DTA measure 11.meres Test Date: 2023927:1535 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.12 s Mass = 1096.000 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3543 -1.5550 266.2811 267.8361 264.0407 2.1768 -1.5556 266.3506 267.9062 264.0476 3.0285 -1.5569 266.3947 267.9516 264.0477 3.7905 -1.5595 266.4325 267.9920 264.0590 4.6125 -1.5629 266.4796 268.0425 264.0600 5.4045 -1.5630 266.5341 268.0970 264.0777 6.1965 -1.5636 266.5816 268.1451 264.1035 7.0485 -1.5682 266.6272 268.1955 264.1191 7.8115 -1.5722 266.6872 268.2593 264.1289 8.6335 -1.5725 266.7415 268.3140 264.1472 9.4555 -1.5744 266.7856 268.3600 264.1908 10.2155 -1.5781 266.8343 268.4124 264.2220 11.0775 -1.5798 266.8816 268.4614 264.2600 11.8168 -1.5796 266.9511 268.5307 264.2828 12.6633 -1.5812 267.0011 268.5823 264.3380 13.4230 -1.5811 267.0423 268.6234 264.3912 14.2410 -1.5877 267.0761 268.6637 264.4447 15.0290 -1.5926 267.1150 268.7076 264.4968 15.8170 -1.5943 267.1586 268.7529 264.5710 16.6663 -1.5956 267.2092 268.8047 264.6387 17.4250 -1.5972 267.2616 268.8588 264.7168 18.2440 -1.6003 267.2992 268.8995 264.8034 19.0333 -1.6022 267.3413 268.9434 264.8828 19.8240 -1.6061 267.3930 268.9991 264.9566 20.6755 -1.6104 267.4536 269.0640 265.0415 21.4690 -1.6096 267.4839 269.0935 265.1426 22.2215 -1.6142 267.5222 269.1364 265.2311 23.0735 -1.6155 267.5747 269.1901 265.3296 23.8655 -1.6206 267.6117 269.2323 265.4174 24.6575 -1.6255 267.6699 269.2954 265.5179 25.4795 -1.6279 267.7087 269.3366 265.6418 26.2415 -1.6303 267.7704 269.4007 265.7364 27.0935 -1.6323 267.8156 269.4478 265.8675 27.8555 -1.6343 267.8481 269.4824 265.9794 28.6775 -1.6374 267.8938 269.5313 266.0919 29.4995 -1.6404 267.9474 269.5878 266.2135 30.2610 -1.6435 267.9798 269.6233 266.3294 31.1130 -1.6440 268.0371 269.6811 266.4719 31.9258 -1.6518 268.0728 269.7246 266.5905 32.7780 -1.6535 268.1093 269.7628 266.7312 33.5398 -1.6587 268.1697 269.8284 266.8508 34.3625 -1.6624 268.2086 269.8709 266.9624 35.1850 -1.6659 268.2518 269.9178 267.0998 35.9465 -1.6680 268.2938 269.9618 267.2037 36.7995 -1.6714 268.3151 269.9865 267.3462 37.5630 -1.6743 268.3863 270.0606 267.4591 38.3875 -1.6795 268.4476 270.1270 267.6085 39.1798 -1.6842 268.4691 270.1533 267.7343 40.0318 -1.6875 268.5275 270.2150 267.8623 40.8235 -1.6882 268.5643 270.2524 267.9874 41.6455 -1.6941 268.5936 270.2877 268.1165 42.4350 -1.6972 268.6544 270.3516 268.2406 43.2530 -1.7009 268.6939 270.3949 268.3762 44.0710 -1.7055 268.7482 270.4537 268.5070 44.8590 -1.7060 268.7841 270.4901 268.6484 45.6780 -1.7092 268.8487 270.5579 268.7930 46.4660 -1.7104 268.8866 270.5969 268.9352 47.2540 -1.7167 268.9321 270.6488 269.0734 48.0720 -1.7198 268.9791 270.6989 269.2327 48.8603 -1.7244 269.0247 270.7491 269.3634 49.6788 -1.7281 269.0754 270.8035 269.4960 50.4675 -1.7333 269.1332 270.8665 269.6369 51.2585 -1.7403 269.1732 270.9136 269.7759 52.1095 -1.7383 269.2146 270.9529 269.9209 52.8705 -1.7389 269.2556 270.9945 270.0596 53.6928 -1.7414 269.3032 271.0446 270.1846 54.4848 -1.7484 269.3479 271.0963 270.3362 55.2765 -1.7503 269.3936 271.1439 270.4928 56.0988 -1.7563 269.4467 271.2030 270.6066 56.8908 -1.7628 269.4887 271.2515 270.7358 57.7128 -1.7668 269.5259 271.2927 270.8810 58.5048 -1.7716 269.5914 271.3630 271.0155 59.2965 -1.7763 269.6390 271.4153 271.1544 60.1185 -1.7802 269.6853 271.4656 271.2939 60.8805 -1.7853 269.7414 271.5267 271.4318 61.7325 -1.7887 269.7928 271.5815 271.5665 62.4978 -1.7927 269.8335 271.6262 271.7208 63.3245 -1.7977 269.8791 271.6768 271.8484 64.1465 -1.8009 269.9241 271.7250 271.9844 64.9085 -1.8052 269.9852 271.7905 272.1101 65.7605 -1.8083 270.0300 271.8383 272.2585 66.5225 -1.8128 270.0755 271.8883 272.3661 67.3445 -1.8285 270.1258 271.9543 272.5058 68.1663 -1.8351 270.1848 272.0198 272.6664 68.9283 -1.8356 270.2494 272.0850 272.7927 69.7803 -1.8389 270.2973 272.1362 272.9112 70.5418 -1.8411 270.3391 272.1802 273.0331 71.3638 -1.8425 270.4037 272.2462 273.1848 72.1860 -1.8445 270.4586 272.3031 273.3019 72.9493 -1.8480 270.5220 272.3701 273.4204 73.8018 -1.8540 270.5605 272.4146 273.5241 74.5600 -1.8600 270.6149 272.4749 273.6415 75.3780 -1.8649 270.6684 272.5333 273.7624 76.1970 -1.8660 270.7167 272.5827 273.8799 76.9550 -1.8654 270.7832 272.6486 273.9879 77.8040 -1.8672 270.8269 272.6941 274.0949 78.5623 -1.8712 270.8859 272.7572 274.2067 79.3803 -1.8748 270.9349 272.8097 274.3234 80.2000 -1.8784 271.0062 272.8845 274.4408 80.9593 -1.8843 271.0498 272.9341 274.5458 81.8090 -1.8870 271.1126 272.9996 274.6831 82.5445 -1.8881 271.1411 273.0292 274.7849 83.4163 -1.8911 271.2182 273.1092 274.9059 84.1778 -1.8973 271.2688 273.1661 275.0261 84.9998 -1.9009 271.3147 273.2156 275.1507 85.7920 -1.9050 271.3744 273.2794 275.2699 86.5835 -1.9092 271.4472 273.3564 275.3829 87.4360 -1.9131 271.4902 273.4034 275.5075 88.1978 -1.9170 271.5356 273.4526 275.6267 89.0198 -1.9209 271.5866 273.5075 275.7550 89.8120 -1.9234 271.6531 273.5766 275.8837 90.6035 -1.9265 271.7055 273.6320 275.9924 91.4560 -1.9330 271.7870 273.7200 276.1061 92.2175 -1.9342 271.8475 273.7817 276.2314 93.0398 -1.9380 271.9104 273.8484 276.3373 93.8320 -1.9408 271.9582 273.8991 276.4453 94.6235 -1.9448 272.0183 273.9631 276.5757 95.4760 -1.9480 272.0654 274.0134 276.7162 96.2375 -1.9502 272.1390 274.0892 276.8188 97.0605 -1.9529 272.1925 274.1453 276.9474 97.8528 -1.9554 272.2557 274.2111 277.0669 98.6445 -1.9597 272.3186 274.2783 277.1801 99.4965 -1.9632 272.4015 274.3647 277.3202 100.2585 -1.9653 272.4312 274.3965 277.4503 101.0813 -1.9685 272.4857 274.4543 277.5712 101.8735 -1.9717 272.5672 274.5389 277.7013 102.6655 -1.9750 272.6325 274.6076 277.8423 103.5175 -1.9775 272.6811 274.6586 277.9897 104.2795 -1.9818 272.7481 274.7299 278.1145 105.1015 -1.9866 272.8281 274.8147 278.2570 105.8933 -1.9882 272.8922 274.8804 278.3609 106.6813 -1.9915 272.9600 274.9515 278.4988 107.5300 -1.9951 273.0123 275.0074 278.6484 108.2883 -2.0002 273.0626 275.0627 278.7544 109.1080 -2.0048 273.1312 275.1360 278.8939 109.8960 -2.0061 273.1990 275.2051 279.0242 110.6840 -2.0078 273.2507 275.2585 279.1501 111.5023 -2.0090 273.3271 275.3361 279.2907 112.2913 -2.0115 273.4096 275.4210 279.4167 113.1115 -2.0152 273.4629 275.4781 279.5512 113.9023 -2.0179 273.5366 275.5545 279.6769 114.6935 -2.0212 273.5750 275.5962 279.8129 115.5155 -2.0256 273.6648 275.6904 279.9310 116.2775 -2.0300 273.7417 275.7717 280.0380 117.1295 -2.0310 273.8034 275.8344 280.1832 117.8915 -2.0353 273.8586 275.8938 280.3169 118.7135 -2.0392 273.9432 275.9824 280.4522 119.5355 -2.0429 274.0013 276.0443 280.5759 120.2975 -2.0488 274.0583 276.1070 280.6846 121.1495 -2.0485 274.1242 276.1727 280.8298 121.9115 -2.0532 274.1990 276.2523 280.9717 122.7333 -2.0549 274.2838 276.3387 281.0915 123.5255 -2.0592 274.3445 276.4037 281.2020 124.3170 -2.0595 274.4142 276.4737 281.3374 125.1690 -2.0625 274.4586 276.5210 281.4554 125.9310 -2.0649 274.5291 276.5940 281.5703 126.7528 -2.0681 274.6062 276.6744 281.7037 127.5450 -2.0676 274.6873 276.7549 281.8203 128.3365 -2.0720 274.7504 276.8224 281.9446 129.1890 -2.0735 274.8281 276.9016 282.0533 129.9508 -2.0800 274.9080 276.9879 282.1967 130.7728 -2.0816 274.9654 277.0471 282.3067 131.5650 -2.0815 275.0353 277.1169 282.4456 132.3565 -2.0881 275.1293 277.2173 282.5654 133.2090 -2.0889 275.2166 277.3055 282.6766 133.9560 -2.0747 275.2746 277.3494 282.8021 134.8140 -2.0908 275.3360 277.4268 282.9437 135.5755 -2.0947 275.4033 277.4980 283.0539 136.3985 -2.0985 275.4839 277.5824 283.1801 137.1905 -2.1044 275.5609 277.6653 283.3041 137.9833 -2.1048 275.6162 277.7209 283.4115 138.8360 -2.1047 275.7056 277.8102 283.5362 139.5950 -2.1062 275.7814 277.8876 283.6693 140.4130 -2.1090 275.8587 277.9677 283.8014 141.2013 -2.1114 275.9509 278.0623 283.9237 141.9890 -2.1136 276.0263 278.1399 284.0475 142.8370 -2.1167 276.1106 278.2273 284.1956 143.5953 -2.1187 276.1614 278.2801 284.3110 144.4148 -2.1229 276.2520 278.3749 284.4466 145.2048 -2.1250 276.3233 278.4484 284.5665 145.9945 -2.1267 276.3958 278.5225 284.7077 146.8440 -2.1294 276.4678 278.5973 284.8756 147.6030 -2.1316 276.5370 278.6686 285.0092 148.4218 -2.1331 276.6167 278.7498 285.1501 149.2128 -2.1373 276.7024 278.8397 285.2906 150.0045 -2.1408 276.7787 278.9195 285.4075 150.8565 -2.1440 276.8686 279.0125 285.5473 151.6185 -2.1453 276.9331 279.0784 285.6933 152.4405 -2.1450 277.0141 279.1591 285.8205 153.2328 -2.1472 277.0904 279.2376 285.9638 154.0245 -2.1508 277.1754 279.3262 286.0918 154.8480 -2.1517 277.2699 279.4216 286.2228 155.6405 -2.1524 277.3469 279.4993 286.3607 156.4625 -2.1554 277.4132 279.5687 286.5063 157.2245 -2.1590 277.4901 279.6492 286.6319 158.0765 -2.1587 277.5944 279.7532 286.7677 158.8685 -2.1636 277.6928 279.8564 286.8950 159.6605 -2.1691 277.7677 279.9368 287.0429 160.4825 -2.1695 277.8331 280.0026 287.1689 161.2445 -2.1699 277.9027 280.0726 287.2919 162.0965 -2.1747 278.0000 280.1747 287.4460 162.8885 -2.1752 278.0744 280.2495 287.5755 163.6805 -2.1769 278.1578 280.3346 287.7141 164.5028 -2.1800 278.2464 280.4265 287.8382 165.2648 -2.1829 278.3320 280.5149 287.9796 166.1170 -2.1841 278.4135 280.5977 288.1078 166.9090 -2.1837 278.4880 280.6717 288.2351 167.7005 -2.1830 278.5817 280.7647 288.3538 168.5230 -2.1868 278.6742 280.8609 288.4872 169.3148 -2.1890 278.7658 280.9548 288.6161 170.1375 -2.1921 278.8567 281.0488 288.7411 170.9295 -2.1950 278.9300 281.1250 288.8785 171.7180 -2.1967 279.0006 281.1973 289.0064 172.5368 -2.1972 279.1052 281.3024 289.1294 173.3253 -2.2010 279.1979 281.3989 289.2541 174.1443 -2.2025 279.2797 281.4822 289.4020 174.8903 -2.2047 279.3565 281.5611 289.5223 175.7583 -2.2073 279.4438 281.6511 289.6667 176.5465 -2.2109 279.5303 281.7411 289.7841 177.3360 -2.2122 279.6217 281.8339 289.9185 178.1548 -2.2139 279.7231 281.9369 290.0460 178.9143 -2.2193 279.7893 282.0087 290.1612 179.7653 -2.2203 279.8951 282.1153 290.2878 180.5570 -2.2235 279.9877 282.2113 290.4116 181.3485 -2.2246 280.0896 282.3141 290.5343 182.1710 -2.2243 280.1713 282.3955 290.6735 182.9335 -2.2271 280.2479 282.4751 290.7881 183.7863 -2.2305 280.3319 282.5624 290.9124 184.5780 -2.2312 280.4201 282.6514 291.0533 185.3695 -2.2303 280.5265 282.7567 291.1721 186.1928 -2.2329 280.6119 282.8449 291.2917 186.9545 -2.2349 280.7001 282.9351 291.4057 187.8070 -2.2379 280.8055 283.0434 291.5362 188.5988 -2.2390 280.8978 283.1368 291.6572 189.3905 -2.2413 280.9920 283.2333 291.7782 190.2130 -2.2433 281.0795 283.3228 291.9017 190.9745 -2.2453 281.1539 283.3992 292.0140 191.8268 -2.2454 281.2625 283.5079 292.1510 192.6188 -2.2464 281.3498 283.5962 292.2646 193.4105 -2.2496 281.4358 283.6854 292.3755 194.2325 -2.2499 281.5411 283.7909 292.5103 195.0245 -2.2501 281.6274 283.8775 292.6247 195.8475 -2.2510 281.7252 283.9762 292.7599 196.6398 -2.2544 281.8227 284.0771 292.8740 197.4325 -2.2557 281.9301 284.1858 292.9778 198.2548 -2.2536 282.0309 284.2845 293.1179 199.0475 -2.2552 282.1200 284.3753 293.2244 199.8695 -2.2580 282.2107 284.4688 293.3408 200.6615 -2.2602 282.3051 284.5653 293.4644 201.4535 -2.2632 282.3778 284.6410 293.6011 202.3060 -2.2645 282.4776 284.7421 293.7274 203.0673 -2.2641 282.5890 284.8531 293.8495 203.8813 -2.2647 282.6729 284.9375 293.9846 204.6715 -2.2682 282.7539 285.0220 294.1121 205.4593 -2.2668 282.8599 285.1267 294.2501 206.2775 -2.2683 282.9741 285.2424 294.3928 207.0658 -2.2719 283.0809 285.3528 294.5275 207.8848 -2.2725 283.1724 285.4449 294.6510 208.6733 -2.2748 283.2819 285.5567 294.7926 209.4620 -2.2761 283.3725 285.6486 294.9161 210.2808 -2.2779 283.4521 285.7300 295.0751 211.0703 -2.2821 283.5473 285.8293 295.2112 211.8903 -2.2848 283.6519 285.9367 295.3504 212.6798 -2.2833 283.7562 286.0395 295.4852 213.4715 -2.2846 283.8552 286.1398 295.6216 214.2935 -2.2845 283.9559 286.2405 295.7644 215.0555 -2.2860 284.0547 286.3407 295.8927 215.9075 -2.2863 284.1503 286.4367 296.0501 216.6995 -2.2895 284.2514 286.5409 296.1740 217.4915 -2.2915 284.3491 286.6406 296.2989 218.3135 -2.2923 284.4580 286.7502 296.4470 219.0753 -2.2962 284.5597 286.8559 296.5753 219.9273 -2.2989 284.6560 286.9549 296.7192 220.6890 -2.2992 284.7541 287.0533 296.8424 221.5108 -2.3011 284.8547 287.1558 296.9803 222.3330 -2.3031 284.9530 287.2561 297.1397 223.0945 -2.3056 285.0755 287.3810 297.2662 223.9470 -2.3035 285.1830 287.4865 297.4201 224.7088 -2.3047 285.2699 287.5746 297.5406 225.5308 -2.3068 285.3847 287.6915 297.6814 226.3153 -2.3086 285.4793 287.7879 297.8117 227.1448 -2.3116 285.5877 287.8993 297.9575 227.9370 -2.3129 285.6977 288.0106 298.0875 228.7285 -2.3128 285.7889 288.1018 298.2124 229.5508 -2.3166 285.8894 288.2061 298.3528 230.3425 -2.3179 286.0041 288.3220 298.4957 231.1648 -2.3200 286.0940 288.4139 298.6284 231.9565 -2.3221 286.1959 288.5180 298.7645 232.7485 -2.3242 286.3026 288.6267 298.8925 233.5710 -2.3234 286.4053 288.7287 299.0277 234.3635 -2.3243 286.5079 288.8321 299.1640 235.1848 -2.3267 286.6178 288.9445 299.2930 235.9715 -2.3274 286.7318 289.0592 299.4148 236.7610 -2.3295 286.8191 289.1485 299.5558 237.5790 -2.3306 286.9352 289.2658 299.6957 238.3670 -2.3313 287.0471 289.3784 299.8035 239.1858 -2.3318 287.1492 289.4810 299.9388 239.9745 -2.3348 287.2477 289.5825 300.0646 240.7640 -2.3374 287.3600 289.6974 300.1794 241.5830 -2.3385 287.4679 289.8064 300.3108 242.3723 -2.3407 287.5756 289.9164 300.4424 243.1925 -2.3443 287.6919 290.0362 300.5911 243.9838 -2.3482 287.8020 290.1502 300.7125 244.7755 -2.3505 287.9011 290.2516 300.8435 245.5978 -2.3506 288.0016 290.3521 300.9792 246.3683 -2.3517 288.1011 290.4528 301.0904 247.2155 -2.3498 288.2318 290.5816 301.2248 247.9775 -2.3543 288.3267 290.6810 301.3378 248.8298 -2.3568 288.4304 290.7872 301.4772 249.5915 -2.3585 288.5549 290.9135 301.5897 250.4135 -2.3581 288.6685 291.0267 301.7199 251.2358 -2.3581 288.7637 291.1218 301.8631 251.9975 -2.3583 288.8623 291.2206 301.9706 252.8500 -2.3547 288.9728 291.3275 302.1116 253.6125 -2.3574 289.0846 291.4420 302.2198 254.4345 -2.3576 289.1887 291.5463 302.3456 255.2565 -2.3610 289.2893 291.6503 302.4541 256.0185 -2.3624 289.4017 291.7641 302.5592 256.8705 -2.3636 289.5287 291.8923 302.7094 257.6625 -2.3662 289.6336 291.9998 302.8322 258.4543 -2.3658 289.7414 292.1072 302.9354 259.2765 -2.3578 289.8749 292.2327 303.0523 260.0380 -2.3603 289.9871 292.3474 303.1755 260.8905 -2.3652 290.0898 292.4550 303.2996 261.6833 -2.3725 290.1986 292.5711 303.4185 262.4745 -2.3777 290.3143 292.6920 303.5263 263.2970 -2.3800 290.4340 292.8141 303.6510 264.0888 -2.3826 290.5516 292.9342 303.7610 264.9115 -2.3838 290.6560 293.0399 303.8870 265.7040 -2.3868 290.7640 293.1508 304.0060 266.4965 -2.3898 290.8819 293.2717 304.1152 267.2878 -2.3888 290.9909 293.3797 304.2448 268.1185 -2.3889 291.1120 293.5009 304.3808 268.9360 -2.3917 291.2165 293.6083 304.4973 269.6940 -2.3929 291.3136 293.7065 304.5997 270.5430 -2.3958 291.4301 293.8259 304.7526 271.3010 -2.3957 291.5349 293.9307 304.8840 272.1190 -2.3985 291.6616 294.0602 305.0121 272.9373 -2.4017 291.7666 294.1683 305.1499 273.6960 -2.4044 291.8865 294.2909 305.2641 274.5450 -2.4054 292.0103 294.4157 305.4163 275.3340 -2.4076 292.1090 294.5166 305.5403 276.1238 -2.4086 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