DTA measure 3pb updown3.txt Date: 2024319:1340 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1519.67 s Mass = 1366.700 mg data_number = 1892 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3015 -4.6770 436.2247 440.9018 424.2931 2.1540 -4.7024 436.4722 441.1745 424.1970 2.9155 -4.7807 436.5650 441.3457 424.4227 3.7378 -4.7478 436.5310 441.2788 424.5497 4.5598 -4.7895 436.6801 441.4696 424.6651 5.3215 -4.7922 436.7738 441.5660 424.7623 6.1743 -4.7896 436.8555 441.6451 424.6716 6.9365 -4.7833 436.8043 441.5876 424.6180 7.7588 -4.7578 436.8616 441.6194 424.4943 8.5508 -4.7670 436.9370 441.7040 424.3483 9.3425 -4.7563 436.9160 441.6723 424.2850 10.1953 -4.7603 437.0137 441.7740 424.1899 10.9560 -4.7502 436.9997 441.7499 424.1583 11.7730 -4.7461 437.0354 441.7816 424.0186 12.5610 -4.7516 437.1006 441.8521 423.8745 13.3490 -4.7577 437.0968 441.8545 423.7843 14.1980 -4.7734 437.0986 441.8719 423.7102 14.9560 -4.7761 437.1913 441.9673 423.5507 15.7740 -4.8088 437.2542 442.0630 423.4749 16.5923 -4.8124 437.1344 441.9468 423.4141 17.3513 -4.8216 437.2469 442.0685 423.2667 18.2015 -4.8340 437.2681 442.1021 423.1082 18.9605 -4.8246 437.4027 442.2273 423.0707 19.7800 -4.8027 437.2450 442.0477 422.9446 20.6010 -4.8311 437.3484 442.1795 422.8284 21.3625 -4.8469 437.4308 442.2777 422.6827 22.2148 -4.8219 437.5780 442.3999 422.5155 22.9765 -4.8285 437.7088 442.5374 422.4258 23.7988 -4.8431 437.6854 442.5285 422.3234 24.5908 -4.8354 437.6527 442.4881 422.2814 25.3825 -4.8206 437.6065 442.4271 422.1795 26.2348 -4.8215 437.6218 442.4433 422.0306 26.9965 -4.8171 437.6694 442.4866 421.9216 27.8185 -4.8405 437.6007 442.4413 421.7972 28.6135 -4.8349 437.6618 442.4967 421.5641 29.4085 -4.8226 437.7108 442.5334 421.5566 30.2305 -4.8390 437.6736 442.5126 421.3810 31.0225 -4.8279 437.6705 442.4985 421.2805 31.8445 -4.8186 437.7454 442.5640 421.0940 32.6365 -4.8352 437.7948 442.6300 421.0381 33.4285 -4.8537 437.7357 442.5894 420.8278 34.2505 -4.8540 437.7919 442.6459 420.7407 35.0425 -4.8546 437.7385 442.5932 420.7102 35.8643 -4.8476 437.7715 442.6191 420.6421 36.6565 -4.8283 437.7241 442.5524 420.5907 37.4483 -4.8419 437.6978 442.5397 420.4733 38.2703 -4.8744 437.6606 442.5350 420.3529 39.0618 -4.8727 437.6162 442.4889 420.2579 39.8838 -4.8779 437.6535 442.5314 420.1055 40.6758 -4.8767 437.7928 442.6695 419.8775 41.4675 -4.8638 437.7752 442.6391 419.8015 42.2898 -4.8636 437.6560 442.5196 419.6000 43.0815 -4.8628 437.8124 442.6752 419.5399 43.9033 -4.8613 437.8128 442.6741 419.6257 44.6910 -4.8873 437.9957 442.8829 419.6564 45.4790 -4.9024 438.0790 442.9813 419.5965 46.2970 -4.8886 437.8607 442.7494 419.5385 47.0850 -4.8941 437.9355 442.8297 419.2782 47.9040 -4.8546 437.9476 442.8022 419.1165 48.6960 -4.8535 437.7859 442.6394 419.1381 49.4980 -4.8766 437.6581 442.5346 419.1654 50.3165 -4.8824 437.6574 442.5398 419.0868 51.0760 -4.8700 437.7715 442.6415 418.7989 51.9248 -4.8681 437.9149 442.7830 418.6016 52.6848 -4.8767 437.8693 442.7460 418.4440 53.5068 -4.8854 437.8491 442.7345 418.4318 54.3288 -4.8705 437.8257 442.6962 418.3788 55.0905 -4.8893 437.8787 442.7680 418.3117 55.9440 -4.8733 437.8513 442.7246 418.1455 56.7055 -4.8885 437.9472 442.8357 418.0423 57.5278 -4.8979 437.9022 442.8001 418.1087 58.3198 -4.9016 437.8727 442.7743 418.0031 59.1115 -4.9110 437.8665 442.7776 418.0256 59.9638 -4.8731 437.8989 442.7720 417.7813 60.7260 -4.8928 438.0601 442.9530 417.8691 61.5498 -4.8814 437.8781 442.7595 417.6872 62.3418 -4.8662 437.8934 442.7596 417.5795 63.1335 -4.8742 437.9970 442.8712 417.5763 63.9558 -4.8925 437.9690 442.8615 417.4570 64.7475 -4.9166 437.8329 442.7495 417.3289 65.5698 -4.8637 437.8351 442.6988 417.1723 66.3618 -4.8817 437.9724 442.8540 417.0964 67.1535 -4.8791 437.9157 442.7948 417.0352 67.9755 -4.8866 437.8860 442.7726 416.9272 68.7675 -4.8901 437.9342 442.8243 416.7538 69.5895 -4.9071 437.8060 442.7132 416.7320 70.3815 -4.9156 437.8802 442.7958 416.6021 71.1735 -4.9284 437.8400 442.7684 416.4915 72.0268 -4.8994 437.9146 442.8140 416.4039 72.7895 -4.9111 437.8971 442.8083 416.3758 73.6128 -4.9234 437.9403 442.8637 416.2082 74.4055 -4.9185 437.9412 442.8597 416.0781 75.1985 -4.9277 437.7980 442.7257 415.9927 76.0183 -4.9205 437.7991 442.7196 415.9040 76.8053 -4.9109 437.7163 442.6272 415.7606 77.6238 -4.8983 437.6427 442.5409 415.6285 78.4118 -4.9135 437.5855 442.4991 415.5731 79.2000 -4.8854 437.8383 442.7236 415.5179 80.0193 -4.9012 437.7672 442.6684 415.4425 80.7795 -4.9019 437.8404 442.7423 415.3534 81.6285 -4.9015 437.7855 442.6869 415.2116 82.4170 -4.8998 437.8540 442.7538 415.1196 83.2060 -4.9007 437.8733 442.7739 415.0350 84.0248 -4.9071 437.6679 442.5750 414.8260 84.8148 -4.9061 437.6533 442.5594 414.7760 85.6365 -4.8872 437.6513 442.5385 414.6784 86.4285 -4.8841 437.7948 442.6789 414.7043 87.2205 -4.8916 437.7904 442.6820 414.5333 88.0433 -4.9003 437.7045 442.6048 414.3645 88.8355 -4.9070 437.6793 442.5863 414.2731 89.6575 -4.9219 437.6055 442.5275 414.1186 90.4505 -4.9239 437.5159 442.4398 414.1289 91.2425 -4.9075 437.4705 442.3780 413.9927 92.0645 -4.8941 437.6055 442.4996 413.8657 92.8565 -4.8966 437.5277 442.4244 413.8422 93.6778 -4.8908 437.4288 442.3196 413.6964 94.4700 -4.9147 437.3134 442.2281 413.5516 95.2618 -4.9140 437.1774 442.0913 413.4891 96.0840 -4.9082 437.2599 442.1681 413.3095 96.8455 -4.9181 437.3229 442.2410 413.1590 97.6990 -4.9073 437.3325 442.2398 413.0525 98.4908 -4.9328 437.2000 442.1327 412.9989 99.2825 -4.9272 437.2590 442.1862 413.0216 100.1050 -4.9066 437.2191 442.1257 412.7280 100.8675 -4.9483 437.2832 442.2315 412.7997 101.7198 -4.9313 437.3671 442.2984 412.6426 102.5118 -4.9419 437.4303 442.3722 412.7223 103.3035 -4.9171 437.3456 442.2626 412.4342 104.1260 -4.9319 437.2257 442.1576 412.2448 104.8885 -4.9259 437.1921 442.1180 412.1152 105.7408 -4.9400 437.1483 442.0883 412.0427 106.5328 -4.9338 437.0630 441.9968 411.9288 107.3245 -4.8846 437.0063 441.8909 411.8909 108.1450 -4.8488 436.9409 441.7897 411.6823 108.9030 -4.8368 436.9398 441.7766 411.5382 109.7510 -4.8505 437.0594 441.9099 411.4721 110.5390 -4.8477 436.9567 441.8043 411.3507 111.3270 -4.8670 436.8641 441.7311 411.3004 112.1450 -4.8950 436.9023 441.7972 411.3586 112.9330 -4.8776 436.9043 441.7818 411.2856 113.7518 -4.9281 436.7126 441.6407 411.0097 114.5400 -4.9307 436.6516 441.5823 410.9367 115.3298 -4.9132 436.7335 441.6467 410.9049 116.1498 -4.9390 436.6581 441.5971 410.7013 116.9415 -4.9244 436.6367 441.5611 410.5833 117.7638 -4.9207 436.6118 441.5325 410.5941 118.5555 -4.9401 436.6154 441.5555 410.4622 119.3475 -4.9275 436.4263 441.3538 410.2554 120.1695 -4.9178 436.4606 441.3784 410.0442 120.9373 -4.8874 436.4741 441.3615 409.8713 121.7895 -4.8823 436.2734 441.1557 409.7570 122.5515 -4.8955 436.2129 441.1084 409.5841 123.3735 -4.8692 436.1096 440.9789 409.4107 124.1955 -4.8648 436.1512 441.0160 409.3448 124.9575 -4.8609 436.2397 441.1006 409.2826 125.8098 -4.8767 435.9884 440.8651 409.2160 126.5715 -4.8831 435.9680 440.8511 409.1062 127.3935 -4.8851 435.9428 440.8279 409.0871 128.2155 -4.8740 435.8716 440.7455 408.9900 128.9775 -4.8641 435.8320 440.6961 408.8053 129.8295 -4.8594 435.8171 440.6765 408.7607 130.5915 -4.8700 435.7583 440.6283 408.6353 131.4135 -4.9068 435.7480 440.6547 408.7020 132.2055 -4.9062 435.7565 440.6627 408.5365 132.9975 -4.8803 435.6996 440.5799 408.4152 133.8495 -4.8890 435.6521 440.5411 408.4131 134.6113 -4.8877 435.4922 440.3799 408.2750 135.4330 -4.8561 435.2748 440.1309 408.2153 136.2250 -4.8806 435.1735 440.0542 408.2439 137.0165 -4.8908 435.1788 440.0696 408.2288 137.8695 -4.9130 435.0875 440.0005 407.9458 138.6315 -4.9158 435.0417 439.9575 408.0339 139.4545 -4.9075 435.0616 439.9691 407.9132 140.2443 -4.9205 434.9131 439.8336 407.7541 141.0345 -4.9158 434.7235 439.6392 407.5966 141.8595 -4.9234 434.8692 439.7926 407.4517 142.6170 -4.9377 434.7775 439.7152 407.4693 143.4653 -4.9189 434.5464 439.4654 407.3742 144.2533 -4.8981 434.5944 439.4925 407.2370 145.0413 -4.9033 434.5305 439.4338 407.2304 145.8605 -4.8939 434.5108 439.4047 407.1213 146.6493 -4.9079 434.2039 439.1118 407.0764 147.4680 -4.9159 434.2707 439.1866 406.9069 148.2575 -4.8958 434.1476 439.0434 406.7572 149.0473 -4.8757 434.0518 438.9275 406.7423 149.8690 -4.9017 434.0392 438.9409 406.7563 150.6308 -4.8975 433.9930 438.8905 406.5029 151.4830 -4.9164 433.8851 438.8015 406.4448 152.2750 -4.9108 433.8574 438.7682 406.2851 153.0665 -4.8974 433.7484 438.6457 406.1703 153.8888 -4.9346 433.6926 438.6273 406.1387 154.6505 -4.9356 433.7000 438.6356 406.1750 155.5030 -4.9430 433.6523 438.5954 405.9994 156.2948 -4.9348 433.6241 438.5588 405.9047 157.0865 -4.9234 433.5059 438.4293 405.8004 157.9088 -4.9328 433.4959 438.4287 405.6525 158.6705 -4.9220 433.4199 438.3419 405.4966 159.5228 -4.9131 433.3657 438.2788 405.2576 160.3148 -4.9272 433.3757 438.3029 405.1567 161.1065 -4.9364 433.2140 438.1503 404.9798 161.9288 -4.9145 433.1580 438.0725 404.8961 162.6905 -4.9169 433.0760 437.9930 404.8427 163.5428 -4.9090 432.9583 437.8674 404.8326 164.3348 -4.9187 432.9780 437.8967 404.6924 165.1275 -4.9227 432.9024 437.8251 404.5281 165.9495 -4.9142 432.7828 437.6970 404.4154 166.7115 -4.9137 432.8315 437.7452 404.4346 167.5635 -4.8832 432.7344 437.6176 404.2156 168.3555 -4.8833 432.7533 437.6366 404.1558 169.1475 -4.8892 432.5687 437.4580 403.9808 169.9695 -4.8976 432.5505 437.4482 403.8016 170.7315 -4.9055 432.5124 437.4178 403.8197 171.5835 -4.8800 432.4860 437.3660 403.7447 172.3755 -4.9150 432.3759 437.2909 403.5938 173.1650 -4.9106 432.3356 437.2462 403.4977 173.9830 -4.9014 432.3094 437.2108 403.4331 174.7403 -4.9261 432.2474 437.1735 403.2721 175.5883 -4.8908 432.1573 437.0481 403.1644 176.3768 -4.8676 432.0138 436.8814 403.0456 177.1650 -4.8942 431.9662 436.8604 402.9649 177.9838 -4.9041 431.9576 436.8617 402.9737 178.7430 -4.8769 431.9651 436.8420 402.8014 179.5915 -4.9206 431.7780 436.6986 402.6590 180.3800 -4.9047 431.7422 436.6469 402.5156 181.1695 -4.9196 431.5556 436.4752 402.4709 181.9905 -4.9110 431.4915 436.4025 402.3014 182.7813 -4.9005 431.5136 436.4141 402.2237 183.6023 -4.8819 431.5546 436.4365 402.1774 184.3935 -4.8946 431.4554 436.3500 402.1340 185.1855 -4.8980 431.3723 436.2703 401.9682 186.0075 -4.9047 431.2449 436.1496 401.8851 186.7700 -4.8910 431.1844 436.0754 401.8334 187.6225 -4.8634 431.1351 435.9984 401.5887 188.3845 -4.8769 431.0631 435.9400 401.5084 189.2095 -4.8968 430.9787 435.8755 401.3901 190.0315 -4.8978 430.8699 435.7677 401.3002 190.7935 -4.8889 430.7197 435.6086 401.2231 191.6453 -4.8933 430.7023 435.5957 401.1204 192.4073 -4.8867 430.5410 435.4277 400.9598 193.2293 -4.8914 430.5892 435.4807 400.8289 194.0208 -4.8971 430.5606 435.4577 400.7557 194.8125 -4.8879 430.5103 435.3982 400.7263 195.6650 -4.8953 430.4182 435.3134 400.7597 196.4265 -4.9048 430.4475 435.3522 400.5491 197.2488 -4.9058 430.2848 435.1907 400.3569 198.0708 -4.8705 430.2413 435.1118 400.3015 198.8325 -4.8854 430.0982 434.9836 400.2395 199.6853 -4.8646 430.0638 434.9284 400.1782 200.4475 -4.8642 430.0063 434.8706 399.9296 201.2698 -4.8817 429.9664 434.8480 399.9034 202.0918 -4.8694 429.7775 434.6470 399.7451 202.8535 -4.8642 429.7141 434.5783 399.5986 203.7063 -4.8826 429.6597 434.5423 399.5239 204.4685 -4.8900 429.6300 434.5200 399.5208 205.2880 -4.8545 429.6031 434.4575 399.4824 206.0770 -4.8537 429.5159 434.3696 399.2074 206.8650 -4.8411 429.3592 434.2003 399.0440 207.7130 -4.8691 429.3353 434.2044 399.1207 208.4710 -4.8774 429.2566 434.1340 399.0929 209.2890 -4.8709 429.1553 434.0262 398.9513 210.0770 -4.8633 428.9670 433.8303 398.8729 210.8650 -4.8463 428.8098 433.6561 398.7350 211.7178 -4.8496 428.8266 433.6762 398.6459 212.4765 -4.8629 428.8337 433.6966 398.5420 213.2973 -4.8773 428.7266 433.6039 398.4738 214.0908 -4.8969 428.6351 433.5320 398.3330 214.8845 -4.8763 428.5263 433.4026 398.1300 215.7065 -4.8404 428.4290 433.2694 398.1325 216.4985 -4.8652 428.3341 433.1993 398.0513 217.3205 -4.8591 428.2210 433.0801 398.0133 218.1128 -4.8388 428.2378 433.0766 397.9044 218.9045 -4.8310 428.1668 432.9978 397.7564 219.7265 -4.8379 428.1550 432.9929 397.7604 220.5185 -4.8441 428.0755 432.9196 397.5683 221.3408 -4.8429 427.9817 432.8245 397.3367 222.1325 -4.8491 427.9385 432.7876 397.3108 222.9270 -4.8592 427.8879 432.7472 397.3100 223.7555 -4.8442 427.8393 432.6835 397.2203 224.5478 -4.8405 427.7882 432.6287 397.0211 225.3705 -4.8365 427.6580 432.4945 396.7818 226.1625 -4.8352 427.5361 432.3714 396.7176 226.9545 -4.8366 427.4390 432.2756 396.6774 227.7765 -4.8073 427.2389 432.0463 396.4572 228.5685 -4.8230 427.3249 432.1479 396.3703 229.3905 -4.8202 427.2206 432.0408 396.3839 230.1825 -4.8220 427.1743 431.9962 396.3146 230.9745 -4.8204 426.9562 431.7766 396.1292 231.7965 -4.8209 426.9256 431.7464 395.9934 232.5883 -4.8183 426.8597 431.6780 395.9042 233.4105 -4.7847 426.7777 431.5624 395.8387 234.2030 -4.7836 426.6802 431.4638 395.6433 234.9945 -4.7793 426.6128 431.3921 395.5302 235.8170 -4.8146 426.5433 431.3579 395.6123 236.6085 -4.7969 426.4533 431.2502 395.4260 237.4270 -4.7867 426.4289 431.2156 395.2763 238.2150 -4.7851 426.3001 431.0852 395.1484 239.0033 -4.7889 426.2830 431.0719 395.0553 239.8210 -4.7742 426.1293 430.9036 394.9128 240.6093 -4.7835 426.1174 430.9009 394.9457 241.4280 -4.7844 425.9623 430.7467 394.8390 242.2165 -4.7570 425.8312 430.5882 394.6336 243.0060 -4.7481 425.8748 430.6230 394.6067 243.8305 -4.7871 425.7052 430.4923 394.5106 244.5920 -4.7730 425.6745 430.4476 394.3905 245.4418 -4.7641 425.6093 430.3734 394.2928 246.2320 -4.7444 425.5692 430.3136 394.2294 247.0233 -4.7585 425.3648 430.1234 394.1882 247.8450 -4.7639 425.3282 430.0921 394.0043 248.6068 -4.7489 425.2175 429.9665 393.9227 249.4588 -4.7455 425.0634 429.8089 393.7796 250.2510 -4.7772 425.0647 429.8419 393.7257 251.0425 -4.7576 424.9790 429.7365 393.6605 251.8648 -4.7849 424.8550 429.6399 393.4800 252.6265 -4.8036 424.8785 429.6821 393.4804 253.4788 -4.7674 424.7123 429.4797 393.2435 254.2708 -4.7474 424.5866 429.3340 393.1028 255.0625 -4.7570 424.5343 429.2913 393.1376 255.8848 -4.7550 424.4566 429.2115 393.0370 256.6465 -4.7283 424.4205 429.1487 392.8584 257.4988 -4.7659 424.3499 429.1159 392.8696 258.2908 -4.7775 424.1890 428.9665 392.6901 259.0825 -4.7527 424.1410 428.8937 392.5748 259.9048 -4.7390 424.0817 428.8207 392.4789 260.6665 -4.7393 424.0691 428.8084 392.4478 261.5188 -4.7198 423.8860 428.6058 392.2983 262.3105 -4.7067 423.6785 428.3852 392.2065 263.1025 -4.7118 423.6462 428.3580 392.0689 263.9268 -4.7485 423.6556 428.4042 391.9193 264.6905 -4.7427 423.5390 428.2818 391.8738 265.5425 -4.7213 423.3906 428.1119 391.7914 266.3048 -4.7021 423.3788 428.0810 391.5786 267.1275 -4.7163 423.2674 427.9837 391.4049 267.9495 -4.6937 423.1752 427.8689 391.3134 268.7105 -4.7108 423.1154 427.8262 391.3193 269.5585 -4.6945 423.0074 427.7019 391.2069 270.3170 -4.7210 422.9536 427.6746 391.0824 271.1350 -4.7100 422.8271 427.5372 390.9225 271.9533 -4.7119 422.8204 427.5323 390.8187 272.7120 -4.6858 422.6883 427.3742 390.8063 273.5605 -4.7057 422.6618 427.3675 390.5155 274.3190 -4.7149 422.6153 427.3302 390.4835 275.1378 -4.6884 422.4812 427.1696 390.3838 275.9563 -4.6813 422.4206 427.1019 390.2977 276.7160 -4.6843 422.2642 426.9486 390.1432 277.5663 -4.6898 422.1503 426.8401 390.1940 278.3275 -4.6806 422.0928 426.7734 390.0360 279.1495 -4.6842 422.0418 426.7260 389.9703 279.9715 -4.6621 421.8968 426.5589 389.7638 280.7335 -4.6607 421.8479 426.5086 389.7781 281.5855 -4.6938 421.8233 426.5171 389.6815 282.3475 -4.6936 421.6580 426.3515 389.4854 283.1695 -4.6864 421.5430 426.2294 389.4628 283.9615 -4.6710 421.4856 426.1565 389.2904 284.7535 -4.6698 421.3150 425.9848 389.2279 285.6055 -4.6960 421.2361 425.9321 389.0954 286.3675 -4.6756 421.1301 425.8057 389.0187 287.1893 -4.6685 421.0718 425.7403 388.9282 287.9815 -4.6765 421.0566 425.7332 388.7579 288.7743 -4.6768 420.8898 425.5666 388.6402 289.5970 -4.6738 420.8204 425.4942 388.5989 290.3893 -4.6814 420.9177 425.5991 388.5249 291.2108 -4.6840 420.6701 425.3541 388.4573 292.0030 -4.6808 420.5660 425.2468 388.3784 292.7945 -4.6493 420.5524 425.2018 388.2187 293.6168 -4.6477 420.5119 425.1596 388.1074 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