DTA measure 1pb4 Test Date: 20231212:1220 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 897.83 s Mass = 1452.5 mg data_number = 1116 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2300 -6.4023 211.5043 217.9065 265.0069 2.0518 -6.4022 211.7261 218.1283 265.0525 2.8425 -6.4032 211.9282 218.3314 265.1036 3.6340 -6.4049 212.1346 218.5395 265.1398 4.4338 -6.4084 212.3458 218.7542 265.2084 5.2493 -6.4075 212.5524 218.9599 265.2578 6.0395 -6.4074 212.7660 219.1735 265.3259 6.8603 -6.4076 212.9742 219.3818 265.4092 7.6498 -6.4082 213.1641 219.5723 265.4722 8.4708 -6.4102 213.3655 219.7757 265.5486 9.2625 -6.4104 213.5723 219.9827 265.6282 10.0525 -6.4101 213.7882 220.1983 265.7083 10.8738 -6.4103 213.9976 220.4079 265.7867 11.6638 -6.4119 214.1824 220.5943 265.8767 12.4858 -6.4105 214.4104 220.8208 265.9830 13.2765 -6.4129 214.6026 221.0155 266.0948 14.0675 -6.4130 214.8035 221.2165 266.1733 14.8763 -6.4140 214.9890 221.4030 266.2819 15.6975 -6.4153 215.1778 221.5932 266.3963 16.4873 -6.4151 215.3865 221.8016 266.5222 17.3080 -6.4168 215.5897 222.0065 266.6223 18.0985 -6.4167 215.8045 222.2212 266.7388 18.8903 -6.4173 216.0037 222.4209 266.8670 19.7105 -6.4159 216.2068 222.6227 267.0035 20.5003 -6.4148 216.4036 222.8185 267.1143 21.3208 -6.4156 216.5936 223.0092 267.2473 22.1095 -6.4153 216.7930 223.2083 267.3934 22.8995 -6.4150 216.9891 223.4041 267.5249 23.7505 -6.4160 217.2022 223.6182 267.6822 24.5015 -6.4159 217.3785 223.7945 267.8035 25.2955 -6.4158 217.5904 224.0062 267.9501 26.1473 -6.4188 217.8007 224.2195 268.1043 26.9370 -6.4195 217.9900 224.4096 268.2352 27.7278 -6.4171 218.1779 224.5950 268.3834 28.5483 -6.4185 218.3901 224.8086 268.5282 29.3380 -6.4192 218.5844 225.0037 268.6612 30.1593 -6.4183 218.7771 225.1954 268.8259 30.9510 -6.4184 218.9621 225.3805 268.9799 31.7418 -6.4197 219.1649 225.5846 269.1024 32.5633 -6.4196 219.3651 225.7847 269.2451 33.3523 -6.4186 219.5453 225.9639 269.3814 34.1735 -6.4178 219.7519 226.1697 269.5351 34.9443 -6.4161 219.9350 226.3511 269.6759 35.7778 -6.4172 220.1407 226.5579 269.8264 36.5685 -6.4178 220.3328 226.7506 269.9621 37.3898 -6.4187 220.5299 226.9486 270.0921 38.1500 -6.4172 220.7161 227.1333 270.2109 39.0015 -6.4193 220.9212 227.3405 270.3430 39.7908 -6.4198 221.1031 227.5229 270.4797 40.5813 -6.4202 221.2848 227.7050 270.5915 41.4025 -6.4200 221.5018 227.9218 270.7133 42.1923 -6.4190 221.6942 228.1132 270.8324 43.0133 -6.4184 221.9002 228.3186 270.9518 43.8043 -6.4182 222.0903 228.5085 271.0667 44.5953 -6.4191 222.2784 228.6975 271.1869 45.4465 -6.4179 222.4911 228.9091 271.3103 46.2070 -6.4175 222.6745 229.0920 271.4017 47.0285 -6.4160 222.8603 229.2763 271.5063 47.8195 -6.4180 223.0413 229.4593 271.6076 48.6103 -6.4185 223.2168 229.6353 271.7250 49.4615 -6.4161 223.4194 229.8355 271.8343 50.2225 -6.4153 223.5992 230.0144 271.9397 51.0443 -6.4153 223.7982 230.2135 272.0372 51.8645 -6.4136 223.9904 230.4040 272.1453 52.6248 -6.4136 224.1738 230.5875 272.2268 53.4755 -6.4139 224.3764 230.7903 272.3494 54.2368 -6.4137 224.5442 230.9579 272.4159 55.0585 -6.4139 224.7519 231.1658 272.5112 55.8310 -6.4104 224.9267 231.3371 272.6013 56.6833 -6.4120 225.1225 231.5345 272.7171 57.4745 -6.4129 225.2984 231.7113 272.7973 58.2650 -6.4125 225.4974 231.9099 272.8862 59.0863 -6.4111 225.6859 232.0970 272.9880 59.8763 -6.4112 225.8761 232.2874 273.0681 60.6975 -6.4099 226.0727 232.4826 273.1521 61.4890 -6.4107 226.2489 232.6597 273.2474 62.2790 -6.4095 226.4330 232.8425 273.3381 63.0998 -6.4097 226.6195 233.0292 273.4336 63.8895 -6.4074 226.8004 233.2079 273.5163 64.7105 -6.4069 226.9846 233.3915 273.6132 65.5005 -6.4054 227.1662 233.5716 273.6938 66.2913 -6.4024 227.3586 233.7610 273.7870 67.1120 -6.4025 227.5543 233.9568 273.8692 67.9013 -6.4027 227.7229 234.1256 273.9555 68.7225 -6.4015 227.9068 234.3082 274.0592 69.5135 -6.3999 228.0845 234.4843 274.1387 70.3045 -6.3994 228.2758 234.6753 274.2325 71.1553 -6.4001 228.4724 234.8725 274.3178 71.9148 -6.3953 228.6341 235.0294 274.4162 72.7360 -6.3958 228.8187 235.2146 274.5054 73.5265 -6.3945 229.0028 235.3972 274.5903 74.3178 -6.3926 229.1759 235.5685 274.6916 75.1693 -6.3900 229.3816 235.7716 274.7980 75.9270 -6.3886 229.5443 235.9329 274.8817 76.7365 -6.3907 229.7231 236.1138 274.9855 77.5273 -6.3921 229.9008 236.2929 275.0715 78.3785 -6.3914 230.0934 236.4848 275.1822 79.1393 -6.3888 230.2603 236.6490 275.2845 79.9593 -6.3873 230.4383 236.8257 275.3951 80.7505 -6.3836 230.6169 237.0005 275.5126 81.5428 -6.3836 230.8017 237.1853 275.6090 82.3933 -6.3829 230.9977 237.3806 275.7178 83.1538 -6.3804 231.1419 237.5223 275.8081 83.9750 -6.3763 231.3356 237.7120 275.9235 84.7655 -6.3761 231.5018 237.8779 276.0273 85.5565 -6.3745 231.6771 238.0516 276.1267 86.3430 -6.3735 231.8587 238.2322 276.2245 87.1750 -6.3730 232.0365 238.4095 276.3496 87.9960 -6.3703 232.2213 238.5916 276.4592 88.7570 -6.3696 232.3944 238.7640 276.5517 89.6088 -6.3670 232.5707 238.9377 276.6806 90.3698 -6.3669 232.7487 239.1156 276.7953 91.1915 -6.3657 232.9294 239.2951 276.8921 91.9818 -6.3649 233.1016 239.4665 277.0052 92.7720 -6.3603 233.2668 239.6272 277.1050 93.6228 -6.3566 233.4560 239.8126 277.2395 94.3828 -6.3574 233.6188 239.9763 277.3459 95.2040 -6.3559 233.7986 240.1545 277.4524 95.9945 -6.3535 233.9744 240.3279 277.5575 96.7898 -6.3534 234.1416 240.4950 277.6738 97.6105 -6.3522 234.3125 240.6646 277.7867 98.3703 -6.3501 234.4612 240.8113 277.8942 99.2213 -6.3506 234.6480 240.9986 278.0009 100.0108 -6.3480 234.8249 241.1729 278.1105 100.8015 -6.3458 235.0032 241.3490 278.2154 101.6245 -6.3460 235.1789 241.5249 278.3468 102.3860 -6.3477 235.3263 241.6740 278.4614 103.2375 -6.3450 235.5136 241.8586 278.5726 103.9988 -6.3450 235.6937 242.0387 278.6859 104.8198 -6.3418 235.8735 242.2154 278.7950 105.6395 -6.3409 236.0403 242.3813 278.9379 106.4213 -6.3404 236.2084 242.5488 279.0570 107.2120 -6.3399 236.3569 242.6968 279.1589 108.0325 -6.3393 236.5323 242.8716 279.2753 108.8228 -6.3372 236.7108 243.0480 279.3763 109.6435 -6.3353 236.8866 243.2219 279.4874 110.4335 -6.3350 237.0573 243.3923 279.6052 111.2235 -6.3326 237.2123 243.5448 279.7261 112.0440 -6.3300 237.3858 243.7158 279.8603 112.8335 -6.3276 237.5510 243.8785 279.9597 113.6548 -6.3275 237.7234 244.0509 280.0759 114.4460 -6.3272 237.8948 244.2220 280.1929 115.2375 -6.3259 238.0638 244.3897 280.2839 116.0588 -6.3261 238.2331 244.5591 280.4089 116.8215 -6.3229 238.3885 244.7114 280.5237 117.6745 -6.3232 238.5654 244.8886 280.6487 118.4355 -6.3241 238.7209 245.0450 280.7575 119.2570 -6.3232 238.8966 245.2198 280.8891 120.0760 -6.3216 239.0657 245.3872 280.9912 120.8353 -6.3215 239.2312 245.5527 281.0941 121.6925 -6.3211 239.3968 245.7179 281.2259 122.4528 -6.3203 239.5565 245.8768 281.3512 123.2728 -6.3169 239.7217 246.0386 281.4603 124.0925 -6.3139 239.8886 246.2025 281.5747 124.8530 -6.3137 240.0490 246.3627 281.6628 125.7025 -6.3125 240.2248 246.5373 281.8038 126.4620 -6.3101 240.3781 246.6881 281.9017 127.3153 -6.3112 240.5585 246.8697 282.0063 128.0563 -6.3125 240.6968 247.0093 282.1034 128.9073 -6.3113 240.8771 247.1884 282.2200 129.6965 -6.3080 241.0478 247.3559 282.3243 130.4873 -6.3086 241.2173 247.5259 282.4437 131.3075 -6.3083 241.3760 247.6843 282.5285 132.0683 -6.3076 241.5331 247.8407 282.6256 132.9193 -6.3087 241.7122 248.0210 282.7448 133.7095 -6.3081 241.8619 248.1700 282.8428 134.5005 -6.3052 242.0180 248.3232 282.9336 135.3198 -6.3038 242.1860 248.4898 283.0210 136.1098 -6.3035 242.3458 248.6493 283.1436 136.9300 -6.3048 242.5195 248.8243 283.2385 137.7205 -6.3040 242.6675 248.9714 283.3320 138.5108 -6.3034 242.8406 249.1440 283.4145 139.3318 -6.3028 243.0097 249.3125 283.5129 140.1210 -6.3010 243.1424 249.4434 283.6078 140.9425 -6.3008 243.3196 249.6204 283.6809 141.7330 -6.2981 243.4827 249.7808 283.7733 142.5238 -6.2966 243.6399 249.9365 283.8691 143.3450 -6.2972 243.8106 250.1077 283.9718 144.1343 -6.2950 243.9535 250.2485 284.0557 144.9558 -6.2939 244.1098 250.4037 284.1543 145.7468 -6.2918 244.2685 250.5603 284.2494 146.5370 -6.2929 244.4287 250.7215 284.3638 147.3693 -6.2921 244.6045 250.8966 284.4514 148.1703 -6.2914 244.7610 251.0524 284.5588 148.9595 -6.2889 244.9054 251.1943 284.6429 149.7503 -6.2891 245.0688 251.3580 284.7414 150.5710 -6.2880 245.2369 251.5249 284.8401 151.3615 -6.2864 245.3996 251.6860 284.9466 152.1833 -6.2853 245.5512 251.8365 285.0588 152.9743 -6.2866 245.7076 251.9943 285.1540 153.7640 -6.2842 245.8533 252.1375 285.2536 154.5845 -6.2825 246.0227 252.3052 285.3773 155.3743 -6.2803 246.1815 252.4617 285.4787 156.1953 -6.2779 246.3416 252.6195 285.5903 156.9858 -6.2764 246.4882 252.7646 285.7055 157.8795 -6.2753 246.6644 252.9397 285.8159 158.8035 -6.2752 246.8489 253.1241 285.9418 159.5933 -6.2744 246.9921 253.2664 286.0535 160.4133 -6.2730 247.1562 253.4291 286.1705 161.2038 -6.2703 247.3006 253.5709 286.2597 161.9953 -6.2692 247.4531 253.7223 286.3832 162.8165 -6.2692 247.6163 253.8855 286.4956 163.6070 -6.2689 247.7743 254.0432 286.6083 164.4273 -6.2658 247.9305 254.1963 286.7192 165.2175 -6.2655 248.0757 254.3412 286.8206 166.0075 -6.2655 248.2245 254.4900 286.9321 166.8593 -6.2644 248.3849 254.6493 287.0479 167.6200 -6.2638 248.5336 254.7974 287.1596 168.4670 -6.2638 248.7142 254.9780 287.2785 169.2263 -6.2602 248.8537 255.1139 287.3871 170.0460 -6.2604 249.0141 255.2746 287.5017 170.8658 -6.2605 249.1705 255.4310 287.6086 171.6250 -6.2595 249.3048 255.5643 287.7221 172.4758 -6.2605 249.4840 255.7445 287.8340 173.2358 -6.2592 249.6351 255.8942 287.9538 174.0570 -6.2586 249.7823 256.0409 288.0671 174.8765 -6.2572 249.9291 256.1863 288.1730 175.6373 -6.2557 250.0701 256.3258 288.2888 176.4878 -6.2559 250.2264 256.4823 288.4053 177.2788 -6.2533 250.3650 256.6182 288.5077 178.0715 -6.2538 250.5129 256.7667 288.6089 178.8943 -6.2521 250.6902 256.9423 288.7355 179.6538 -6.2510 250.8300 257.0810 288.8558 180.5045 -6.2483 250.9944 257.2427 288.9814 181.2945 -6.2466 251.1499 257.3965 289.0880 182.0853 -6.2477 251.2868 257.5345 289.1971 182.9065 -6.2447 251.4536 257.6983 289.3068 183.6960 -6.2441 251.6012 257.8453 289.4211 184.5165 -6.2462 251.7520 257.9982 289.5449 185.3065 -6.2447 251.9027 258.1474 289.6541 186.0973 -6.2423 252.0541 258.2964 289.7653 186.9485 -6.2421 252.1974 258.4395 289.8858 187.7100 -6.2407 252.3416 258.5823 289.9917 188.5560 -6.2389 252.5067 258.7456 290.1104 189.3118 -6.2374 252.6562 258.8936 290.2418 190.1633 -6.2392 252.8056 259.0448 290.3475 190.9243 -6.2381 252.9381 259.1762 290.4491 191.7450 -6.2382 253.0917 259.3299 290.5632 192.5353 -6.2372 253.2434 259.4806 290.6622 193.3255 -6.2372 253.3913 259.6286 290.7863 194.1765 -6.2378 253.5388 259.7766 290.8986 194.9358 -6.2351 253.6800 259.9151 291.0191 195.7570 -6.2361 253.8376 260.0737 291.1356 196.5765 -6.2353 253.9952 260.2305 291.2333 197.3370 -6.2352 254.1292 260.3645 291.3461 198.1878 -6.2366 254.2868 260.5233 291.4566 198.9823 -6.2352 254.4371 260.6723 291.5669 199.7623 -6.2327 254.5891 260.8218 291.6688 200.5823 -6.2322 254.7311 260.9633 291.7722 201.3718 -6.2333 254.8731 261.1064 291.8772 202.1618 -6.2319 255.0204 261.2523 291.9829 203.0133 -6.2296 255.1673 261.3969 292.0848 203.7738 -6.2303 255.3135 261.5438 292.1720 204.5950 -6.2326 255.4524 261.6850 292.2597 205.3865 -6.2314 255.6135 261.8450 292.3591 206.1770 -6.2322 255.7562 261.9884 292.4481 207.0280 -6.2286 255.9059 262.1345 292.5475 207.7888 -6.2289 256.0551 262.2840 292.6335 208.6105 -6.2266 256.1976 262.4242 292.7190 209.4255 -6.2272 256.3359 262.5631 292.8265 210.2153 -6.2289 256.4899 262.7188 292.9219 211.0058 -6.2270 256.6160 262.8430 293.0105 211.8255 -6.2281 256.7596 262.9877 293.0878 212.6163 -6.2244 256.9049 263.1293 293.1856 213.4373 -6.2239 257.0548 263.2787 293.2865 214.2273 -6.2236 257.1961 263.4197 293.3626 215.0178 -6.2246 257.3204 263.5450 293.4657 215.8683 -6.2233 257.4806 263.7039 293.5785 216.6273 -6.2212 257.6281 263.8493 293.6665 217.4475 -6.2214 257.7810 264.0025 293.7670 218.2388 -6.2206 257.9373 264.1579 293.8642 219.0280 -6.2211 258.0730 264.2941 293.9640 219.8795 -6.2197 258.2241 264.4437 294.0678 220.6388 -6.2194 258.3546 264.5740 294.1790 221.4590 -6.2188 258.4987 264.7175 294.2740 222.2788 -6.2162 258.6458 264.8620 294.3768 223.0385 -6.2169 258.7776 264.9945 294.4730 223.8898 -6.2177 258.9420 265.1597 294.5811 224.6493 -6.2170 259.0756 265.2926 294.6708 225.4700 -6.2169 259.2242 265.4411 294.7659 226.2895 -6.2145 259.3613 265.5758 294.8856 227.0510 -6.2153 259.4990 265.7143 294.9831 227.9025 -6.2160 259.6416 265.8576 295.0959 228.6628 -6.2128 259.7762 265.9890 295.1941 229.5123 -6.2117 259.9301 266.1418 295.3008 230.2705 -6.2092 260.0550 266.2642 295.4122 231.1223 -6.2096 260.2095 266.4191 295.5321 231.8823 -6.2103 260.3400 266.5503 295.6251 232.7035 -6.2077 260.4776 266.6854 295.7387 233.4945 -6.2102 260.6151 266.8253 295.8447 234.2858 -6.2106 260.7594 266.9700 295.9417 235.1075 -6.2079 260.9110 267.1189 296.0649 235.8995 -6.2086 261.0507 267.2593 296.1597 236.7215 -6.2087 261.1755 267.3842 296.2587 237.5118 -6.2094 261.3154 267.5248 296.3662 238.3028 -6.2099 261.4607 267.6706 296.4885 239.1220 -6.2064 261.5950 267.8014 296.6024 239.9418 -6.2066 261.7411 267.9478 296.6948 240.6920 -6.2100 261.8628 268.0728 296.7921 241.5438 -6.2093 262.0086 268.2178 296.9014 242.3038 -6.2074 262.1456 268.3530 297.0137 243.1240 -6.2075 262.2946 268.5021 297.1322 243.9155 -6.2081 262.4288 268.6369 297.2284 244.7055 -6.2084 262.5696 268.7780 297.3353 245.5570 -6.2065 262.7054 268.9118 297.4488 246.3163 -6.2075 262.8644 269.0718 297.5608 247.1378 -6.2076 263.0003 269.2079 297.6812 247.9288 -6.2070 263.1255 269.3325 297.7796 248.7190 -6.2050 263.2539 269.4589 297.8745 249.5693 -6.2063 263.4235 269.6298 297.9954 250.5348 -6.2044 263.5564 269.7608 298.1127 251.3560 -6.2049 263.6947 269.8996 298.2343 252.1450 -6.2072 263.8415 270.0487 298.3493 252.9363 -6.2077 263.9816 270.1893 298.4479 253.7575 -6.2084 264.1196 270.3279 298.5666 254.5180 -6.2066 264.2606 270.4673 298.6634 255.3695 -6.2047 264.4102 270.6149 298.7834 256.1598 -6.2074 264.5350 270.7424 298.8893 256.9513 -6.2075 264.6653 270.8728 298.9870 257.7725 -6.2084 264.8119 271.0203 299.1053 258.5340 -6.2076 264.9424 271.1500 299.2014 259.3853 -6.2057 265.0780 271.2837 299.3181 260.1748 -6.2066 265.2189 271.4254 299.4188 260.9660 -6.2055 265.3643 271.5698 299.5223 261.7865 -6.2048 265.5024 271.7071 299.6406 262.5480 -6.2074 265.6156 271.8230 299.7296 263.3993 -6.2075 265.7550 271.9625 299.8420 264.1598 -6.2061 265.8861 272.0922 299.9454 264.9810 -6.2062 266.0173 272.2235 300.0422 265.8015 -6.2060 266.1588 272.3648 300.1582 266.5615 -6.2068 266.2991 272.5058 300.2533 267.4123 -6.2085 266.4511 272.6596 300.3783 268.1730 -6.2094 266.5692 272.7786 300.4720 268.9940 -6.2106 266.6969 272.9076 300.5901 269.8145 -6.2110 266.8338 273.0447 300.6895 270.5753 -6.2103 266.9625 273.1728 300.7981 271.4258 -6.2084 267.1088 273.3172 300.9124 272.1860 -6.2088 267.2458 273.4546 301.0169 273.0070 -6.2101 267.3782 273.5884 301.1153 273.8280 -6.2095 267.5063 273.7158 301.2283 274.5883 -6.2080 267.6372 273.8452 301.3307 275.4400 -6.2103 267.7729 273.9832 301.4435 276.2018 -6.2091 267.9008 274.1099 301.5385 277.0240 -6.2111 268.0314 274.2425 301.6523 277.8158 -6.2110 268.1701 274.3810 301.7445 278.6068 -6.2100 268.2985 274.5084 301.8650 279.4578 -6.2085 268.4340 274.6426 301.9665 280.2185 -6.2087 268.5662 274.7749 302.0582 281.2258 -6.2098 268.7403 274.9500 302.1759 282.0465 -6.2125 268.8758 275.0882 302.2891 282.8375 -6.2119 269.0022 275.2141 302.3991 283.6595 -6.2111 269.1426 275.3537 302.5082 284.4508 -6.2121 269.2732 275.4854 302.6173 285.2423 -6.2124 269.4082 275.6206 302.7210 286.0635 -6.2136 269.5417 275.7552 302.8207 286.8540 -6.2141 269.6642 275.8783 302.9200 287.6755 -6.2158 269.7987 276.0145 303.0316 288.4675 -6.2167 269.9263 276.1430 303.1267 289.2588 -6.2193 270.0826 276.3019 303.2317 290.0795 -6.2194 270.2146 276.4340 303.3482 290.8405 -6.2189 270.3448 276.5637 303.4409 291.6918 -6.2193 270.4745 276.6938 303.5525 292.4835 -6.2168 270.6034 276.8202 303.6461 293.2755 -6.2177 270.7296 276.9474 303.7450 294.0965 -6.2192 270.8618 277.0809 303.8477 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