4556 240.9349 271.0392 79.8770 -1.4790 239.5745 241.0535 271.1390 80.6378 -1.4880 239.6951 241.1830 271.2065 81.4890 -1.4865 239.8153 241.3018 271.2831 82.2498 -1.4837 239.9306 241.4143 271.3598 83.0710 -1.4813 240.0707 241.5520 271.4733 83.8630 -1.4858 240.1812 241.6670 271.5728 84.6535 -1.4827 240.3115 241.7941 271.6564 85.5035 -1.4733 240.4515 241.9248 271.7851 86.2645 -1.4678 240.5717 242.0395 271.8642 87.0858 -1.4394 240.6836 242.1230 271.9482 87.9055 -1.4321 240.8131 242.2452 272.0467 88.6673 -1.4241 240.9262 242.3503 272.1140 89.5185 -1.4255 241.0730 242.4985 272.2262 90.2805 -1.4231 241.1880 242.6111 272.3149 91.1020 -1.4253 241.3028 242.7281 272.4020 91.9235 -1.4219 241.4263 242.8483 272.5395 92.6855 -1.4193 241.5315 242.9507 272.6232 93.5375 -1.4205 241.6739 243.0944 272.7233 94.2985 -1.4205 241.7956 243.2161 272.8379 95.1178 -1.4268 241.9028 243.3296 272.9382 95.9375 -1.4427 242.0364 243.4791 273.0494 96.7073 -1.4559 242.1574 243.6133 273.1647 97.5275 -1.4541 242.2970 243.7511 273.2589 98.3180 -1.4418 242.4045 243.8463 273.3569 99.1385 -1.4455 242.5469 243.9924 273.4750 99.8993 -1.4735 242.6509 244.1244 273.5784 100.7543 -1.5059 242.7728 244.2787 273.7009 101.5465 -1.5055 242.8823 244.3878 273.8436 102.3365 -1.4984 243.0025 244.5009 273.9812 103.1568 -1.4888 243.1331 244.6219 274.0755 103.9160 -1.4897 243.2633 244.7529 274.1668 104.7688 -1.5072 243.3760 244.8832 274.3084 105.5583 -1.4975 243.4893 244.9868 274.4188 106.3480 -1.4910 243.6305 245.1214 274.5391 107.1683 -1.4984 243.7317 245.2301 274.6352 107.9580 -1.5009 243.8519 245.3528 274.7497 108.7818 -1.4916 243.9822 245.4738 274.8715 109.5738 -1.4619 244.0942 245.5561 275.0089 110.3643 -1.4556 244.2256 245.6811 275.1214 111.1863 -1.4555 244.3464 245.8020 275.2431 111.9768 -1.4520 244.4643 245.9163 275.3384 112.7965 -1.4524 244.5949 246.0473 275.4632 113.5888 -1.4563 244.7048 246.1611 275.5901 114.3795 -1.4596 244.8448 246.3044 275.7032 115.2005 -1.4613 244.9567 246.4181 275.8079 115.9915 -1.4542 245.0997 246.5539 275.9303 116.8118 -1.4621 245.2296 246.6917 276.0716 117.5720 -1.4620 245.3235 246.7855 276.1770 118.4348 -1.4649 245.4455 246.9104 276.3012 119.1965 -1.4662 245.5547 247.0210 276.4377 120.0198 -1.4573 245.6802 247.1375 276.5276 120.8110 -1.4690 245.8015 247.2704 276.6531 121.6033 -1.4700 245.9190 247.3890 276.7571 122.4268 -1.4748 246.0500 247.5248 276.8871 123.2190 -1.4832 246.1749 247.6581 276.9968 124.0403 -1.4803 246.2814 247.7618 277.0992 124.8315 -1.4783 246.4071 247.8854 277.2259 125.6235 -1.4748 246.5199 247.9947 277.3333 126.4453 -1.4708 246.6752 248.1460 277.4432 127.2058 -1.4749 246.7821 248.2571 277.5324 128.0325 -1.4848 246.8905 248.3753 277.6379 128.8535 -1.5174 247.0090 248.5264 277.7365 129.6438 -1.5123 247.1389 248.6512 277.8456 130.4345 -1.5230 247.2609 248.7839 277.9353 131.2570 -1.5432 247.3817 248.9249 278.0377 132.0465 -1.5436 247.4880 249.0315 278.1306 132.8673 -1.5138 247.6224 249.1362 278.2520 133.6580 -1.5057 247.7350 249.2407 278.3477 134.4490 -1.5043 247.8544 249.3587 278.4362 135.2708 -1.5059 247.9763 249.4822 278.5354 136.0605 -1.5052 248.0970 249.6022 278.6254 136.8815 -1.4952 248.2142 249.7094 278.7398 137.6738 -1.4992 248.3373 249.8365 278.8294 138.4683 -1.5039 248.4615 249.9653 278.9282 139.2885 -1.5120 248.5843 250.0963 279.0084 140.0488 -1.5183 248.6948 250.2130 279.0910 140.9003 -1.5160 248.8262 250.3422 279.2019 141.6910 -1.5099 248.9367 250.4466 279.3084 142.4835 -1.5087 249.0576 250.5663 279.3846 143.3055 -1.5108 249.1822 250.6930 279.4938 144.0675 -1.5095 249.3041 250.8136 279.5678 144.9193 -1.5153 249.4202 250.9354 279.6742 145.6795 -1.5233 249.5377 251.0610 279.7550 146.5015 -1.5238 249.6609 251.1846 279.8575 147.3235 -1.5215 249.7902 251.3117 279.9515 148.1078 -1.5200 249.9035 251.4235 280.0412 148.9118 -1.5068 250.0291 251.5359 280.1347 149.7028 -1.5173 250.1496 251.6669 280.2432 150.5225 -1.5164 250.2501 251.7665 280.3360 151.2835 -1.5236 250.3623 251.8860 280.4275 152.1360 -1.5252 250.4893 252.0144 280.5467 152.9273 -1.5234 250.6060 252.1294 280.6391 153.7185 -1.5260 250.7162 252.2422 280.7431 154.5413 -1.5243 250.8415 252.3658 280.8286 155.3023 -1.5173 250.9667 252.4840 280.9318 156.1555 -1.5137 251.0954 252.6091 281.0502 156.9170 -1.5058 251.2035 252.7093 281.1411 157.7393 -1.5009 251.3488 252.8497 281.2412 158.5293 -1.5036 251.4465 252.9501 281.3432 159.3600 -1.5077 251.5630 253.0707 281.4818 160.1205 -1.5059 251.6767 253.1827 281.5797 160.9728 -1.5046 251.7946 253.2992 281.6765 161.7338 -1.5035 251.9052 253.4087 281.7797 162.5550 -1.5005 252.0233 253.5237 281.9042 163.3465 -1.5018 252.1531 253.6549 282.0063 164.1378 -1.5021 252.2668 253.7689 282.1047 164.9595 -1.5028 252.3781 253.8809 282.2250 165.7505 -1.5042 252.5031 254.0073 282.3233 166.5710 -1.5056 252.6372 254.1429 282.4364 167.3625 -1.5099 252.7381 254.2480 282.5467 168.1545 -1.5138 252.8809 254.3947 282.6570 168.9608 -1.5110 252.9950 254.5060 282.7662 169.7805 -1.5101 253.0966 254.6067 282.8902 170.5420 -1.5114 253.2076 254.7190 283.0068 171.3935 -1.5137 253.3398 254.8535 283.1134 172.1550 -1.5127 253.4547 254.9675 283.2291 172.9763 -1.5192 253.5582 255.0775 283.3320 173.7975 -1.5201 253.7090 255.2291 283.4297 174.5595 -1.5219 253.8293 255.3513 283.5099 175.4105 -1.5211 253.9422 255.4633 283.6663 176.1720 -1.5218 254.0466 255.5684 283.7632 176.9910 -1.5190 254.1677 255.6866 283.8872 177.7825 -1.5210 254.2710 255.7919 283.9768 178.5930 -1.5223 254.3904 255.9127 284.0855 179.3828 -1.5239 254.5132 256.0371 284.1814 180.2043 -1.5269 254.6389 256.1659 284.3165 180.9938 -1.5277 254.7548 256.2825 284.4146 181.8140 -1.5280 254.8768 256.4048 284.5370 182.6040 -1.5283 254.9851 256.5134 284.6458 183.3940 -1.5314 255.0830 256.6145 284.7338 184.2150 -1.5358 255.2226 256.7584 284.8436 185.0050 -1.5375 255.3383 256.8758 284.9630 185.8258 -1.5410 255.4462 256.9872 285.0833 186.6180 -1.5401 255.5576 257.0978 285.1676 187.4103 -1.5411 255.6738 257.2149 285.2734 188.2318 -1.5424 255.7792 257.3216 285.3905 189.0330 -1.5435 255.9156 257.4591 285.5107 189.8055 -1.5464 256.0244 257.5708 285.5967 190.6578 -1.5466 256.1702 257.7169 285.7179 191.4190 -1.5513 256.2530 257.8043 285.8307 192.2400 -1.5497 256.3735 257.9232 285.9433 193.0305 -1.5509 256.4963 258.0472 286.0400 193.8215 -1.5520 256.6154 258.1674 286.1560 194.6425 -1.5508 256.7408 258.2916 286.2725 195.4335 -1.5528 256.8577 258.4105 286.3899 196.2555 -1.5513 256.9763 258.5277 286.4758 197.0463 -1.5534 257.1155 258.6689 286.5863 197.8365 -1.5565 257.2119 258.7684 286.6904 198.6575 -1.5573 257.3416 258.8989 286.7932 199.4775 -1.5586 257.4551 259.0138 286.9056 200.2285 -1.5600 257.5530 259.1130 287.0211 201.0803 -1.5614 257.6877 259.2491 287.1403 201.8408 -1.5651 257.7778 259.3428 287.2324 202.6645 -1.5634 257.9083 259.4717 287.3408 203.4853 -1.5661 258.0351 259.6013 287.4576 204.2460 -1.5687 258.1181 259.6868 287.5655 205.0980 -1.5702 258.2640 259.8342 287.6984 205.8590 -1.5704 258.3867 259.9571 287.7978 206.6803 -1.5722 258.4937 260.0659 287.8893 207.4710 -1.5709 258.6236 260.1945 288.0043 208.2625 -1.5745 258.7208 260.2953 288.1134 209.1148 -1.5728 258.8422 260.4150 288.2162 209.9190 -1.5719 258.9592 260.5311 288.3254 210.6798 -1.5780 259.0755 260.6535 288.4200 211.5010 -1.5802 259.1859 260.7661 288.5433 212.2910 -1.5736 259.3160 260.8896 288.6467 213.0820 -1.5752 259.4222 260.9973 288.7732 213.9338 -1.5736 259.5309 261.1045 288.8782 214.6938 -1.5756 259.6427 261.2183 288.9586 215.5148 -1.5781 259.7720 261.3501 289.0425 216.3355 -1.5897 259.8738 261.4635 289.1784 217.0958 -1.5914 259.9879 261.5793 289.2870 217.9463 -1.5933 260.1275 261.7208 289.3968 218.7075 -1.5951 260.2406 261.8358 289.4931 219.5490 -1.5950 260.3519 261.9469 289.6145 220.3415 -1.5952 260.4637 262.0589 289.7014 221.1325 -1.5960 260.5837 262.1797 289.8051 221.9233 -1.5961 260.7068 262.3029 289.9212 222.7735 -1.5970 260.8276 262.4246 290.0411 223.5350 -1.6020 260.9368 262.5388 290.1296 224.3553 -1.6011 261.0493 262.6504 290.2670 225.1455 -1.6037 261.1548 262.7585 290.3729 225.9368 -1.6049 261.2756 262.8805 290.4558 226.7883 -1.6069 261.4112 263.0181 290.5859 227.5495 -1.6139 261.5178 263.1317 290.6788 228.3713 -1.6214 261.6420 263.2633 290.7806 229.1625 -1.6325 261.7471 263.3796 290.8808 229.9768 -1.6305 261.8582 263.4887 291.0059 230.7573 -1.6327 261.9734 263.6061 291.1016 231.5788 -1.6282 262.0971 263.7253 291.2089 232.4000 -1.6233 262.2179 263.8413 291.2891 233.1603 -1.6318 262.3106 263.9424 291.4111 234.0120 -1.6307 262.4439 264.0746 291.5078 234.7730 -1.6334 262.5557 264.1891 291.6220 235.5930 -1.6299 262.6660 264.2959 291.7168 236.4140 -1.6204 262.7775 264.3979 291.8300 237.1755 -1.6194 262.9048 264.5242 291.9509 238.0278 -1.6280 263.0305 264.6585 292.0523 238.7888 -1.6399 263.1363 264.7762 292.1679 239.6098 -1.6455 263.2445 264.8900 292.2598 240.4308 -1.6386 263.3776 265.0162 292.3694 241.1908 -1.6407 263.4746 265.1153 292.4846 242.0425 -1.6477 263.5959 265.2436 292.5751 242.8045 -1.6424 263.7174 265.3597 292.6754 243.6258 -1.6438 263.8571 265.5009 292.7717 244.4455 -1.6518 263.9495 265.6013 292.8851 245.2053 -1.6641 264.0563 265.7204 292.9844 246.0565 -1.6553 264.1810 265.8363 293.0980 246.8468 -1.6542 264.2764 265.9306 293.2085 247.6373 -1.6637 264.4011 266.0648 293.3110 248.4883 -1.6647 264.5406 266.2053 293.4352 249.2495 -1.6672 264.6457 266.3129 293.5304 250.0715 -1.6714 264.7661 266.4375 293.6209 250.8783 -1.7082 264.8641 266.5723 293.7166 251.6695 -1.7076 264.9908 266.6984 293.8297 252.4615 -1.7218 265.0976 266.8193 293.9188 253.2833 -1.7019 265.2457 266.9477 294.0236 254.0730 -1.6699 265.3471 267.0170 294.1250 254.8938 -1.6686 265.4739 267.1424 294.2263 255.6865 -1.7082 265.5494 267.2576 294.3159 256.4780 -1.7498 265.6911 267.4409 294.4264 257.3013 -1.7322 265.8019 267.5340 294.5166 258.0610 -1.6961 265.9070 267.6031 294.6137 258.9170 -1.6850 266.0499 267.7349 294.7367 259.6788 -1.6844 266.1535 267.8379 294.8271 260.5180 -1.6774 266.2773 267.9547 294.9164 261.3008 -1.6830 266.3701 268.0531 295.0131 262.1230 -1.6888 266.4873 268.1761 295.1065 262.8850 -1.6871 266.6034 268.2906 295.1953 263.7368 -1.6904 266.7224 268.4128 295.3130 264.4978 -1.7005 266.8270 268.5276 295.3988 265.3190 -1.7035 266.9389 268.6424 295.5123 266.1405 -1.7213 267.0563 268.7776 295.6091 266.9015 -1.7205 267.1712 268.8918 295.6987 267.7528 -1.7325 267.2950 269.0275 295.8330 268.5140 -1.7372 267.3966 269.1338 295.9096 269.3353 -1.7350 267.5118 269.2468 295.9948 270.1565 -1.7438 267.6345 269.3783 296.0828 270.9353 -1.7412 267.7419 269.4831 296.1892 271.7445 -1.7255 267.8720 269.5975 296.3004 272.5363 -1.7264 267.9926 269.7190 296.3860 273.3575 -1.7245 268.1018 269.8263 296.4927 274.1488 -1.7301 268.2234 269.9535 296.5825 274.9705 -1.7256 268.3584 270.0840 296.6899 275.7623 -1.7217 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