DTA measure 16_masodik Date: 2024430:1151 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1130.98 s Mass = 956.400 mg data_number = 1408 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1445 -1.4353 235.7170 237.1522 261.9376 1.9953 -1.4510 235.8267 237.2777 261.9048 2.7548 -1.4473 235.9176 237.3649 261.8965 3.5748 -1.4355 236.0168 237.4523 261.8905 4.3655 -1.4472 236.0992 237.5464 261.8729 5.1560 -1.4507 236.1971 237.6478 261.8820 6.0070 -1.4485 236.2961 237.7446 261.8632 6.7663 -1.4536 236.3687 237.8223 261.8733 7.5870 -1.4504 236.4731 237.9236 261.8880 8.4070 -1.4480 236.5733 238.0212 261.9086 9.1668 -1.4498 236.6544 238.1042 261.9153 10.0180 -1.4444 236.7766 238.2210 261.9510 10.7790 -1.4473 236.8606 238.3079 261.9733 11.5995 -1.4464 236.9438 238.3902 261.9974 12.4210 -1.4461 237.0409 238.4870 262.0375 13.1818 -1.4452 237.1279 238.5731 262.1040 14.0330 -1.4414 237.2220 238.6634 262.1390 14.8220 -1.4427 237.2957 238.7384 262.1970 15.6128 -1.4429 237.3921 238.8350 262.2471 16.4335 -1.4431 237.5073 238.9504 262.3190 17.1943 -1.4426 237.6064 239.0490 262.4002 18.0475 -1.4236 237.6927 239.1163 262.4871 18.8368 -1.4190 237.7939 239.2128 262.5854 19.6285 -1.4299 237.8900 239.3200 262.6815 20.4495 -1.4369 237.9705 239.4074 262.7755 21.2393 -1.4421 238.0627 239.5049 262.8795 22.0603 -1.4407 238.1626 239.6032 262.9941 22.8505 -1.4347 238.2528 239.6874 263.0916 23.6418 -1.4375 238.3362 239.7736 263.1985 24.4975 -1.4372 238.4469 239.8841 263.3372 25.2595 -1.4431 238.5372 239.9803 263.4496 26.0800 -1.4442 238.6136 240.0578 263.5501 26.8715 -1.4437 238.7092 240.1528 263.6771 27.6620 -1.4466 238.8069 240.2535 263.7964 28.5123 -1.4445 238.9048 240.3493 263.9180 29.2715 -1.4403 238.9962 240.4365 264.0636 30.0925 -1.4431 239.0886 240.5318 264.1997 30.8835 -1.4417 239.1726 240.6143 264.3567 31.6745 -1.4420 239.2606 240.7025 264.4855 32.5258 -1.4434 239.3597 240.8031 264.6337 33.2860 -1.4466 239.4657 240.9123 264.7768 34.1073 -1.4448 239.5400 240.9848 264.9127 34.8988 -1.4415 239.6316 241.0730 265.0633 35.6915 -1.4404 239.7249 241.1652 265.2185 36.5428 -1.4429 239.8311 241.2740 265.3730 37.3070 -1.4410 239.9270 241.3680 265.5216 38.1298 -1.4391 240.0176 241.4567 265.6747 38.9213 -1.4483 240.1063 241.5545 265.8276 39.7115 -1.4512 240.2068 241.6580 265.9723 40.5628 -1.4542 240.3006 241.7547 266.1267 41.3245 -1.4441 240.3944 241.8385 266.2694 42.1465 -1.4391 240.4849 241.9241 266.4188 42.9383 -1.4503 240.5752 242.0255 266.5665 43.7283 -1.4547 240.6738 242.1285 266.7040 44.5795 -1.4586 240.7918 242.2504 266.8726 45.3400 -1.4625 240.8755 242.3381 267.0145 46.1608 -1.4668 240.9530 242.4198 267.1619 46.9505 -1.4678 241.0516 242.5194 267.3121 47.7413 -1.4660 241.1654 242.6314 267.4520 48.5925 -1.4691 241.2668 242.7359 267.5937 49.3528 -1.4716 241.3649 242.8365 267.7145 50.1740 -1.4696 241.4634 242.9330 267.8458 50.9655 -1.4686 241.5418 243.0104 267.9832 51.7575 -1.4676 241.6353 243.1030 268.0964 52.6088 -1.4553 241.7315 243.1868 268.2405 53.3698 -1.4698 241.8238 243.2936 268.3658 54.1903 -1.4776 241.9232 243.4008 268.4809 54.9815 -1.4798 242.0234 243.5031 268.6143 55.7735 -1.4821 242.1330 243.6151 268.7219 56.6248 -1.4720 242.2072 243.6792 268.8503 57.3848 -1.4725 242.3219 243.7944 268.9490 58.2063 -1.4838 242.4284 243.9123 269.0803 58.9970 -1.4852 242.5126 243.9978 269.1808 59.7870 -1.4860 242.6150 244.1010 269.2850 60.6378 -1.4893 242.7049 244.1942 269.3886 61.3970 -1.4834 242.8035 244.2869 269.4815 62.2188 -1.4800 242.9161 244.3961 269.6034 63.0103 -1.4890 243.0217 244.5108 269.6986 63.8005 -1.4954 243.0814 244.5768 269.7849 64.6518 -1.4989 243.2125 244.7114 269.8874 65.4128 -1.5003 243.2995 244.7998 269.9696 66.2340 -1.4899 243.3941 244.8841 270.0820 67.0258 -1.4914 243.5028 244.9941 270.1701 67.8163 -1.4984 243.5837 245.0821 270.2509 68.6425 -1.4985 243.6888 245.1873 270.3574 69.4045 -1.5021 243.8034 245.3055 270.4356 70.2565 -1.5033 243.9054 245.4087 270.5105 71.0465 -1.4940 243.9880 245.4820 270.5945 71.8385 -1.4937 244.0932 245.5869 270.6828 72.6593 -1.5022 244.1804 245.6826 270.7605 73.4195 -1.5062 244.2775 245.7837 270.8451 74.2715 -1.5067 244.3932 245.8999 270.9442 75.0628 -1.5000 244.4894 245.9893 271.0288 75.8538 -1.4855 244.5784 246.0639 271.1156 76.6755 -1.4892 244.6780 246.1672 271.1995 77.4368 -1.5002 244.7968 246.2970 271.2868 78.2885 -1.5008 244.8968 246.3976 271.3793 79.0505 -1.5093 244.9913 246.5006 271.4634 79.8723 -1.5058 245.0900 246.5958 271.5733 80.6633 -1.5035 245.1880 246.6915 271.6511 81.4560 -1.5116 245.2657 246.7773 271.7293 82.3073 -1.5196 245.3727 246.8923 271.8241 83.0663 -1.5147 245.4626 246.9773 271.9154 83.8858 -1.5156 245.5608 247.0765 271.9935 84.6783 -1.5194 245.6701 247.1894 272.0838 85.4683 -1.5135 245.7727 247.2862 272.1705 86.3203 -1.5091 245.8703 247.3794 272.2755 87.0813 -1.5045 245.9670 247.4715 272.3737 87.9028 -1.5072 246.0760 247.5832 272.4560 88.6943 -1.5116 246.1625 247.6741 272.5512 89.4843 -1.5248 246.2672 247.7920 272.6362 90.3095 -1.5240 246.3569 247.8808 272.7378 91.1015 -1.5229 246.4638 247.9867 272.8147 91.9228 -1.5347 246.5479 248.0825 272.9110 92.7140 -1.5311 246.6390 248.1701 273.0113 93.5053 -1.5240 246.7512 248.2752 273.1255 94.3260 -1.5307 246.8368 248.3675 273.2139 95.0870 -1.5309 246.9468 248.4777 273.3025 95.9385 -1.5450 247.0606 248.6056 273.4223 96.7295 -1.5493 247.1490 248.6983 273.5194 97.5208 -1.5494 247.2455 248.7948 273.6314 98.3415 -1.5529 247.3450 248.8980 273.7522 99.1030 -1.5631 247.4408 249.0039 273.8537 99.9543 -1.5680 247.5444 249.1124 273.9697 100.7438 -1.5649 247.6435 249.2084 274.0750 101.5343 -1.5678 247.7553 249.3231 274.1944 102.3555 -1.5686 247.8471 249.4156 274.3026 103.1158 -1.5679 247.9460 249.5139 274.4072 103.9673 -1.5389 248.0342 249.5732 274.5161 104.7568 -1.5297 248.1531 249.6829 274.6108 105.5485 -1.4956 248.2528 249.7484 274.7325 106.3705 -1.4441 248.3483 249.7924 274.8612 107.1300 -1.4569 248.4685 249.9254 274.9858 107.9808 -1.4452 248.5487 249.9939 275.0960 108.7705 -1.4318 248.6438 250.0756 275.2100 109.5600 -1.4599 248.7430 250.2029 275.3186 110.3813 -1.5260 248.8470 250.3730 275.4259 111.1408 -1.5643 248.9545 250.5188 275.5472 111.9930 -1.5791 249.0736 250.6527 275.6561 112.7833 -1.5786 249.1554 250.7341 275.7819 113.5730 -1.5667 249.2576 250.8243 275.9079 114.3940 -1.5212 249.3596 250.8808 276.0093 115.1540 -1.5618 249.4428 251.0046 276.1466 116.0058 -1.5775 249.5582 251.1357 276.2484 116.7950 -1.5707 249.6557 251.2264 276.3557 117.5850 -1.5808 249.7479 251.3287 276.4735 118.4058 -1.5840 249.8608 251.4448 276.5853 119.1963 -1.5828 249.9546 251.5374 276.7239 120.0165 -1.5847 250.0642 251.6488 276.8333 120.8085 -1.5860 250.1619 251.7479 276.9563 121.6005 -1.5877 250.2690 251.8567 277.0859 122.4225 -1.5932 250.3634 251.9566 277.2024 123.1843 -1.5944 250.4558 252.0502 277.2800 124.0385 -1.5892 250.5668 252.1560 277.4247 124.8278 -1.5873 250.6564 252.2437 277.5461 125.6190 -1.5859 250.7619 252.3478 277.6493 126.4405 -1.5872 250.8908 252.4780 277.7523 127.2023 -1.5916 250.9867 252.5783 277.8629 128.0533 -1.5971 251.0703 252.6675 277.9824 128.8438 -1.6042 251.1651 252.7693 278.0917 129.6355 -1.6036 251.2797 252.8833 278.1857 130.4565 -1.6009 251.3874 252.9883 278.2976 131.2178 -1.5979 251.4883 253.0862 278.4049 132.0693 -1.6121 251.5909 253.2030 278.5032 132.8603 -1.6201 251.6844 253.3046 278.5949 133.6505 -1.6196 251.7724 253.3921 278.6968 134.4723 -1.6228 251.8781 253.5009 278.7843 135.2333 -1.6231 251.9990 253.6221 278.8834 136.0840 -1.6191 252.0995 253.7186 278.9871 136.8743 -1.6208 252.1911 253.8120 279.0941 137.6648 -1.6219 252.2834 253.9053 279.1874 138.4870 -1.6267 252.3976 254.0243 279.2813 139.2478 -1.6292 252.4918 254.1210 279.3729 140.0998 -1.6316 252.6110 254.2426 279.4692 140.8910 -1.6337 252.7162 254.3500 279.5398 141.6818 -1.6333 252.8188 254.4521 279.6434 142.5025 -1.6322 252.9298 254.5621 279.7410 143.2915 -1.6330 253.0187 254.6517 279.8299 144.1118 -1.6361 253.1380 254.7741 279.9181 144.9023 -1.6419 253.2211 254.8630 280.0028 145.6923 -1.6436 253.3166 254.9602 280.1113 146.5135 -1.6387 253.4237 255.0625 280.2033 147.3040 -1.6316 253.5192 255.1509 280.2893 148.1250 -1.6237 253.6236 255.2473 280.3873 148.9163 -1.6353 253.7366 255.3719 280.4793 149.7068 -1.6458 253.8315 255.4773 280.5778 150.5285 -1.6492 253.9434 255.5926 280.6761 151.3183 -1.6500 254.0380 255.6880 280.7858 152.1388 -1.6523 254.1511 255.8034 280.8853 152.9285 -1.6529 254.2334 255.8863 280.9936 153.7190 -1.6586 254.3215 255.9801 281.1050 154.5693 -1.6640 254.4467 256.1107 281.2187 155.3295 -1.6666 254.5408 256.2075 281.3278 156.1513 -1.6686 254.6613 256.3299 281.4322 156.9425 -1.6646 254.7623 256.4269 281.5100 157.7333 -1.6500 254.8574 256.5074 281.6234 158.5845 -1.6488 254.9836 256.6324 281.7534 159.3465 -1.6524 255.0552 256.7077 281.8381 160.1678 -1.6672 255.1602 256.8273 281.9514 160.9590 -1.6767 255.2877 256.9644 282.0638 161.7520 -1.6783 255.3892 257.0675 282.1752 162.5775 -1.6747 255.4748 257.1495 282.2809 163.3700 -1.6765 255.5653 257.2419 282.3953 164.1918 -1.6765 255.6800 257.3565 282.5215 164.9840 -1.6799 255.7971 257.4771 282.6386 165.7748 -1.6796 255.9171 257.5968 282.7310 166.5965 -1.6804 256.0004 257.6808 282.8318 167.3873 -1.6779 256.0879 257.7658 282.9342 168.2088 -1.6816 256.2119 257.8935 283.0661 169.0000 -1.6830 256.3131 257.9961 283.1491 169.7903 -1.6865 256.4159 258.1023 283.2652 170.6118 -1.6844 256.5248 258.2092 283.3851 171.3735 -1.6732 256.6076 258.2808 283.4877 172.2253 -1.6753 256.7244 258.3996 283.6122 173.0165 -1.6894 256.8279 258.5174 283.7114 173.8085 -1.7013 256.9296 258.6309 283.7846 174.6305 -1.7116 257.0507 258.7623 283.8840 175.3920 -1.7087 257.1319 258.8406 284.0093 176.2435 -1.7105 257.2428 258.9533 284.1383 177.0338 -1.7128 257.3514 259.0642 284.2406 177.8240 -1.7116 257.4531 259.1648 284.3380 178.6445 -1.7113 257.5549 259.2661 284.4441 179.4050 -1.7186 257.6658 259.3844 284.5516 180.2563 -1.7251 257.7713 259.4964 284.6568 181.0468 -1.7214 257.8651 259.5866 284.7815 181.8380 -1.7206 257.9650 259.6856 284.8977 182.6583 -1.7125 258.0809 259.7934 284.9848 183.4183 -1.7112 258.1742 259.8853 285.0763 184.2693 -1.7112 258.2832 259.9944 285.1784 185.0595 -1.7176 258.3854 260.1029 285.2936 185.8500 -1.7200 258.4896 260.2096 285.4058 186.6723 -1.7165 258.5961 260.3125 285.5189 187.4338 -1.7172 258.7097 260.4269 285.6164 188.2853 -1.7234 258.8063 260.5297 285.7166 189.0440 -1.7270 258.9015 260.6284 285.8245 189.8668 -1.7323 259.0234 260.7557 285.9152 190.6880 -1.7305 259.1373 260.8677 286.0324 191.4490 -1.7356 259.2360 260.9716 286.1280 192.3008 -1.7347 259.3384 261.0731 286.2422 193.0610 -1.7316 259.4419 261.1735 286.3418 193.8828 -1.7367 259.5332 261.2699 286.4460 194.6750 -1.7399 259.6318 261.3716 286.5576 195.4655 -1.7409 259.7406 261.4815 286.6682 196.2868 -1.7421 259.8624 261.6045 286.7675 197.0785 -1.7433 259.9530 261.6963 286.8583 197.9000 -1.7431 260.0492 261.7923 286.9547 198.6905 -1.7451 260.1637 261.9088 287.0602 199.4818 -1.7498 260.2671 262.0169 287.1618 200.3035 -1.7515 260.3749 262.1264 287.2679 201.0645 -1.7547 260.4818 262.2365 287.3746 201.9163 -1.7548 260.5712 262.3260 287.4622 202.6768 -1.7423 260.6873 262.4295 287.5416 203.4983 -1.7263 260.7944 262.5206 287.6592 204.3195 -1.7312 260.9050 262.6361 287.7732 205.0808 -1.7438 260.9855 262.7293 287.8659 205.9315 -1.7506 261.1221 262.8727 287.9778 206.6925 -1.7542 261.2164 262.9707 288.0727 207.5138 -1.7577 261.3152 263.0728 288.1725 208.3045 -1.7641 261.4125 263.1767 288.2671 209.0958 -1.7652 261.5162 263.2815 288.3638 209.9460 -1.7601 261.6295 263.3895 288.4767 210.7068 -1.7622 261.7337 263.4960 288.5710 211.5278 -1.7603 261.8538 263.6141 288.6930 212.3190 -1.7539 261.9482 263.7021 288.7719 213.1083 -1.7496 262.0533 263.8029 288.8743 213.9598 -1.7417 262.1617 263.9034 288.9795 214.7198 -1.7491 262.2652 264.0143 289.0836 215.5418 -1.7662 262.3747 264.1410 289.1856 216.3340 -1.7702 262.4649 264.2351 289.2770 217.1280 -1.7723 262.5884 264.3607 289.3722 217.9520 -1.7726 262.6906 264.4632 289.4900 218.7135 -1.7809 262.7756 264.5566 289.5755 219.5658 -1.7840 262.8853 264.6693 289.6823 220.3260 -1.7827 262.9842 264.7668 289.7667 221.1473 -1.7612 263.0922 264.8534 289.8690 221.9688 -1.7393 263.2100 264.9493 289.9857 222.7283 -1.7367 263.3108 265.0475 290.0643 223.5793 -1.7547 263.4352 265.1899 290.1817 224.3395 -1.7741 263.5294 265.3035 290.2569 225.1615 -1.7812 263.6082 265.3894 290.3812 225.9835 -1.7855 263.7444 265.5299 290.4847 226.7450 -1.7794 263.8328 265.6121 290.5789 227.5965 -1.7748 263.9491 265.7239 290.6943 228.3575 -1.7805 264.0493 265.8298 290.7734 229.1795 -1.7904 264.1546 265.9450 290.8859 229.9715 -1.8013 264.2597 266.0610 290.9954 230.7628 -1.8069 264.3658 266.1727 291.1224 231.5845 -1.8123 264.4776 266.2898 291.2375 232.3753 -1.8139 264.5814 266.3953 291.3769 233.1965 -1.8170 264.6778 266.4948 291.4768 233.9885 -1.8168 264.7874 266.6042 291.5736 234.7798 -1.8133 264.8861 266.6993 291.6841 235.6003 -1.8204 264.9948 266.8152 291.8020 236.3898 -1.8215 265.0997 266.9212 291.9079 237.2090 -1.8153 265.1917 267.0069 292.0239 237.9990 -1.8209 265.3023 267.1233 292.1292 238.7898 -1.8235 265.4231 267.2466 292.2482 239.6410 -1.8262 265.5296 267.3558 292.3586 240.4028 -1.8336 265.6154 267.4491 292.4759 241.2248 -1.8332 265.7123 267.5456 292.6161 242.0160 -1.8319 265.8528 267.6848 292.7262 242.8085 -1.8355 265.9482 267.7837 292.8345 243.6310 -1.8362 266.0302 267.8664 292.9472 244.3925 -1.8399 266.1253 267.9652 293.0679 245.2450 -1.8404 266.2527 268.0930 293.2074 246.0363 -1.8406 266.3654 268.2060 293.3162 246.8268 -1.8425 266.4788 268.3213 293.4243 247.6470 -1.8447 266.5901 268.4348 293.5430 248.4085 -1.8477 266.6877 268.5354 293.6279 249.2605 -1.8506 266.7972 268.6478 293.7544 250.0508 -1.8545 266.9021 268.7566 293.8672 250.8423 -1.8596 267.0106 268.8702 293.9748 251.6635 -1.8628 267.1224 268.9852 294.0733 252.4250 -1.8630 267.2202 269.0832 294.1753 253.2765 -1.8644 267.3197 269.1841 294.2815 254.0385 -1.8663 267.4146 269.2809 294.3919 254.8635 -1.8675 267.5306 269.3981 294.5062 255.6845 -1.8705 267.6587 269.5292 294.5997 256.4460 -1.8704 267.7674 269.6378 294.6999 257.2975 -1.8718 267.8778 269.7496 294.8042 258.0595 -1.8757 267.9543 269.8300 294.8864 258.8813 -1.8749 268.0620 269.9369 294.9934 259.6725 -1.8746 268.1601 270.0347 295.1039 260.4638 -1.8766 268.2697 270.1463 295.1948 261.3155 -1.8816 268.3934 270.2750 295.3006 262.0763 -1.8816 268.5102 270.3918 295.3994 262.8978 -1.8847 268.6296 270.5142 295.4867 263.6883 -1.8840 268.7225 270.6066 295.5763 264.4788 -1.8826 268.8219 270.7045 295.6764 265.3310 -1.8801 268.9303 270.8104 295.7690 266.0913 -1.8817 269.0297 270.9113 295.8523 266.9125 -1.8872 269.1411 271.0283 295.9571 267.7030 -1.8874 269.2316 271.1190 296.0667 268.4938 -1.8875 269.3364 271.2239 296.1459 269.3458 -1.8828 269.4481 271.3309 296.2529 270.1068 -1.8861 269.5594 271.4455 296.3345 270.9288 -1.8955 269.6744 271.5698 296.4198 271.7208 -1.8998 269.7763 271.6761 296.5331 272.5113 -1.9021 269.8704 271.7725 296.6225 273.3628 -1.9070 269.9935 271.9005 296.7449 274.1235 -1.9097 270.0849 271.9946 296.8157 274.9453 -1.9083 270.2120 272.1202 296.9261 275.7365 -1.9114 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