DTA measure 2masodikolom Test Date: 2023104:1443 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.07 s Mass = 1452.000 mg data_number = 1573 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1003 0.2573 268.6797 268.4224 267.7122 1.8625 0.2663 268.7119 268.4456 267.7351 2.7140 0.2597 268.7691 268.5094 267.7626 3.5065 0.2648 268.7579 268.4931 267.6762 4.2978 0.2638 268.5879 268.3241 267.7039 5.1200 0.2647 268.6974 268.4327 267.7319 5.8815 0.2579 268.7640 268.5061 267.6402 6.7338 0.2547 268.7590 268.5043 267.7839 7.4948 0.2375 268.7441 268.5066 267.7064 8.3250 0.2539 268.7106 268.4567 267.6075 9.1165 0.2534 268.7787 268.5253 267.6253 9.9388 0.2588 268.7323 268.4735 267.7091 10.7308 0.2614 268.7705 268.5090 267.6853 11.5225 0.2548 268.8357 268.5809 267.7679 12.3448 0.2587 268.7252 268.4664 267.9066 13.1065 0.2722 268.8086 268.5364 267.8731 13.9585 0.2608 268.7772 268.5165 267.8421 14.7210 0.2643 268.8312 268.5669 267.8184 15.5445 0.2466 268.8365 268.5899 267.8826 16.3665 0.2454 268.8874 268.6420 267.9633 17.1285 0.2616 268.8058 268.5442 268.1110 17.9808 0.2606 268.8135 268.5529 268.1891 18.7425 0.2443 268.7750 268.5307 268.1287 19.5645 0.2504 268.7746 268.5242 268.3017 20.3565 0.2663 268.7425 268.4762 268.3663 21.1485 0.2485 268.7768 268.5283 268.4253 22.0005 0.2457 268.8182 268.5726 268.5160 22.7625 0.2431 268.7880 268.5448 268.6463 23.5845 0.2392 268.7889 268.5497 268.7165 24.3773 0.2569 268.8070 268.5501 268.7866 25.1695 0.2495 268.7733 268.5238 268.9476 25.9913 0.2469 268.7352 268.4883 269.0141 26.7525 0.2622 268.7678 268.5056 269.1017 27.6055 0.2513 268.8414 268.5901 269.2101 28.3715 0.2517 268.7889 268.5371 269.2714 29.1930 0.2453 268.7986 268.5533 269.4532 30.0153 0.2342 268.8467 268.6125 269.4929 30.7773 0.2417 268.8412 268.5996 269.6598 31.6290 0.2385 268.9046 268.6661 269.7354 32.3908 0.2346 268.8506 268.6160 269.8569 33.2128 0.2415 268.8093 268.5678 269.9719 34.0050 0.2278 268.8513 268.6235 270.0874 34.7965 0.2361 268.7600 268.5238 270.3214 35.6488 0.2400 268.8704 268.6304 270.4066 36.4110 0.2362 268.8918 268.6556 270.5161 37.2328 0.2353 268.8928 268.6575 270.7006 38.0255 0.2404 268.7732 268.5328 270.8259 38.8175 0.2201 268.7966 268.5765 270.8827 39.6395 0.2084 268.8095 268.6011 271.0056 40.4015 0.2179 268.9364 268.7185 271.0791 41.2535 0.2257 268.8862 268.6605 271.2398 42.0455 0.2145 268.8808 268.6662 271.3931 42.8375 0.2117 268.9263 268.7147 271.5239 43.6595 0.1990 268.9695 268.7706 271.7496 44.4215 0.2052 268.9417 268.7364 271.7616 45.2735 0.1877 268.9096 268.7219 271.8247 46.0355 0.1889 268.9331 268.7441 271.9993 46.8575 0.1735 268.8943 268.7208 272.1283 47.6795 0.1707 268.8713 268.7006 272.1993 48.4510 0.1827 268.9381 268.7554 272.2302 49.2795 0.1708 269.0628 268.8920 272.3442 50.0405 0.1514 269.0049 268.8535 272.4959 50.8925 0.1341 268.9802 268.8461 272.6041 51.6545 0.1296 269.0276 268.8980 272.6466 52.4765 0.1197 269.0663 268.9467 272.7528 53.2985 0.1296 269.1415 269.0119 272.8113 54.0605 0.1258 269.1209 268.9950 272.9307 54.9120 0.1052 269.1636 269.0584 273.0966 55.6743 0.1059 269.0661 268.9602 273.2139 56.4960 0.1118 269.1040 268.9923 273.3811 57.2883 0.1098 269.1130 269.0032 273.5358 58.0795 0.1086 269.1448 269.0362 273.6176 58.9320 0.0858 269.1647 269.0789 273.7438 59.6945 0.0959 269.0607 268.9648 273.7332 60.5168 0.0819 269.1564 269.0745 273.8643 61.3095 0.0665 269.1884 269.1218 274.0144 62.1005 0.0673 269.2025 269.1352 274.1959 62.9228 0.0700 269.2304 269.1605 274.3426 63.7150 0.0647 269.2556 269.1909 274.3398 64.5368 0.0532 269.1891 269.1359 274.5607 65.3288 0.0517 269.2320 269.1804 274.8030 66.1228 0.0388 269.2851 269.2463 274.7390 66.9468 0.0281 269.2957 269.2677 274.8818 67.7085 0.0319 269.2810 269.2491 274.9626 68.5618 -0.0053 269.2675 269.2728 275.1877 69.3323 0.0095 269.2520 269.2425 275.3744 70.1545 0.0104 269.4320 269.4215 275.4032 70.9465 0.0096 269.4059 269.3963 275.5596 71.7385 -0.0026 269.4980 269.5006 275.7137 72.5605 -0.0055 269.4486 269.4541 275.8939 73.3525 -0.0030 269.4856 269.4886 276.0514 74.1745 -0.0162 269.5133 269.5295 276.0408 74.9665 -0.0207 269.4712 269.4918 276.1558 75.7585 -0.0298 269.5058 269.5356 276.2390 76.5805 -0.0451 269.5301 269.5752 276.3031 77.3425 -0.0626 269.5526 269.6152 276.4849 78.1945 -0.0555 269.5784 269.6339 276.5537 78.9865 -0.0526 269.5842 269.6368 276.5724 79.7785 -0.0685 269.6083 269.6768 276.6675 80.6005 -0.0917 269.6624 269.7541 276.7521 81.3625 -0.0951 269.6982 269.7933 276.8780 82.2143 -0.0803 269.7421 269.8224 277.0252 82.9763 -0.0877 269.8010 269.8887 277.1561 83.7973 -0.0871 269.6832 269.7703 277.2744 84.6193 -0.1001 269.7508 269.8509 277.3363 85.3808 -0.1036 269.8393 269.9428 277.3926 86.2328 -0.0994 269.8880 269.9874 277.4183 86.9938 -0.1309 269.9181 270.0490 277.5568 87.8158 -0.1238 269.8637 269.9875 277.8932 88.6078 -0.1259 269.8709 269.9969 277.9749 89.4083 -0.1354 269.9225 270.0579 278.0502 90.2368 -0.1545 269.9676 270.1222 278.0363 90.9985 -0.1446 269.9310 270.0755 278.1461 91.8508 -0.1501 269.9203 270.0704 278.2399 92.6130 -0.1572 270.0271 270.1842 278.2791 93.4365 -0.1546 270.0566 270.2112 278.3893 94.2285 -0.1505 270.0986 270.2491 278.4288 95.0205 -0.1492 270.0994 270.2486 278.5512 95.8725 -0.1826 270.1648 270.3474 278.6647 96.6345 -0.1745 270.2374 270.4120 278.6118 97.4565 -0.1883 270.1673 270.3556 278.7321 98.2485 -0.1933 270.1893 270.3826 278.8222 99.0400 -0.1891 270.1120 270.3011 279.0308 99.8208 -0.2020 270.2532 270.4552 279.0396 100.6895 -0.2237 270.3297 270.5534 279.1416 101.4515 -0.2491 270.3250 270.5741 279.2600 102.2735 -0.2464 270.4354 270.6818 279.3430 103.0655 -0.2397 270.3490 270.5887 279.4147 103.8575 -0.2709 270.4585 270.7294 279.4504 104.6795 -0.2702 270.5127 270.7829 279.5720 105.4415 -0.2528 270.5254 270.7782 279.6603 106.2928 -0.2623 270.6327 270.8950 279.7545 107.0835 -0.2729 270.6628 270.9357 279.8943 107.8753 -0.2899 270.6733 270.9633 279.9648 108.6973 -0.2987 270.6775 270.9762 280.1405 109.4593 -0.2931 270.7578 271.0509 280.1698 110.2608 -0.2962 270.7137 271.0098 280.3411 111.1118 -0.3097 270.7304 271.0402 280.3807 111.9043 -0.3145 270.7058 271.0203 280.5196 112.6955 -0.3187 270.6981 271.0167 280.6673 113.5178 -0.3359 270.9209 271.2568 280.6652 114.2798 -0.3402 270.8717 271.2119 280.7413 115.1320 -0.3504 270.9469 271.2972 280.9186 115.8938 -0.3451 271.0178 271.3630 280.9141 116.7153 -0.3558 270.9784 271.3342 280.9808 117.5368 -0.3652 270.9614 271.3266 281.1032 118.2975 -0.3631 270.9811 271.3442 281.3118 119.1498 -0.3717 271.0920 271.4637 281.4285 119.8990 -0.3838 271.1454 271.5292 281.4905 120.7125 -0.3813 271.2405 271.6218 281.5574 121.5345 -0.4006 271.2423 271.6429 281.6133 122.3568 -0.3921 271.3340 271.7261 281.6686 123.1198 -0.4125 271.2988 271.7113 281.8487 123.9755 -0.4186 271.2893 271.7079 282.0337 124.7375 -0.4400 271.3472 271.7872 282.1476 125.5595 -0.4462 271.3582 271.8044 282.2120 126.3523 -0.4308 271.3371 271.7679 282.3491 127.1455 -0.4339 271.4683 271.9022 282.4275 127.9675 -0.4503 271.4474 271.8976 282.5244 128.7295 -0.4727 271.4593 271.9320 282.6260 129.5815 -0.4625 271.4968 271.9593 282.6722 130.3440 -0.4648 271.5181 271.9829 282.8255 131.1655 -0.4786 271.6295 272.1081 282.8963 131.9575 -0.4972 271.5185 272.0157 283.0607 132.7795 -0.5036 271.5919 272.0955 283.1237 133.5715 -0.5112 271.6787 272.1899 283.1979 134.3933 -0.5037 271.7998 272.3035 283.3739 135.1855 -0.5145 271.8347 272.3492 283.4187 135.9768 -0.5242 271.7972 272.3214 283.6232 136.7993 -0.5122 271.8191 272.3314 283.6800 137.5605 -0.5284 271.8934 272.4217 283.7555 138.4130 -0.5373 271.9135 272.4508 283.8153 139.2050 -0.5549 271.8993 272.4542 284.0548 139.9960 -0.5595 272.0343 272.5938 284.1466 140.7898 -0.5528 272.0449 272.5977 284.2773 141.6223 -0.5608 272.0745 272.6353 284.3495 142.3830 -0.5646 272.1454 272.7100 284.3545 143.2348 -0.5767 272.2058 272.7825 284.5444 143.9965 -0.5773 272.1979 272.7752 284.6232 144.8185 -0.5774 272.2196 272.7969 284.7961 145.6405 -0.5872 272.1669 272.7541 284.9084 146.4025 -0.6023 272.2505 272.8528 284.9913 147.2548 -0.6200 272.4137 273.0337 285.0812 148.0173 -0.6207 272.2933 272.9140 285.1369 148.8405 -0.6235 272.2990 272.9225 285.3241 149.6325 -0.6357 272.3842 273.0198 285.3983 150.4245 -0.6412 272.4171 273.0583 285.4574 151.2198 -0.6315 272.4749 273.1064 285.6165 152.0785 -0.6487 272.4471 273.0958 285.8277 152.8405 -0.6517 272.5453 273.1970 285.9405 153.6625 -0.6580 272.6323 273.2903 286.0476 154.4545 -0.6675 272.5619 273.2295 286.2526 155.2465 -0.6632 272.5617 273.2248 286.3196 156.0685 -0.6746 272.6009 273.2755 286.3352 156.8598 -0.6761 272.6965 273.3725 286.4437 157.6815 -0.6828 272.8362 273.5190 286.5343 158.4735 -0.6886 272.8261 273.5146 286.7195 159.2655 -0.7008 272.9952 273.6960 286.8802 160.0873 -0.7119 273.0150 273.7270 287.1092 160.8643 -0.7131 272.9937 273.7067 287.2239 161.6718 -0.7092 272.9081 273.6173 287.2926 162.4938 -0.7330 273.0090 273.7419 287.4442 163.2930 -0.7318 273.0494 273.7812 287.5735 164.0850 -0.7425 273.1804 273.9229 287.6243 164.9083 -0.7580 273.1798 273.9377 287.7960 165.6703 -0.7569 273.2501 274.0070 287.9813 166.5220 -0.7566 273.2874 274.0440 288.0141 167.2838 -0.7552 273.3612 274.1164 288.0772 168.1058 -0.7626 273.4348 274.1974 288.1610 168.8980 -0.7697 273.3461 274.1157 288.2892 169.7200 -0.7903 273.4660 274.2563 288.3966 170.6320 -0.7887 273.6318 274.4205 288.2867 171.3925 -0.7837 273.5465 274.3302 288.4296 172.2448 -0.7858 273.6276 274.4134 288.5367 173.0068 -0.7985 273.6508 274.4493 288.5907 173.8285 -0.7957 273.6667 274.4624 288.7968 174.6210 -0.8208 273.7866 274.6074 288.8000 175.4135 -0.8120 273.8104 274.6224 288.8291 176.2358 -0.8126 274.0199 274.8325 289.0039 177.0275 -0.8230 273.8692 274.6923 289.0089 177.8495 -0.8200 274.0136 274.8336 289.0639 178.6415 -0.8361 274.0614 274.8975 289.0449 179.4335 -0.8364 274.0884 274.9248 289.2376 180.2555 -0.8471 274.1052 274.9524 289.3792 181.0175 -0.8327 274.2526 275.0854 289.4532 181.8695 -0.8558 274.3922 275.2480 289.5418 182.6615 -0.8596 274.3399 275.1995 289.5940 183.4535 -0.8626 274.2494 275.1120 289.6559 184.2755 -0.8727 274.4439 275.3166 289.8219 185.0375 -0.8905 274.4878 275.3783 289.9328 185.8895 -0.8796 274.4718 275.3514 289.9254 186.6515 -0.8648 274.4892 275.3540 290.0364 187.4730 -0.8883 274.5664 275.4546 290.0668 188.2953 -0.8953 274.7431 275.6384 290.1741 189.0568 -0.8953 274.7663 275.6616 290.2564 189.9090 -0.9158 274.7838 275.6996 290.2959 190.6713 -0.9204 274.9527 275.8731 290.3270 191.4928 -0.9090 274.9971 275.9061 290.3810 192.2848 -0.9249 275.1268 276.0517 290.4778 193.0768 -0.9113 275.1436 276.0549 290.5451 193.9290 -0.9286 275.2165 276.1451 290.6818 194.6908 -0.9324 275.2589 276.1913 290.7802 195.5128 -0.9477 275.3469 276.2946 290.8189 196.3053 -0.9629 275.3684 276.3313 290.8256 197.0975 -0.9779 275.4814 276.4594 290.9351 197.9198 -0.9778 275.5435 276.5213 291.1723 198.6815 -1.0072 275.4389 276.4461 291.3370 199.5335 -1.0210 275.6380 276.6590 291.4085 200.3255 -1.0369 275.8158 276.8527 291.5687 201.1175 -1.0258 275.7927 276.8184 291.6599 201.9168 -1.0389 275.7847 276.8236 291.7151 202.7095 -1.0189 275.8550 276.8739 291.8356 203.5613 -1.0307 275.8411 276.8718 291.9904 204.3225 -1.0262 275.9986 277.0247 292.1741 205.1445 -1.0323 276.0926 277.1250 292.2806 205.9365 -1.0378 276.0674 277.1052 292.3746 206.7278 -1.0271 276.1967 277.2238 292.5376 207.5795 -1.0568 276.3914 277.4482 292.5587 208.3415 -1.0507 276.4668 277.5175 292.6999 209.1635 -1.0740 276.5151 277.5891 292.8383 209.9555 -1.0823 276.5066 277.5889 292.9961 210.7475 -1.0786 276.5002 277.5788 293.0952 211.5695 -1.0728 276.6524 277.7253 293.1336 212.3315 -1.0951 276.7633 277.8584 293.2640 213.1835 -1.0964 276.7762 277.8726 293.4987 213.9755 -1.0968 276.8470 277.9438 293.5816 214.7673 -1.0877 276.9190 278.0067 293.7975 215.5890 -1.1123 277.0443 278.1566 293.8170 216.3508 -1.1178 277.0760 278.1938 293.9793 217.2040 -1.1447 277.1215 278.2661 294.1912 217.9655 -1.1403 277.2601 278.4003 294.3372 218.7880 -1.1429 277.2984 278.4413 294.5378 219.5805 -1.1578 277.5291 278.6869 294.5641 220.3725 -1.1592 277.6523 278.8115 294.9068 221.2250 -1.1573 277.6285 278.7858 294.9319 221.9895 -1.1563 277.7347 278.8910 295.1001 223.0140 -1.1587 277.7715 278.9302 295.1723 223.8058 -1.1704 277.8916 279.0620 295.2340 224.5975 -1.2024 277.9382 279.1406 295.4166 225.4198 -1.1934 278.0122 279.2056 295.5891 226.1820 -1.2073 278.0144 279.2217 295.7417 227.0343 -1.2341 278.1911 279.4252 295.8014 227.8285 -1.2242 278.3188 279.5430 295.9435 228.6245 -1.2225 278.3904 279.6129 296.0731 229.4168 -1.2283 278.3144 279.5427 296.1158 230.2175 -1.2465 278.3522 279.5986 296.2459 231.0455 -1.2487 278.6232 279.8720 296.3332 231.8078 -1.2424 278.6397 279.8821 296.4041 232.6645 -1.2579 278.6342 279.8921 296.5504 233.4013 -1.2662 278.6835 279.9496 296.5972 234.2575 -1.2745 278.7627 280.0372 296.6068 235.0495 -1.2772 278.8965 280.1737 296.7596 235.8415 -1.2784 278.9363 280.2147 296.8132 236.6645 -1.2728 279.0793 280.3521 296.9374 237.4275 -1.2940 279.2037 280.4978 297.0329 238.2833 -1.2911 279.2573 280.5484 297.0797 239.0455 -1.2913 279.3123 280.6036 297.1775 239.8668 -1.3013 279.4334 280.7347 297.1984 240.6635 -1.3142 279.4558 280.7700 297.2521 241.4553 -1.3039 279.5407 280.8445 297.3771 242.2773 -1.3068 279.6080 280.9149 297.5263 243.0675 -1.3236 279.6391 280.9628 297.5634 243.8893 -1.3320 279.8091 281.1411 297.6693 244.6823 -1.3371 279.9229 281.2601 297.8124 245.4748 -1.3261 279.8532 281.1793 297.7875 246.2970 -1.3434 279.9779 281.3213 297.8219 247.0585 -1.3509 280.0234 281.3743 298.0144 247.9108 -1.3492 280.1934 281.5426 298.1699 248.7043 -1.3589 280.2367 281.5956 298.1738 249.4965 -1.3606 280.3115 281.6722 298.2260 250.3188 -1.3753 280.3406 281.7159 298.2883 251.0805 -1.3830 280.4372 281.8203 298.4353 251.9328 -1.3724 280.5785 281.9509 298.5645 252.6945 -1.3700 280.6491 282.0192 298.6817 253.5165 -1.3906 280.6895 282.0800 298.8132 254.3385 -1.4134 280.8283 282.2417 298.8671 255.1005 -1.4001 280.8762 282.2763 298.8807 255.9525 -1.3966 280.9478 282.3445 299.0424 256.7150 -1.4068 280.9627 282.3695 299.1349 257.5385 -1.4115 281.0295 282.4410 299.2926 258.3305 -1.3992 281.1617 282.5609 299.3375 259.1225 -1.4174 281.2748 282.6922 299.3148 259.9445 -1.4220 281.4160 282.8380 299.4369 260.7365 -1.4318 281.4279 282.8597 299.5284 261.5585 -1.4351 281.5703 283.0055 299.7503 262.3505 -1.4523 281.5866 283.0389 299.7829 263.1428 -1.4460 281.5866 283.0326 299.8545 263.9660 -1.4637 281.7064 283.1701 300.0190 264.7285 -1.4658 281.7879 283.2537 300.1377 265.5805 -1.4605 281.9037 283.3643 300.2567 266.3443 -1.4592 281.8807 283.3399 300.3690 267.1693 -1.4610 281.9995 283.4605 300.4767 267.9615 -1.4659 282.0561 283.5219 300.5354 268.7535 -1.4765 282.2065 283.6831 300.6278 269.6060 -1.4860 282.3417 283.8277 300.7835 270.3680 -1.4806 282.3580 283.8386 300.8773 271.1938 -1.4907 282.3842 283.8749 301.0671 271.9940 -1.5065 282.5257 284.0323 301.1030 272.7865 -1.5099 282.5710 284.0809 301.2019 273.7118 -1.5082 282.6587 284.1669 301.3774 274.5775 -1.5184 282.6469 284.1653 301.6634 275.4335 -1.5208 282.8529 284.3737 301.5930 276.1948 -1.5264 282.9163 284.4427 301.7229 277.0168 -1.5250 282.9891 284.5141 301.8493 277.8088 -1.5258 283.0500 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