DTA measure 1masodikmeres Date: 2024312:1216 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1136.08 s Mass = 1129.200 mg data_number = 1400 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2425 -1.4563 227.4618 228.9181 261.3816 2.0345 -1.4554 227.5938 229.0492 261.3699 2.8565 -1.4493 227.7513 229.2007 261.3602 3.6485 -1.4495 227.8755 229.3250 261.3349 4.4420 -1.4464 227.9945 229.4408 261.3282 5.2683 -1.4426 228.1498 229.5924 261.3332 6.0903 -1.4434 228.2669 229.7103 261.3377 6.8800 -1.4428 228.3866 229.8294 261.3373 7.7023 -1.4434 228.5066 229.9500 261.3570 8.4923 -1.4461 228.6424 230.0885 261.3443 9.3128 -1.4444 228.8031 230.2476 261.3480 10.1048 -1.4412 228.9177 230.3589 261.4015 10.8955 -1.4429 229.0457 230.4886 261.4229 11.7195 -1.4203 229.1790 230.5993 261.4701 12.4798 -1.4213 229.2861 230.7073 261.5119 13.3318 -1.4245 229.4385 230.8629 261.5747 14.1220 -1.4229 229.5658 230.9887 261.6224 14.9133 -1.4204 229.6925 231.1129 261.6732 15.7350 -1.4165 229.8118 231.2283 261.7470 16.4955 -1.4172 229.9110 231.3283 261.8195 17.3478 -1.4144 230.0604 231.4748 261.9235 18.1095 -1.4084 230.2069 231.6153 261.9921 19.1020 -1.4021 230.3332 231.7353 262.0970 19.9533 -1.4019 230.4856 231.8874 262.2324 20.7145 -1.4058 230.6123 232.0181 262.3358 21.5358 -1.4069 230.7173 232.1242 262.4354 22.3565 -1.4071 230.8573 232.2644 262.5687 23.1175 -1.4079 230.9913 232.3992 262.6753 23.9683 -1.4060 231.1071 232.5132 262.8235 24.7588 -1.4024 231.2303 232.6327 262.9605 25.5498 -1.3967 231.3721 232.7688 263.0852 26.3705 -1.4011 231.5034 232.9045 263.2261 27.1310 -1.3929 231.6032 232.9962 263.3442 27.9825 -1.3711 231.7455 233.1166 263.5095 28.7450 -1.3982 231.8776 233.2758 263.6549 29.5723 -1.4083 232.0034 233.4116 263.8037 30.3633 -1.4098 232.1344 233.5442 263.9656 31.1533 -1.4076 232.2634 233.6710 264.1228 32.0038 -1.4066 232.3749 233.7815 264.2691 32.7645 -1.4076 232.5027 233.9103 264.4266 33.5858 -1.4104 232.6255 234.0359 264.5982 34.3783 -1.4083 232.7374 234.1457 264.7606 35.1688 -1.4039 232.8765 234.2803 264.9165 36.0208 -1.4079 233.0194 234.4273 265.0710 36.7810 -1.4107 233.1302 234.5408 265.2178 37.6020 -1.4119 233.2548 234.6667 265.3855 38.3915 -1.4022 233.3873 234.7896 265.5475 39.1818 -1.4066 233.5099 234.9165 265.7025 40.0040 -1.4028 233.6461 235.0490 265.8654 40.7940 -1.4082 233.7634 235.1716 266.0228 41.6158 -1.4146 233.9013 235.3158 266.1685 42.4070 -1.4184 234.0130 235.4314 266.3270 43.1985 -1.4211 234.1353 235.5564 266.4869 44.0205 -1.4195 234.2759 235.6954 266.6265 44.8108 -1.4250 234.3906 235.8157 266.7700 45.6323 -1.4241 234.5164 235.9405 266.9112 46.4223 -1.4220 234.6375 236.0595 267.0747 47.2123 -1.4236 234.7733 236.1968 267.1884 48.0335 -1.4265 234.9142 236.3408 267.3227 48.8248 -1.4284 235.0200 236.4483 267.4696 49.8218 -1.4276 235.1819 236.6095 267.6456 50.6435 -1.4303 235.3050 236.7353 267.7798 51.4333 -1.4315 235.4360 236.8675 267.8872 52.2540 -1.4323 235.5522 236.9845 268.0173 53.0455 -1.4356 235.6804 237.1160 268.1491 53.8375 -1.4395 235.8265 237.2661 268.2500 54.6595 -1.4401 235.9540 237.3941 268.3727 55.4505 -1.4420 236.0732 237.5153 268.4791 56.2720 -1.4420 236.1952 237.6372 268.6098 57.0635 -1.4438 236.3337 237.7776 268.7132 57.8548 -1.4406 236.4628 237.9034 268.8062 58.6763 -1.4421 236.5723 238.0144 268.9247 59.4395 -1.4435 236.6939 238.1374 269.0368 60.2923 -1.4442 236.8189 238.2630 269.1471 61.0823 -1.4445 236.9425 238.3870 269.2439 61.8730 -1.4465 237.0630 238.5095 269.3364 62.6950 -1.4445 237.1985 238.6431 269.4395 63.4558 -1.4480 237.3266 238.7745 269.5225 64.3080 -1.4484 237.4645 238.9129 269.6364 65.1000 -1.4505 237.5831 239.0336 269.7438 65.8915 -1.4539 237.7058 239.1597 269.8187 66.7140 -1.4566 237.8373 239.2939 269.9240 67.4745 -1.4567 237.9636 239.4204 269.9999 68.3265 -1.4576 238.0901 239.5476 270.0801 69.1165 -1.4562 238.1965 239.6527 270.1604 69.9085 -1.4577 238.3145 239.7722 270.2417 70.7305 -1.4579 238.4482 239.9061 270.3321 71.4935 -1.4559 238.5813 240.0372 270.4275 72.3453 -1.4545 238.6983 240.1528 270.5020 73.1065 -1.4500 238.8105 240.2606 270.5778 73.9293 -1.4515 238.9516 240.4032 270.6788 74.7505 -1.4464 239.0644 240.5108 270.7668 75.5108 -1.4425 239.1951 240.6376 270.8417 76.3623 -1.4379 239.3389 240.7768 270.9204 77.1235 -1.4418 239.4427 240.8845 270.9964 77.9453 -1.4413 239.5910 241.0322 271.0908 78.7665 -1.4425 239.7134 241.1559 271.1841 79.5275 -1.4449 239.8178 241.2627 271.2369 80.3793 -1.4439 239.9451 241.3890 271.3357 81.1405 -1.4458 240.0690 241.5148 271.4221 81.9615 -1.4465 240.2031 241.6495 271.5016 82.7833 -1.4450 240.3218 241.7668 271.5862 83.5443 -1.4452 240.4257 241.8709 271.6419 84.3958 -1.4384 240.5647 242.0031 271.7637 85.1863 -1.4369 240.6982 242.1351 271.8461 85.9770 -1.4427 240.8121 242.2549 271.9077 86.7973 -1.4417 240.9227 242.3645 271.9949 87.5575 -1.4430 241.0414 242.4844 272.0944 88.4098 -1.4320 241.1860 242.6180 272.1908 89.2010 -1.4308 241.3123 242.7431 272.2820 89.9925 -1.4437 241.4411 242.8848 272.3744 90.8135 -1.4462 241.5583 243.0044 272.4592 91.5728 -1.4444 241.6759 243.1203 272.5491 92.4250 -1.4472 241.8011 243.2483 272.6536 93.2170 -1.3974 241.9076 243.3051 272.7492 94.0073 -1.2741 242.0398 243.3139 272.8470 94.8278 -1.3923 242.1558 243.5481 272.9381 95.5895 -1.4370 242.2836 243.7206 273.0388 96.4415 -1.4450 242.4091 243.8541 273.1636 97.2035 -1.4430 242.5310 243.9740 273.2436 98.0255 -1.4501 242.6451 244.0952 273.3550 98.8475 -1.4611 242.7729 244.2340 273.4527 99.6085 -1.4627 242.8884 244.3511 273.5398 100.5563 -1.4624 243.0256 244.4880 273.6944 101.4448 -1.4633 243.1620 244.6253 273.8103 102.2343 -1.4645 243.2851 244.7497 273.9235 103.0555 -1.4609 243.4318 244.8927 274.0577 103.8458 -1.4595 243.5437 245.0031 274.1398 104.6675 -1.4568 243.6480 245.1048 274.2602 105.4603 -1.4547 243.7716 245.2263 274.3804 106.2523 -1.4463 243.8943 245.3405 274.4839 107.0735 -1.4592 244.0239 245.4831 274.6007 107.8355 -1.4643 244.1346 245.5989 274.7128 108.6868 -1.4694 244.2814 245.7508 274.8167 109.4773 -1.4664 244.3791 245.8455 274.9170 110.2680 -1.4540 244.4752 245.9292 275.0431 111.0938 -1.4322 244.6403 246.0725 275.1923 111.8538 -1.4440 244.7570 246.2011 275.2985 112.7060 -1.4644 244.8917 246.3562 275.4154 113.4680 -1.4752 244.9728 246.4480 275.5256 114.2898 -1.4790 245.1088 246.5878 275.6336 115.0810 -1.4805 245.2251 246.7056 275.7397 115.8720 -1.4819 245.3474 246.8294 275.8558 116.7238 -1.4777 245.4899 246.9676 276.0023 117.4838 -1.4819 245.6106 247.0925 276.1000 118.3058 -1.4880 245.7422 247.2302 276.2173 119.0970 -1.4898 245.8375 247.3273 276.3322 119.8870 -1.4903 245.9456 247.4359 276.4240 120.7078 -1.4909 246.0779 247.5688 276.5585 121.4985 -1.4903 246.1734 247.6637 276.6939 122.3203 -1.4942 246.3022 247.7964 276.8211 123.1105 -1.4974 246.4284 247.9258 276.9338 123.9025 -1.5051 246.5522 248.0572 277.0564 124.7245 -1.5060 246.6951 248.2011 277.1731 125.4855 -1.4994 246.8042 248.3036 277.2857 126.3373 -1.4878 246.9087 248.3965 277.4076 127.1285 -1.4916 247.0534 248.5450 277.5188 127.9193 -1.4984 247.1832 248.6816 277.6278 128.7405 -1.5021 247.2745 248.7766 277.7469 129.5010 -1.5017 247.3861 248.8878 277.8500 130.3523 -1.5035 247.5279 249.0314 277.9731 131.1135 -1.5024 247.6361 249.1385 278.0775 131.9340 -1.5032 247.7490 249.2522 278.1854 132.7555 -1.5052 247.8723 249.3775 278.2988 133.5170 -1.5115 247.9838 249.4953 278.3885 134.3678 -1.5139 248.1068 249.6207 278.5381 135.1295 -1.5176 248.2361 249.7536 278.6158 135.9505 -1.5183 248.3494 249.8677 278.7206 136.7420 -1.5181 248.4689 249.9870 278.8375 137.5328 -1.5166 248.5689 250.0855 278.9302 138.3850 -1.5184 248.7081 250.2266 279.0284 139.1458 -1.5208 248.8190 250.3397 279.1243 139.9675 -1.5223 248.9400 250.4623 279.2112 140.7580 -1.5207 249.0593 250.5799 279.3268 141.5485 -1.5224 249.1901 250.7124 279.4320 142.3700 -1.5252 249.3127 250.8380 279.5371 143.1610 -1.5283 249.4353 250.9635 279.6240 143.9820 -1.5279 249.5517 251.0796 279.7201 144.7725 -1.5320 249.6747 251.2067 279.8213 145.5638 -1.5340 249.7982 251.3322 279.9187 146.3848 -1.5305 249.8869 251.4174 280.0081 147.1748 -1.5327 250.0222 251.5549 280.1010 147.9960 -1.5347 250.1668 251.7015 280.2161 148.7865 -1.5346 250.2766 251.8113 280.2996 149.5775 -1.5373 250.3871 251.9245 280.3965 150.3985 -1.5399 250.5136 252.0534 280.5183 151.1890 -1.5385 250.6194 252.1579 280.6102 152.0085 -1.5403 250.7410 252.2814 280.7097 152.7995 -1.5458 250.8550 252.4008 280.7936 153.5908 -1.5452 250.9902 252.5354 280.8781 154.4125 -1.5454 251.0991 252.6445 280.9745 155.1728 -1.5473 251.1989 252.7462 281.0766 156.0245 -1.5502 251.3455 252.8957 281.1644 156.8148 -1.5514 251.4714 253.0228 281.2469 157.6058 -1.5522 251.5757 253.1279 281.3390 158.4265 -1.5560 251.6944 253.2504 281.4785 159.1868 -1.5584 251.8231 253.3815 281.5758 160.0378 -1.5538 251.9433 253.4971 281.6551 160.8285 -1.5561 252.0579 253.6140 281.7571 161.6183 -1.5550 252.1475 253.7024 281.8889 162.4450 -1.5572 252.2734 253.8306 281.9733 163.2055 -1.5604 252.4034 253.9638 282.0576 164.0578 -1.5624 252.5208 254.0831 282.1654 164.8188 -1.5629 252.6381 254.2010 282.2753 165.6408 -1.5641 252.7558 254.3199 282.3785 166.4630 -1.5651 252.9058 254.4709 282.4948 167.2235 -1.5681 253.0197 254.5879 282.6142 168.0758 -1.5696 253.1331 254.7027 282.7086 168.8368 -1.5701 253.2415 254.8116 282.8085 169.6588 -1.5746 253.3403 254.9149 282.9167 170.4508 -1.5690 253.4559 255.0250 283.0390 171.2425 -1.5717 253.5917 255.1633 283.1365 172.0945 -1.5687 253.7115 255.2802 283.2389 172.8548 -1.5726 253.8098 255.3824 283.3530 173.6758 -1.5802 253.9440 255.5242 283.4882 174.4665 -1.5760 254.0540 255.6299 283.5840 175.2580 -1.5767 254.1730 255.7497 283.6818 176.1093 -1.5805 254.2937 255.8742 283.8122 176.8688 -1.5830 254.4046 255.9876 283.9141 177.6903 -1.5840 254.5394 256.1234 284.0319 178.4805 -1.5847 254.6575 256.2422 284.1221 179.2713 -1.5896 254.7697 256.3593 284.2186 180.1225 -1.5871 254.8812 256.4683 284.3396 180.8828 -1.5905 254.9963 256.5868 284.4653 181.7043 -1.5887 255.1258 256.7146 284.5839 182.5040 -1.5949 255.2402 256.8351 284.6806 183.3003 -1.5943 255.3454 256.9398 284.8071 184.1215 -1.5965 255.4775 257.0740 284.9332 184.8818 -1.5987 255.5839 257.1826 285.0179 185.7328 -1.5977 255.7002 257.2979 285.1279 186.5233 -1.5983 255.8153 257.4136 285.2215 187.3130 -1.6008 255.9365 257.5374 285.3348 188.1340 -1.6008 256.0636 257.6644 285.4629 188.8945 -1.6002 256.1728 257.7730 285.5730 189.7460 -1.6028 256.2840 257.8868 285.6787 190.5365 -1.6031 256.3991 258.0022 285.7726 191.3260 -1.6065 256.5282 258.1347 285.8791 192.1470 -1.6089 256.6529 258.2619 285.9942 192.9383 -1.6119 256.7601 258.3719 286.1112 193.7593 -1.6125 256.8695 258.4821 286.2156 194.5505 -1.6145 256.9759 258.5903 286.3199 195.3400 -1.6157 257.1016 258.7173 286.4240 196.1608 -1.6144 257.2100 258.8244 286.5494 196.9513 -1.6184 257.3201 258.9386 286.6456 197.7723 -1.6206 257.4665 259.0871 286.7626 198.5625 -1.6164 257.5783 259.1947 286.8737 199.3540 -1.6179 257.6867 259.3045 286.9697 200.2053 -1.6196 257.8137 259.4333 287.0762 200.9658 -1.6219 257.9264 259.5483 287.1816 201.7870 -1.6228 258.0433 259.6660 287.3078 202.5765 -1.6248 258.1684 259.7932 287.3941 203.3673 -1.6280 258.2719 259.8998 287.5086 204.2183 -1.6258 258.3883 260.0140 287.6256 204.9795 -1.6308 258.5061 260.1369 287.7176 205.8013 -1.6308 258.6199 260.2507 287.8491 206.5918 -1.6307 258.7376 260.3684 287.9530 207.3830 -1.6358 258.8642 260.5000 288.0524 208.2343 -1.6354 258.9820 260.6174 288.1573 208.9955 -1.6388 259.1019 260.7407 288.2606 209.8170 -1.6412 259.2137 260.8549 288.3837 210.6085 -1.6437 259.3397 260.9834 288.4672 211.4005 -1.6424 259.4489 261.0913 288.5874 212.2520 -1.6442 259.5784 261.2227 288.7023 213.0130 -1.6463 259.6830 261.3294 288.7980 213.8365 -1.6461 259.8030 261.4492 288.9286 214.6280 -1.6488 259.9209 261.5697 289.0225 215.4195 -1.6490 260.0376 261.6866 289.1302 216.2420 -1.6515 260.1596 261.8111 289.2285 217.0028 -1.6534 260.2380 261.8913 289.3163 217.8550 -1.6581 260.3663 262.0244 289.4249 218.6460 -1.6581 260.4826 262.1407 289.5573 219.4370 -1.6589 260.6047 262.2636 289.6344 220.2590 -1.6604 260.7230 262.3834 289.7422 221.0198 -1.6604 260.8314 262.4919 289.8442 221.8720 -1.6624 260.9805 262.6429 289.9211 222.6640 -1.6622 261.0825 262.7447 290.0382 223.4555 -1.6629 261.1925 262.8554 290.1629 224.2778 -1.6619 261.3180 262.9799 290.2691 225.0385 -1.6646 261.4291 263.0937 290.3478 225.8903 -1.6677 261.5422 263.2100 290.4604 226.6508 -1.6672 261.6546 263.3217 290.5768 227.4725 -1.6692 261.7723 263.4415 290.6748 228.2945 -1.6697 261.9135 263.5832 290.7952 229.0558 -1.6730 261.9953 263.6683 290.8833 229.9073 -1.6758 262.1213 263.7971 290.9919 230.6685 -1.6771 262.2318 263.9089 291.0935 231.4898 -1.6772 262.3415 264.0186 291.1826 232.3105 -1.6807 262.4687 264.1494 291.2861 233.0720 -1.6827 262.5858 264.2685 291.3675 233.9233 -1.6847 262.7009 264.3856 291.4866 234.6835 -1.6861 262.8076 264.4937 291.5925 235.5053 -1.6884 262.9108 264.5992 291.6835 236.3270 -1.6878 263.0385 264.7263 291.7905 237.0878 -1.6884 263.1504 264.8388 291.8861 237.9390 -1.6885 263.2689 264.9574 292.0115 238.7010 -1.6910 263.3705 265.0615 292.0941 239.5228 -1.6907 263.4994 265.1901 292.1939 240.3148 -1.6943 263.6179 265.3121 292.2911 241.1058 -1.6984 263.7372 265.4355 292.3687 241.9280 -1.7016 263.8457 265.5473 292.4697 242.7190 -1.7016 263.9567 265.6583 292.5830 243.5403 -1.7006 264.0773 265.7779 292.6936 244.3313 -1.7034 264.2091 265.9125 292.7953 245.1218 -1.7044 264.3122 266.0166 292.8845 245.9440 -1.7066 264.4414 266.1480 292.9689 246.7038 -1.7056 264.5409 266.2465 293.0870 247.5555 -1.7095 264.6536 266.3631 293.2147 248.3458 -1.7112 264.7845 266.4957 293.2940 249.1360 -1.7116 264.8740 266.5856 293.3826 249.9565 -1.7105 265.0134 266.7239 293.5024 250.7468 -1.7178 265.1304 266.8482 293.5973 251.5678 -1.7156 265.2354 266.9509 293.6852 252.3588 -1.7171 265.3629 267.0801 293.7778 253.1500 -1.7260 265.4576 267.1836 293.8775 253.9715 -1.7203 265.5941 267.3144 293.9762 254.7625 -1.7199 265.7108 267.4306 294.0734 255.5845 -1.7199 265.8124 267.5323 294.1983 256.3753 -1.7239 265.9145 267.6385 294.2872 257.1665 -1.7187 266.0452 267.7639 294.3755 257.9885 -1.7197 266.1556 267.8753 294.4711 258.7498 -1.7253 266.2747 268.0000 294.5815 259.6015 -1.7257 266.3724 268.0981 294.6787 260.3915 -1.7285 266.4757 268.2043 294.7780 261.1833 -1.7303 266.6007 268.3311 294.8884 262.0045 -1.7293 266.7102 268.4395 294.9815 262.7665 -1.7328 266.8383 268.5711 295.0815 263.6180 -1.7375 266.9563 268.6938 295.1871 264.3580 -1.7369 267.0545 268.7915 295.2813 265.2180 -1.7346 267.1911 268.9257 295.3921 265.9788 -1.7353 267.2958 269.0311 295.4782 266.8005 -1.7388 267.4199 269.1586 295.5891 267.6220 -1.7399 267.5250 269.2649 295.7091 268.3825 -1.7441 267.6134 269.3575 295.8178 269.2348 -1.7446 267.7549 269.4995 295.9247 269.9940 -1.7457 267.8705 269.6162 296.0281 270.8158 -1.7457 267.9835 269.7292 296.1459 271.6068 -1.7475 268.0986 269.8461 296.2815 272.3970 -1.7501 268.2082 269.9583 296.3792 273.2490 -1.7522 268.3413 270.0935 296.5194 274.0108 -1.7536 268.4386 270.1922 296.6308 274.8320 -1.7519 268.5571 270.3091 296.7375 275.6235 -1.7572 268.6680 270.4252 296.8596 276.4155 -1.7564 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