DTA measure 1pb_updown4 Date: 202449:1140 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 893.39 s Mass = 1118.000 mg data_number = 1111 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2950 -1.1167 263.0639 264.1806 263.9455 2.0865 -1.1169 263.0559 264.1728 263.8948 2.8773 -1.1132 263.0672 264.1804 263.8479 3.7273 -1.1124 263.0502 264.1626 263.8042 4.4873 -1.1113 263.0497 264.1610 263.7699 5.3085 -1.1086 263.0303 264.1389 263.7133 6.1000 -1.1088 263.0290 264.1378 263.6764 6.8903 -1.1062 263.0185 264.1248 263.6507 7.7418 -1.1075 263.0173 264.1248 263.6167 8.5010 -1.1057 263.0049 264.1106 263.5877 9.3223 -1.1052 262.9939 264.0991 263.5709 10.1140 -1.1085 263.0007 264.1092 263.5776 10.9040 -1.1117 262.9810 264.0928 263.5622 11.7545 -1.1101 262.9742 264.0842 263.5619 12.5140 -1.1101 262.9588 264.0689 263.5715 13.3355 -1.1117 262.9491 264.0608 263.5876 14.1255 -1.1116 262.9349 264.0465 263.5945 14.9160 -1.1112 262.9230 264.0342 263.6104 15.7663 -1.1098 262.9356 264.0454 263.6384 16.5253 -1.1094 262.9245 264.0339 263.6708 17.3463 -1.1126 262.9242 264.0368 263.7109 18.1365 -1.1159 262.9201 264.0360 263.7486 18.9273 -1.1149 262.9140 264.0289 263.8017 19.7783 -1.1134 262.9222 264.0357 263.8503 20.5210 -1.1141 262.9069 264.0210 263.9066 21.3495 -1.1143 262.8944 264.0086 263.9714 22.1400 -1.1167 262.8839 264.0005 264.0377 22.9903 -1.1168 262.8882 264.0050 264.1201 23.7493 -1.1170 262.8874 264.0045 264.2066 24.5698 -1.1174 262.9018 264.0193 264.3073 25.3595 -1.1176 262.8877 264.0054 264.3948 26.1498 -1.1211 262.8755 263.9966 264.5009 27.0008 -1.1220 262.8613 263.9833 264.5995 27.7595 -1.1238 262.8712 263.9950 264.6981 28.5800 -1.1236 262.8756 263.9992 264.8142 29.4000 -1.1244 262.8504 263.9748 264.9389 30.1593 -1.1256 262.8537 263.9794 265.0388 31.0108 -1.1264 262.8749 264.0013 265.1811 31.7708 -1.1264 262.8646 263.9910 265.2971 32.5920 -1.1286 262.8440 263.9726 265.4204 33.4163 -1.1289 262.8357 263.9647 265.5560 34.1760 -1.1286 262.8462 263.9748 265.6790 35.0265 -1.1313 262.8537 263.9850 265.8253 35.7868 -1.1340 262.8527 263.9867 265.9468 36.6100 -1.1381 262.8300 263.9680 266.0890 37.4295 -1.1385 262.8358 263.9743 266.2317 38.1898 -1.1396 262.8505 263.9901 266.3769 39.0405 -1.1429 262.8569 263.9998 266.5373 39.8293 -1.1449 262.8561 264.0009 266.6812 40.6190 -1.1468 262.8688 264.0156 266.8198 41.3893 -1.1483 262.8652 264.0135 266.9477 42.2543 -1.1498 262.8634 264.0132 267.1115 43.0435 -1.1546 262.8871 264.0417 267.2482 43.8330 -1.1572 262.8828 264.0400 267.3844 44.6525 -1.1586 262.8805 264.0391 267.5266 45.4423 -1.1600 262.8854 264.0455 267.6792 46.2628 -1.1631 262.8833 264.0463 267.8259 47.0518 -1.1679 262.8970 264.0649 267.9725 47.8420 -1.1701 262.9011 264.0713 268.1120 48.6625 -1.1731 262.9110 264.0840 268.2563 49.4523 -1.1732 262.9116 264.0848 268.3969 50.2728 -1.1792 262.9064 264.0856 268.5458 51.0635 -1.1822 262.9230 264.1052 268.6579 51.8535 -1.1795 262.9385 264.1180 268.7930 52.7033 -1.1860 262.9433 264.1293 268.9429 53.4630 -1.1893 262.9412 264.1305 269.0721 54.2848 -1.1940 262.9567 264.1507 269.2114 55.0760 -1.1941 262.9769 264.1709 269.3190 55.8665 -1.1966 262.9832 264.1798 269.4367 56.7180 -1.1992 262.9900 264.1892 269.5787 57.4785 -1.2028 262.9977 264.2005 269.7007 58.2990 -1.2060 263.0116 264.2176 269.8248 59.1190 -1.2086 263.0251 264.2337 269.9446 59.8800 -1.2125 263.0369 264.2495 270.0376 60.7313 -1.2179 263.0370 264.2550 270.1619 61.4738 -1.2193 263.0570 264.2763 270.2635 62.3080 -1.2204 263.0803 264.3008 270.3716 63.0993 -1.2244 263.0813 264.3057 270.4765 63.9505 -1.2294 263.1054 264.3348 270.6044 64.7118 -1.2316 263.1049 264.3365 270.6890 65.5335 -1.2328 263.1191 264.3519 270.7813 66.3245 -1.2389 263.1352 264.3741 270.8852 67.1163 -1.2397 263.1606 264.4003 270.9846 67.9665 -1.2391 263.1786 264.4177 271.0873 68.7263 -1.2464 263.2105 264.4569 271.1650 69.5470 -1.2522 263.2327 264.4850 271.2484 70.3385 -1.2658 263.2186 264.4844 271.3511 71.1303 -1.2657 263.2363 264.5020 271.4398 71.9813 -1.2615 263.2502 264.5117 271.5246 72.7420 -1.2635 263.2582 264.5217 271.5957 73.5633 -1.2701 263.2831 264.5532 271.6875 74.3545 -1.2690 263.2996 264.5686 271.7830 75.1465 -1.2711 263.3142 264.5853 271.8695 75.9685 -1.2735 263.3516 264.6251 271.9590 76.7598 -1.2768 263.3892 264.6660 272.0454 77.5813 -1.2818 263.3865 264.6683 272.1310 78.3733 -1.2829 263.3960 264.6789 272.2107 79.1655 -1.2821 263.4161 264.6981 272.2849 80.0180 -1.2878 263.4329 264.7207 272.3649 80.7790 -1.2912 263.4568 264.7480 272.4469 81.6005 -1.2938 263.4837 264.7774 272.5386 82.4513 -1.2910 263.4874 264.7784 272.6217 83.2720 -1.2948 263.5239 264.8188 272.7152 84.0358 -1.2979 263.5562 264.8541 272.7874 84.8890 -1.3044 263.5503 264.8547 272.9028 85.6503 -1.3088 263.5729 264.8817 272.9556 86.4718 -1.3100 263.6032 264.9132 273.0344 87.2628 -1.3140 263.6260 264.9400 273.1210 88.0538 -1.3155 263.6522 264.9677 273.2015 88.9035 -1.3190 263.6844 265.0034 273.2884 89.6635 -1.3238 263.7070 265.0308 273.3851 90.4848 -1.3263 263.7321 265.0584 273.4735 91.3033 -1.3276 263.7476 265.0752 273.5652 92.0635 -1.3314 263.7738 265.1052 273.6438 92.9138 -1.3343 263.8140 265.1483 273.7384 93.6745 -1.3398 263.8338 265.1736 273.8323 94.4965 -1.3433 263.8545 265.1978 273.9159 95.3175 -1.3429 263.8726 265.2155 274.0219 96.0783 -1.3479 263.8971 265.2450 274.1077 96.9295 -1.3489 263.9391 265.2881 274.2260 97.6915 -1.3519 263.9390 265.2908 274.3187 98.5133 -1.3531 263.9819 265.3350 274.4141 99.3345 -1.3575 264.0295 265.3871 274.5084 100.0948 -1.3610 264.0602 265.4212 274.5922 100.9463 -1.3636 264.0795 265.4431 274.7010 101.7065 -1.3666 264.0986 265.4652 274.7788 102.5278 -1.3681 264.1350 265.5030 274.8996 103.3478 -1.3707 264.1719 265.5426 274.9891 104.1078 -1.3713 264.1897 265.5609 275.0760 104.9580 -1.3765 264.2117 265.5882 275.1778 105.7183 -1.3805 264.2430 265.6235 275.2681 106.5390 -1.3777 264.2782 265.6559 275.3844 107.3578 -1.3739 264.3143 265.6882 275.5059 108.1175 -1.3840 264.3428 265.7268 275.6044 108.9700 -1.3836 264.3560 265.7395 275.7021 109.7623 -1.3886 264.4042 265.7928 275.8098 110.5545 -1.3963 264.4428 265.8391 275.9029 111.3770 -1.4019 264.4694 265.8712 275.9998 112.1680 -1.4088 264.4944 265.9033 276.1096 112.9888 -1.4105 264.5262 265.9367 276.2137 113.7785 -1.4137 264.5805 265.9942 276.3069 114.5705 -1.4163 264.6142 266.0305 276.3938 115.3925 -1.4147 264.6426 266.0572 276.5025 116.1845 -1.4125 264.6779 266.0904 276.6091 117.0058 -1.4163 264.7182 266.1345 276.7169 117.7963 -1.4193 264.7581 266.1774 276.8184 118.5865 -1.4207 264.7765 266.1972 276.9104 119.4075 -1.4211 264.8027 266.2238 277.0255 120.1695 -1.4252 264.8333 266.2585 277.1262 121.0258 -1.4259 264.8808 266.3068 277.2340 121.8175 -1.4285 264.9214 266.3499 277.3504 122.6093 -1.4325 264.9495 266.3820 277.4404 123.4305 -1.4337 264.9816 266.4153 277.5574 124.1920 -1.4455 265.0152 266.4608 277.6681 125.0433 -1.4488 265.0613 266.5101 277.7952 125.8045 -1.4492 265.0879 266.5371 277.9018 126.6255 -1.4466 265.1185 266.5651 278.0113 127.4448 -1.4525 265.1757 266.6282 278.1403 128.2058 -1.4565 265.2183 266.6747 278.2457 129.0570 -1.4581 265.2433 266.7014 278.3609 129.8168 -1.4602 265.3022 266.7624 278.4465 130.6385 -1.4619 265.3317 266.7936 278.5776 131.4300 -1.4663 265.3494 266.8157 278.6875 132.2210 -1.4694 265.3975 266.8669 278.7966 133.0728 -1.4751 265.4303 266.9054 278.9075 133.8325 -1.4778 265.4754 266.9532 279.0176 134.6538 -1.4793 265.5364 267.0157 279.1363 135.4460 -1.4802 265.5593 267.0396 279.2497 136.2370 -1.4851 265.5849 267.0701 279.3593 137.0590 -1.4885 265.6430 267.1315 279.4707 137.8495 -1.4901 265.6924 267.1825 279.5926 138.6705 -1.4917 265.7270 267.2187 279.7219 139.4618 -1.4969 265.7626 267.2595 279.8432 140.2535 -1.5009 265.8285 267.3294 279.9573 141.0755 -1.5046 265.8635 267.3681 280.0470 141.8375 -1.5086 265.9013 267.4098 280.1518 142.6895 -1.5117 265.9317 267.4433 280.2752 143.4808 -1.5126 265.9780 267.4906 280.3798 144.2718 -1.5138 266.0328 267.5466 280.4749 145.0935 -1.5157 266.0870 267.6027 280.5863 145.8540 -1.5193 266.1285 267.6477 280.6805 146.7055 -1.5266 266.1844 267.7110 280.8007 147.4675 -1.5277 266.2194 267.7471 280.8962 148.2890 -1.5319 266.2486 267.7805 281.0009 149.1105 -1.5357 266.3044 267.8401 281.1014 149.8713 -1.5407 266.3464 267.8872 281.1922 150.7225 -1.5408 266.4074 267.9482 281.2951 151.4845 -1.5449 266.4388 267.9837 281.3917 152.3060 -1.5458 266.4878 268.0336 281.4906 153.0975 -1.5487 266.5426 268.0913 281.5861 153.8883 -1.5514 266.5818 268.1333 281.6832 154.7390 -1.5564 266.6200 268.1764 281.7719 155.5000 -1.5597 266.6465 268.2062 281.8671 156.3213 -1.5643 266.7101 268.2744 281.9738 157.1130 -1.5622 266.7659 268.3281 282.0660 157.9038 -1.5662 266.8279 268.3941 282.1460 158.7548 -1.5675 266.8801 268.4476 282.2403 159.5150 -1.5694 266.9159 268.4853 282.3401 160.3368 -1.5726 266.9749 268.5474 282.4208 161.1290 -1.5769 267.0092 268.5861 282.5136 161.9198 -1.5796 267.0662 268.6457 282.6239 162.7420 -1.5803 267.1233 268.7036 282.7129 163.5335 -1.5827 267.1839 268.7666 282.8024 164.3548 -1.5837 267.2254 268.8091 282.8883 165.1438 -1.5895 267.2751 268.8646 282.9859 165.9355 -1.5903 267.3399 268.9302 283.0759 166.7575 -1.5916 267.3804 268.9719 283.1690 167.5490 -1.5958 267.4308 269.0266 283.2808 168.3693 -1.5961 267.4830 269.0791 283.3728 169.1595 -1.5982 267.5269 269.1251 283.4624 169.9515 -1.6021 267.5835 269.1856 283.5533 170.7735 -1.6055 267.6351 269.2406 283.6683 171.5650 -1.6107 267.6754 269.2861 283.7567 172.3865 -1.6106 267.7374 269.3480 283.8584 173.1788 -1.6126 267.7825 269.3952 283.9409 173.9738 -1.6179 267.8260 269.4440 284.0426 174.8003 -1.6182 267.9009 269.5191 284.1362 175.5613 -1.6193 267.9626 269.5819 284.2294 176.4125 -1.6231 268.0101 269.6332 284.3367 177.1745 -1.6274 268.0585 269.6859 284.4245 177.9963 -1.6296 268.1040 269.7336 284.5197 178.8175 -1.6293 268.1600 269.7893 284.6348 179.5793 -1.6333 268.2018 269.8351 284.7289 180.4310 -1.6351 268.2829 269.9180 284.8026 181.1928 -1.6383 268.3197 269.9580 284.8845 182.0143 -1.6405 268.3962 270.0367 284.9927 182.8060 -1.6408 268.4492 270.0900 285.1000 183.5975 -1.6442 268.5146 270.1588 285.2060 184.4500 -1.6475 268.5401 270.1876 285.3005 185.2108 -1.6442 268.6035 270.2477 285.3797 186.0323 -1.6451 268.6815 270.3266 285.5056 186.8230 -1.6469 268.7367 270.3836 285.6098 187.6133 -1.6518 268.7758 270.4276 285.6974 188.4648 -1.6530 268.8377 270.4907 285.7986 189.2265 -1.6580 268.8898 270.5478 285.9214 190.0468 -1.6620 268.9530 270.6150 286.0135 190.8653 -1.6607 269.0057 270.6665 286.1248 191.6255 -1.6653 269.0443 270.7097 286.2469 192.4775 -1.6695 269.1363 270.8058 286.3429 193.2403 -1.6741 269.1997 270.8738 286.4458 194.0623 -1.6777 269.2592 270.9369 286.5771 194.8340 -1.6800 269.3055 270.9855 286.6778 195.6663 -1.6839 269.3925 271.0764 286.7919 196.4875 -1.6860 269.4379 271.1239 286.8920 197.2483 -1.6848 269.4926 271.1774 287.0059 198.0993 -1.6872 269.5530 271.2402 287.1612 198.8595 -1.6896 269.5991 271.2886 287.2592 199.6810 -1.6913 269.6694 271.3607 287.3595 200.5025 -1.6947 269.7361 271.4308 287.4564 201.2643 -1.6960 269.7898 271.4858 287.5900 202.1153 -1.6985 269.8581 271.5566 287.7095 202.9055 -1.6999 269.9099 271.6098 287.8111 203.6975 -1.7042 269.9689 271.6731 287.9288 204.5195 -1.7108 270.0554 271.7661 288.0258 205.2810 -1.7086 270.1131 271.8217 288.1316 206.1330 -1.7119 270.1724 271.8843 288.2516 206.9233 -1.7114 270.2234 271.9348 288.3751 207.7125 -1.7148 270.2790 271.9938 288.4977 208.5328 -1.7193 270.3420 272.0612 288.6108 209.2925 -1.7210 270.4091 272.1301 288.7183 210.1450 -1.7231 270.4762 272.1993 288.8294 210.9370 -1.7261 270.5272 272.2533 288.9402 211.7280 -1.7257 270.5972 272.3229 289.0545 212.5500 -1.7278 270.6532 272.3810 289.1745 213.3115 -1.7321 270.7185 272.4506 289.2838 214.1635 -1.7356 270.7958 272.5314 289.3929 214.9530 -1.7379 270.8489 272.5868 289.5065 215.7430 -1.7425 270.9169 272.6595 289.6005 216.5635 -1.7461 270.9909 272.7370 289.7204 217.3555 -1.7485 271.0473 272.7958 289.8322 218.1773 -1.7476 271.1203 272.8679 289.9544 218.9678 -1.7487 271.1827 272.9314 290.0533 219.7583 -1.7547 271.2440 272.9987 290.1581 220.5795 -1.7550 271.2980 273.0530 290.2665 221.3715 -1.7602 271.3710 273.1311 290.3896 222.1935 -1.7635 271.4485 273.2119 290.5111 222.9848 -1.7643 271.5174 273.2817 290.6204 223.7753 -1.7676 271.5779 273.3455 290.7228 224.5965 -1.7688 271.6465 273.4153 290.8277 225.3590 -1.7720 271.7095 273.4816 290.9186 226.2148 -1.7751 271.7963 273.5714 291.0258 227.0058 -1.7787 271.8588 273.6374 291.0960 227.7975 -1.7804 271.9202 273.7006 291.2043 228.6185 -1.7833 272.0002 273.7835 291.3191 229.3805 -1.7853 272.0659 273.8512 291.4281 230.2325 -1.7879 272.1293 273.9172 291.5008 231.0243 -1.7891 272.1849 273.9740 291.5995 231.8138 -1.7927 272.2579 274.0507 291.6980 232.6340 -1.7941 272.3397 274.1338 291.7840 233.3950 -1.7965 272.3996 274.1961 291.8780 234.2468 -1.7978 272.4791 274.2769 291.9624 235.0078 -1.8009 272.5504 274.3513 292.0647 235.8298 -1.8039 272.6002 274.4041 292.1339 236.6515 -1.8086 272.6841 274.4926 292.2311 237.4108 -1.8099 272.7547 274.5646 292.3150 238.2630 -1.8132 272.8274 274.6406 292.3913 239.0248 -1.8191 272.8886 274.7077 292.4652 239.8468 -1.8214 272.9574 274.7789 292.5757 240.6385 -1.8234 273.0305 274.8539 292.6708 241.4303 -1.8230 273.0965 274.9196 292.7576 242.2518 -1.8241 273.1607 274.9848 292.8443 243.0435 -1.8272 273.2551 275.0823 292.9426 243.8645 -1.8319 273.3309 275.1627 293.0319 244.6555 -1.8330 273.3962 275.2292 293.1279 245.4468 -1.8360 273.4678 275.3037 293.2216 246.2510 -1.8343 273.5263 275.3606 293.3064 247.0468 -1.8358 273.5955 275.4314 293.3966 247.8685 -1.8375 273.6684 275.5059 293.4869 248.6588 -1.8406 273.7543 275.5949 293.5816 249.4805 -1.8491 273.8323 275.6814 293.6758 250.2725 -1.8484 273.9148 275.7633 293.7707 251.0645 -1.8497 273.9859 275.8356 293.8836 251.8855 -1.8508 274.0644 275.9152 293.9698 252.6760 -1.8535 274.1167 275.9702 294.0527 253.4968 -1.8578 274.2121 276.0699 294.1359 254.2863 -1.8584 274.2736 276.1319 294.2329 255.0775 -1.8602 274.3306 276.1908 294.3247 255.8990 -1.8676 274.4169 276.2844 294.4542 256.6593 -1.8693 274.4853 276.3546 294.5382 257.5110 -1.8683 274.5661 276.4344 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