DTA measure 1pb updown3.txt Date: 2024319:1314 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.54 s Mass = 1366.700 mg data_number = 1269 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2948 -1.0975 250.9056 252.0031 266.1220 2.1458 -1.0899 250.9259 252.0158 266.1558 2.9065 -1.0801 251.0018 252.0819 266.1110 3.7283 -1.0707 251.0164 252.0871 266.0839 4.5198 -1.0601 251.0532 252.1133 266.1831 5.3115 -1.0567 251.2701 252.3268 266.1131 6.1638 -1.0550 251.4290 252.4840 266.0536 6.9255 -1.0509 251.4678 252.5187 266.1113 7.7478 -1.0425 251.6590 252.7016 266.2150 8.5398 -1.0365 251.8341 252.8706 266.2423 9.3315 -1.0159 251.6013 252.6172 266.3758 10.1565 -1.0101 251.6315 252.6416 266.4837 10.9485 -0.9925 251.6791 252.6716 266.6070 11.7705 -1.0054 251.7816 252.7870 266.6889 12.5625 -1.0150 251.8297 252.8446 266.7669 13.3545 -1.0044 252.0102 253.0145 266.7045 14.1765 -0.9827 252.1124 253.0951 266.9067 14.9385 -0.9687 251.9926 252.9613 267.0234 15.7905 -0.9663 251.9977 252.9640 267.0797 16.5825 -0.9756 252.1122 253.0877 267.1747 17.3745 -0.9755 252.2079 253.1834 267.2926 18.1965 -0.9674 252.4376 253.4051 267.4609 18.9885 -0.9553 252.5014 253.4567 267.6154 19.8105 -0.9565 252.5810 253.5375 267.8081 20.6025 -0.9599 252.7520 253.7119 267.9908 21.3945 -0.9548 252.8827 253.8376 268.1039 22.2163 -0.9515 253.1071 254.0585 268.2330 22.9780 -0.9491 253.2754 254.2245 268.4700 23.8300 -0.9534 253.4451 254.3985 268.5764 24.6228 -0.9681 253.6684 254.6365 268.6497 25.4155 -0.9740 253.7713 254.7453 268.7130 26.2360 -0.9596 253.9476 254.9073 268.9583 26.9930 -0.9667 253.9695 254.9362 269.2093 27.8410 -0.9796 253.9967 254.9763 269.1341 28.6290 -0.9636 254.1463 255.1099 269.4734 29.4173 -0.9642 254.3293 255.2935 269.6746 30.2370 -0.9587 254.5494 255.5080 269.7677 30.9960 -0.9440 254.7620 255.7059 270.0030 31.8463 -0.9544 255.0583 256.0127 269.9096 32.6355 -0.9648 255.1949 256.1597 270.0396 33.4250 -0.9458 255.3903 256.3361 270.4470 34.2448 -0.9459 255.6169 256.5628 270.5094 35.0335 -0.9586 255.6923 256.6509 270.5736 35.8555 -0.9539 255.7957 256.7496 270.7696 36.6473 -0.9639 255.8375 256.8014 270.9050 37.4390 -0.9620 255.9952 256.9572 271.1335 38.2613 -0.9611 256.1856 257.1468 271.3101 39.0230 -0.9656 256.2188 257.1844 271.4179 39.8750 -0.9623 256.2995 257.2618 271.5961 40.6670 -0.9744 256.4745 257.4489 271.8019 41.4585 -0.9780 256.5169 257.4949 271.9359 42.2808 -0.9800 256.7774 257.7575 272.1033 43.0425 -0.9969 256.8384 257.8353 272.2131 43.8950 -0.9871 256.8503 257.8375 272.3792 44.6868 -0.9833 256.9973 257.9806 272.5415 45.4785 -0.9688 257.1044 258.0732 272.6498 46.3008 -0.9588 257.1846 258.1434 272.8972 47.0625 -0.9332 257.2872 258.2205 273.1391 47.9150 -0.9498 257.3897 258.3394 273.2760 48.7068 -0.9300 257.5711 258.5011 273.4294 49.4985 -0.9155 257.7506 258.6660 273.6762 50.3208 -0.9323 257.8535 258.7858 273.7114 51.1125 -0.9174 258.0818 258.9992 273.7632 51.9348 -0.9484 258.1084 259.0568 273.9983 52.7265 -0.9759 258.2161 259.1921 274.0364 53.5185 -0.9662 258.4806 259.4468 274.1149 54.3405 -0.9122 258.5464 259.4586 274.3035 55.1325 -0.8904 258.5701 259.4605 274.4446 55.9545 -0.8946 258.7337 259.6283 274.4049 56.7465 -0.8984 258.8974 259.7958 274.5132 57.5385 -0.8947 259.0170 259.9118 274.6282 58.3880 -0.9090 259.1410 260.0499 274.7045 59.1458 -0.9335 259.3330 260.2665 274.7322 59.9640 -0.9497 259.3256 260.2753 274.9923 60.7520 -0.9605 259.5214 260.4819 275.0174 61.5400 -0.9595 259.5103 260.4698 275.1250 62.3885 -0.9383 259.7299 260.6683 275.1589 63.1470 -0.9383 259.9738 260.9120 275.2312 63.9658 -0.9376 260.1249 261.0625 275.2269 64.7848 -0.9249 260.2622 261.1871 275.3920 65.5443 -0.9287 260.4197 261.3483 275.5111 66.3935 -0.9251 260.4857 261.4108 275.5056 67.1845 -0.9279 260.6055 261.5333 275.6361 67.9765 -0.9001 260.7210 261.6211 275.6396 68.7985 -0.8946 260.8599 261.7545 275.6381 69.5605 -0.8872 261.0310 261.9182 275.7652 70.4125 -0.9133 261.1435 262.0568 275.9743 71.1745 -0.9021 261.2428 262.1449 276.1518 71.9965 -0.8943 261.3570 262.2512 276.1529 72.8185 -0.8973 261.4361 262.3334 276.2186 73.5805 -0.8911 261.5528 262.4440 276.3073 74.4325 -0.9036 261.7846 262.6882 276.5250 75.2245 -0.9122 261.8661 262.7783 276.6924 76.0165 -0.9055 262.0551 262.9606 276.8744 76.8385 -0.9035 262.1105 263.0140 277.1143 77.6005 -0.8955 262.1991 263.0946 277.0672 78.4575 -0.8840 262.3065 263.1905 277.4030 79.2493 -0.8928 262.4610 263.3537 277.4659 80.0415 -0.8932 262.6509 263.5442 277.6245 80.8633 -0.8937 262.8108 263.7045 277.7468 81.6248 -0.9114 262.8207 263.7321 277.9319 82.4768 -0.9035 262.9294 263.8328 278.1622 83.2690 -0.9020 263.1465 264.0485 278.2556 84.0605 -0.9240 263.2393 264.1634 278.4855 84.8828 -0.9134 263.3555 264.2688 278.6559 85.6445 -0.9350 263.5040 264.4390 278.8183 86.4973 -0.9306 263.5551 264.4857 279.0882 87.2595 -0.9376 263.6349 264.5725 279.2693 88.0818 -0.9420 263.7901 264.7321 279.3145 88.9038 -0.9368 263.9945 264.9313 279.4138 89.6655 -0.9271 264.0146 264.9416 279.6146 90.5150 -0.9325 264.1594 265.0919 279.7760 91.2730 -0.9333 264.3630 265.2964 279.9398 92.0910 -0.9414 264.4181 265.3595 280.0634 92.9090 -0.9508 264.5130 265.4638 280.1519 93.6670 -0.9416 264.6914 265.6329 280.4470 94.5150 -0.9246 264.7806 265.7052 280.6719 95.3033 -0.9387 264.9437 265.8824 280.6930 96.0920 -0.9497 265.0480 265.9977 280.7839 96.9113 -0.9527 265.0692 266.0219 280.9583 97.7008 -0.9465 265.1306 266.0770 281.1907 98.5215 -0.9513 265.3352 266.2865 281.2293 99.3128 -0.9581 265.4866 266.4447 281.2863 100.1045 -0.9571 265.5320 266.4891 281.3051 100.9268 -0.9704 265.8669 266.8372 281.5435 101.6885 -0.9500 265.9704 266.9204 281.5947 102.5408 -0.9538 266.0173 266.9711 281.8309 103.3328 -0.9570 266.1086 267.0656 281.9628 104.1245 -0.9712 266.2646 267.2359 281.9815 104.9468 -0.9647 266.3933 267.3580 282.1703 105.7085 -0.9626 266.5452 267.5078 282.3726 106.5608 -0.9707 266.5756 267.5464 282.5022 107.3225 -0.9812 266.7510 267.7322 282.6345 108.1448 -1.0007 266.8885 267.8891 282.5146 108.9665 -0.9889 266.9899 267.9787 282.6666 109.7285 -0.9665 267.1372 268.1037 282.8342 110.5805 -0.9627 267.2396 268.2023 282.8913 111.3425 -0.9799 267.3598 268.3396 283.1971 112.1645 -0.9743 267.5167 268.4910 283.2388 112.9865 -0.9627 267.6059 268.5687 283.2922 113.7485 -0.9682 267.7535 268.7217 283.4637 114.6005 -0.9740 267.9659 268.9399 283.4571 115.3625 -0.9627 268.0711 269.0338 283.5277 116.1845 -0.9837 268.1375 269.1212 283.6924 117.0065 -0.9976 268.2432 269.2408 284.0706 117.7685 -0.9857 268.4248 269.4105 284.2399 118.6205 -0.9760 268.4711 269.4471 284.1891 119.3823 -0.9700 268.6508 269.6208 284.3260 120.2040 -0.9837 268.6880 269.6717 284.6878 121.0258 -0.9796 268.8810 269.8606 284.8321 121.7875 -0.9803 269.0721 270.0524 285.0499 122.6398 -0.9909 269.2492 270.2401 285.0957 123.3993 -0.9882 269.2957 270.2839 285.1403 124.2170 -0.9956 269.4729 270.4685 285.2510 125.0055 -0.9806 269.5131 270.4937 285.2785 125.7943 -0.9870 269.7004 270.6875 285.4506 126.6433 -1.0099 269.7234 270.7333 285.6339 127.4013 -1.0144 269.9068 270.9212 285.6863 128.2208 -1.0052 270.0802 271.0854 285.8091 129.0385 -1.0041 269.9943 270.9984 285.7628 129.7965 -1.0218 270.2301 271.2520 285.8582 130.6450 -1.0071 270.4899 271.4970 286.0291 131.4045 -1.0161 270.6016 271.6177 286.1289 132.2243 -1.0077 270.6363 271.6440 286.0818 133.0463 -1.0109 270.6909 271.7018 286.2342 133.8080 -1.0008 270.8666 271.8675 286.3129 134.6598 -0.9978 271.0811 272.0789 286.3426 135.4220 -1.0201 271.2138 272.2339 286.5002 136.2453 -1.0164 271.3215 272.3379 286.5678 137.0380 -1.0167 271.3182 272.3348 286.7851 137.8298 -1.0090 271.4452 272.4542 286.9898 138.6820 -1.0035 271.6410 272.6444 287.1823 139.4470 -1.0068 271.8718 272.8786 287.4249 140.2698 -1.0084 272.1001 273.1085 287.5478 141.0618 -1.0284 272.1450 273.1734 287.8012 141.8535 -1.0275 272.2790 273.3065 288.0796 142.6758 -1.0206 272.5826 273.6032 288.1109 143.4675 -1.0185 272.6704 273.6889 288.2371 144.2898 -1.0325 272.8512 273.8836 288.5246 145.0818 -1.0443 273.0869 274.1312 288.4690 145.8735 -1.0376 273.3267 274.3643 288.5415 146.6958 -1.0345 273.5234 274.5579 288.9216 147.4875 -1.0353 273.6993 274.7346 289.1523 148.3098 -1.0456 273.8563 274.9020 289.2592 149.1018 -1.0397 273.8978 274.9374 289.4248 149.8945 -1.0368 273.9965 275.0334 289.5626 150.7165 -1.0804 274.0403 275.1207 289.8691 151.5085 -1.0672 274.2780 275.3451 290.0073 152.3305 -1.0395 274.4890 275.5285 290.2793 153.1225 -1.0386 274.6717 275.7103 290.5533 153.9145 -1.0331 274.7631 275.7962 290.7375 154.7363 -1.0352 274.9554 275.9906 290.7377 155.5245 -1.0466 275.0097 276.0563 290.6249 156.3415 -1.0512 275.0647 276.1159 290.9023 157.1300 -1.0498 275.2709 276.3207 290.7159 157.9190 -1.0554 275.4936 276.5490 290.8728 158.7683 -1.0580 275.5789 276.6369 291.1548 159.5270 -1.0539 275.6095 276.6634 291.2641 160.3468 -1.0762 275.8703 276.9466 291.4024 161.1353 -1.0704 275.7678 276.8382 291.4868 161.9250 -1.0764 275.8157 276.8920 291.6101 162.7735 -1.0758 275.9336 277.0094 291.7561 163.5333 -1.0526 275.8667 276.9192 291.8555 164.3535 -1.0658 276.0206 277.0864 291.9374 165.1755 -1.0897 276.3208 277.4105 292.0422 165.9375 -1.1009 276.3303 277.4312 292.2913 166.7895 -1.1006 276.6275 277.7282 292.4183 167.5515 -1.1006 276.5725 277.6731 292.5237 168.3735 -1.1005 276.6434 277.7438 292.6590 169.1655 -1.1121 276.8430 277.9552 292.7350 169.9575 -1.1240 276.9725 278.0966 292.9170 170.8095 -1.1189 277.1346 278.2535 293.0555 171.5715 -1.1111 277.2505 278.3616 293.0426 172.3935 -1.1099 277.4064 278.5163 293.1507 173.1855 -1.1120 277.4771 278.5891 293.3697 173.9775 -1.1086 277.6138 278.7224 293.4371 174.8295 -1.1167 277.7330 278.8497 293.5033 175.5915 -1.1289 277.7850 278.9139 293.6000 176.4133 -1.1285 277.8652 278.9937 293.8451 177.2353 -1.1289 278.0472 279.1760 293.9119 177.9965 -1.1489 278.2156 279.3646 294.0189 178.8490 -1.1376 278.3546 279.4922 294.1380 179.6105 -1.1414 278.2811 279.4225 294.2588 180.4328 -1.1524 278.6322 279.7845 294.4228 181.2548 -1.1529 278.6911 279.8439 294.5385 182.0165 -1.1446 278.8219 279.9665 294.6346 182.8688 -1.1310 278.8562 279.9872 294.8695 183.6608 -1.1372 278.8877 280.0249 295.0501 184.4525 -1.1516 279.1330 280.2846 295.0416 185.2748 -1.1543 279.3283 280.4826 295.2450 186.0365 -1.1477 279.3479 280.4956 295.3093 186.8883 -1.1432 279.4685 280.6117 295.4133 187.6748 -1.1574 279.6459 280.8033 295.5478 188.4620 -1.1571 279.8487 281.0058 295.6257 189.2800 -1.1523 280.0444 281.1966 295.6746 190.0380 -1.1808 280.0684 281.2493 295.7648 190.8870 -1.1760 280.0994 281.2754 295.9542 191.6750 -1.1651 280.3146 281.4797 296.0765 192.4630 -1.1788 280.4972 281.6760 296.2122 193.2813 -1.1948 280.5629 281.7576 296.3314 194.0410 -1.1987 280.4989 281.6976 296.4881 194.8910 -1.1846 280.7652 281.9498 296.6489 195.6828 -1.1795 280.9095 282.0890 296.7258 196.4740 -1.1847 281.0466 282.2314 296.9135 197.2953 -1.1946 281.3769 282.5715 297.0956 198.0575 -1.1903 281.4139 282.6041 297.1455 198.9095 -1.1839 281.4670 282.6510 297.3746 199.6715 -1.1804 281.7546 282.9350 297.3806 200.4935 -1.1914 281.7140 282.9053 297.5345 201.3158 -1.1924 281.9678 283.1603 297.7564 202.0775 -1.1990 281.9517 283.1507 297.9297 202.9295 -1.1921 282.0597 283.2517 297.9995 203.6915 -1.2047 282.2914 283.4961 298.1888 204.5138 -1.2167 282.5267 283.7434 298.3364 205.3055 -1.2225 282.4318 283.6542 298.5507 206.0975 -1.2216 282.6253 283.8469 298.7630 206.9495 -1.2274 282.7911 284.0185 298.8690 207.7115 -1.2519 283.1156 284.3674 298.9051 208.5335 -1.2747 283.2721 284.5468 299.0959 209.3255 -1.2538 283.2949 284.5487 299.1753 210.1175 -1.2550 283.3607 284.6158 299.2618 210.9695 -1.2534 283.4844 284.7378 299.4583 211.7315 -1.2477 283.6602 284.9078 299.5457 212.5535 -1.2654 283.9059 285.1712 299.6430 213.3758 -1.2634 284.0123 285.2758 299.7625 214.1385 -1.2574 283.9806 285.2380 299.9202 214.9905 -1.2508 284.0020 285.2528 300.1243 215.7525 -1.2657 284.3186 285.5842 300.1992 216.5740 -1.2666 284.5309 285.7974 300.2942 217.3963 -1.2786 284.6830 285.9615 300.4232 218.1585 -1.2871 284.8059 286.0931 300.6119 219.0100 -1.2989 284.9059 286.2048 300.7087 219.7680 -1.2906 285.0165 286.3071 300.8001 220.5863 -1.2779 285.2276 286.5055 300.9411 221.3768 -1.2965 285.4313 286.7278 300.9835 222.1670 -1.2931 285.4237 286.7168 301.1826 223.0158 -1.2917 285.4328 286.7245 301.2753 223.7733 -1.2919 285.7468 287.0388 301.4805 224.5913 -1.2886 285.8018 287.0904 301.5987 225.3800 -1.2850 286.0051 287.2901 301.7519 226.1678 -1.2856 286.1966 287.4823 301.7813 227.0183 -1.2952 286.2661 287.5613 301.9597 227.7783 -1.2901 286.2848 287.5750 302.0966 228.5990 -1.2872 286.2774 287.5646 302.2527 229.4203 -1.2949 286.3373 287.6322 302.4123 230.1813 -1.2917 286.6117 287.9034 302.4653 231.0335 -1.3034 286.4715 287.7749 302.7551 231.7950 -1.3062 286.5478 287.8540 302.8852 232.6168 -1.3182 286.6382 287.9564 303.0469 233.4090 -1.3134 286.7361 288.0495 303.0590 234.2008 -1.3052 286.9087 288.2139 303.2379 235.0530 -1.3037 286.8848 288.1886 303.4380 235.8145 -1.3339 286.9596 288.2934 303.4648 236.6368 -1.3451 287.0510 288.3960 303.6464 237.4288 -1.3439 287.2054 288.5493 303.7107 238.2205 -1.3457 287.2940 288.6397 303.9756 239.0448 -1.3579 287.4084 288.7663 304.0206 239.8375 -1.3644 287.5068 288.8712 304.1890 240.6598 -1.3588 287.5634 288.9222 304.2500 241.4518 -1.3775 287.8660 289.2436 304.4982 242.2435 -1.3607 287.9523 289.3130 304.8379 243.0658 -1.3587 288.0791 289.4378 305.0445 243.8575 -1.3474 288.2027 289.5501 305.0735 244.6798 -1.3203 288.4302 289.7505 305.1255 245.4715 -1.3239 288.6360 289.9600 305.3051 246.2635 -1.3204 288.8262 290.1465 305.5437 247.0855 -1.3145 288.9820 290.2965 305.5320 247.8775 -1.3123 289.2380 290.5503 305.6196 248.6995 -1.3314 289.3909 290.7223 305.6734 249.4915 -1.3372 289.5597 290.8969 305.8144 250.2835 -1.3192 289.6613 290.9806 305.9340 251.1055 -1.3342 289.9299 291.2641 306.0575 251.8970 -1.3161 290.0927 291.4088 306.2056 252.7160 -1.3083 290.2363 291.5446 306.2941 253.5050 -1.3151 290.3789 291.6940 306.3437 254.2930 -1.3146 290.5256 291.8403 306.5563 255.1113 -1.3262 290.6509 291.9771 306.6668 255.9003 -1.3355 290.7378 292.0734 306.7942 256.7200 -1.3499 290.9374 292.2873 306.9154 257.5080 -1.3526 291.0656 292.4181 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