DTA measure 3pb_updown4 Date: 202449:127 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1529.65 s Mass = 1118.000 mg data_number = 1902 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2553 -3.7837 363.0153 366.7990 380.0065 2.0155 -3.7807 363.1143 366.8950 380.0236 2.8368 -3.7791 363.2107 366.9898 380.0081 3.6275 -3.7786 363.3055 367.0841 380.0205 4.4203 -3.7741 363.3964 367.1706 380.0379 5.2748 -3.7681 363.4873 367.2554 380.0649 6.0360 -3.7590 363.5745 367.3335 380.0713 6.8565 -3.7536 363.6687 367.4223 380.0800 7.6480 -3.7522 363.7487 367.5009 380.1081 8.4398 -3.7502 363.8488 367.5990 380.1259 9.2913 -3.7501 363.9665 367.7166 380.1289 10.0505 -3.7484 364.0470 367.7954 380.1276 10.8710 -3.7438 364.1376 367.8814 380.1405 11.6915 -3.7440 364.2260 367.9700 380.1374 12.4528 -3.7482 364.3121 368.0602 380.1428 13.3038 -3.7452 364.3998 368.1450 380.1307 14.0643 -3.7418 364.4827 368.2245 380.1186 14.8850 -3.7398 364.5733 368.3131 380.1093 15.7050 -3.7381 364.6688 368.4068 380.1221 16.4663 -3.7382 364.7540 368.4921 380.1061 17.3180 -3.7389 364.8548 368.5937 380.0713 18.0790 -3.7376 364.9222 368.6597 380.0522 18.9003 -3.7317 365.0223 368.7540 380.0256 19.7220 -3.7293 365.1113 368.8405 379.9938 20.4848 -3.7280 365.1756 368.9036 379.9556 21.3368 -3.7235 365.2716 368.9951 379.9241 22.0970 -3.7187 365.3655 369.0843 379.8956 22.9188 -3.7208 365.4462 369.1670 379.8656 23.7108 -3.7192 365.5335 369.2527 379.8186 24.5025 -3.7153 365.6095 369.3248 379.7726 25.5083 -3.7121 365.7202 369.4323 379.7079 26.3205 -3.7100 365.8041 369.5141 379.6472 27.1425 -3.7040 365.9029 369.6068 379.5989 27.9335 -3.6973 365.9755 369.6728 379.5572 28.7255 -3.6958 366.0460 369.7419 379.4921 29.5475 -3.6968 366.1124 369.8092 379.4291 30.3085 -3.6947 366.2063 369.9009 379.3792 31.1603 -3.6945 366.2911 369.9856 379.3050 31.9513 -3.6919 366.3733 370.0652 379.2355 32.7415 -3.6865 366.4513 370.1378 379.1674 33.5625 -3.6826 366.5349 370.2175 379.0982 34.3235 -3.6793 366.6014 370.2807 379.0277 35.1755 -3.6758 366.6749 370.3507 378.9539 35.9668 -3.6736 366.7426 370.4162 378.8974 36.7578 -3.6677 366.8433 370.5110 378.8240 37.5773 -3.6624 366.9101 370.5725 378.7316 38.3385 -3.6589 366.9734 370.6323 378.6782 39.1900 -3.6563 367.0595 370.7157 378.5985 39.9813 -3.6511 367.1334 370.7845 378.5164 40.7720 -3.6456 367.2099 370.8555 378.4445 41.5940 -3.6433 367.2991 370.9424 378.3850 42.3533 -3.6372 367.3722 371.0094 378.3009 43.2050 -3.6323 367.4424 371.0748 378.1996 43.9645 -3.6267 367.5043 371.1310 378.1311 44.7850 -3.6222 367.5694 371.1916 378.0710 45.6060 -3.6181 367.6626 371.2807 377.9875 46.3675 -3.6163 367.7269 371.3432 377.9110 47.2198 -3.6083 367.7816 371.3899 377.8260 47.9810 -3.6039 367.8485 371.4524 377.7586 48.8040 -3.6000 367.9131 371.5131 377.6752 49.6235 -3.5947 367.9984 371.5931 377.5972 50.3843 -3.5915 368.0518 371.6432 377.5410 51.2348 -3.5882 368.1081 371.6963 377.4438 51.9948 -3.5837 368.1655 371.7492 377.3654 52.8148 -3.5787 368.2484 371.8271 377.3027 53.6343 -3.5723 368.3214 371.8936 377.2168 54.3953 -3.5665 368.3778 371.9443 377.1528 55.2458 -3.5604 368.4571 372.0175 377.0662 56.0115 -3.5589 368.5086 372.0675 377.0047 56.8343 -3.5566 368.5706 372.1272 376.9418 57.6230 -3.5472 368.6294 372.1765 376.8843 58.4120 -3.5442 368.6977 372.2418 376.8091 59.2625 -3.5428 368.7605 372.3033 376.7130 60.0235 -3.5379 368.7962 372.3341 376.6317 60.8443 -3.5342 368.8698 372.4040 376.5713 61.6355 -3.5304 368.9323 372.4627 376.5189 62.4258 -3.5261 368.9950 372.5211 376.4597 63.2753 -3.5219 369.0705 372.5924 376.3823 64.0345 -3.5161 369.1158 372.6319 376.3190 64.8553 -3.5101 369.1608 372.6709 376.2475 65.6755 -3.5061 369.2352 372.7413 376.2033 66.4343 -3.5031 369.2908 372.7939 376.1505 67.2848 -3.4959 369.3381 372.8340 376.0872 68.0440 -3.4936 369.3975 372.8911 376.0222 68.8650 -3.4896 369.4495 372.9392 375.9721 69.6850 -3.4845 369.5046 372.9891 375.9269 70.4443 -3.4768 369.5631 373.0399 375.8811 71.2958 -3.4758 369.6050 373.0808 375.8255 72.0550 -3.4719 369.6607 373.1327 375.7632 72.8763 -3.4640 369.7039 373.1679 375.7564 73.6978 -3.4606 369.7565 373.2171 375.7124 74.4580 -3.4557 369.8079 373.2635 375.6641 75.3085 -3.4511 369.8590 373.3102 375.5956 76.1433 -3.4434 369.9160 373.3594 375.5396 77.1295 -3.4357 369.9676 373.4033 375.5015 77.9205 -3.4326 370.0402 373.4728 375.4570 78.7408 -3.4261 370.0606 373.4867 375.3974 79.5038 -3.4237 370.1183 373.5420 375.3634 80.3565 -3.4209 370.1641 373.5850 375.3150 81.1475 -3.4184 370.2165 373.6350 375.2594 81.9393 -3.4123 370.2753 373.6875 375.2183 82.7590 -3.4111 370.3009 373.7120 375.1460 83.5183 -3.4091 370.3414 373.7505 375.1087 84.3685 -3.3983 370.3881 373.7865 375.0429 85.1580 -3.3947 370.4366 373.8313 375.0055 85.9483 -3.3965 370.4859 373.8825 374.9820 86.7695 -3.3889 370.5225 373.9114 374.9251 87.5310 -3.3864 370.5550 373.9414 374.8896 88.3823 -3.3766 370.6097 373.9863 374.8312 89.1723 -3.3717 370.6629 374.0347 374.7854 89.9625 -3.3719 370.7144 374.0864 374.7175 90.7828 -3.3681 370.7446 374.1126 374.6787 91.5728 -3.3628 370.7759 374.1387 374.6277 92.3930 -3.3558 370.8087 374.1645 374.5535 93.1835 -3.3525 370.8593 374.2117 374.5037 93.9740 -3.3471 370.9042 374.2513 374.4559 94.7953 -3.3402 370.9366 374.2768 374.3835 95.5855 -3.3392 370.9661 374.3054 374.3414 96.4060 -3.3350 371.0015 374.3365 374.2949 97.1958 -3.3312 371.0405 374.3717 374.2364 97.9855 -3.3344 371.0705 374.4050 374.1770 98.8070 -3.3311 371.1020 374.4332 374.1151 99.5980 -3.3299 371.1431 374.4730 374.0621 100.4188 -3.3218 371.1834 374.5052 373.9726 101.2085 -3.3172 371.2161 374.5333 373.9220 102.0000 -3.3137 371.2496 374.5633 373.8736 102.8225 -3.3027 371.2880 374.5907 373.8161 103.6128 -3.2986 371.3162 374.6148 373.7706 104.4345 -3.2967 371.3490 374.6457 373.6991 105.2258 -3.2938 371.3746 374.6684 373.6614 106.0183 -3.2894 371.3997 374.6891 373.5851 106.8395 -3.2909 371.4385 374.7294 373.5116 107.6310 -3.2905 371.4791 374.7696 373.4604 108.4520 -3.2871 371.5104 374.7975 373.4002 109.2425 -3.2859 371.5314 374.8174 373.3480 110.0345 -3.2776 371.5554 374.8330 373.2765 110.8555 -3.2716 371.5763 374.8479 373.2240 111.6168 -3.2664 371.6085 374.8748 373.1511 112.4675 -3.2623 371.6375 374.8998 373.1078 113.2573 -3.2650 371.6694 374.9345 373.0630 114.0498 -3.2578 371.6877 374.9455 373.0166 114.8753 -3.2509 371.7232 374.9740 372.9522 115.6355 -3.2509 371.7500 375.0009 372.9016 116.4860 -3.2487 371.7841 375.0328 372.8426 117.2508 -3.2473 371.8055 375.0528 372.7909 118.0800 -3.2424 371.8286 375.0710 372.7276 118.8700 -3.2374 371.8507 375.0881 372.6785 119.6600 -3.2362 371.8693 375.1055 372.6131 120.5100 -3.2300 371.8918 375.1218 372.5505 121.2690 -3.2257 371.9333 375.1591 372.4893 122.0905 -3.2220 371.9517 375.1737 372.4160 122.9110 -3.2229 371.9589 375.1818 372.3650 123.6713 -3.2199 371.9944 375.2143 372.2929 124.5218 -3.2147 371.9978 375.2125 372.2271 125.2828 -3.2119 372.0285 375.2404 372.1677 126.1055 -3.2068 372.0609 375.2677 372.1209 126.8975 -3.2007 372.0693 375.2699 372.0613 127.6880 -3.1942 372.0845 375.2787 371.9900 128.5383 -3.1908 372.0971 375.2879 371.9185 129.2978 -3.1865 372.0998 375.2862 371.8539 130.1178 -3.1832 372.1342 375.3174 371.7886 130.9370 -3.1786 372.1586 375.3372 371.7220 131.6973 -3.1745 372.1834 375.3579 371.6621 132.5483 -3.1719 372.2093 375.3812 371.5953 133.3378 -3.1684 372.2123 375.3808 371.5420 134.1283 -3.1646 372.2197 375.3844 371.4944 134.9495 -3.1621 372.2463 375.4084 371.4258 135.7093 -3.1585 372.2578 375.4163 371.3775 136.5603 -3.1525 372.2818 375.4343 371.3029 137.3498 -3.1482 372.3047 375.4529 371.2526 138.1403 -3.1435 372.3044 375.4480 371.1799 138.9615 -3.1415 372.3213 375.4628 371.1221 139.7513 -3.1366 372.3333 375.4699 371.0668 140.5715 -3.1336 372.3292 375.4628 371.0098 141.3613 -3.1319 372.3517 375.4836 370.9505 142.1500 -3.1272 372.3585 375.4856 370.8891 142.9990 -3.1239 372.3895 375.5134 370.8337 143.7580 -3.1219 372.3911 375.5130 370.7841 144.5790 -3.1178 372.4057 375.5235 370.7192 145.3988 -3.1106 372.4031 375.5136 370.6584 146.1573 -3.1104 372.4090 375.5194 370.6046 147.0088 -3.1069 372.4327 375.5396 370.5590 147.7980 -3.1049 372.4443 375.5493 370.4953 148.5878 -3.1011 372.4550 375.5561 370.4511 149.4088 -3.0990 372.4755 375.5746 370.3935 150.1985 -3.0944 372.4798 375.5742 370.3461 151.0190 -3.0913 372.4896 375.5810 370.2760 151.8088 -3.0860 372.4913 375.5773 370.2274 152.5993 -3.0852 372.4879 375.5732 370.1659 153.4205 -3.0799 372.4921 375.5720 370.1135 154.2100 -3.0735 372.5029 375.5764 370.0683 155.0298 -3.0702 372.5165 375.5867 370.0160 155.8195 -3.0676 372.5272 375.5948 369.9681 156.6100 -3.0633 372.5133 375.5766 369.9014 157.4603 -3.0601 372.5385 375.5985 369.8393 158.2198 -3.0578 372.5191 375.5769 369.7763 159.0408 -3.0540 372.5355 375.5894 369.7287 159.8600 -3.0456 372.5365 375.5820 369.6616 160.6203 -3.0433 372.5344 375.5777 369.6182 161.4713 -3.0398 372.5604 375.6003 369.5435 162.2318 -3.0380 372.5388 375.5767 369.4980 163.0530 -3.0360 372.5521 375.5881 369.4251 163.8735 -3.0308 372.5669 375.5977 369.3747 164.6333 -3.0262 372.5462 375.5725 369.3050 165.4843 -3.0213 372.5512 375.5725 369.2460 166.2455 -3.0168 372.5672 375.5841 369.1962 167.0660 -3.0092 372.5496 375.5588 369.1439 167.8870 -3.0099 372.5580 375.5679 369.0754 168.6468 -3.0069 372.5541 375.5611 369.0081 169.4988 -3.0041 372.5648 375.5689 368.9259 170.2895 -3.0016 372.5579 375.5594 368.8748 171.0798 -3.0005 372.5521 375.5526 368.8054 171.9010 -2.9959 372.5551 375.5510 368.7629 172.6613 -2.9924 372.5597 375.5520 368.7020 173.5128 -2.9884 372.5530 375.5414 368.6326 174.3020 -2.9859 372.5569 375.5428 368.5769 175.0913 -2.9818 372.5472 375.5291 368.5038 175.9113 -2.9784 372.5409 375.5193 368.4394 176.6725 -2.9756 372.5516 375.5272 368.3877 177.5238 -2.9705 372.5353 375.5058 368.3309 178.3148 -2.9671 372.5374 375.5045 368.2518 179.1065 -2.9625 372.5300 375.4925 368.2003 179.9275 -2.9616 372.5344 375.4960 368.1298 180.6878 -2.9588 372.5329 375.4917 368.0707 181.5395 -2.9562 372.5276 375.4838 368.0058 182.3008 -2.9537 372.5220 375.4757 367.9493 183.1220 -2.9477 372.5076 375.4553 367.8795 183.9425 -2.9416 372.4987 375.4403 367.8255 184.7038 -2.9354 372.4894 375.4248 367.7619 185.5558 -2.9289 372.5090 375.4380 367.7096 186.3158 -2.9276 372.5036 375.4312 367.6604 187.1370 -2.9330 372.4751 375.4081 367.6053 187.9575 -2.9281 372.4659 375.3939 367.5370 188.7185 -2.9237 372.4606 375.3843 367.4763 189.5710 -2.9223 372.4606 375.3828 367.4092 190.3308 -2.9199 372.4530 375.3729 367.3681 191.1525 -2.9141 372.4497 375.3638 367.3080 191.9453 -2.9132 372.4268 375.3400 367.2509 192.7373 -2.9137 372.4203 375.3341 367.1977 193.5880 -2.9050 372.4077 375.3127 367.1164 194.3490 -2.9027 372.4073 375.3100 367.0627 195.1700 -2.8999 372.3955 375.2954 366.9959 195.9623 -2.8965 372.3869 375.2834 366.9343 196.7545 -2.8927 372.3611 375.2538 366.8861 197.6068 -2.8919 372.3831 375.2749 366.8145 198.3663 -2.8874 372.3574 375.2448 366.7383 199.1878 -2.8800 372.3454 375.2254 366.6774 199.9800 -2.8757 372.3360 375.2118 366.6291 200.7708 -2.8743 372.3096 375.1839 366.5589 201.5918 -2.8735 372.3000 375.1735 366.4886 202.3823 -2.8720 372.2923 375.1643 366.4300 203.2035 -2.8701 372.2794 375.1495 366.3507 203.9958 -2.8653 372.2659 375.1311 366.2912 204.7868 -2.8616 372.2442 375.1057 366.2385 205.6085 -2.8548 372.2363 375.0911 366.1566 206.3688 -2.8517 372.2147 375.0664 366.0984 207.2203 -2.8483 372.2206 375.0689 366.0345 208.0098 -2.8470 372.1781 375.0252 365.9687 208.8000 -2.8438 372.1648 375.0086 365.9063 209.6205 -2.8436 372.1814 375.0250 365.8288 210.4118 -2.8399 372.1586 374.9985 365.7576 211.2333 -2.8391 372.1329 374.9720 365.6880 212.0238 -2.8364 372.1106 374.9471 365.6168 212.8140 -2.8335 372.0946 374.9281 365.5598 213.6345 -2.8321 372.0958 374.9278 365.4925 214.4253 -2.8273 372.0623 374.8896 365.4349 215.2450 -2.8245 372.0633 374.8878 365.3549 216.0365 -2.8221 372.0307 374.8529 365.2854 216.8270 -2.8174 372.0034 374.8208 365.2245 217.6473 -2.8165 371.9772 374.7937 365.1397 218.4068 -2.8143 371.9764 374.7907 365.0764 219.2578 -2.8078 371.9552 374.7630 365.0107 220.0228 -2.8071 371.9380 374.7452 364.9570 220.8480 -2.8052 371.9183 374.7235 364.8931 221.6680 -2.8015 371.9039 374.7054 364.8322 222.4273 -2.8001 371.8684 374.6685 364.7645 223.2788 -2.7961 371.8462 374.6423 364.7083 224.0375 -2.7951 371.8356 374.6308 364.6582 224.8580 -2.7915 371.8156 374.6071 364.5951 225.6780 -2.7856 371.7989 374.5844 364.5160 226.4370 -2.7834 371.7752 374.5586 364.4435 227.2878 -2.7821 371.7515 374.5336 364.3626 228.0770 -2.7798 371.7294 374.5092 364.3101 228.8673 -2.7772 371.7057 374.4829 364.2610 229.6885 -2.7718 371.6892 374.4610 364.1859 230.4493 -2.7678 371.6576 374.4254 364.1313 231.3003 -2.7662 371.6323 374.3985 364.0678 232.0908 -2.7644 371.6191 374.3835 363.9977 232.8815 -2.7608 371.5895 374.3502 363.9265 233.7025 -2.7544 371.5727 374.3270 363.8625 234.4638 -2.7516 371.5329 374.2845 363.8201 235.3148 -2.7478 371.5176 374.2654 363.7464 236.0765 -2.7488 371.5115 374.2603 363.6878 236.8978 -2.7446 371.4837 374.2282 363.6167 237.7185 -2.7416 371.4567 374.1983 363.5619 238.4783 -2.7400 371.4434 374.1834 363.5050 239.3298 -2.7314 371.4199 374.1514 363.4513 240.1205 -2.7335 371.3954 374.1289 363.3854 240.9125 -2.7313 371.3664 374.0978 363.3317 241.7345 -2.7276 371.3317 374.0593 363.2850 242.4950 -2.7247 371.3152 374.0400 363.2311 243.3458 -2.7218 371.2913 374.0131 363.1523 244.1353 -2.7176 371.2635 373.9811 363.0873 244.9253 -2.7168 371.2311 373.9479 363.0467 245.7468 -2.7174 371.2067 373.9241 362.9767 246.5060 -2.7140 371.1852 373.8992 362.9166 247.3578 -2.7113 371.1588 373.8701 362.8650 248.1483 -2.7089 371.1325 373.8414 362.8160 248.9385 -2.7098 371.1025 373.8123 362.7567 249.7600 -2.7062 371.0851 373.7912 362.7140 250.5275 -2.7022 371.0671 373.7693 362.6508 251.3820 -2.6999 371.0281 373.7280 362.5702 252.1420 -2.6988 370.9877 373.6864 362.5193 252.9623 -2.6965 370.9566 373.6531 362.4745 253.7830 -2.6932 370.9329 373.6261 362.4065 254.5423 -2.6909 370.9063 373.5973 362.3582 255.3925 -2.6877 370.8731 373.5608 362.3125 256.1518 -2.6856 370.8642 373.5498 362.2548 256.9735 -2.6848 370.8203 373.5050 362.1960 257.7955 -2.6819 370.7972 373.4792 362.1226 258.5565 -2.6826 370.7700 373.4526 362.0852 259.4105 -2.6767 370.7178 373.3945 362.0146 260.1718 -2.6738 370.6989 373.3727 361.9583 261.0208 -2.6690 370.6722 373.3412 361.8894 261.7825 -2.6723 370.6519 373.3242 361.8254 262.6038 -2.6695 370.6173 373.2868 361.7736 263.3935 -2.6646 370.5915 373.2561 361.7189 264.1843 -2.6628 370.5597 373.2225 361.6599 265.0353 -2.6569 370.5143 373.1713 361.5887 265.7948 -2.6562 370.4863 373.1424 361.5351 266.6163 -2.6518 370.4819 373.1337 361.4607 267.4375 -2.6486 370.4391 373.0878 361.4093 268.1995 -2.6499 370.4097 373.0596 361.3325 269.0508 -2.6421 370.3731 373.0152 361.2691 269.8103 -2.6422 370.3397 372.9819 361.2019 270.6358 -2.6420 370.3178 372.9598 361.1323 271.4118 -2.6411 370.2758 372.9169 361.0976 272.2328 -2.6381 370.2360 372.8741 361.0167 273.0540 -2.6346 370.2225 372.8571 360.9445 273.8133 -2.6358 370.1837 372.8195 360.8800 274.6648 -2.6307 370.1378 372.7685 360.8206 275.4538 -2.6303 370.1119 372.7422 360.7552 276.2430 -2.6312 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