DTA measure 2pbupdown Test Date: 2024131:1726 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.09 s Mass = 1.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3191 -5.5393 440.6273 446.1667 424.3456 3.9195 -5.5512 440.6358 446.1871 424.3355 5.5196 -5.5606 440.6494 446.2100 424.2975 7.1345 -5.5703 440.6628 446.2331 424.2776 8.7486 -5.5790 440.6700 446.2490 424.2247 10.3559 -5.5870 440.6830 446.2700 424.1308 11.9481 -5.5967 440.6890 446.2857 424.0138 13.5414 -5.6053 440.6862 446.2914 423.9012 15.1398 -5.6140 440.7066 446.3206 423.7392 16.7506 -5.6203 440.7075 446.3278 423.5542 18.3736 -5.6284 440.7175 446.3459 423.3808 19.9685 -5.6332 440.7033 446.3365 423.1788 21.5656 -5.6416 440.7170 446.3586 422.9687 23.1651 -5.6469 440.7055 446.3524 422.7552 24.7795 -5.6514 440.7140 446.3654 422.5175 26.4058 -5.6576 440.7074 446.3650 422.2803 28.0055 -5.6649 440.7023 446.3672 422.0420 29.6045 -5.6696 440.6945 446.3641 421.7952 31.2188 -5.6740 440.6697 446.3437 421.5458 32.8176 -5.6806 440.6616 446.3422 421.3097 34.4175 -5.6832 440.6495 446.3327 421.0787 36.0441 -5.6861 440.6330 446.3191 420.8694 37.6556 -5.6886 440.5997 446.2883 420.6569 39.2551 -5.6938 440.5789 446.2727 420.4415 40.8711 -5.6958 440.5633 446.2591 420.2527 42.4646 -5.6994 440.5342 446.2336 420.0620 44.0560 -5.7021 440.5105 446.2126 419.8575 45.6773 -5.7044 440.4639 446.1683 419.6752 47.2718 -5.7097 440.4440 446.1537 419.4988 48.8805 -5.7125 440.4095 446.1219 419.3137 50.4735 -5.7149 440.3711 446.0861 419.1243 52.0835 -5.7192 440.3312 446.0504 418.9373 53.6971 -5.7220 440.2920 446.0140 418.7199 55.3108 -5.7279 440.2417 445.9696 418.5281 56.9140 -5.7282 440.1925 445.9207 418.3237 58.5216 -5.7312 440.1544 445.8856 418.1187 60.1216 -5.7331 440.1019 445.8350 417.9215 61.7240 -5.7329 440.0488 445.7817 417.7212 63.3536 -5.7357 439.9980 445.7337 417.5298 64.9535 -5.7379 439.9407 445.6786 417.3521 66.6250 -5.7387 439.8800 445.6187 417.1525 68.3865 -5.7431 439.8140 445.5571 416.9373 69.9851 -5.7459 439.7560 445.5019 416.7676 71.5838 -5.7472 439.6864 445.4335 416.5522 73.1976 -5.7482 439.6355 445.3837 416.3694 74.7929 -5.7505 439.5652 445.3157 416.1540 76.4349 -5.7544 439.4899 445.2443 415.9342 78.1928 -5.7558 439.4286 445.1844 415.7304 79.8146 -5.7560 439.3444 445.1004 415.5204 81.4071 -5.7594 439.2641 445.0235 415.3108 83.0169 -5.7610 439.1893 444.9503 415.0999 84.6114 -5.7624 439.1124 444.8748 414.8938 86.2230 -5.7606 439.0330 444.7936 414.6833 87.8403 -5.7656 438.9601 444.7257 414.4651 89.4549 -5.7687 438.8657 444.6344 414.2643 91.0538 -5.7701 438.7962 444.5663 414.0726 92.6526 -5.7702 438.7114 444.4816 413.8736 94.2666 -5.7708 438.6157 444.3864 413.6766 95.8658 -5.7724 438.5387 444.3111 413.4882 97.4771 -5.7755 438.4308 444.2063 413.2839 99.0888 -5.7782 438.3411 444.1193 413.1016 100.7055 -5.7779 438.2456 444.0235 412.9120 102.3049 -5.7798 438.1597 443.9395 412.7080 103.9045 -5.7771 438.0613 443.8384 412.5072 105.5174 -5.7762 437.9440 443.7202 412.3052 107.1258 -5.7761 437.8677 443.6438 412.0807 108.7185 -5.7770 437.7608 443.5378 411.8724 110.3273 -5.7742 437.6425 443.4167 411.6518 111.9194 -5.7743 437.5522 443.3265 411.4398 113.5271 -5.7749 437.4421 443.2170 411.2233 115.1366 -5.7761 437.3470 443.1231 410.9915 116.7465 -5.7771 437.2244 443.0015 410.7779 118.3459 -5.7748 437.1196 442.8944 410.5730 119.9505 -5.7794 437.0169 442.7963 410.3646 121.5645 -5.7793 436.9072 442.6865 410.1638 123.1635 -5.7806 436.7892 442.5698 409.9336 124.7776 -5.7829 436.6679 442.4508 409.7360 126.3954 -5.7836 436.5461 442.3296 409.5219 128.0045 -5.7816 436.4264 442.2079 409.3247 129.5988 -5.7829 436.3063 442.0892 409.1229 131.1993 -5.7817 436.1927 441.9744 408.9165 132.8146 -5.7836 436.0703 441.8539 408.7095 134.4295 -5.7841 435.9458 441.7300 408.5014 136.0438 -5.7829 435.8139 441.5969 408.3164 137.6429 -5.7829 435.6933 441.4762 408.1188 139.2470 -5.7837 435.5642 441.3479 407.9172 140.8380 -5.7818 435.4430 441.2247 407.7276 142.4324 -5.7798 435.3103 441.0901 407.5450 144.0559 -5.7811 435.1761 440.9572 407.3541 145.6623 -5.7781 435.0439 440.8220 407.1668 147.2570 -5.7774 434.9125 440.6899 406.9609 148.8540 -5.7773 434.7811 440.5584 406.7573 150.4674 -5.7764 434.6461 440.4224 406.5559 152.0823 -5.7753 434.5086 440.2838 406.3434 153.6968 -5.7708 434.3671 440.1379 406.1261 155.2956 -5.7693 434.2462 440.0155 405.9145 156.8946 -5.7688 434.1139 439.8827 405.7119 158.5146 -5.7687 433.9587 439.7274 405.4925 160.1155 -5.7645 433.8224 439.5869 405.2866 161.7445 -5.7519 433.6812 439.4331 405.0754 163.3440 -5.7395 433.5462 439.2857 404.8625 164.9445 -5.7346 433.3992 439.1338 404.6438 166.5584 -5.7325 433.2564 438.9890 404.4352 168.1585 -5.7296 433.1156 438.8451 404.2372 169.7803 -5.7284 432.9577 438.6861 404.0237 171.3880 -5.7234 432.8197 438.5431 403.8274 172.9815 -5.7220 432.6703 438.3923 403.6280 174.5729 -5.7207 432.5237 438.2444 403.4246 176.1806 -5.7174 432.3763 438.0938 403.2198 177.7914 -5.7122 432.2314 437.9436 403.0342 179.3969 -5.7103 432.0801 437.7905 402.8281 181.0031 -5.7105 431.9150 437.6256 402.6272 182.6013 -5.7088 431.7682 437.4770 402.4477 184.2151 -5.7064 431.6210 437.3275 402.2477 185.8145 -5.7041 431.4544 437.1585 402.0347 187.4143 -5.6975 431.3038 437.0013 401.8445 189.0320 -5.6976 431.1427 436.8403 401.6591 190.6468 -5.6964 431.0019 436.6984 401.4510 192.2460 -5.6935 430.8434 436.5369 401.2489 193.8456 -5.6900 430.6781 436.3680 401.0392 195.4596 -5.6874 430.5357 436.2231 400.8158 197.0744 -5.6855 430.3666 436.0521 400.6080 198.6886 -5.6827 430.2033 435.8860 400.3881 200.2906 -5.6781 430.0476 435.7257 400.1739 201.8960 -5.6755 429.8812 435.5567 399.9607 203.4926 -5.6719 429.7263 435.3982 399.7207 205.0854 -5.6678 429.5541 435.2219 399.5142 206.7119 -5.6667 429.3966 435.0633 399.2968 208.3030 -5.6646 429.2210 434.8856 399.0570 209.9678 -5.6604 429.0598 434.7202 398.8522 211.7264 -5.6576 428.8913 434.5489 398.6052 213.3210 -5.6511 428.7236 434.3747 398.4004 214.9335 -5.6506 428.5541 434.2047 398.1680 216.5313 -5.6487 428.3929 434.0416 397.9612 218.1455 -5.6488 428.2221 433.8710 397.7539 219.7649 -5.6490 428.0461 433.6951 397.5318 221.3645 -5.6443 427.8736 433.5178 397.3294 222.9639 -5.6397 427.7105 433.3502 397.1053 224.5785 -5.6332 427.5292 433.1624 396.9118 226.1770 -5.6301 427.3531 432.9832 396.7041 227.8059 -5.6272 427.1887 432.8159 396.4974 229.4068 -5.6275 427.0135 432.6410 396.3075 231.0186 -5.6229 426.8514 432.4742 396.1019 232.6226 -5.6187 426.6836 432.3023 395.9082 234.2366 -5.6142 426.5091 432.1233 395.7076 235.8319 -5.6092 426.3372 431.9464 395.5137 237.4541 -5.6091 426.1653 431.7743 395.3102 239.0466 -5.6072 425.9959 431.6031 395.1131 240.6621 -5.6017 425.8143 431.4161 394.9162 242.2494 -5.5972 425.6340 431.2311 394.7265 243.8441 -5.5966 425.4565 431.0531 394.5323 245.4695 -5.5939 425.2655 430.8594 394.3444 247.0818 -5.5898 425.0966 430.6864 394.1597 248.6806 -5.5859 424.9263 430.5122 393.9524 250.2824 -5.5843 424.7577 430.3420 393.7721 251.8960 -5.5826 424.5708 430.1534 393.5672 253.5096 -5.5760 424.3839 429.9600 393.3530 255.1238 -5.5738 424.2246 429.7984 393.1440 256.7235 -5.5692 424.0364 429.6056 392.9296 258.3375 -5.5640 423.8678 429.4317 392.7180 259.9371 -5.5569 423.6724 429.2293 392.4967 261.5528 -5.5546 423.5158 429.0704 392.2765 263.1584 -5.5504 423.3114 428.8619 392.0481 264.7724 -5.5452 423.1233 428.6684 391.8410 266.3859 -5.5402 422.9435 428.4838 391.6270 267.9804 -5.5348 422.7819 428.3167 391.3925 269.5719 -5.5325 422.5963 428.1288 391.1655 271.1825 -5.5279 422.4079 427.9358 390.9690 272.8008 -5.5245 422.2115 427.7360 390.7469 274.3924 -5.5202 422.0321 427.5523 390.5227 276.0019 -5.5136 421.8535 427.3672 390.3155 277.5979 -5.5089 421.6649 427.1737 390.0995 279.2113 -5.5058 421.4929 426.9987 389.8841 280.8255 -5.5019 421.3101 426.8120 389.6668 282.4326 -5.4993 421.1167 426.6160 389.4509 284.0316 -5.4928 420.9335 426.4263 389.2451 285.6308 -5.4895 420.7512 426.2408 389.0384 287.2304 -5.4893 420.5630 426.0522 388.8261 288.8446 -5.4825 420.3721 425.8546 388.6234 290.4588 -5.4770 420.1880 425.6651 388.4188 292.0660 -5.4732 419.9900 425.4632 388.2075 293.6736 -5.4680 419.8146 425.2826 388.0105 295.2725 -5.4642 419.6312 425.0954 387.8076 296.8729 -5.4609 419.4519 424.9128 387.6076 298.4871 -5.4568 419.2698 424.7266 387.4021 300.0980 -5.4510 419.0619 424.5129 387.1991 301.6939 -5.4457 418.8738 424.3195 386.9969 303.2973 -5.4398 418.6891 424.1288 386.7982 304.8893 -5.4337 418.5110 423.9447 386.5941 306.4816 -5.4276 418.3311 423.7587 386.3900 308.0896 -5.4241 418.1413 423.5654 386.1849 309.6988 -5.4192 417.9373 423.3566 385.9883 311.3124 -5.4138 417.7469 423.1607 385.7911 312.8990 -5.4078 417.5543 422.9621 385.5968 314.5196 -5.4056 417.3627 422.7683 385.4005 316.1191 -5.4000 417.1888 422.5888 385.2196 317.7193 -5.3939 417.0011 422.3949 385.0277 319.3335 -5.3885 416.8043 422.1928 384.8326 320.9475 -5.3815 416.6158 421.9973 384.6282 322.5465 -5.3732 416.4207 421.7939 384.4363 324.1459 -5.3656 416.2302 421.5958 384.2363 325.7608 -5.3620 416.0326 421.3947 384.0028 327.3598 -5.3596 415.8478 421.2074 383.8099 328.9888 -5.3479 415.6472 420.9952 383.5967 330.5881 -5.3416 415.4594 420.8009 383.3713 332.1859 -5.3358 415.2672 420.6030 383.1477 333.7891 -5.3325 415.0785 420.4111 382.9386 335.3819 -5.3256 414.8823 420.2078 382.7263 336.9733 -5.3211 414.6926 420.0137 382.5249 338.5953 -5.3157 414.4984 419.8141 382.3035 340.2034 -5.3113 414.3085 419.6198 382.0923 341.7984 -5.3094 414.1106 419.4200 381.8913 343.3950 -5.3031 413.9146 419.2177 381.6752 344.9936 -5.2972 413.7355 419.0327 381.4556 346.6219 -5.2947 413.5402 418.8349 381.2539 348.2218 -5.2893 413.3378 418.6272 381.0379 349.8208 -5.2843 413.1465 418.4308 380.8356 351.4346 -5.2762 412.9450 418.2211 380.6131 353.0403 -5.2695 412.7573 418.0268 380.4161 354.6455 -5.2639 412.5775 417.8415 380.1978 356.2460 -5.2619 412.3731 417.6351 379.9986 357.8755 -5.2528 412.1768 417.4296 379.7778 359.4745 -5.2482 411.9727 417.2209 379.5712 361.0735 -5.2430 411.7769 417.0199 379.3697 362.6875 -5.2364 411.5931 416.8295 379.1598 364.2853 -5.2300 411.3881 416.6181 378.9639 365.8920 -5.2242 411.1905 416.4148 378.7543 367.4988 -5.2149 411.0010 416.2159 378.5616 369.0916 -5.2122 410.8156 416.0278 378.3750 370.6854 -5.2054 410.6029 415.8084 378.1813 372.2926 -5.1959 410.4138 415.6097 377.9727 373.9165 -5.1916 410.2318 415.4234 377.7638 375.5131 -5.1869 410.0216 415.2084 377.5678 377.1118 -5.1813 409.8277 415.0089 377.3772 378.7115 -5.1763 409.6314 414.8077 377.1721 380.3113 -5.1721 409.4359 414.6079 376.9632 381.9404 -5.1649 409.2492 414.4141 376.7548 383.5420 -5.1562 409.0449 414.2011 376.5434 385.1539 -5.1501 408.8386 413.9886 376.3078 386.7533 -5.1445 408.6499 413.7944 376.0894 388.3536 -5.1396 408.4574 413.5970 375.8832 389.9548 -5.1354 408.2532 413.3886 375.6528 391.5846 -5.1306 408.0507 413.1814 375.4253 393.1848 -5.1196 407.8614 412.9810 375.2092 394.7986 -5.1159 407.6676 412.7834 374.9893 396.3949 -5.1084 407.4704 412.5788 374.7720 397.9904 -5.1013 407.2648 412.3662 374.5593 399.5846 -5.0945 407.0693 412.1638 374.3303 401.1913 -5.0912 406.8668 411.9580 374.1110 402.8013 -5.0828 406.6809 411.7636 373.9115 404.3935 -5.0786 406.4786 411.5572 373.7024 406.0033 -5.0845 406.2845 411.3690 373.4715 407.5975 -5.0778 406.0682 411.1460 373.2712 409.2246 -5.0758 405.8688 410.9446 373.0579 410.8239 -5.0661 405.6772 410.7433 372.8429 412.4235 -5.0601 405.4697 410.5297 372.6436 414.0225 -5.0672 405.2589 410.3261 372.4279 415.6406 -5.0502 405.0715 410.1217 372.2261 417.2545 -5.0402 404.8654 409.9056 372.0131 418.8535 -5.0332 404.6596 409.6928 371.8144 420.4675 -5.0264 404.4690 409.4954 371.6036 422.0664 -5.0224 404.2808 409.3032 371.3966 423.6650 -5.0167 404.0935 409.1103 371.2038 425.2939 -5.0121 403.8734 408.8854 371.0027 426.8931 -5.0028 403.6568 408.6595 370.8031 428.5034 -4.9949 403.4631 408.4580 370.6054 430.0940 -4.9897 403.2665 408.2561 370.3904 431.6869 -4.9871 403.0658 408.0530 370.1918 433.3086 -4.9850 402.8607 407.8457 369.9910 434.9071 -4.9771 402.6579 407.6350 369.7952 436.5190 -4.9703 402.4664 407.4367 369.5928 438.1128 -4.9646 402.2674 407.2320 369.4007 439.7226 -4.9583 402.0617 407.0200 369.1990 441.3198 -4.9555 401.8745 406.8300 368.9878 442.9500 -4.9488 401.6663 406.6151 368.7959 444.5489 -4.9428 401.4814 406.4242 368.5940 446.1488 -4.9383 401.2572 406.1954 368.3974 447.7626 -4.9303 401.0476 405.9779 368.2010 449.3625 -4.9242 400.8590 405.7831 368.0028 450.9778 -4.9176 400.6570 405.5746 367.7863 452.5809 -4.9125 400.4676 405.3800 367.5768 454.1955 -4.9104 400.2518 405.1622 367.3703 455.8066 -4.9173 400.0648 404.9821 367.1678 457.4025 -4.9008 399.8651 404.7659 366.9455 459.0165 -4.8710 399.6629 404.5338 366.7206 460.6446 -4.8647 399.4527 404.3175 366.4905 462.2369 -4.8629 399.2445 404.1074 366.2888 463.8280 -4.8387 399.0527 403.8914 366.0828 465.4206 -4.8336 398.8536 403.6872 365.8657 467.0280 -4.8365 398.6460 403.4825 365.6489 468.6504 -4.8274 398.4479 403.2753 365.4106 470.2443 -4.8297 398.2386 403.0683 365.2108 471.8403 -4.8157 398.0419 402.8575 364.9947 473.4536 -4.7864 397.8585 402.6449 364.7793 475.0566 -4.7829 397.6503 402.4332 364.5457 476.6705 -4.7747 397.4281 402.2028 364.3512 478.2845 -4.7816 397.2391 402.0207 364.1289 479.8839 -4.7882 397.0200 401.8082 363.9155 481.4829 -4.7720 396.8293 401.6013 363.7132 483.0818 -4.7791 396.6261 401.4052 363.5052 484.7106 -4.7535 396.4244 401.1779 363.2719 486.3159 -4.7707 396.2317 401.0023 363.0780 487.9256 -4.7441 396.0334 400.7774 362.8739 489.5396 -4.7728 395.8212 400.5940 362.6641 491.1394 -4.7979 395.6109 400.4088 362.4537 492.7528 -4.8117 395.4012 400.2129 362.2419 494.3610 -4.8346 395.1947 400.0293 362.0418 495.9525 -4.8426 394.9972 399.8398 361.8471 497.5455 -4.8344 394.7934 399.6278 361.6436 499.1536 -4.8317 394.6008 399.4325 361.4421 500.7626 -4.8294 394.3969 399.2263 361.2359 502.3709 -4.8230 394.1846 399.0077 361.0280 503.9671 -4.8188 393.9854 398.8042 360.8318 505.5663 -4.8107 393.7789 398.5896 360.6331 507.1964 -4.8019 393.5803 398.3823 360.4335 508.7896 -4.7943 393.3806 398.1749 360.2414 510.3894 -4.7937 393.1658 397.9595 360.0589 512.0186 -4.7882 392.9644 397.7526 359.8448 513.6175 -4.7815 392.7628 397.5443 359.6412 515.2165 -4.7745 392.5566 397.3311 359.4503 516.8168 -4.7685 392.3518 397.1203 359.2511 518.4315 -4.7615 392.1506 396.9121 359.0474 520.0605 -4.7571 391.9483 396.7054 358.8362 521.6591 -4.7493 391.7582 396.5075 358.6274 523.2581 -4.7425 391.5428 396.2853 358.4161 524.8715 -4.7392 391.3409 396.0802 358.1929 526.4640 -4.7342 391.1463 395.8805 357.9962 528.0783 -4.7271 390.9220 395.6491 357.7821 529.6886 -4.7243 390.7386 395.4629 357.5647 531.2811 -4.7155 390.5232 395.2387 357.3419 532.8895 -4.7104 390.3346 395.0450 357.1344 534.4845 -4.7046 390.1137 394.8183 356.9203 536.0805 -4.6887 389.9164 394.6050 356.6963 537.7091 -4.6911 389.7140 394.4051 356.4856 539.3071 -4.6740 389.5151 394.1890 356.2790 540.9208 -4.6725 389.3107 393.9832 356.0688 542.5198 -4.6708 389.1048 393.7757 355.8592 544.1194 -4.6644 388.9004 393.5649 355.6356 545.7488 -4.6592 388.6900 393.3491 355.4506 547.3481 -4.6537 388.4877 393.1413 355.2448 548.9626 -4.6440 388.2754 392.9194 355.0433 550.5625 -4.6402 388.0751 392.7152 354.8310 552.1616 -4.6379 387.8652 392.5031 354.6282 553.7915 -4.6344 387.6731 392.3075 354.4294 555.3905 -4.6255 387.4683 392.0938 354.2401 556.9883 -4.6202 387.2732 391.8934 354.0320 558.5944 -4.6126 387.0749 391.6875 353.8465 560.1906 -4.6068 386.8707 391.4775 353.6380 561.8128 -4.6011 386.6575 391.2586 353.4439 563.4051 -4.5940 386.4548 391.0488 353.2437 565.0143 -4.5880 386.2466 390.8346 353.0590 566.6099 -4.5792 386.0441 390.6232 352.8587 568.2066 -4.5721 385.8512 390.4233 352.6522 569.8358 -4.5686 385.6293 390.1978 352.4728 571.4358 -4.5621 385.4401 390.0022 352.2638 573.0365 -4.5556 385.2453 389.8009 352.0622 574.6505 -4.5493 385.0278 389.5771 351.8496 576.2495 -4.5322 384.8288 389.3609 351.6443 577.8485 -4.5376 384.6155 389.1531 351.4345 579.4723 -4.5377 384.4023 388.9400 351.2112 581.0861 -4.5308 384.2141 388.7449 351.0050 582.6866 -4.5259 384.0072 388.5331 350.7845 584.3006 -4.5179 383.8154 388.3333 350.5525 585.9005 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