DTA measure 1dta_elso Date: 2024312:118 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 931.10 s Mass = 1386.800 mg data_number = 1157 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2763 0.8487 237.9498 237.1011 266.0358 2.0978 0.8446 238.1682 237.3236 266.0479 2.9200 0.8379 238.3743 237.5364 266.0441 3.6815 0.8362 238.5933 237.7570 266.0588 4.5340 0.8375 238.8112 237.9737 266.0508 5.2958 0.8375 239.0200 238.1824 266.0760 6.1178 0.8339 239.2353 238.4015 266.0947 6.9398 0.8291 239.4620 238.6330 266.1386 7.7015 0.8245 239.6530 238.8285 266.1719 8.5538 0.8219 239.8647 239.0428 266.2106 9.3155 0.8191 240.0503 239.2312 266.2660 10.1378 0.8194 240.2797 239.4603 266.3075 10.9600 0.8153 240.5030 239.6877 266.3662 11.7225 0.8127 240.7000 239.8873 266.4305 12.5748 0.8085 240.9081 240.0996 266.4984 13.3365 0.8051 241.0986 240.2935 266.6080 14.1588 0.8024 241.3114 240.5090 266.6916 14.9810 0.7978 241.5306 240.7328 266.7927 15.7435 0.7959 241.7200 240.9242 266.8871 16.5958 0.7922 241.9349 241.1428 267.0075 17.3575 0.7886 242.1180 241.3294 267.1392 18.1795 0.7866 242.3307 241.5441 267.2673 18.9985 0.7865 242.5182 241.7317 267.4050 19.7570 0.7887 242.7155 241.9268 267.5294 20.6050 0.7836 242.9170 242.1333 267.6779 21.3630 0.7796 243.1132 242.3336 267.8234 22.1818 0.7739 243.3241 242.5502 267.9722 23.0003 0.7707 243.5159 242.7452 268.1196 23.7590 0.7696 243.6887 242.9191 268.2666 24.6078 0.7620 243.8902 243.1282 268.4365 25.3973 0.7567 244.0880 243.3314 268.5808 26.1868 0.7511 244.2793 243.5283 268.7204 27.0065 0.7447 244.4873 243.7426 268.8994 27.7680 0.7396 244.6620 243.9224 269.0493 28.6195 0.7364 244.8405 244.1041 269.2094 29.4118 0.7276 245.0305 244.3029 269.3701 30.2035 0.7189 245.2229 244.5040 269.5458 31.0255 0.7143 245.4289 244.7146 269.7162 31.7875 0.7112 245.6066 244.8954 269.8720 32.6395 0.7047 245.8048 245.1001 270.0352 33.4315 0.6972 245.9885 245.2913 270.1939 34.2235 0.6876 246.1817 245.4941 270.3347 35.0455 0.6788 246.3683 245.6895 270.4888 35.8075 0.6710 246.5307 245.8597 270.6363 36.6595 0.6600 246.7253 246.0654 270.8160 37.4515 0.6541 246.9039 246.2498 270.9424 38.2435 0.6492 247.1000 246.4509 271.0913 39.0655 0.6445 247.2863 246.6419 271.2369 39.8275 0.6340 247.4835 246.8495 271.3670 40.6795 0.6178 247.6680 247.0502 271.5269 41.4715 0.6002 247.8428 247.2426 271.6796 42.2635 0.5818 248.0341 247.4523 271.8250 43.0853 0.5896 248.2023 247.6127 271.9721 43.8475 0.5814 248.3868 247.8053 272.0969 44.6988 0.5589 248.5866 248.0278 272.2328 45.4910 0.5495 248.7632 248.2138 272.3573 46.2825 0.5610 248.9301 248.3691 272.4929 47.1058 0.5751 249.1003 248.5253 272.6122 47.8675 0.5765 249.2737 248.6972 272.7494 48.7203 0.5624 249.4941 248.9317 272.8731 49.5128 0.5515 249.6613 249.1098 272.9965 50.3643 0.5396 249.8414 249.3018 273.1219 51.1525 0.5366 249.9862 249.4497 273.2477 52.0000 0.5295 250.1828 249.6534 273.3582 52.7880 0.5306 250.3563 249.8257 273.4637 53.5760 0.5257 250.5370 250.0113 273.5930 54.3948 0.5197 250.7279 250.2082 273.7090 55.1830 0.5138 250.9001 250.3863 273.8080 56.0020 0.5090 251.0710 250.5620 273.9163 56.7928 0.4994 251.2600 250.7606 274.0456 57.5848 0.4921 251.4298 250.9376 274.1575 58.4035 0.4857 251.6258 251.1401 274.2716 59.1938 0.4788 251.7920 251.3132 274.3892 60.0148 0.4679 251.9581 251.4902 274.5161 60.8068 0.4589 252.1362 251.6773 274.6197 61.5985 0.4510 252.3185 251.8675 274.7384 62.4208 0.4429 252.4899 252.0470 274.8559 63.1825 0.4246 252.6595 252.2349 274.9816 64.0348 0.3121 252.8487 252.5366 275.1171 64.8268 0.2500 253.0010 252.7510 275.2306 65.6185 0.2145 253.1635 252.9490 275.3556 66.4408 0.2444 253.3302 253.0857 275.4967 67.2025 0.3571 253.5008 253.1437 275.6193 68.0548 0.2553 253.6813 253.4260 275.7417 68.8165 0.1965 253.8385 253.6419 275.8601 69.6388 0.3088 254.0188 253.7101 275.9996 70.4605 0.3498 254.1818 253.8321 276.1290 71.2225 0.2411 254.3562 254.1150 276.2473 72.0745 0.1138 254.5246 254.4108 276.3804 72.8365 0.1597 254.6796 254.5199 276.5087 73.6585 0.2800 254.8424 254.5624 276.6421 74.4805 0.2661 255.0123 254.7462 276.7714 75.2425 0.1280 255.1727 255.0448 276.9120 76.0950 0.0762 255.3579 255.2816 277.0571 76.8575 0.0907 255.5033 255.4126 277.2018 77.6803 0.0942 255.6816 255.5875 277.3445 78.5025 0.2247 255.8634 255.6387 277.4741 79.2645 0.1522 256.0069 255.8547 277.6107 80.1165 0.0644 256.1970 256.1326 277.7524 80.8785 0.0471 256.3409 256.2938 277.9025 81.7005 0.0351 256.5109 256.4758 278.0675 82.5225 0.0580 256.6799 256.6219 278.2137 83.2835 0.0311 256.8212 256.7901 278.3450 84.1303 0.0265 257.0176 256.9911 278.5129 84.9180 -0.0020 257.1577 257.1597 278.6541 85.7060 -0.0163 257.3316 257.3479 278.8063 86.5245 0.0470 257.5039 257.4569 278.9490 87.2825 0.1743 257.6584 257.4842 279.0881 88.1308 0.2019 257.8317 257.6298 279.2408 88.9190 0.1182 257.9876 257.8694 279.3555 89.7080 0.0076 258.1572 258.1497 279.4943 90.5263 -0.0294 258.3084 258.3378 279.6444 91.3158 -0.0534 258.4698 258.5232 279.7854 92.1365 -0.0617 258.6364 258.6981 279.9097 92.9285 -0.0426 258.7993 258.8419 280.0291 93.7205 -0.0493 258.9430 258.9923 280.1609 94.5425 -0.0040 259.1156 259.1196 280.2964 95.3045 0.1010 259.2701 259.1691 280.4199 96.1565 0.1354 259.4547 259.3193 280.5615 96.9485 0.1345 259.6164 259.4819 280.6991 97.7405 0.1305 259.7523 259.6218 280.8319 98.5625 0.1225 259.9212 259.7987 280.9587 99.3238 0.1146 260.0728 259.9582 281.0589 100.1760 0.1087 260.2387 260.1300 281.1879 100.9683 0.1015 260.3925 260.2910 281.3124 101.7600 0.0926 260.5528 260.4602 281.4373 102.5820 0.0858 260.7333 260.6476 281.5777 103.3438 0.0794 260.8708 260.7914 281.6895 104.1958 0.0751 261.0291 260.9540 281.8376 104.9883 0.0668 261.2076 261.1408 281.9657 105.7795 0.0585 261.3591 261.3005 282.0805 106.6018 0.0520 261.5131 261.4610 282.2099 107.3635 0.0440 261.6684 261.6244 282.3333 108.2158 0.0374 261.8403 261.8029 282.4593 109.0078 0.0312 262.0025 261.9712 282.5931 109.8005 0.0237 262.1418 262.1181 282.6940 110.6230 0.0166 262.3106 262.2940 282.8099 111.3855 0.0099 262.4658 262.4559 282.9263 112.2378 0.0090 262.6192 262.6102 283.0703 113.0298 0.0130 262.7830 262.7699 283.1851 113.8215 0.0055 262.9285 262.9230 283.3185 114.6435 -0.0009 263.0965 263.0974 283.4601 115.4053 -0.0080 263.2540 263.2620 283.5868 116.2538 -0.0154 263.4284 263.4438 283.7344 117.0120 -0.0212 263.5605 263.5817 283.8613 117.8300 -0.0257 263.7132 263.7389 283.9938 118.6480 -0.0346 263.8816 263.9161 284.1424 119.4060 -0.0416 264.0366 264.0782 284.2593 120.2545 -0.0492 264.1943 264.2435 284.4376 121.0130 -0.0567 264.3422 264.3989 284.5742 121.8318 -0.0592 264.5024 264.5616 284.6980 122.6508 -0.0667 264.6703 264.7370 284.8485 123.4110 -0.0738 264.8075 264.8813 284.9770 124.2618 -0.0787 264.9753 265.0540 285.1209 125.0235 -0.0851 265.1231 265.2081 285.2612 125.8458 -0.0918 265.2887 265.3805 285.4106 126.6678 -0.1000 265.4415 265.5415 285.5610 127.4295 -0.1034 265.5911 265.6946 285.6890 128.2818 -0.1111 265.7417 265.8527 285.8394 129.0435 -0.1161 265.8942 266.0103 285.9823 129.8658 -0.1243 266.0429 266.1672 286.1324 130.6578 -0.1310 266.2070 266.3380 286.2792 131.4495 -0.1355 266.3676 266.5030 286.4000 132.3015 -0.1419 266.5142 266.6561 286.5466 133.0635 -0.1473 266.6647 266.8119 286.6737 133.8855 -0.1551 266.8277 266.9828 286.8127 134.6775 -0.1646 266.9740 267.1386 286.9451 135.4695 -0.1696 267.1289 267.2985 287.0636 136.3215 -0.1745 267.2842 267.4587 287.2176 137.0835 -0.1833 267.4421 267.6254 287.3266 137.9063 -0.1897 267.5880 267.7777 287.4439 138.6985 -0.1931 267.7409 267.9340 287.5537 139.4915 -0.1998 267.9119 268.1116 287.6810 140.3138 -0.2068 268.0706 268.2774 287.8021 141.1063 -0.2133 268.2021 268.4154 287.9185 141.9283 -0.2204 268.3644 268.5848 288.0322 142.7200 -0.2218 268.4972 268.7191 288.1404 143.5115 -0.2282 268.6410 268.8693 288.2502 144.3340 -0.2358 268.8039 269.0397 288.3857 145.1255 -0.2418 268.9495 269.1912 288.4957 145.9485 -0.2515 269.1181 269.3696 288.5997 146.7408 -0.2530 269.2717 269.5247 288.7269 147.5328 -0.2575 269.4388 269.6963 288.8654 148.3513 -0.2599 269.5731 269.8330 289.0003 149.1103 -0.2650 269.7191 269.9841 289.1004 149.9590 -0.2724 269.8821 270.1545 289.2486 150.7473 -0.2784 270.0264 270.3048 289.3827 151.5360 -0.2832 270.1783 270.4615 289.5200 152.3553 -0.2889 270.3385 270.6275 289.6466 153.1443 -0.2960 270.4835 270.7795 289.7532 153.9638 -0.3048 270.6372 270.9419 289.8900 154.7530 -0.3064 270.7699 271.0762 290.0158 155.5438 -0.3123 270.9210 271.2334 290.1478 156.3663 -0.3186 271.0764 271.3950 290.2899 157.1278 -0.3252 271.2428 271.5679 290.4017 157.9803 -0.3293 271.3861 271.7154 290.5461 158.7443 -0.3336 271.5431 271.8767 290.6609 159.5718 -0.3409 271.7122 272.0531 290.8028 160.3638 -0.3483 271.8413 272.1896 290.9265 161.1555 -0.3552 271.9850 272.3401 291.0584 162.0078 -0.3577 272.1348 272.4925 291.1997 162.7695 -0.3637 272.2855 272.6493 291.3280 163.5918 -0.3705 272.4449 272.8154 291.4630 164.3838 -0.3753 272.5972 272.9725 291.5837 165.1755 -0.3801 272.7413 273.1214 291.7252 165.9978 -0.3848 272.9057 273.2905 291.8634 166.7895 -0.3899 273.0550 273.4448 291.9819 167.6118 -0.3943 273.1970 273.5913 292.1012 168.4038 -0.3989 273.3490 273.7479 292.2275 169.1980 -0.4038 273.5008 273.9046 292.3570 170.0258 -0.4107 273.6587 274.0694 292.4958 170.7875 -0.4144 273.7850 274.1994 292.6214 171.6403 -0.4205 273.9536 274.3741 292.7601 172.4038 -0.4249 274.1011 274.5261 292.8730 173.2285 -0.4307 274.2500 274.6808 293.0122 174.0510 -0.4366 274.4027 274.8394 293.1351 174.8135 -0.4429 274.5311 274.9740 293.2480 175.6663 -0.4456 274.6992 275.1447 293.3853 176.4285 -0.4496 274.8379 275.2875 293.5143 177.2513 -0.4525 274.9956 275.4481 293.6426 178.0435 -0.4595 275.1524 275.6119 293.7724 178.8355 -0.4634 275.2889 275.7523 293.9223 179.6875 -0.4675 275.4461 275.9135 294.0623 180.4465 -0.4712 275.5908 276.0620 294.1948 181.2648 -0.4777 275.7355 276.2133 294.3415 182.0530 -0.4836 275.8831 276.3667 294.4692 182.8410 -0.4874 276.0329 276.5203 294.6190 183.6890 -0.4930 276.1918 276.6848 294.7831 184.4470 -0.4986 276.3355 276.8341 294.9200 185.2658 -0.5055 276.4892 276.9946 295.0681 186.0843 -0.5090 276.6493 277.1583 295.2038 186.8430 -0.5122 276.7849 277.2972 295.3550 187.6925 -0.5101 276.9350 277.4451 295.5242 188.4538 -0.5189 277.0771 277.5960 295.6591 189.2755 -0.5265 277.2248 277.7513 295.8047 190.0975 -0.5286 277.3884 277.9171 295.9643 190.8595 -0.5338 277.5245 278.0583 296.0920 191.7115 -0.5344 277.6677 278.2021 296.2357 192.4735 -0.5437 277.8185 278.3622 296.3627 193.2955 -0.5447 277.9950 278.5397 296.5060 194.0875 -0.5521 278.1377 278.6898 296.6329 194.8795 -0.5606 278.2612 278.8218 296.7492 195.7315 -0.5639 278.4104 278.9743 296.8994 196.4935 -0.5687 278.5494 279.1181 297.0147 197.3155 -0.5749 278.7271 279.3020 297.1538 198.1075 -0.5775 278.8613 279.4388 297.2599 198.8995 -0.5801 278.9994 279.5795 297.3966 199.7513 -0.5906 279.1580 279.7486 297.5278 200.5133 -0.5958 279.3160 279.9118 297.6584 201.3348 -0.5995 279.4607 280.0603 297.7827 202.1273 -0.6046 279.6013 280.2060 297.8895 202.9185 -0.6110 279.7528 280.3638 298.0151 203.7708 -0.6162 279.9217 280.5379 298.1341 204.5325 -0.6179 280.0544 280.6723 298.2462 205.3548 -0.6204 280.2074 280.8278 298.3782 206.1770 -0.6285 280.3406 280.9690 298.5086 206.9395 -0.6324 280.4797 281.1120 298.6230 207.7923 -0.6366 280.6595 281.2961 298.7516 208.5545 -0.6429 280.7959 281.4388 298.8886 209.3775 -0.6456 280.9509 281.5964 299.0084 210.2000 -0.6489 281.1064 281.7553 299.1427 210.9625 -0.6517 281.2283 281.8799 299.2497 211.8153 -0.6554 281.3835 282.0389 299.3781 212.5770 -0.6544 281.5131 282.1675 299.5115 213.3970 -0.6561 281.6727 282.3287 299.6460 214.2150 -0.6599 281.8206 282.4804 299.7973 214.9730 -0.6617 281.9519 282.6136 299.9433 215.8210 -0.6658 282.1233 282.7891 300.0724 216.5790 -0.6692 282.2654 282.9346 300.2057 217.3978 -0.6770 282.4232 283.1001 300.3668 218.2170 -0.6863 282.5779 283.2641 300.5017 218.9770 -0.6927 282.7107 283.4034 300.6146 219.8258 -0.6940 282.8451 283.5390 300.7787 220.6168 -0.7012 282.9887 283.6899 300.9075 221.4093 -0.7084 283.1624 283.8708 301.0474 222.2305 -0.7118 283.2947 284.0065 301.2051 222.9925 -0.7180 283.4243 284.1423 301.3496 223.8448 -0.7184 283.5829 284.3013 301.5040 224.6368 -0.7262 283.7324 284.4587 301.6543 225.4285 -0.7284 283.8914 284.6198 301.7969 226.2508 -0.7357 284.0305 284.7662 301.9289 227.0125 -0.7431 284.1799 284.9231 302.0619 227.8648 -0.7456 284.3299 285.0755 302.2056 228.6568 -0.7503 284.4669 285.2172 302.3425 229.4485 -0.7525 284.6227 285.3752 302.4784 230.2705 -0.7521 284.7572 285.5092 302.6201 231.0325 -0.7590 284.8998 285.6588 302.7384 231.8848 -0.7652 285.0568 285.8220 302.8810 232.6765 -0.7714 285.2013 285.9727 302.9941 233.4685 -0.7765 285.3472 286.1238 303.0886 234.2908 -0.7770 285.5030 286.2800 303.2376 235.0835 -0.7711 285.6554 286.4265 303.3649 235.9055 -0.7803 285.8085 286.5888 303.4776 236.6975 -0.7859 285.9491 286.7351 303.5987 237.4895 -0.7935 286.0949 286.8885 303.7014 238.3118 -0.7954 286.2403 287.0358 303.8200 239.1045 -0.7986 286.3913 287.1899 303.9272 239.9265 -0.8036 286.5392 287.3428 304.0586 240.7183 -0.8082 286.6922 287.5005 304.1883 241.5103 -0.8153 286.8329 287.6482 304.2839 242.3320 -0.8169 286.9809 287.7978 304.4189 243.1235 -0.8205 287.1206 287.9410 304.5490 243.9468 -0.8238 287.2620 288.0858 304.6917 244.7373 -0.8286 287.4014 288.2300 304.8194 245.5250 -0.8337 287.5397 288.3734 304.9437 246.3730 -0.8365 287.7065 288.5430 305.0829 247.1310 -0.8393 287.8592 288.6985 305.2092 247.9493 -0.8420 287.9888 288.8309 305.3533 248.7378 -0.8489 288.1137 288.9626 305.4903 249.5263 -0.8507 288.2556 289.1063 305.6085 250.3753 -0.8612 288.4152 289.2764 305.7345 251.1075 -0.8654 288.5530 289.4184 305.8651 251.9720 -0.8700 288.7211 289.5911 306.0096 252.7628 -0.8717 288.8770 289.7487 306.1475 253.5525 -0.8753 289.0128 289.8880 306.2878 254.3728 -0.8783 289.1602 290.0385 306.4001 255.1338 -0.8799 289.2970 290.1769 306.5359 255.9860 -0.8830 289.4526 290.3356 306.6731 256.7478 -0.8884 289.6011 290.4895 306.8039 257.5698 -0.8956 289.7483 290.6440 306.9418 258.3918 -0.9027 289.8919 290.7946 307.0873 259.1535 -0.9046 290.0169 290.9214 307.2126 260.0060 -0.9115 290.1774 291.0888 307.3764 260.7675 -0.9125 290.3230 291.2355 307.4922 261.5898 -0.9169 290.4710 291.3879 307.6185 262.4118 -0.9224 290.6206 291.5430 307.7739 263.1735 -0.9278 290.7517 291.6795 307.8979 264.0258 -0.9325 290.9003 291.8328 308.0329 264.7875 -0.9348 291.0495 291.9843 308.1502 265.6098 -0.9359 291.1895 292.1254 308.2886 266.4318 -0.9432 291.3544 292.2976 308.4133 267.1935 -0.9459 291.4849 292.4308 308.5399 268.0463 -0.9485 291.6385 292.5870 308.6934 268.8085 -0.9548 291.7675 292.7223 308.8015 269.6308 -0.9596 291.9145 292.8741 308.9379 270.4528 -0.9633 292.0850 293.0482 309.0702 271.2145 -0.9660 292.2260 293.1921 309.1936 272.0673 -0.9660 292.3723 293.3383 309.3344 272.8295 -0.9726 292.5118 293.4844 309.4580 273.6515 -0.9788 292.6670 293.6458 309.6079 274.4435 -0.9827 292.7981 293.7808 309.7448 275.2355 -0.9826 292.9562 293.9387 309.8464 276.0875 -0.9907 293.1037 294.0944 309.9771 276.8470 -0.9957 293.2472 294.2429 310.1033 277.6650 -0.9964 293.3943 294.3907 310.2339 278.4530 -0.9997 293.5429 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