DTA measure 1lassumeres Date: 2024312:1548 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.65 s Mass = 100.000 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2585 -0.8430 250.1821 251.0251 266.1593 2.0473 -0.8340 250.2963 251.1304 266.1806 2.8378 -0.8284 250.4327 251.2611 266.1831 3.6590 -0.8237 250.5633 251.3871 266.2039 4.4205 -0.8188 250.6827 251.5015 266.2132 5.2725 -0.8110 250.8367 251.6477 266.2288 6.0335 -0.8050 250.9600 251.7651 266.2420 6.8555 -0.7988 251.0911 251.8899 266.2888 7.6778 -0.7936 251.2161 252.0097 266.3177 8.4395 -0.7882 251.3316 252.1198 266.3323 9.2915 -0.7835 251.4652 252.2488 266.3992 10.0535 -0.7748 251.5875 252.3623 266.4246 10.8765 -0.7675 251.7180 252.4855 266.4827 11.6988 -0.7648 251.8318 252.5966 266.5375 12.4605 -0.7575 251.9784 252.7359 266.5919 13.3125 -0.7516 252.0956 252.8471 266.6537 14.0745 -0.7495 252.2110 252.9604 266.7307 14.8965 -0.7444 252.3629 253.1073 266.8186 15.7185 -0.7373 252.4771 253.2144 266.9019 16.4805 -0.7360 252.5927 253.3287 267.0055 17.3325 -0.7301 252.7241 253.4542 267.0967 18.1245 -0.7247 252.8564 253.5810 267.1903 18.9175 -0.7191 252.9739 253.6931 267.2890 19.7398 -0.7142 253.1012 253.8154 267.4033 20.5020 -0.7105 253.2201 253.9307 267.5014 21.3540 -0.7060 253.3398 254.0458 267.6196 22.1463 -0.7031 253.4695 254.1725 267.7646 22.9375 -0.6986 253.5966 254.2952 267.8775 23.7613 -0.6942 253.7385 254.4327 267.9862 24.5248 -0.6902 253.8530 254.5433 268.1125 25.3768 -0.6857 253.9849 254.6707 268.2284 26.1688 -0.6832 254.0991 254.7822 268.3642 26.9605 -0.6820 254.2035 254.8855 268.4855 27.7825 -0.6772 254.3371 255.0142 268.6197 28.5410 -0.6717 254.4496 255.1212 268.7466 29.3900 -0.6684 254.5718 255.2402 268.8627 30.1780 -0.6656 254.6932 255.3588 268.9975 30.9660 -0.6634 254.8258 255.4892 269.1413 31.7848 -0.6648 254.9590 255.6237 269.2679 32.5430 -0.6627 255.0695 255.7321 269.3878 33.3910 -0.6566 255.1998 255.8564 269.5063 34.1793 -0.6563 255.3196 255.9759 269.6367 34.9680 -0.6512 255.4481 256.0993 269.7565 35.7883 -0.6503 255.5563 256.2065 269.8756 36.5490 -0.6488 255.6762 256.3250 270.0026 37.4000 -0.6468 255.8112 256.4580 270.1175 38.1600 -0.6462 255.9394 256.5856 270.2254 38.9818 -0.6453 256.0763 256.7216 270.3300 39.8038 -0.6434 256.1878 256.8312 270.4394 40.5655 -0.6431 256.3153 256.9584 270.5396 41.4178 -0.6417 256.4186 257.0603 270.6588 42.1795 -0.6359 256.5355 257.1713 270.7525 43.0018 -0.6350 256.6653 257.3003 270.8856 43.7938 -0.6314 256.7849 257.4163 270.9747 44.5855 -0.6310 256.9144 257.5454 271.0800 45.4378 -0.6262 257.0350 257.6612 271.1790 46.1995 -0.6250 257.1619 257.7868 271.3050 47.0218 -0.6271 257.2818 257.9089 271.4125 47.8138 -0.6264 257.3822 258.0086 271.5019 48.6055 -0.6224 257.5115 258.1338 271.5978 49.4575 -0.6205 257.6212 258.2417 271.7309 50.2195 -0.6216 257.7468 258.3683 271.8422 51.0415 -0.6210 257.8742 258.4951 271.9335 51.8335 -0.6197 257.9938 258.6134 272.0176 52.6255 -0.6202 258.1149 258.7351 272.1241 53.4780 -0.6188 258.2644 258.8832 272.2308 54.2405 -0.6182 258.3752 258.9934 272.3212 55.0635 -0.6147 258.4852 259.0999 272.4278 55.8555 -0.6107 258.6018 259.2125 272.5173 56.6475 -0.6134 258.7242 259.3376 272.6359 57.4715 -0.6146 258.8435 259.4581 272.7387 58.2635 -0.6132 258.9682 259.5814 272.8392 59.0863 -0.6120 259.0975 259.7095 272.9403 59.8783 -0.6114 259.2119 259.8233 273.0444 60.6665 -0.6130 259.3349 259.9479 273.1537 61.4848 -0.6126 259.4471 260.0596 273.2558 62.2725 -0.6115 259.5663 260.1778 273.3253 63.0908 -0.6138 259.6887 260.3025 273.4260 63.8790 -0.6098 259.8236 260.4334 273.5371 64.6670 -0.6105 259.9346 260.5451 273.6314 65.5158 -0.6097 260.0548 260.6646 273.7393 66.2750 -0.6090 260.1710 260.7800 273.8285 67.0938 -0.6103 260.2930 260.9034 273.9357 67.9123 -0.6089 260.4102 261.0191 274.0254 68.6710 -0.6089 260.5261 261.1350 274.1147 69.5215 -0.6087 260.6426 261.2513 274.2218 70.2835 -0.6105 260.7696 261.3802 274.3128 71.1055 -0.6106 260.8826 261.4932 274.4303 71.9275 -0.6105 260.9994 261.6099 274.5124 72.6895 -0.6113 261.1178 261.7291 274.6126 73.5425 -0.6130 261.2541 261.8671 274.7238 74.3043 -0.6112 261.3681 261.9793 274.8245 75.1265 -0.6122 261.4823 262.0945 274.9200 75.9485 -0.6132 261.6225 262.2357 275.0187 76.7103 -0.6137 261.7344 262.3481 275.1279 77.5623 -0.6142 261.8369 262.4510 275.2317 78.3243 -0.6155 261.9625 262.5780 275.3307 79.1458 -0.6109 262.1003 262.7113 275.4289 79.9683 -0.6135 262.2143 262.8278 275.5199 80.7295 -0.6148 262.3247 262.9395 275.6423 81.5818 -0.6189 262.4470 263.0660 275.7670 82.3738 -0.6170 262.5616 263.1786 275.8851 83.1655 -0.6164 262.6684 263.2848 275.9895 83.9878 -0.6167 262.8091 263.4259 276.1020 84.7795 -0.6208 262.9130 263.5338 276.2081 85.6018 -0.6220 263.0433 263.6653 276.3335 86.3938 -0.6214 263.1626 263.7840 276.4581 87.1865 -0.6238 263.2782 263.9020 276.5775 88.0088 -0.6238 263.3787 264.0025 276.6934 88.7705 -0.6258 263.5139 264.1397 276.8095 89.6233 -0.6278 263.6516 264.2794 276.9259 90.4158 -0.6293 263.7537 264.3830 277.0448 91.2085 -0.6308 263.8689 264.4996 277.1681 92.0298 -0.6325 263.9949 264.6275 277.2949 92.7880 -0.6317 264.1053 264.7370 277.4088 93.6360 -0.6319 264.2327 264.8645 277.5326 94.4240 -0.6333 264.3423 264.9755 277.6345 95.2120 -0.6356 264.4623 265.0980 277.7605 96.0313 -0.6401 264.5769 265.2170 277.8694 96.7900 -0.6400 264.6982 265.3382 277.9635 97.6398 -0.6397 264.8133 265.4530 278.0863 98.4285 -0.6432 264.9307 265.5739 278.1904 99.2183 -0.6456 265.0393 265.6848 278.2794 100.0383 -0.6470 265.1728 265.8198 278.3794 100.7983 -0.6467 265.2985 265.9453 278.4725 101.6498 -0.6494 265.4116 266.0611 278.5856 102.4115 -0.6466 265.5150 266.1616 278.6858 103.2335 -0.6507 265.6415 266.2922 278.7703 104.0558 -0.6539 265.7556 266.4095 278.8831 104.8175 -0.6550 265.8707 266.5257 278.9829 105.6698 -0.6561 265.9860 266.6421 279.0951 106.4315 -0.6590 266.0992 266.7582 279.1886 107.2538 -0.6600 266.2342 266.8942 279.2987 108.0455 -0.6641 266.3491 267.0132 279.3896 108.8375 -0.6622 266.4668 267.1290 279.4776 109.6895 -0.6638 266.6069 267.2707 279.5816 110.4515 -0.6659 266.7075 267.3735 279.6727 111.2735 -0.6660 266.8335 267.4996 279.7664 112.0655 -0.6675 266.9466 267.6141 279.8544 112.8575 -0.6669 267.0696 267.7365 279.9432 113.6795 -0.6683 267.1945 267.8628 280.0312 114.4715 -0.6690 267.3061 267.9750 280.1323 115.2935 -0.6708 267.4242 268.0951 280.2293 116.0855 -0.6705 267.5488 268.2193 280.3363 116.8785 -0.6735 267.6681 268.3416 280.4257 117.7005 -0.6753 267.7759 268.4512 280.5324 118.4923 -0.6783 267.8869 268.5652 280.6490 119.3148 -0.6809 268.0053 268.6862 280.7659 120.1075 -0.6813 268.1159 268.7972 280.8825 120.9005 -0.6825 268.2262 268.9088 281.0016 121.7230 -0.6865 268.3564 269.0429 281.1105 122.5145 -0.6896 268.4773 269.1669 281.2084 123.3375 -0.6873 268.5965 269.2838 281.3209 124.1288 -0.6889 268.7090 269.3979 281.4342 124.9173 -0.6899 268.8344 269.5243 281.5570 125.7393 -0.6926 268.9566 269.6491 281.6743 126.4970 -0.6962 269.0682 269.7644 281.7818 127.3453 -0.6956 269.1683 269.8639 281.9015 128.1338 -0.6967 269.2904 269.9870 282.0152 128.9235 -0.7057 269.4086 270.1143 282.1220 129.7415 -0.7127 269.5166 270.2293 282.2478 130.5300 -0.7397 269.6529 270.3926 282.3649 131.3498 -0.7352 269.7660 270.5013 282.4923 132.1388 -0.7268 269.8784 270.6052 282.6127 132.9295 -0.7259 270.0006 270.7264 282.7168 133.7510 -0.7320 270.1210 270.8530 282.8303 134.5425 -0.7529 270.2407 270.9936 282.9511 135.3648 -0.8088 270.3510 271.1598 283.0672 136.1573 -0.7972 270.4882 271.2855 283.1635 136.9488 -0.7533 270.5788 271.3321 283.2856 137.7708 -0.7245 270.7216 271.4461 283.4036 138.5625 -0.7195 270.8364 271.5559 283.4933 139.3848 -0.7197 270.9530 271.6727 283.5980 140.1768 -0.7233 271.0411 271.7643 283.6944 140.9685 -0.7250 271.1664 271.8913 283.7997 141.7908 -0.7270 271.2894 272.0164 283.9147 142.5825 -0.7270 271.4055 272.1325 284.0028 143.4048 -0.7228 271.5176 272.2405 284.0844 144.1968 -0.7211 271.6338 272.3549 284.1850 144.9885 -0.7168 271.7649 272.4817 284.2732 145.8108 -0.7178 271.8680 272.5858 284.3464 146.6025 -0.7250 271.9831 272.7081 284.4509 147.4248 -0.7320 272.1023 272.8342 284.5431 148.2168 -0.7340 272.2203 272.9544 284.6400 149.0085 -0.7376 272.3332 273.0709 284.7306 149.8608 -0.7384 272.4696 273.2080 284.8310 150.6225 -0.7400 272.5625 273.3025 284.9194 151.4453 -0.7456 272.6886 273.4342 285.0258 152.2675 -0.7485 272.8080 273.5565 285.1445 153.0298 -0.7484 272.9308 273.6792 285.2396 153.8820 -0.7520 273.0677 273.8196 285.3433 154.6445 -0.7528 273.1673 273.9201 285.4395 155.4675 -0.7593 273.2793 274.0386 285.5438 156.2895 -0.7623 273.4017 274.1640 285.6478 157.0505 -0.7647 273.5040 274.2687 285.7748 157.8990 -0.7657 273.6398 274.4055 285.8743 158.6565 -0.7696 273.7419 274.5115 285.9819 159.4748 -0.7716 273.8620 274.6337 286.0890 160.2930 -0.7747 273.9871 274.7618 286.1955 161.0510 -0.7790 274.0952 274.8742 286.2942 161.8995 -0.7815 274.2114 274.9929 286.4072 162.6580 -0.7884 274.3302 275.1186 286.5093 163.4778 -0.7897 274.4358 275.2255 286.6291 164.2963 -0.7868 274.5437 275.3305 286.7494 165.0558 -0.7892 274.6659 275.4551 286.8435 165.9065 -0.7897 274.7857 275.5754 286.9526 166.6675 -0.7935 274.9066 275.7001 287.0529 167.4895 -0.7931 275.0220 275.8151 287.1754 168.2815 -0.7968 275.1290 275.9258 287.2839 169.0735 -0.7987 275.2412 276.0398 287.3992 169.8970 -0.8019 275.3679 276.1699 287.5071 170.6905 -0.8056 275.4840 276.2896 287.6103 171.5125 -0.8110 275.6087 276.4197 287.7251 172.3045 -0.8112 275.7177 276.5289 287.8430 173.0965 -0.8110 275.8460 276.6569 287.9497 173.9185 -0.8109 275.9571 276.7680 288.0552 174.6805 -0.8128 276.0593 276.8721 288.1673 175.5323 -0.8120 276.1898 277.0018 288.2665 176.2940 -0.8139 276.3070 277.1209 288.3739 177.1160 -0.8184 276.4077 277.2261 288.4798 177.9388 -0.8243 276.5249 277.3492 288.5824 178.7008 -0.8286 276.6395 277.4681 288.6971 179.5530 -0.8290 276.7702 277.5992 288.8146 180.3145 -0.8327 276.8767 277.7094 288.9260 181.1375 -0.8364 277.0136 277.8500 289.0372 181.9598 -0.8380 277.1191 277.9571 289.1435 182.7215 -0.8413 277.2317 278.0731 289.2365 183.5743 -0.8446 277.3691 278.2137 289.3480 184.3365 -0.8464 277.4625 278.3089 289.4491 185.1595 -0.8500 277.5770 278.4270 289.5605 185.9518 -0.8533 277.7083 278.5615 289.6874 186.7435 -0.8542 277.8339 278.6881 289.7871 187.5963 -0.8574 277.9331 278.7904 289.9136 188.3585 -0.8613 278.0347 278.8960 290.0182 189.1800 -0.8618 278.1603 279.0220 290.1203 189.9680 -0.8639 278.2775 279.1414 290.2288 190.7560 -0.8658 278.3915 279.2573 290.3413 191.5750 -0.8640 278.5235 279.3875 290.4550 192.3640 -0.8603 278.6276 279.4879 290.5401 193.1830 -0.8563 278.7591 279.6154 290.6518 193.9715 -0.8570 278.8607 279.7177 290.7608 194.7613 -0.8578 278.9543 279.8120 290.8631 195.6115 -0.8599 279.0823 279.9422 290.9809 196.3703 -0.8637 279.2067 280.0704 291.0838 197.1900 -0.8640 279.3261 280.1901 291.1844 197.9820 -0.8710 279.4243 280.2953 291.2810 198.7735 -0.8729 279.5425 280.4154 291.3834 199.5955 -0.8757 279.6729 280.5486 291.4759 200.3875 -0.8765 279.7770 280.6535 291.5877 201.2098 -0.8849 279.9066 280.7915 291.6920 202.0018 -0.8829 280.0235 280.9064 291.8008 202.7935 -0.8825 280.1377 281.0202 291.9093 203.6158 -0.8859 280.2537 281.1395 292.0078 204.4075 -0.8849 280.3592 281.2441 292.0992 205.2298 -0.8879 280.4808 281.3687 292.2292 206.0215 -0.8911 280.5897 281.4808 292.3325 206.8160 -0.8977 280.7077 281.6054 292.4210 207.6435 -0.9009 280.8348 281.7358 292.5281 208.4055 -0.9008 280.9462 281.8470 292.6356 209.2575 -0.9038 281.0784 281.9823 292.7483 210.0495 -0.9064 281.1893 282.0957 292.8483 210.8415 -0.9066 281.2876 282.1942 292.9428 211.6635 -0.9047 281.4047 282.3094 293.0463 212.4255 -0.9076 281.5224 282.4300 293.1553 213.2775 -0.9120 281.6573 282.5693 293.2727 214.0695 -0.9135 281.7575 282.6709 293.3527 214.8615 -0.9164 281.8630 282.7794 293.4696 215.6833 -0.9182 281.9736 282.8918 293.5676 216.4753 -0.9212 282.0975 283.0187 293.6773 217.2968 -0.9232 282.2211 283.1443 293.7830 218.0893 -0.9265 282.3416 283.2681 293.8879 218.8805 -0.9298 282.4643 283.3941 293.9889 219.7328 -0.9331 282.5696 283.5027 294.0867 220.4948 -0.9334 282.6923 283.6258 294.1883 221.3150 -0.9344 282.8033 283.7377 294.2941 222.1033 -0.9370 282.9024 283.8395 294.3828 222.8910 -0.9398 283.0210 283.9608 294.4842 223.7390 -0.9438 283.1457 284.0895 294.5948 224.4973 -0.9460 283.2646 284.2106 294.6838 225.3163 -0.9468 283.3668 284.3135 294.7730 226.1348 -0.9509 283.4789 284.4297 294.8843 226.8940 -0.9514 283.5945 284.5459 294.9737 227.7430 -0.9525 283.7304 284.6830 295.0560 228.5015 -0.9547 283.8361 284.7908 295.1694 229.3210 -0.9555 283.9396 284.8951 295.2765 230.1410 -0.9572 284.0560 285.0132 295.3749 230.9023 -0.9623 284.1803 285.1426 295.4770 231.7540 -0.9680 284.3102 285.2782 295.5610 232.5158 -0.9710 284.4078 285.3789 295.6571 233.3378 -0.9725 284.5107 285.4832 295.7548 234.1320 -0.9739 284.6374 285.6113 295.8525 234.9248 -0.9732 284.7483 285.7215 295.9450 235.7768 -0.9750 284.8737 285.8487 296.0410 236.5388 -0.9759 284.9843 285.9602 296.1501 237.3608 -0.9809 285.1064 286.0873 296.2532 238.1530 -0.9796 285.2222 286.2018 296.3462 238.9445 -0.9822 285.3396 286.3218 296.4452 239.7668 -0.9982 285.4400 286.4381 296.5804 240.5585 -1.0039 285.5537 286.5576 296.6794 241.3808 -1.0153 285.6733 286.6886 296.7943 242.1728 -1.0154 285.7920 286.8074 296.9167 242.9645 -1.0022 285.9102 286.9124 296.9964 243.7868 -1.0004 286.0403 287.0407 297.1330 244.5785 -1.0021 286.1528 287.1549 297.2394 245.4008 -1.0031 286.2613 287.2644 297.3416 246.1928 -1.0069 286.3665 287.3734 297.4569 246.9855 -1.0080 286.4781 287.4861 297.5753 247.8080 -1.0126 286.5835 287.5961 297.6969 248.5705 -1.0161 286.7122 287.7283 297.8088 249.4225 -1.0180 286.8502 287.8682 297.9237 250.2145 -1.0233 286.9535 287.9768 298.0370 251.0065 -1.0262 287.0759 288.1021 298.1562 251.8288 -1.0284 287.1851 288.2135 298.2795 252.5915 -1.0307 287.2862 288.3170 298.3860 253.4420 -1.0323 287.4161 288.4484 298.5193 254.1998 -1.0350 287.5258 288.5609 298.6313 255.0178 -1.0399 287.6347 288.6746 298.7388 255.8360 -1.0433 287.7533 288.7966 298.8555 256.5940 -1.0433 287.8600 288.9033 298.9676 257.4420 -1.0461 287.9762 289.0224 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