DTA measure 1pbupdown Test Date: 2024131:1656 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.50 s Mass = 1.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1560 1.7493 239.8211 238.0718 266.2234 1.9503 1.7459 240.0292 238.2833 266.2505 2.7435 1.7480 240.2267 238.4787 266.2483 3.5673 1.7396 240.4519 238.7124 266.2449 4.3295 1.7321 240.6499 238.9178 266.2617 5.1818 1.7182 240.8755 239.1573 266.2979 5.9438 1.7128 241.0722 239.3594 266.3285 6.7688 1.7067 241.2810 239.5744 266.3490 7.5908 1.7003 241.4951 239.7949 266.3813 8.3525 1.6980 241.7012 240.0032 266.4310 9.2003 1.6843 241.9100 240.2257 266.4636 9.9618 1.6758 242.0954 240.4196 266.5056 10.8138 1.6668 242.3221 240.6553 266.5877 11.5760 1.6526 242.5292 240.8765 266.6583 12.4015 1.6414 242.7223 241.0809 266.7223 13.2238 1.6348 242.9138 241.2790 266.8246 13.9855 1.6282 243.1246 241.4964 266.9052 14.8390 1.6196 243.3150 241.6953 267.0164 15.6015 1.6128 243.4979 241.8850 267.1320 16.4235 1.6021 243.6929 242.0907 267.2373 17.2455 1.5958 243.9188 242.3231 267.3776 18.0075 1.5901 244.1043 242.5141 267.4815 18.8618 1.5847 244.3110 242.7263 267.6283 19.6198 1.5794 244.4866 242.9073 267.7533 20.4380 1.5698 244.6637 243.0940 267.9119 21.2558 1.5566 244.8780 243.3214 268.0649 22.0153 1.5474 245.0556 243.5082 268.2178 22.8660 1.5405 245.2594 243.7189 268.3692 23.6240 1.5293 245.4274 243.8981 268.5001 24.4428 1.5191 245.6059 244.0868 268.6676 25.2313 1.5113 245.8061 244.2947 268.8298 26.0210 1.5016 245.9827 244.4811 268.9813 26.8695 1.4895 246.1998 244.7103 269.1552 27.6280 1.4796 246.3685 244.8889 269.3011 28.4473 1.4676 246.5604 245.0927 269.4762 29.2788 1.4565 246.7532 245.2967 269.6585 30.0518 1.4462 246.9300 245.4839 269.8236 30.8735 1.4419 247.1038 245.6619 269.9715 31.6345 1.4327 247.2791 245.8464 270.1149 32.4855 1.4205 247.4756 246.0551 270.2905 33.2495 1.4108 247.6597 246.2489 270.4389 34.0725 1.3990 247.8383 246.4393 270.6006 34.8653 1.3863 248.0288 246.6425 270.7641 35.6575 1.3759 248.2079 246.8321 270.9020 36.5095 1.3655 248.3862 247.0207 271.0539 37.2715 1.3560 248.5556 247.1996 271.1984 38.0945 1.3452 248.7474 247.4022 271.3644 38.8865 1.3350 248.9242 247.5892 271.5084 39.6785 1.3246 249.0965 247.7719 271.6662 40.5305 1.3142 249.2735 247.9593 271.7914 41.2923 1.3001 249.4374 248.1373 271.9301 42.1148 1.2952 249.6379 248.3427 272.0707 42.9070 1.2864 249.8238 248.5374 272.1918 43.6985 1.2727 249.9915 248.7188 272.3146 44.5233 1.2586 250.1777 248.9191 272.4476 45.3165 1.2456 250.3516 249.1061 272.5717 46.1388 1.2359 250.5219 249.2860 272.7036 46.9315 1.2272 250.6938 249.4666 272.8070 47.7235 1.2183 250.8740 249.6557 272.9140 48.5458 1.2066 251.0643 249.8577 273.0380 49.3375 1.1941 251.2421 250.0481 273.1564 50.1813 1.1805 251.4086 250.2281 273.2885 50.9423 1.1652 251.5631 250.3979 273.3888 51.7588 1.1560 251.7497 250.5937 273.5059 52.5760 1.1443 251.9203 250.7760 273.6312 53.3340 1.1354 252.0711 250.9357 273.7304 54.1823 1.1244 252.2524 251.1280 273.8465 54.9405 1.1150 252.4206 251.3056 273.9480 55.7608 1.1025 252.6041 251.5016 274.0725 56.5795 1.0918 252.7734 251.6816 274.2123 57.3380 1.0835 252.9384 251.8549 274.3186 58.1868 1.0720 253.1198 252.0478 274.4426 58.9755 1.0604 253.2790 252.2186 274.5769 59.7655 1.0487 253.4369 252.3882 274.7069 60.5853 1.0387 253.6217 252.5830 274.8280 61.3750 1.0270 253.7815 252.7546 274.9435 62.1958 1.0153 253.9664 252.9511 275.0846 62.9865 1.0095 254.1213 253.1118 275.2072 63.7775 1.0013 254.2906 253.2893 275.3341 64.5998 0.9932 254.4630 253.4698 275.4775 65.3615 0.9822 254.6090 253.6268 275.6195 66.2138 0.9679 254.8068 253.8389 275.7431 67.0058 0.9533 254.9564 254.0031 275.8841 67.7975 0.9390 255.1137 254.1748 276.0051 68.6198 0.9247 255.2994 254.3747 276.1314 69.3815 0.9141 255.4520 254.5378 276.2585 70.2338 0.9038 255.6233 254.7195 276.4027 71.0255 0.8950 255.7687 254.8737 276.5390 71.8175 0.8828 255.9479 255.0651 276.6650 72.6395 0.8695 256.1281 255.2586 276.7959 73.4015 0.8579 256.2663 255.4083 276.9231 74.2535 0.8485 256.4498 255.6013 277.0651 75.0455 0.8365 256.6008 255.7643 277.2007 75.8375 0.8260 256.7671 255.9411 277.3407 76.6595 0.8189 256.9330 256.1141 277.4671 77.4215 0.8104 257.0870 256.2766 277.5903 78.2735 0.8027 257.2529 256.4503 277.7237 79.0655 0.7842 257.4176 256.6334 277.8507 79.8575 0.7711 257.5804 256.8093 277.9817 80.6683 0.7615 257.7386 256.9771 278.1049 81.4655 0.7393 257.9013 257.1620 278.2401 82.2880 0.7147 258.0690 257.3542 278.3688 83.0798 0.6946 258.2227 257.5281 278.5052 83.9005 0.6845 258.3916 257.7071 278.6431 84.6875 0.6784 258.5601 257.8816 278.7730 85.4750 0.6686 258.7066 258.0380 278.9026 86.2935 0.6634 258.8728 258.2094 279.0392 87.0820 0.6508 259.0261 258.3753 279.1685 87.9000 0.6373 259.1857 258.5484 279.2846 88.6875 0.6247 259.3298 258.7051 279.4095 89.4750 0.6118 259.4969 258.8850 279.5493 90.2938 0.5973 259.6595 259.0622 279.6805 91.0818 0.5861 259.8063 259.2202 279.7988 91.9018 0.5751 259.9805 259.4054 279.9457 92.6900 0.5683 260.1401 259.5718 280.0830 93.4790 0.5603 260.2819 259.7216 280.2022 94.3283 0.5511 260.4468 259.8957 280.3567 95.0873 0.5401 260.5956 260.0555 280.4897 95.9085 0.5288 260.7592 260.2304 280.6433 96.7305 0.5263 260.9123 260.3860 280.7868 97.4923 0.5228 261.0741 260.5514 280.9422 98.3453 0.5133 261.2403 260.7270 281.0876 99.1085 0.5087 261.3758 260.8671 281.2087 99.9308 0.5015 261.5323 261.0308 281.3660 100.7230 0.4911 261.6983 261.2072 281.5161 101.5158 0.4787 261.8463 261.3676 281.6787 102.3680 0.4196 262.0170 261.5973 281.8222 103.1298 0.2880 262.1775 261.8895 281.9645 103.9528 0.2320 262.3275 262.0955 282.0889 104.7458 0.2075 262.4941 262.2866 282.2397 105.5375 0.1920 262.6421 262.4501 282.3711 106.3898 0.1821 262.8053 262.6231 282.5192 107.1518 0.1860 262.9403 262.7543 282.6390 107.9738 0.1841 263.1234 262.9392 282.7510 108.7658 0.2017 263.2629 263.0612 282.8855 109.5575 0.2412 263.4256 263.1844 283.0251 110.4098 0.1566 263.5874 263.4308 283.1515 111.1745 0.1245 263.7183 263.5938 283.2719 111.9995 0.1166 263.8921 263.7755 283.4032 112.7915 0.1494 264.0320 263.8826 283.5174 113.5835 0.1142 264.1855 264.0713 283.6432 114.4355 0.0954 264.3351 264.2396 283.7656 115.1975 0.0843 264.4915 264.4073 283.8781 116.0180 0.0800 264.6613 264.5813 284.0082 116.8060 0.1174 264.8014 264.6840 284.1299 117.5940 0.1342 264.9530 264.8188 284.2383 118.4428 0.0658 265.1040 265.0383 284.3851 119.2010 0.0489 265.2522 265.2032 284.4914 120.0198 0.1476 265.4139 265.2663 284.6072 120.8095 0.2549 265.5683 265.3134 284.7330 121.5990 0.2763 265.7229 265.4466 284.8665 122.4475 0.2521 265.8839 265.6318 284.9834 123.2060 0.2365 266.0170 265.7805 285.1044 124.0240 0.2224 266.1697 265.9473 285.2297 124.8135 0.2140 266.3111 266.0970 285.3705 125.6055 0.2106 266.4698 266.2591 285.4977 126.4585 0.2099 266.6315 266.4216 285.6348 127.2198 0.2048 266.7829 266.5781 285.7685 128.0425 0.1938 266.9272 266.7334 285.9045 128.8343 0.1849 267.0925 266.9075 286.0487 129.7155 0.1816 267.2452 267.0636 286.1916 130.5378 0.1736 267.4148 267.2412 286.3251 131.3305 0.1704 267.5600 267.3897 286.4681 132.1633 0.1661 267.7080 267.5419 286.6173 132.9255 0.1629 267.8465 267.6837 286.7563 133.7775 0.1452 268.0045 267.8593 286.9156 134.5395 0.1354 268.1546 268.0191 287.0340 135.3915 0.1260 268.3171 268.1912 287.1556 136.2135 0.1296 268.4660 268.3364 287.2969 137.0055 0.1238 268.6189 268.4951 287.4340 137.7975 0.1160 268.7781 268.6621 287.5836 138.6195 0.1032 268.9269 268.8237 287.7206 139.4110 0.0876 269.0622 268.9746 287.8651 140.2333 0.0810 269.2238 269.1427 287.9986 141.0250 0.0795 269.3859 269.3065 288.1259 141.8165 0.0770 269.5235 269.4465 288.2555 142.6390 0.0708 269.6852 269.6145 288.3917 143.4305 0.0626 269.8338 269.7712 288.5267 144.2528 0.0601 269.9757 269.9156 288.6659 145.0448 0.0558 270.1096 270.0538 288.8096 145.8365 0.0481 270.2714 270.2232 288.9427 146.6598 0.0445 270.4279 270.3834 289.0848 147.4518 0.0376 270.5679 270.5302 289.2211 148.2710 0.0266 270.7116 270.6850 289.3623 149.0590 0.0163 270.8563 270.8400 289.4888 149.8470 0.0119 270.9995 270.9876 289.6053 150.6653 0.0060 271.1660 271.1600 289.7609 151.4530 0.0026 271.3169 271.3144 289.8952 152.2715 -0.0040 271.4797 271.4837 290.0285 153.0603 -0.0087 271.6209 271.6297 290.1587 153.8480 -0.0172 271.7678 271.7849 290.2850 154.6960 -0.0273 271.9282 271.9555 290.4192 155.4543 -0.0346 272.0604 272.0950 290.5476 156.2740 -0.0377 272.2130 272.2507 290.6977 157.0633 -0.0460 272.3632 272.4092 290.8347 157.8538 -0.0545 272.5029 272.5573 290.9562 158.7045 -0.0639 272.6629 272.7268 291.0841 159.4653 -0.0663 272.8098 272.8761 291.2117 160.2868 -0.0729 272.9638 273.0367 291.3534 161.1088 -0.0802 273.1121 273.1923 291.4788 161.8705 -0.0866 273.2605 273.3470 291.6202 162.7228 -0.0953 273.4207 273.5160 291.7495 163.4845 -0.1057 273.5493 273.6550 291.8585 164.3068 -0.1176 273.7092 273.8268 291.9942 165.0990 -0.1229 273.8484 273.9713 292.1272 165.8905 -0.1282 273.9893 274.1175 292.2646 166.7428 -0.1351 274.1540 274.2891 292.4071 167.5045 -0.1378 274.3053 274.4431 292.5159 168.3268 -0.1424 274.4473 274.5898 292.6402 169.1185 -0.1460 274.5880 274.7341 292.7722 169.9105 -0.1551 274.7350 274.8901 292.8875 170.7633 -0.1631 274.8795 275.0426 293.0277 171.5255 -0.1727 275.0186 275.1913 293.1463 172.3475 -0.1741 275.1725 275.3466 293.2760 173.1395 -0.1801 275.3294 275.5095 293.4067 173.9315 -0.1904 275.4636 275.6540 293.5524 174.7835 -0.1949 275.6207 275.8156 293.6789 175.5455 -0.1963 275.7489 275.9453 293.7966 176.3675 -0.2005 275.9124 276.1129 293.9304 177.1895 -0.2077 276.0660 276.2737 294.0574 177.9515 -0.2119 276.2188 276.4307 294.1807 178.8035 -0.2117 276.3803 276.5920 294.3015 179.5638 -0.2194 276.5025 276.7218 294.4312 180.3820 -0.2272 276.6494 276.8766 294.5690 181.1673 -0.2302 276.7963 277.0265 294.6861 181.9568 -0.2367 276.9497 277.1864 294.8045 182.8113 -0.2398 277.0987 277.3386 294.9343 183.5460 -0.2470 277.2408 277.4878 295.0526 184.3940 -0.2636 277.3993 277.6629 295.1894 185.1820 -0.2730 277.5404 277.8134 295.3030 186.0010 -0.2768 277.7022 277.9790 295.4280 186.8198 -0.2769 277.8414 278.1183 295.5568 187.6383 -0.2758 277.9741 278.2499 295.6711 188.3970 -0.2778 278.1301 278.4079 295.7989 189.2463 -0.2824 278.2886 278.5710 295.9459 190.0353 -0.2876 278.4353 278.7229 296.0719 190.8260 -0.2956 278.5711 278.8668 296.1861 191.6485 -0.2991 278.7234 279.0225 296.3248 192.4113 -0.3084 278.8677 279.1761 296.4386 193.2615 -0.3126 279.0141 279.3266 296.5707 194.0535 -0.3196 279.1518 279.4713 296.6825 194.8455 -0.3274 279.3011 279.6285 296.8096 195.6683 -0.3400 279.4450 279.7850 296.9478 196.4305 -0.3465 279.5949 279.9413 297.0785 197.2823 -0.3497 279.7510 280.1007 297.2182 198.1045 -0.3511 279.8927 280.2438 297.3631 198.8660 -0.3504 280.0188 280.3692 297.4944 199.7188 -0.3570 280.1835 280.5405 297.6406 200.5110 -0.3643 280.3317 280.6960 297.7700 201.3025 -0.3646 280.4727 280.8373 297.9309 202.1250 -0.3622 280.6398 281.0020 298.0600 202.8865 -0.3678 280.7718 281.1396 298.2063 203.7630 -0.3729 280.9126 281.2856 298.3572 204.5245 -0.3783 281.0587 281.4370 298.4795 205.3468 -0.3834 281.2115 281.5949 298.6516 206.1688 -0.3889 281.3511 281.7400 298.8044 206.9305 -0.3945 281.5005 281.8950 298.9507 207.7833 -0.4016 281.6475 282.0490 299.1001 208.5455 -0.4051 281.7954 282.2005 299.2423 209.3678 -0.4104 281.9528 282.3632 299.3976 210.1898 -0.4155 282.1012 282.5167 299.5395 210.9515 -0.4248 282.2187 282.6435 299.6735 211.8035 -0.4339 282.3668 282.8007 299.8184 212.5643 -0.4385 282.5190 282.9575 299.9385 213.3815 -0.4457 282.6656 283.1113 300.0923 214.1980 -0.4507 282.8175 283.2683 300.2224 214.9860 -0.4560 282.9609 283.4168 300.3505 215.8040 -0.4577 283.1233 283.5811 300.4692 216.5930 -0.4613 283.2559 283.7173 300.5914 217.3830 -0.4601 283.4165 283.8766 300.7119 218.2010 -0.4631 283.5519 284.0150 300.8438 218.9890 -0.4681 283.6876 284.1557 300.9746 219.8078 -0.4729 283.8362 284.3091 301.0964 220.5963 -0.4790 283.9855 284.4645 301.2016 221.3860 -0.4853 284.1286 284.6140 301.3230 222.2345 -0.4930 284.2687 284.7617 301.4501 222.9933 -0.4970 284.3947 284.8917 301.5541 223.8128 -0.5006 284.5526 285.0533 301.6891 224.6335 -0.5057 284.7128 285.2184 301.8064 225.3955 -0.5081 284.8621 285.3702 301.9191 226.2498 -0.5190 285.0190 285.5380 302.0324 227.0115 -0.5251 285.1536 285.6788 302.1290 227.8335 -0.5296 285.2928 285.8225 302.2495 228.6265 -0.5343 285.4260 285.9603 302.3867 229.4195 -0.5444 285.5674 286.1118 302.5280 230.2715 -0.5437 285.7284 286.2722 302.6389 231.0335 -0.5515 285.8653 286.4168 302.7735 231.8555 -0.5579 286.0168 286.5747 302.9073 232.6510 -0.5690 286.1631 286.7321 303.0376 233.4465 -0.5709 286.3123 286.8831 303.1719 234.2705 -0.5735 286.4469 287.0205 303.3126 235.0635 -0.5772 286.5957 287.1728 303.4525 235.8855 -0.5842 286.7538 287.3380 303.5832 236.6778 -0.5890 286.8877 287.4767 303.7150 237.4705 -0.5967 287.0359 287.6326 303.8543 238.2933 -0.6007 287.1679 287.7686 304.0002 239.0853 -0.6063 287.3128 287.9191 304.1421 239.9068 -0.6190 287.4582 288.0772 304.2777 240.6988 -0.6181 287.6091 288.2271 304.3933 241.4905 -0.6272 287.7525 288.3797 304.5230 242.3428 -0.6405 287.9179 288.5584 304.6814 243.1045 -0.6487 288.0533 288.7019 304.8156 243.9268 -0.6506 288.1873 288.8380 304.9641 244.7190 -0.6494 288.3281 288.9775 305.0874 245.5080 -0.6427 288.4657 289.1084 305.2228 246.3270 -0.6396 288.6086 289.2482 305.3693 247.1150 -0.6390 288.7608 289.3998 305.5043 247.9340 -0.6452 288.9043 289.5495 305.6438 248.7248 -0.6514 289.0342 289.6856 305.7810 249.5150 -0.6629 289.1863 289.8492 305.9136 250.3353 -0.6689 289.3486 290.0175 306.0690 251.0950 -0.6693 289.4728 290.1421 306.1891 251.9433 -0.6734 289.6402 290.3136 306.3492 252.7313 -0.6800 289.7792 290.4592 306.4831 253.5200 -0.6838 289.9233 290.6070 306.6073 254.3393 -0.6884 290.0701 290.7584 306.7550 255.0993 -0.6948 290.2011 290.8958 306.9023 255.9520 -0.7014 290.3589 291.0603 307.0369 256.7438 -0.7061 290.5042 291.2102 307.1768 257.5355 -0.7087 290.6394 291.3481 307.3015 258.3578 -0.7089 290.8017 291.5106 307.4408 259.1195 -0.7093 290.9303 291.6396 307.5718 259.9730 -0.7151 291.0860 291.8011 307.7337 260.7355 -0.7211 291.2124 291.9334 307.8515 261.5580 -0.7250 291.3534 292.0785 307.9839 262.3498 -0.7329 291.5001 292.2330 308.1217 263.1415 -0.7386 291.6364 292.3750 308.2459 263.9938 -0.7449 291.7840 292.5289 308.3865 264.7593 -0.7497 291.9238 292.6735 308.5072 265.5868 -0.7589 292.0776 292.8365 308.6482 266.3790 -0.7639 292.2099 292.9738 308.7750 267.1715 -0.7699 292.3586 293.1285 308.9085 267.9938 -0.7710 292.5034 293.2744 309.0692 268.7555 -0.7763 292.6536 293.4299 309.1764 269.6085 -0.7855 292.8052 293.5907 309.3118 270.4008 -0.7919 292.9494 293.7413 309.4497 271.1935 -0.7943 293.1040 293.8983 309.5793 272.0155 -0.7976 293.2311 294.0287 309.7188 272.7775 -0.8038 293.3690 294.1728 309.8435 273.6295 -0.8066 293.5267 294.3333 309.9767 274.3920 -0.8140 293.6633 294.4773 310.1083 275.2175 -0.8152 293.8333 294.6485 310.2311 276.0395 -0.8192 293.9743 294.7934 310.3659 276.8308 -0.8270 294.1102 294.9372 310.4969 277.6493 -0.8375 294.2713 295.1088 310.6352 278.4380 -0.8328 294.4017 295.2345 310.7791 279.2260 -0.8346 294.5461 295.3807 310.8891 280.0445 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