DTA measure 1pb3 Test Date: 20231212:118 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 909.33 s Mass = 1452.5 mg data_number = 1129 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1648 -9.5927 199.2801 208.8728 264.6605 1.9565 -9.5870 199.5176 209.1047 264.7306 2.7785 -9.5780 199.7707 209.3487 264.7901 3.5383 -9.5701 200.0320 209.6020 264.8323 4.3893 -9.5612 200.2822 209.8434 264.9032 5.1498 -9.5563 200.5109 210.0672 264.9690 5.9708 -9.5492 200.7781 210.3273 265.0429 6.7925 -9.5394 201.0580 210.5974 265.1191 7.5943 -9.5323 201.2992 210.8315 265.2077 8.3643 -9.5221 201.5458 211.0678 265.2791 9.1865 -9.5151 201.7932 211.3083 265.3668 9.9770 -9.5083 202.0452 211.5535 265.4417 10.7985 -9.4992 202.3062 211.8055 265.5675 11.5898 -9.4923 202.5476 212.0399 265.6587 12.3815 -9.4827 202.7953 212.2780 265.7679 13.2038 -9.4724 203.0308 212.5033 265.8768 13.9938 -9.4623 203.2734 212.7357 266.0034 14.8155 -9.4539 203.5346 212.9885 266.1233 15.6068 -9.4471 203.7976 213.2447 266.2421 16.3973 -9.4377 204.0322 213.4699 266.3754 17.2185 -9.4269 204.2763 213.7032 266.5137 18.0368 -9.4186 204.5342 213.9528 266.6543 18.7863 -9.4111 204.7679 214.1790 266.7948 19.6375 -9.3996 205.0153 214.4149 266.9312 20.3978 -9.3939 205.2535 214.6473 267.0864 21.2188 -9.3845 205.5070 214.8915 267.2243 22.0385 -9.3758 205.7603 215.1361 267.3809 22.8005 -9.3691 205.9743 215.3434 267.5444 23.6525 -9.3576 206.2295 215.5871 267.7014 24.4140 -9.3507 206.4732 215.8239 267.8538 25.2355 -9.3417 206.7382 216.0799 268.0480 26.0275 -9.3338 206.9742 216.3080 268.1958 26.8180 -9.3254 207.2012 216.5266 268.3655 27.6685 -9.3163 207.4466 216.7628 268.5553 28.6298 -9.3033 207.7359 217.0392 268.7486 29.4515 -9.2958 207.9790 217.2748 268.9219 30.2435 -9.2869 208.2277 217.5147 269.0957 31.0355 -9.2787 208.4668 217.7455 269.2764 31.8560 -9.2719 208.7102 217.9821 269.4411 32.6453 -9.2636 208.9616 218.2252 269.6120 33.4665 -9.2542 209.1984 218.4526 269.7809 34.2585 -9.2465 209.4191 218.6656 269.9484 35.0488 -9.2395 209.6408 218.8803 270.1189 35.8705 -9.2309 209.8767 219.1076 270.2882 36.6310 -9.2233 210.1129 219.3363 270.4593 37.4830 -9.2136 210.3790 219.5926 270.6204 38.2740 -9.2068 210.6062 219.8129 270.7985 39.0645 -9.1970 210.8367 220.0337 270.9754 39.8858 -9.1893 211.0793 220.2687 271.1335 40.6468 -9.1827 211.3047 220.4874 271.2747 41.4988 -9.1727 211.5454 220.7181 271.4416 42.2595 -9.1674 211.7821 220.9496 271.6110 43.0815 -9.1579 212.0146 221.1724 271.7735 43.9018 -9.1494 212.2614 221.4108 271.9090 44.6625 -9.1439 212.4969 221.6408 272.0544 45.5145 -9.1374 212.7250 221.8624 272.2121 46.2758 -9.1278 212.9457 222.0735 272.3554 47.0975 -9.1192 213.1793 222.2985 272.4893 47.8895 -9.1104 213.4052 222.5155 272.6369 48.6803 -9.1007 213.6604 222.7611 272.7666 49.5315 -9.0958 213.9121 223.0079 272.9210 50.2935 -9.0906 214.1202 223.2108 273.0251 51.1150 -9.0803 214.3649 223.4452 273.1710 51.9055 -9.0722 214.5727 223.6449 273.3041 52.6973 -9.0652 214.8024 223.8675 273.4302 53.5185 -9.0573 215.0446 224.1020 273.5858 54.3095 -9.0518 215.2741 224.3259 273.6916 55.1310 -9.0389 215.5115 224.5504 273.8063 55.9213 -9.0322 215.7213 224.7535 273.9296 56.7125 -9.0222 215.9418 224.9640 274.0551 57.5345 -9.0148 216.1787 225.1934 274.1872 58.2943 -9.0066 216.4025 225.4091 274.3085 59.1453 -9.0001 216.6385 225.6386 274.4244 59.9373 -8.9939 216.8559 225.8498 274.5395 60.7285 -8.9869 217.1002 226.0871 274.6497 61.5495 -8.9789 217.3175 226.2964 274.7797 62.3103 -8.9694 217.5419 226.5113 274.8884 63.1618 -8.9616 217.7780 226.7397 275.0157 63.9530 -8.9546 218.0106 226.9652 275.1167 64.7443 -8.9462 218.2219 227.1680 275.2379 65.5655 -8.9433 218.4275 227.3708 275.3524 66.3255 -8.9367 218.6556 227.5923 275.4530 67.1768 -8.9270 218.8940 227.8211 275.5642 67.9670 -8.9158 219.1115 228.0273 275.6727 68.7585 -8.9084 219.3406 228.2490 275.7932 69.5795 -8.8987 219.5641 228.4628 275.9331 70.3400 -8.8911 219.7886 228.6797 276.0448 71.1910 -8.8854 220.0279 228.9132 276.1525 71.9828 -8.8772 220.2295 229.1067 276.2659 72.7735 -8.8668 220.4520 229.3188 276.3854 73.5945 -8.8566 220.6740 229.5306 276.5108 74.3560 -8.8506 220.8790 229.7296 276.6293 75.2073 -8.8405 221.1221 229.9626 276.7340 75.9970 -8.8332 221.3304 230.1636 276.8490 76.7865 -8.8323 221.5458 230.3781 276.9711 77.6075 -8.8188 221.7583 230.5771 277.1018 78.3980 -8.8097 221.9849 230.7946 277.2093 79.2190 -8.8038 222.2083 231.0121 277.3481 80.0095 -8.7954 222.4180 231.2135 277.4886 80.8013 -8.7872 222.6268 231.4140 277.6002 81.6225 -8.7817 222.8417 231.6235 277.7284 82.4123 -8.7715 223.0709 231.8424 277.8503 83.2335 -8.7635 223.2884 232.0519 277.9768 84.0255 -8.7555 223.5048 232.2602 278.1081 84.8175 -8.7499 223.7243 232.4742 278.2622 85.6395 -8.7400 223.9514 232.6913 278.3942 86.4293 -8.7309 224.1596 232.8906 278.5228 87.2505 -8.7244 224.3956 233.1200 278.6688 88.0415 -8.7175 224.5823 233.2998 278.8002 88.8335 -8.7084 224.7855 233.4938 278.9366 89.6555 -8.7012 225.0085 233.7096 279.0868 90.4448 -8.6950 225.2173 233.9123 279.2164 91.2655 -8.6876 225.4377 234.1252 279.3584 92.0560 -8.6816 225.6597 234.3414 279.5010 92.8470 -8.6727 225.8723 234.5450 279.6502 93.6690 -8.6647 226.0823 234.7470 279.8144 94.4588 -8.6576 226.2911 234.9487 279.9579 95.2808 -8.6494 226.4969 235.1463 280.1028 96.0718 -8.6427 226.7162 235.3590 280.2905 96.8635 -8.6351 226.9190 235.5541 280.4208 97.7155 -8.6255 227.1476 235.7731 280.5645 98.4765 -8.6177 227.3711 235.9888 280.7058 99.2985 -8.6101 227.5869 236.1970 280.8489 100.0890 -8.6049 227.7695 236.3745 281.0053 100.8805 -8.5982 227.9688 236.5670 281.1613 101.7325 -8.5907 228.1815 236.7722 281.3150 102.4945 -8.5825 228.3901 236.9726 281.4610 103.3165 -8.5768 228.6003 237.1771 281.6166 104.1085 -8.5712 228.8121 237.3833 281.7593 104.9003 -8.5645 229.0526 237.6172 281.8807 105.7513 -8.5565 229.2667 237.8231 282.0483 106.5115 -8.5472 229.4396 237.9867 282.1784 107.3330 -8.5409 229.6512 238.1921 282.3189 108.1245 -8.5358 229.8518 238.3875 282.4692 108.9165 -8.5306 230.0540 238.5846 282.6054 109.8185 -8.5237 230.2956 238.8193 282.7481 110.7288 -8.5133 230.5380 239.0513 282.9124 111.5513 -8.5059 230.7454 239.2513 283.0414 112.3425 -8.5022 230.9584 239.4606 283.1896 113.1338 -8.4983 231.1592 239.6575 283.3382 113.9855 -8.4922 231.3676 239.8599 283.4775 114.7475 -8.4857 231.5497 240.0354 283.6120 115.5690 -8.4764 231.7715 240.2480 283.7559 116.3598 -8.4687 231.9604 240.4291 283.8856 117.1503 -8.4638 232.1570 240.6209 284.0203 118.0008 -8.4582 232.3856 240.8439 284.1479 118.7608 -8.4506 232.5871 241.0376 284.2783 119.5823 -8.4422 232.7920 241.2343 284.3840 120.4028 -8.4347 232.9870 241.4217 284.5194 121.1628 -8.4303 233.1818 241.6120 284.6575 122.0148 -8.4251 233.4056 241.8307 284.7947 122.7755 -8.4178 233.5982 242.0160 284.9027 123.5973 -8.4112 233.7900 242.2013 285.0228 124.4178 -8.4023 233.9860 242.3883 285.1463 125.1780 -8.3959 234.2047 242.6006 285.2607 126.0295 -8.3899 234.4246 242.8144 285.3736 126.8198 -8.3849 234.6289 243.0137 285.4886 127.6115 -8.3796 234.8268 243.2065 285.6081 128.4335 -8.3737 235.0066 243.3804 285.7276 129.1945 -8.3711 235.2142 243.5853 285.8357 130.0463 -8.3607 235.4108 243.7715 285.9620 130.8368 -8.3540 235.6027 243.9567 286.0844 131.6280 -8.3489 235.8127 244.1615 286.2047 132.4495 -8.3422 236.0100 244.3522 286.3359 133.2105 -8.3389 236.1975 244.5364 286.4510 134.0623 -8.3298 236.4113 244.7411 286.5721 134.8535 -8.3238 236.6021 244.9259 286.6945 135.6453 -8.3175 236.8009 245.1185 286.8219 136.4665 -8.3110 237.0066 245.3176 286.9411 137.2285 -8.3040 237.1962 245.5002 287.0421 138.0803 -8.3019 237.3956 245.6975 287.1765 138.8708 -8.2964 237.5872 245.8836 287.3154 139.6623 -8.2899 237.7919 246.0819 287.4209 140.5273 -8.2809 237.9896 246.2705 287.5573 141.4795 -8.2747 238.2190 246.4937 287.7042 142.2705 -8.2701 238.4113 246.6815 287.8247 143.0915 -8.2629 238.6266 246.8895 287.9661 143.8520 -8.2570 238.8030 247.0600 288.1022 144.7040 -8.2504 239.0147 247.2651 288.2066 145.4950 -8.2432 239.1914 247.4346 288.3258 146.2853 -8.2397 239.3776 247.6174 288.4659 147.1068 -8.2338 239.5871 247.8209 288.6056 147.8675 -8.2288 239.7672 247.9960 288.7235 148.7200 -8.2200 239.9790 248.1990 288.8634 149.5120 -8.2161 240.1621 248.3782 289.0260 150.3030 -8.2153 240.3390 248.5543 289.1449 151.1248 -8.2083 240.5413 248.7496 289.2786 151.8860 -8.1990 240.7295 248.9284 289.4150 152.7373 -8.1911 240.9355 249.1266 289.5767 153.5288 -8.1888 241.1297 249.3184 289.7144 154.3205 -8.1819 241.3250 249.5069 289.8425 155.1425 -8.1734 241.5331 249.7065 290.0003 155.9038 -8.1693 241.6896 249.8588 290.1342 156.7543 -8.1652 241.8932 250.0584 290.2835 157.5455 -8.1593 242.0765 250.2357 290.4241 158.3375 -8.1521 242.2733 250.4254 290.5804 159.1595 -8.1457 242.4586 250.6043 290.7387 159.9203 -8.1426 242.6353 250.7778 290.8729 160.7713 -8.1374 242.8485 250.9859 291.0273 161.5605 -8.1320 243.0434 251.1754 291.1656 162.3515 -8.1259 243.2337 251.3596 291.3245 163.1720 -8.1193 243.4311 251.5504 291.4917 163.9335 -8.1140 243.5937 251.7077 291.6117 164.7853 -8.1213 243.7946 251.9159 291.7750 165.5748 -8.1116 243.9987 252.1103 291.9245 166.3665 -8.1039 244.2005 252.3044 292.0691 167.1875 -8.1010 244.3676 252.4685 292.2255 167.9495 -8.0956 244.5487 252.6442 292.3562 168.8015 -8.0896 244.7324 252.8220 292.4846 169.5923 -8.0863 244.9301 253.0164 292.6302 170.3823 -8.0824 245.1309 253.2133 292.7590 171.2463 -8.0741 245.3187 253.3927 292.9008 172.2003 -8.0674 245.5202 253.5877 293.0582 172.9913 -8.0683 245.7238 253.7921 293.2071 173.8120 -8.0658 245.9080 253.9738 293.3450 174.5735 -8.0618 246.0835 254.1452 293.4850 175.4255 -8.0575 246.2848 254.3423 293.6287 176.2150 -8.0534 246.4559 254.5093 293.7473 177.0063 -8.0468 246.6509 254.6976 293.8595 177.8280 -8.0421 246.8375 254.8796 294.0031 178.5895 -8.0395 247.0349 255.0744 294.1128 179.4415 -8.0383 247.2212 255.2595 294.2621 180.2015 -8.0305 247.4053 255.4359 294.3877 181.0828 -8.0254 247.5905 255.6158 294.5250 181.8900 -8.0217 247.7690 255.7906 294.6360 182.7115 -8.0175 247.9712 255.9887 294.7662 183.4720 -8.0120 248.1394 256.1515 294.8917 184.3235 -8.0077 248.3330 256.3407 295.0304 185.0855 -8.0020 248.5088 256.5107 295.1428 185.9058 -8.0004 248.6937 256.6941 295.2617 186.6958 -7.9987 248.8796 256.8783 295.3823 187.4875 -7.9919 249.0536 257.0454 295.5071 188.3388 -7.9872 249.2485 257.2356 295.6468 189.1005 -7.9820 249.4361 257.4182 295.7764 189.9215 -7.9814 249.6206 257.6020 295.8771 190.7125 -7.9747 249.8093 257.7840 295.9999 191.5048 -7.9731 249.9715 257.9446 296.1326 192.3170 -7.9650 250.1666 258.1316 296.2617 193.1385 -7.9641 250.3646 258.3287 296.3826 193.9005 -7.9619 250.5265 258.4884 296.5029 194.7523 -7.9557 250.7117 258.6673 296.6313 195.5428 -7.9523 250.8867 258.8389 296.7544 196.3343 -7.9489 251.0923 259.0412 296.8659 197.1560 -7.9461 251.2640 259.2101 297.0039 197.9170 -7.9435 251.4369 259.3804 297.1154 198.7690 -7.9395 251.6245 259.5639 297.2384 199.5310 -7.9362 251.7967 259.7330 297.3640 200.3523 -7.9316 251.9759 259.9075 297.5034 201.1725 -7.9261 252.1739 260.0999 297.6046 201.9510 -7.9256 252.3482 260.2739 297.7362 202.7348 -7.9201 252.5063 260.4264 297.8731 203.5865 -7.9196 252.6921 260.6117 297.9991 204.3475 -7.9181 252.8662 260.7843 298.1211 205.1693 -7.9153 253.0489 260.9642 298.2447 205.9908 -7.9093 253.2430 261.1523 298.3759 206.7513 -7.9080 253.4075 261.3155 298.5153 207.6028 -7.9048 253.5994 261.5042 298.6486 208.3638 -7.9003 253.7674 261.6677 298.7733 209.1853 -7.8968 253.9496 261.8463 298.9349 210.0065 -7.8937 254.1202 262.0139 299.0633 210.7678 -7.8873 254.2645 262.1518 299.1923 211.6195 -7.8810 254.4597 262.3407 299.3484 212.3930 -7.8769 254.6440 262.5209 299.4844 213.1875 -7.8747 254.8407 262.7154 299.6238 214.0095 -7.8774 255.0233 262.9007 299.7608 214.8015 -7.8742 255.1942 263.0684 299.8986 215.5928 -7.8686 255.3561 263.2247 300.0473 216.4135 -7.8638 255.5471 263.4109 300.1892 217.2045 -7.8614 255.7156 263.5771 300.3395 218.0265 -7.8568 255.8856 263.7424 300.4845 218.8185 -7.8497 256.0577 263.9074 300.6203 219.6100 -7.8469 256.2352 264.0821 300.7659 220.4315 -7.8449 256.4267 264.2717 300.9233 221.2228 -7.8428 256.6193 264.4621 301.0606 222.0445 -7.8416 256.7785 264.6201 301.1957 222.8305 -7.8379 256.9331 264.7710 301.3614 223.6393 -7.8341 257.1189 264.9530 301.4904 224.4303 -7.8318 257.2901 265.1219 301.6409 225.2523 -7.8317 257.4739 265.3056 301.7808 226.0120 -7.8322 257.6333 265.4655 301.9140 226.8640 -7.8302 257.8194 265.6495 302.0780 227.6560 -7.8246 257.9826 265.8072 302.2244 228.4468 -7.8217 258.1509 265.9726 302.3595 229.2690 -7.8195 258.3406 266.1601 302.4946 230.0590 -7.8149 258.5053 266.3202 302.6373 230.8808 -7.8123 258.6960 266.5083 302.7809 231.6718 -7.8099 258.8615 266.6714 302.9024 232.4628 -7.8050 259.0283 266.8333 303.0239 233.2705 -7.8047 259.2018 267.0065 303.1788 234.0925 -7.8056 259.3870 267.1927 303.3146 234.8545 -7.8062 259.5703 267.3765 303.4279 235.7063 -7.8009 259.7495 267.5504 303.5839 236.5265 -7.7953 259.9099 267.7053 303.7092 237.4085 -7.7927 260.0943 267.8870 303.8519 238.1993 -7.7911 260.2671 268.0582 303.9634 238.9895 -7.7907 260.4431 268.2338 304.0784 239.8105 -7.7910 260.6241 268.4151 304.2162 240.6003 -7.7886 260.8013 268.5899 304.3579 241.4200 -7.7860 260.9662 268.7522 304.4950 242.2105 -7.7816 261.1298 268.9114 304.6161 243.0015 -7.7775 261.2996 269.0771 304.7320 243.8518 -7.7778 261.4818 269.2596 304.8733 244.6125 -7.7777 261.6456 269.4234 304.9749 245.4340 -7.7752 261.8173 269.5926 305.0925 246.3455 -7.7710 262.0297 269.8008 305.2234 247.1360 -7.7681 262.1826 269.9508 305.3467 247.9873 -7.7644 262.3594 270.1237 305.4829 248.7768 -7.7620 262.5319 270.2938 305.6044 249.5685 -7.7606 262.7055 270.4660 305.7160 250.3890 -7.7575 262.8704 270.6279 305.8305 251.1488 -7.7562 263.0103 270.7665 305.9533 252.0003 -7.7535 263.1924 270.9459 306.0807 252.7923 -7.7522 263.3744 271.1266 306.2027 253.5820 -7.7485 263.5445 271.2929 306.3183 254.4030 -7.7466 263.7278 271.4743 306.4390 255.1930 -7.7448 263.9097 271.6545 306.5666 256.0140 -7.7429 264.0522 271.7951 306.6918 256.8048 -7.7416 264.2318 271.9735 306.8146 257.5960 -7.7418 264.4002 272.1420 306.9511 258.4178 -7.7409 264.5654 272.3063 307.0814 259.2080 -7.7405 264.7482 272.4887 307.2051 260.0298 -7.7403 264.9186 272.6589 307.3530 260.7943 -7.7382 265.0701 272.8083 307.4662 261.6178 -7.7351 265.2497 272.9848 307.5975 262.4370 -7.7356 265.4118 273.1474 307.7579 263.1970 -7.7337 265.5613 273.2951 307.8710 264.0193 -7.7319 265.7361 273.4680 308.0037 264.8410 -7.7267 265.9108 273.6375 308.1528 265.6325 -7.7248 266.0637 273.7885 308.2978 266.4233 -7.7208 266.2314 273.9522 308.4168 267.2445 -7.7235 266.4153 274.1388 308.5486 268.0355 -7.7239 266.5710 274.2949 308.6948 268.8570 -7.7211 266.7450 274.4660 308.8283 269.6485 -7.7197 266.9040 274.6236 308.9643 270.4393 -7.7204 267.0673 274.7877 309.1055 271.2605 -7.7176 267.2447 274.9624 309.2535 272.0515 -7.7175 267.4123 275.1298 309.3933 272.8730 -7.7142 267.5833 275.2975 309.5306 273.6635 -7.7158 267.7370 275.4528 309.6757 274.4545 -7.7121 267.8877 275.5998 309.8204 275.2755 -7.7118 268.0729 275.7847 309.9791 276.0370 -7.7094 268.2326 275.9420 310.0917 276.8910 -7.7060 268.4183 276.1243 310.2531 277.6508 -7.7052 268.5610 276.2662 310.3836 278.4720 -7.7028 268.7208 276.4237 310.5385 279.2923 -7.7019 268.9196 276.6214 310.6611 280.0523 -7.6995 269.0758 276.7753 310.7949 280.9035 -7.6994 269.2490 276.9484 310.9442 281.6643 -7.7046 269.3832 277.0878 311.0874 282.4853 -7.7024 269.5629 277.2654 311.2281 283.2758 -7.6990 269.7184 277.4174 311.3858 284.0843 -7.6980 269.8925 277.5905 311.5228 284.8948 -7.7014 270.0552 277.7567 311.6530 285.6865 -7.6989 270.2167 277.9156 311.7857 286.5078 -7.6973 270.3902 278.0875 311.9293 287.2685 -7.6935 270.5300 278.2235 312.0560 288.1205 -7.6947 270.7089 278.4035 312.2134 288.8815 -7.6960 270.8664 278.5624 312.3501 289.7030 -7.6968 271.0443 278.7412 312.5037 290.5240 -7.6957 271.2024 278.8981 312.6360 291.2845 -7.6941 271.3671 279.0613 312.7687 292.1363 -7.6921 271.5327 279.2249 312.9298 292.8975 -7.6934 271.6807 279.3741 313.0504 293.7190 -7.6927 271.8504 279.5431 313.1944 294.5703 -7.6884 272.0341 279.7225 313.3300 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