DTA measure 1pbup Test Date: 202429:1555 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 688.81 s Mass = 1.000 mg data_number = 1715 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.6550 -6.6636 218.3750 225.0386 265.6996 1.0805 -6.6699 218.5297 225.1996 265.7138 1.4445 -6.6683 218.6332 225.3016 265.7257 1.8085 -6.6518 218.7311 225.3829 265.7333 2.2925 -6.6121 218.8848 225.4969 265.7289 2.6575 -6.6133 218.9982 225.6115 265.7384 3.0220 -6.6346 219.1182 225.7528 265.7365 3.5055 -6.6538 219.2721 225.9259 265.7351 3.8710 -6.6682 219.3825 226.0507 265.7488 4.2345 -6.6705 219.4952 226.1656 265.7405 4.6590 -6.6734 219.6493 226.3227 265.7671 5.0835 -6.6785 219.7914 226.4699 265.7754 5.4480 -6.6669 219.9158 226.5828 265.7803 5.8720 -6.6584 220.0620 226.7204 265.8026 6.2975 -6.6580 220.1936 226.8517 265.8145 6.6635 -6.6592 220.3036 226.9628 265.8100 7.0295 -6.6605 220.4002 227.0608 265.8267 7.5155 -6.6580 220.5585 227.2165 265.8365 7.8815 -6.6723 220.6600 227.3324 265.8605 8.2470 -6.6999 220.7807 227.4807 265.8842 8.6735 -6.7172 220.9420 227.6591 265.8975 9.0990 -6.7276 221.0734 227.8010 265.9106 9.4645 -6.7342 221.1768 227.9110 265.9279 9.8915 -6.7369 221.3147 228.0516 265.9578 10.3175 -6.7418 221.4462 228.1880 265.9846 10.6825 -6.7455 221.5600 228.3056 266.0102 11.0490 -6.7462 221.6791 228.4253 266.0401 11.5355 -6.7494 221.8058 228.5552 266.0981 11.9005 -6.7501 221.9286 228.6787 266.1227 12.2670 -6.7291 222.0513 228.7804 266.1543 12.6930 -6.7048 222.1892 228.8941 266.2002 13.1190 -6.6787 222.3209 228.9996 266.2557 13.4845 -6.6658 222.4254 229.0913 266.2960 13.9110 -6.6889 222.5608 229.2498 266.3486 14.3370 -6.7346 222.6790 229.4136 266.4061 14.7025 -6.7161 222.7938 229.5100 266.4569 15.0685 -6.7121 222.9001 229.6122 266.5097 15.5550 -6.7556 223.0611 229.8167 266.5808 15.9205 -6.7757 223.1828 229.9585 266.6191 16.2865 -6.7833 223.3013 230.0845 266.6733 16.7125 -6.7359 223.4286 230.1646 266.7387 17.1390 -6.7064 223.5554 230.2618 266.8099 17.5045 -6.6953 223.6676 230.3629 266.8624 17.9305 -6.7106 223.7931 230.5038 266.9413 18.3570 -6.7620 223.9237 230.6857 267.0116 18.7225 -6.7681 224.0409 230.8090 267.0821 19.0885 -6.7491 224.1465 230.8956 267.1476 19.5750 -6.7456 224.2981 231.0437 267.2307 19.9405 -6.7563 224.4109 231.1672 267.2902 20.3065 -6.7722 224.5164 231.2885 267.3560 20.7930 -6.7685 224.6890 231.4575 267.4544 21.1595 -6.7779 224.7911 231.5690 267.5203 21.5255 -6.7958 224.8808 231.6766 267.5955 21.9515 -6.8070 225.0102 231.8172 267.6751 22.3780 -6.7896 225.1361 231.9257 267.7618 22.7435 -6.8163 225.2362 232.0525 267.8291 23.1095 -6.8368 225.3541 232.1909 267.9024 23.5960 -6.8546 225.4897 232.3443 268.0061 23.9615 -6.8629 225.6073 232.4702 268.0696 24.3275 -6.8664 225.7071 232.5735 268.1290 24.8140 -6.8686 225.8618 232.7304 268.2464 25.1805 -6.8726 225.9947 232.8673 268.3053 25.5465 -6.8761 226.1022 232.9782 268.3749 25.9725 -6.8800 226.2079 233.0879 268.4782 26.3985 -6.8831 226.3345 233.2176 268.5589 26.7645 -6.8872 226.4383 233.3255 268.6392 27.1905 -6.8914 226.5596 233.4509 268.7381 27.6175 -6.8940 226.6811 233.5750 268.8235 27.9835 -6.8946 226.7834 233.6780 268.9031 28.3495 -6.9018 226.8944 233.7962 268.9713 28.8355 -6.9052 227.0318 233.9370 269.0676 29.2025 -6.9080 227.1445 234.0526 269.1344 29.5685 -6.9109 227.2650 234.1759 269.2095 29.9930 -6.9146 227.3870 234.3016 269.2977 30.4160 -6.9167 227.5128 234.4294 269.3951 30.7800 -6.9217 227.6363 234.5580 269.4677 31.2040 -6.9249 227.7726 234.6975 269.5489 31.6280 -6.9270 227.8793 234.8063 269.6371 31.9920 -6.9293 227.9765 234.9058 269.7124 32.3560 -6.9296 228.0748 235.0044 269.7814 32.8405 -6.9335 228.2057 235.1392 269.8732 33.2050 -6.9379 228.3132 235.2511 269.9514 33.5695 -6.9393 228.4286 235.3679 270.0108 33.9940 -6.9427 228.5510 235.4937 270.0906 34.4185 -6.9492 228.6731 235.6224 270.1771 34.7830 -6.9506 228.7920 235.7425 270.2539 35.2070 -6.9526 228.9042 235.8569 270.3294 35.6315 -6.9562 229.0280 235.9842 270.4140 35.9960 -6.9594 229.1260 236.0854 270.4754 36.3600 -6.9617 229.2394 236.2011 270.5514 36.8440 -6.9666 229.3915 236.3581 270.6341 37.2095 -6.9686 229.4935 236.4621 270.7239 37.5740 -6.9725 229.5894 236.5619 270.7920 38.0595 -6.9761 229.7317 236.7078 270.8848 38.4255 -6.9814 229.8284 236.8098 270.9482 38.7915 -6.9847 229.9234 236.9081 271.0114 39.2175 -6.9862 230.0516 237.0378 271.0811 39.6435 -6.9874 230.1828 237.1702 271.1464 40.0095 -6.9885 230.2765 237.2650 271.2066 40.3755 -6.9909 230.3792 237.3702 271.2769 40.8620 -6.9962 230.5171 237.5134 271.3578 41.2285 -6.9986 230.6356 237.6343 271.4202 41.5945 -7.0011 230.7475 237.7486 271.4893 42.0810 -7.0057 230.8715 237.8772 271.5775 42.4465 -7.0066 230.9775 237.9840 271.6255 42.8125 -7.0087 231.0766 238.0854 271.6829 43.2385 -7.0133 231.2089 238.2222 271.7598 43.6645 -7.0150 231.3283 238.3433 271.8161 44.0305 -7.0185 231.4366 238.4552 271.8561 44.3965 -7.0189 231.5370 238.5559 271.9172 44.8825 -7.0224 231.6772 238.6996 271.9934 45.2485 -7.0290 231.7762 238.8052 272.0419 45.6145 -7.0325 231.8772 238.9097 272.1050 46.1005 -7.0383 232.0223 239.0606 272.2172 46.4665 -7.0425 232.1248 239.1673 272.2775 46.8325 -7.0459 232.2251 239.2711 272.3285 47.2585 -7.0496 232.3456 239.3952 272.3815 47.6845 -7.0533 232.4733 239.5267 272.4444 48.0505 -7.0592 232.5637 239.6229 272.4996 48.4165 -7.0617 232.6529 239.7146 272.5628 48.9025 -7.0611 232.7914 239.8525 272.6424 49.2685 -7.0668 232.9009 239.9677 272.6926 49.6345 -7.0699 233.0071 240.0770 272.7574 50.1205 -7.0702 233.1428 240.2130 272.8512 50.4865 -7.0718 233.2419 240.3137 272.8918 50.8525 -7.0767 233.3382 240.4149 272.9685 51.2785 -7.0787 233.4730 240.5516 273.0423 51.7045 -7.0804 233.5946 240.6750 273.0944 52.0705 -7.0832 233.6828 240.7660 273.1512 52.4965 -7.0836 233.7902 240.8738 273.2127 52.9225 -7.0872 233.9135 241.0006 273.2859 53.2880 -7.0896 234.0151 241.1047 273.3412 53.6545 -7.0909 234.1291 241.2200 273.3922 54.1405 -7.0944 234.2534 241.3478 273.4710 54.5065 -7.0989 234.3474 241.4463 273.5247 54.8725 -7.1007 234.4481 241.5488 273.5679 55.2990 -7.1061 234.5680 241.6741 273.6388 55.7250 -7.1090 234.6900 241.7990 273.7137 56.0905 -7.1093 234.7863 241.8956 273.7681 56.5170 -7.1123 234.9046 242.0169 273.8166 56.9435 -7.1169 235.0244 242.1413 273.8892 57.3095 -7.1220 235.1232 242.2451 273.9465 57.6755 -7.1225 235.2157 242.3382 274.0112 58.1620 -7.1292 235.3583 242.4875 274.0803 58.5285 -7.1316 235.4468 242.5784 274.1222 58.8945 -7.1337 235.5384 242.6721 274.1832 59.3205 -7.1370 235.6584 242.7954 274.2402 59.7470 -7.1396 235.7729 242.9125 274.3016 60.1125 -7.1401 235.8879 243.0280 274.3554 60.5385 -7.1414 235.9967 243.1381 274.4376 60.9665 -7.1420 236.1093 243.2513 274.4905 61.3325 -7.1481 236.2058 243.3539 274.5441 61.6985 -7.1477 236.3135 243.4612 274.6019 62.1850 -7.1518 236.4514 243.6031 274.6792 62.5515 -7.1547 236.5513 243.7060 274.7262 62.9160 -7.1592 236.6348 243.7941 274.7997 63.3405 -7.1623 236.7452 243.9076 274.8768 63.7640 -7.1619 236.8788 244.0407 274.9288 64.1280 -7.1601 236.9732 244.1333 274.9991 64.4920 -7.1589 237.0652 244.2241 275.0398 64.9770 -7.1582 237.1797 244.3380 275.1252 65.3420 -7.1617 237.2687 244.4304 275.1907 65.7060 -7.1624 237.3754 244.5378 275.2518 66.1900 -7.1646 237.5237 244.6883 275.3388 66.5550 -7.1673 237.6228 244.7901 275.4008 66.9190 -7.1718 237.7335 244.9053 275.4694 67.3430 -7.1759 237.8328 245.0087 275.5402 67.7670 -7.1833 237.9506 245.1339 275.6074 68.1310 -7.1872 238.0331 245.2202 275.6816 68.4950 -7.1912 238.1356 245.3268 275.7395 68.9805 -7.1994 238.2479 245.4473 275.8172 69.3450 -7.2058 238.3551 245.5608 275.8740 69.7090 -7.2048 238.4483 245.6531 275.9475 70.1940 -7.2079 238.5728 245.7807 276.0240 70.5595 -7.2139 238.6700 245.8839 276.0767 70.9240 -7.2168 238.7652 245.9820 276.1479 71.3485 -7.2226 238.8814 246.1040 276.2290 71.7740 -7.2259 239.0066 246.2326 276.3027 72.1395 -7.2280 239.0925 246.3205 276.3661 72.5655 -7.2286 239.1953 246.4239 276.4412 72.9920 -7.2316 239.3090 246.5406 276.5111 73.3575 -7.2345 239.4195 246.6540 276.5892 73.7235 -7.2392 239.5156 246.7548 276.6471 74.2100 -7.2415 239.6276 246.8691 276.7248 74.5755 -7.2412 239.7355 246.9767 276.7854 74.9415 -7.2433 239.8427 247.0860 276.8381 75.3675 -7.2515 239.9412 247.1927 276.9040 75.7940 -7.2566 240.0374 247.2940 276.9884 76.1595 -7.2577 240.1535 247.4111 277.0487 76.5255 -7.2598 240.2494 247.5092 277.1098 77.0120 -7.2607 240.3671 247.6277 277.2012 77.3775 -7.2635 240.4679 247.7314 277.2741 77.7440 -7.2638 240.5604 247.8242 277.3210 78.1695 -7.2656 240.6696 247.9352 277.3999 78.5960 -7.2668 240.7807 248.0475 277.4799 78.9615 -7.2682 240.8716 248.1398 277.5523 79.3875 -7.2705 240.9721 248.2426 277.6193 79.8140 -7.2716 241.0762 248.3479 277.7002 80.1795 -7.2722 241.1664 248.4386 277.7559 80.5455 -7.2768 241.2622 248.5390 277.8169 81.0320 -7.2807 241.4074 248.6880 277.8981 81.3975 -7.2845 241.4976 248.7821 277.9648 81.7635 -7.2881 241.5954 248.8835 278.0247 82.2500 -7.2901 241.7339 249.0240 278.1101 82.6155 -7.2930 241.8112 249.1042 278.1748 82.9815 -7.2955 241.9025 249.1980 278.2555 83.4080 -7.2978 242.0132 249.3110 278.3169 83.8345 -7.2986 242.1291 249.4277 278.3889 84.2005 -7.3011 242.2305 249.5316 278.4594 84.5665 -7.3053 242.3187 249.6240 278.5102 85.0525 -7.3042 242.4295 249.7337 278.5919 85.4185 -7.3054 242.5150 249.8205 278.6702 85.7845 -7.3095 242.5944 249.9039 278.7290 86.2105 -7.3108 242.7221 250.0330 278.8055 86.6365 -7.3139 242.8316 250.1456 278.8959 87.0025 -7.3152 242.9357 250.2508 278.9621 87.4285 -7.3192 243.0332 250.3525 279.0158 87.8545 -7.3235 243.1401 250.4636 279.1074 88.2205 -7.3257 243.2315 250.5572 279.1718 88.5865 -7.3273 243.3247 250.6519 279.2280 89.0725 -7.3319 243.4526 250.7845 279.3201 89.4395 -7.3333 243.5465 250.8798 279.3940 89.8055 -7.3344 243.6512 250.9857 279.4573 90.2315 -7.3372 243.7404 251.0776 279.5222 90.6570 -7.3399 243.8439 251.1837 279.5869 91.0235 -7.3427 243.9399 251.2826 279.6355 91.3895 -7.3466 244.0292 251.3757 279.6912 91.8755 -7.3499 244.1618 251.5117 279.7761 92.2420 -7.3549 244.2584 251.6133 279.8360 92.6080 -7.3592 244.3388 251.6979 279.8837 93.0945 -7.3614 244.4702 251.8316 279.9699 93.4610 -7.3660 244.5609 251.9269 280.0310 93.8265 -7.3681 244.6501 252.0183 280.0877 94.2530 -7.3664 244.7531 252.1195 280.1373 94.6795 -7.3683 244.8624 252.2307 280.2097 95.0430 -7.3706 244.9538 252.3244 280.2706 95.4070 -7.3732 245.0450 252.4183 280.3134 95.8915 -7.3750 245.1788 252.5537 280.4088 96.2555 -7.3781 245.2618 252.6399 280.4705 96.6190 -7.3791 245.3436 252.7228 280.5162 97.0435 -7.3818 245.4473 252.8291 280.5790 97.4685 -7.3832 245.5533 252.9366 280.6380 97.8325 -7.3872 245.6445 253.0317 280.7039 98.2565 -7.3878 245.7499 253.1377 280.7704 98.6810 -7.3919 245.8443 253.2362 280.8484 99.0450 -7.3948 245.9513 253.3461 280.8806 99.4090 -7.3980 246.0455 253.4435 280.9237 99.8925 -7.3994 246.1727 253.5720 280.9754 100.2580 -7.4029 246.2588 253.6617 281.0130 100.6215 -7.4056 246.3459 253.7515 281.0658 101.0460 -7.4101 246.4499 253.8600 281.1319 101.4710 -7.4141 246.5569 253.9710 281.2047 101.8360 -7.4176 246.6466 254.0642 281.2545 102.2610 -7.4195 246.7342 254.1536 281.3274 102.6855 -7.4193 246.8406 254.2600 281.3891 103.0510 -7.4239 246.9321 254.3560 281.4390 103.4160 -7.4270 247.0111 254.4381 281.4985 103.9005 -7.4267 247.1348 254.5615 281.5811 104.2665 -7.4316 247.2272 254.6588 281.6427 104.6325 -7.4348 247.3059 254.7408 281.6896 105.0585 -7.4363 247.4160 254.8524 281.7559 105.4845 -7.4387 247.5225 254.9613 281.8285 105.8505 -7.4415 247.6126 255.0542 281.8743 106.2165 -7.4453 247.7102 255.1554 281.9351 106.7025 -7.4483 247.8383 255.2866 282.0242 107.0685 -7.4507 247.9141 255.3648 282.0817 107.4345 -7.4539 248.0047 255.4585 282.1364 107.9205 -7.4567 248.1207 255.5774 282.2364 108.2865 -7.4576 248.2226 255.6802 282.2858 108.6525 -7.4596 248.3060 255.7656 282.3343 109.0785 -7.4630 248.4116 255.8746 282.4019 109.5040 -7.4674 248.5205 255.9879 282.4754 109.8695 -7.4697 248.5949 256.0646 282.5381 110.2360 -7.4697 248.6840 256.1537 282.6077 110.7225 -7.4723 248.8075 256.2798 282.6786 111.0875 -7.4753 248.8930 256.3684 282.7391 111.4535 -7.4796 248.9870 256.4667 282.7990 111.8805 -7.4815 249.0885 256.5701 282.8719 112.3060 -7.4851 249.1869 256.6720 282.9444 112.6715 -7.4851 249.2607 256.7458 283.0100 113.0975 -7.4868 249.3781 256.8649 283.0786 113.5245 -7.4902 249.4858 256.9761 283.1541 113.8895 -7.4910 249.5687 257.0597 283.2170 114.2555 -7.4934 249.6559 257.1493 283.2816 114.7420 -7.4944 249.7775 257.2719 283.3745 115.1075 -7.4981 249.8635 257.3615 283.4311 115.4735 -7.5019 249.9490 257.4509 283.4895 115.8995 -7.5039 250.0443 257.5482 283.5583 116.3260 -7.5076 250.1487 257.6563 283.6296 116.6915 -7.5098 250.2338 257.7436 283.6952 117.1175 -7.5118 250.3419 257.8537 283.7684 117.5440 -7.5139 250.4422 257.9561 283.8312 117.9095 -7.5153 250.5202 258.0355 283.9019 118.2755 -7.5174 250.6225 258.1399 283.9686 118.7620 -7.5200 250.7512 258.2711 284.0508 119.1275 -7.5217 250.8349 258.3566 284.1131 119.4935 -7.5255 250.9040 258.4295 284.1643 119.9195 -7.5271 250.9940 258.5210 284.2511 120.3465 -7.5316 251.0919 258.6235 284.3087 120.7125 -7.5356 251.1778 258.7135 284.3645 121.1385 -7.5401 251.2840 258.8241 284.4379 121.5650 -7.5444 251.3957 258.9401 284.5250 121.9305 -7.5449 251.4763 259.0212 284.5926 122.2965 -7.5453 251.5699 259.1153 284.6427 122.7830 -7.5489 251.6874 259.2363 284.7146 123.1485 -7.5525 251.7749 259.3273 284.7806 123.5145 -7.5567 251.8531 259.4099 284.8449 123.9405 -7.5571 251.9578 259.5149 284.9283 124.3665 -7.5572 252.0529 259.6101 284.9966 124.7325 -7.5589 252.1508 259.7097 285.0700 125.1585 -7.5610 252.2414 259.8023 285.1418 125.5850 -7.5653 252.3341 259.8994 285.2262 125.9515 -7.5667 252.4155 259.9822 285.2732 126.3175 -7.5688 252.5122 260.0810 285.3301 126.8035 -7.5727 252.6223 260.1950 285.4266 127.1680 -7.5745 252.7196 260.2941 285.4839 127.5320 -7.5776 252.7957 260.3732 285.5347 127.9560 -7.5793 252.8889 260.4682 285.5940 128.3800 -7.5815 252.9934 260.5748 285.6775 128.7440 -7.5833 253.0768 260.6601 285.7449 129.1680 -7.5885 253.1697 260.7583 285.8187 129.5920 -7.5854 253.2726 260.8580 285.8914 129.9560 -7.5883 253.3706 260.9589 285.9544 130.3200 -7.5913 253.4408 261.0321 286.0000 130.8040 -7.5951 253.5688 261.1638 286.0769 131.1690 -7.5976 253.6476 261.2452 286.1393 131.5330 -7.6002 253.7325 261.3327 286.2023 131.9570 -7.6034 253.8351 261.4384 286.2900 132.3820 -7.6066 253.9220 261.5286 286.3656 132.7475 -7.6093 254.0028 261.6121 286.4245 133.1720 -7.6124 254.1052 261.7176 286.4908 133.5965 -7.6128 254.2061 261.8188 286.5582 133.9620 -7.6144 254.2846 261.8989 286.6150 134.3260 -7.6183 254.3798 261.9981 286.6699 134.8110 -7.6183 254.4914 262.1097 286.7527 135.1765 -7.6200 254.5729 262.1930 286.8277 135.5420 -7.6216 254.6513 262.2728 286.8887 136.0275 -7.6241 254.7577 262.3817 286.9738 136.3935 -7.6244 254.8364 262.4609 287.0242 136.7595 -7.6288 254.9032 262.5320 287.0955 137.1855 -7.6328 255.0005 262.6334 287.1697 137.6115 -7.6343 255.1231 262.7574 287.2320 137.9775 -7.6376 255.2102 262.8478 287.3012 138.3435 -7.6395 255.3093 262.9488 287.3453 138.8295 -7.6435 255.4229 263.0664 287.4367 139.1955 -7.6473 255.4940 263.1413 287.5034 139.5615 -7.6494 255.5718 263.2212 287.5585 139.9875 -7.6523 255.6672 263.3195 287.6444 140.4135 -7.6538 255.7691 263.4229 287.7139 140.7795 -7.6562 255.8567 263.5129 287.7622 141.2055 -7.6579 255.9481 263.6060 287.8254 141.6315 -7.6608 256.0493 263.7100 287.8902 141.9975 -7.6619 256.1363 263.7982 287.9576 142.3635 -7.6626 256.2185 263.8811 288.0284 142.8495 -7.6639 256.3326 263.9965 288.1061 143.2155 -7.6679 256.4097 264.0776 288.1735 143.5815 -7.6680 256.5050 264.1730 288.2249 144.0075 -7.6700 256.5877 264.2577 288.2902 144.4335 -7.6739 256.6841 264.3580 288.3568 144.7995 -7.6762 256.7677 264.4440 288.4156 145.2255 -7.6799 256.8717 264.5516 288.4811 145.6515 -7.6800 256.9706 264.6506 288.5400 146.0175 -7.6822 257.0601 264.7423 288.6006 146.3835 -7.6850 257.1392 264.8242 288.6653 146.8695 -7.6858 257.2405 264.9263 288.7578 147.2355 -7.6890 257.3348 265.0238 288.8196 147.6015 -7.6884 257.4075 265.0959 288.8843 148.0275 -7.6934 257.5138 265.2071 288.9476 148.4535 -7.6979 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