DTA measure 4elsomeres Date: 2024312:1137 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.01 s Mass = 1129.200 mg data_number = 1022 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4334 -4.2021 407.8061 412.0082 419.8941 4.0446 -4.1958 407.9803 412.1760 419.9210 5.6420 -4.1936 408.1396 412.3332 419.9377 7.2679 -4.1907 408.3011 412.4918 419.9332 8.8793 -4.1884 408.4628 412.6511 419.9220 10.4776 -4.1839 408.5906 412.7745 419.8810 12.0745 -4.1715 408.7484 412.9199 419.7847 13.6875 -4.1719 408.9126 413.0845 419.7105 15.3004 -4.1648 409.0624 413.2271 419.6036 16.9004 -4.1614 409.1994 413.3607 419.4414 18.5051 -4.1493 409.3527 413.5020 419.2657 20.1038 -4.1526 409.4821 413.6347 419.0947 21.7176 -4.1476 409.6203 413.7679 418.9014 23.3340 -4.1388 409.7491 413.8880 418.6918 24.9318 -4.1312 409.8987 414.0299 418.4845 26.5413 -4.1155 410.0325 414.1480 418.2510 28.1375 -4.1105 410.1494 414.2599 418.0226 29.7428 -4.1055 410.2790 414.3845 417.7848 31.3568 -4.0954 410.4083 414.5037 417.5330 32.9690 -4.0872 410.5399 414.6271 417.2816 34.5676 -4.0750 410.6462 414.7212 417.0418 36.1779 -4.0590 410.7576 414.8165 416.7761 37.7804 -4.0492 410.8605 414.9097 416.5303 39.3803 -4.0383 410.9831 415.0214 416.2654 40.9936 -4.0291 411.1046 415.1337 416.0113 42.6055 -4.0158 411.1876 415.2034 415.7506 44.2045 -4.0079 411.2757 415.2836 415.5068 45.8029 -3.9877 411.3712 415.3589 415.2893 47.4165 -3.9802 411.4879 415.4681 415.0557 49.0384 -3.9720 411.5848 415.5568 414.8343 50.6368 -3.9604 411.6767 415.6371 414.6073 52.2490 -3.9475 411.7578 415.7053 414.4003 53.8463 -3.9392 411.8328 415.7720 414.1910 55.4438 -3.9230 411.9262 415.8492 413.9950 57.0716 -3.9123 411.9840 415.8963 413.7867 58.6701 -3.8962 412.0644 415.9606 413.5784 60.2735 -3.8889 412.1300 416.0189 413.3977 61.8726 -3.8768 412.2043 416.0811 413.2399 63.4850 -3.8619 412.2657 416.1276 413.0594 65.0881 -3.8468 412.3221 416.1690 412.8900 66.7003 -3.7587 412.3697 416.1285 412.7135 68.2961 -3.7006 412.4367 416.1373 412.5485 69.9031 -3.8026 412.4876 416.2903 412.4095 71.5165 -3.8140 412.5447 416.3586 412.2368 73.1125 -3.7216 412.6009 416.3225 412.0704 74.7093 -3.3921 412.6561 416.0482 411.9049 76.3365 -3.5408 412.6736 416.2144 411.7364 77.9340 -3.6090 412.7329 416.3419 411.5826 79.5460 -3.6411 412.7819 416.4230 411.4269 81.1430 -3.6621 412.8095 416.4716 411.2652 82.7403 -3.6796 412.8296 416.5092 411.1031 84.3389 -3.6483 412.8553 416.5036 410.9373 85.9674 -3.6266 412.8900 416.5166 410.7399 87.5649 -3.6261 412.9279 416.5540 410.5585 89.1635 -3.6483 412.9700 416.6182 410.3913 90.7676 -3.6847 412.9760 416.6606 410.2205 92.3656 -3.6432 412.9995 416.6426 410.0467 93.9646 -3.6729 413.0154 416.6883 409.8671 95.5929 -3.6695 413.0216 416.6910 409.6574 97.1910 -3.6789 413.0661 416.7451 409.4553 98.7701 -3.6719 413.0671 416.7390 409.2747 100.3979 -3.6617 413.0536 416.7153 409.0865 102.0099 -3.6489 413.0772 416.7262 408.8841 103.6070 -3.6210 413.0904 416.7114 408.6970 105.2185 -3.6073 413.0943 416.7016 408.4833 106.8163 -3.5986 413.0828 416.6813 408.2778 108.4139 -3.5904 413.0853 416.6757 408.0513 110.0288 -3.5794 413.0763 416.6557 407.8829 111.6265 -3.5716 413.0850 416.6566 407.6964 113.2244 -3.5632 413.0644 416.6276 407.4653 114.8529 -3.5563 413.0591 416.6154 407.2730 116.4515 -3.5450 413.0454 416.5904 407.0890 118.0481 -3.5342 413.0321 416.5663 406.8756 119.6320 -3.5219 413.0234 416.5453 406.6914 121.2729 -3.5131 412.9891 416.5022 406.4739 122.8715 -3.5050 412.9695 416.4744 406.2951 124.4705 -3.4939 412.9516 416.4455 406.1076 126.0684 -3.4846 412.9331 416.4177 405.9233 127.6803 -3.4745 412.9078 416.3822 405.7433 129.2980 -3.4586 412.8701 416.3287 405.5506 130.8964 -3.4538 412.8351 416.2889 405.3496 132.4945 -3.4446 412.8231 416.2677 405.1633 134.0930 -3.4370 412.7765 416.2134 404.9619 135.7199 -3.4247 412.7507 416.1754 404.7812 137.3161 -3.4207 412.7111 416.1318 404.5776 138.9139 -3.4128 412.6795 416.0923 404.3756 140.5266 -3.4019 412.6139 416.0159 404.1914 142.1319 -3.3931 412.5783 415.9715 403.9863 143.7296 -3.3861 412.5394 415.9254 403.7777 145.3414 -3.3736 412.4939 415.8675 403.5739 146.9385 -3.3645 412.4438 415.8083 403.3890 148.5515 -3.3556 412.3928 415.7484 403.1972 150.1573 -3.3494 412.3347 415.6841 402.9969 151.7491 -3.3393 412.2693 415.6086 402.7897 153.3759 -3.3281 412.2290 415.5571 402.6060 154.9739 -3.3219 412.1691 415.4910 402.4135 156.5719 -3.3144 412.0910 415.4054 402.2133 158.1833 -3.3007 412.0349 415.3356 402.0342 159.7891 -3.2948 411.9880 415.2828 401.8510 161.3940 -3.2903 411.9215 415.2118 401.6541 163.0053 -3.2816 411.8566 415.1382 401.4496 164.6018 -3.2725 411.7871 415.0596 401.2588 166.1991 -3.2647 411.7377 415.0024 401.0560 167.8265 -3.2523 411.6439 414.8963 400.8547 169.4221 -3.2438 411.5767 414.8205 400.6604 171.0198 -3.2357 411.5004 414.7361 400.4426 172.6379 -3.2279 411.4370 414.6649 400.2466 174.2503 -3.2179 411.3609 414.5788 400.0124 175.8478 -3.2083 411.2770 414.4853 399.8170 177.4444 -3.1990 411.2169 414.4159 399.6137 179.0553 -3.1910 411.1095 414.3005 399.4095 180.6826 -3.1804 411.0566 414.2370 399.2268 182.2704 -3.1732 410.9745 414.1477 399.0215 183.8823 -3.1689 410.8883 414.0572 398.8179 185.4955 -3.1576 410.7764 413.9340 398.6071 187.1078 -3.1489 410.6920 413.8408 398.4185 188.7035 -3.1421 410.6211 413.7632 398.2241 190.2994 -3.1345 410.5362 413.6707 398.0242 191.9155 -3.1251 410.4301 413.5552 397.8473 193.5279 -3.1156 410.3447 413.4603 397.6570 195.1265 -3.1094 410.2619 413.3712 397.4590 196.7231 -3.1045 410.1543 413.2589 397.2659 198.3501 -3.0956 410.0580 413.1536 397.0560 199.9473 -3.0875 409.9554 413.0429 396.8524 201.5491 -3.0805 409.8617 412.9422 396.6552 203.1618 -3.0749 409.7640 412.8389 396.4539 204.7740 -3.0668 409.6745 412.7413 396.2400 206.3711 -3.0569 409.5572 412.6141 396.0348 207.9684 -3.0511 409.4621 412.5132 395.8622 209.5805 -3.0445 409.3413 412.3858 395.6441 211.1964 -3.0351 409.2472 412.2824 395.4498 212.7891 -3.0249 409.1379 412.1628 395.2367 214.4019 -3.0169 409.0285 412.0454 395.0321 215.9999 -3.0122 408.9244 411.9366 394.8324 217.6123 -3.0038 408.8009 411.8047 394.6253 219.2251 -2.9994 408.7038 411.7032 394.4262 220.8229 -2.9905 408.6014 411.5919 394.2003 222.4269 -2.9837 408.4901 411.4738 394.0203 224.0350 -2.9755 408.3564 411.3319 393.8409 225.6470 -2.9676 408.2554 411.2230 393.6381 227.2445 -2.9630 408.1573 411.1204 393.4282 228.8401 -2.9582 408.0166 410.9748 393.2549 230.4513 -2.9490 407.9015 410.8504 393.0629 232.0723 -2.9394 407.7749 410.7143 392.8578 233.6501 -2.9373 407.6621 410.5993 392.6830 235.2624 -2.9318 407.5290 410.4608 392.4646 236.8744 -2.9236 407.4212 410.3449 392.2746 238.4863 -2.9170 407.3076 410.2246 392.0947 240.0823 -2.9102 407.1718 410.0820 391.8999 241.6906 -2.9039 407.0642 409.9681 391.7017 243.2960 -2.8982 406.9325 409.8307 391.4932 244.8939 -2.8912 406.8016 409.6929 391.2951 246.4916 -2.8813 406.6737 409.5550 391.0905 248.1033 -2.8758 406.5490 409.4248 390.8898 249.7008 -2.8711 406.4089 409.2801 390.6832 251.3268 -2.8636 406.2990 409.1626 390.4894 253.0728 -2.8573 406.1356 408.9929 390.2648 254.7198 -2.8570 406.0149 408.8719 390.0382 256.3299 -2.8465 405.8845 408.7310 389.8327 257.9246 -2.8382 405.7376 408.5757 389.6264 259.5500 -2.8299 405.6209 408.4508 389.4356 261.1453 -2.8276 405.4785 408.3061 389.2490 262.7438 -2.8242 405.3459 408.1702 389.0446 264.3550 -2.8166 405.1956 408.0122 388.8411 265.9541 -2.8085 405.0641 407.8726 388.6489 267.5685 -2.8028 404.9378 407.7406 388.4657 269.1814 -2.7969 404.7925 407.5894 388.2621 270.7784 -2.7917 404.6599 407.4516 388.0692 272.3756 -2.7863 404.5323 407.3187 387.8627 273.9731 -2.7797 404.3869 407.1666 387.6758 275.6013 -2.7743 404.2244 406.9987 387.4871 277.2000 -2.7668 404.1079 406.8747 387.2966 278.7976 -2.7617 403.9553 406.7170 387.1100 280.3958 -2.7587 403.7966 406.5553 386.8964 282.0073 -2.7530 403.6651 406.4181 386.7027 283.7665 -2.7467 403.5086 406.2553 386.5139 285.4223 -2.7408 403.3718 406.1126 386.2979 287.0340 -2.7362 403.2160 405.9522 386.0875 288.6306 -2.7301 403.0653 405.7954 385.8980 290.2274 -2.7261 402.9205 405.6466 385.6928 291.8555 -2.7195 402.7741 405.4936 385.4892 293.4545 -2.7170 402.6283 405.3453 385.2768 295.0551 -2.7107 402.4761 405.1868 385.0889 296.6529 -2.7043 402.3406 405.0450 384.8668 298.2654 -2.6981 402.1870 404.8851 384.6795 299.8781 -2.6953 402.0344 404.7297 384.4586 301.4893 -2.6875 401.8790 404.5664 384.2875 303.0853 -2.6795 401.7443 404.4237 384.0782 304.6974 -2.6768 401.5897 404.2665 383.8656 306.2941 -2.6675 401.4385 404.1060 383.6654 307.9214 -2.6598 401.2714 403.9312 383.4829 309.5179 -2.6583 401.1169 403.7752 383.2920 311.1139 -2.6533 400.9657 403.6191 383.0918 312.7261 -2.6471 400.8213 403.4684 382.8912 314.4858 -2.6416 400.6415 403.2831 382.6744 316.1406 -2.6348 400.4887 403.1235 382.4467 317.7525 -2.6291 400.3363 402.9655 382.2594 319.3498 -2.6238 400.1665 402.7903 382.0512 320.9613 -2.6144 400.0252 402.6396 381.8299 322.5730 -2.6122 399.8652 402.4774 381.6270 324.1710 -2.6043 399.7177 402.3220 381.4264 325.7826 -2.5951 399.5440 402.1391 381.2052 327.3794 -2.5906 399.4046 401.9952 380.9995 329.0069 -2.5842 399.2500 401.8342 380.7807 330.6048 -2.5794 399.0856 401.6651 380.5627 332.2176 -2.5715 398.9295 401.5010 380.3537 333.8148 -2.5646 398.7654 401.3300 380.1521 335.4111 -2.5621 398.5908 401.1529 379.9441 337.0394 -2.5542 398.4406 400.9948 379.7254 338.6378 -2.5502 398.2702 400.8204 379.5132 340.2491 -2.5417 398.1070 400.6487 379.3080 341.8449 -2.5384 397.9498 400.4882 379.0971 343.4434 -2.5315 397.7917 400.3232 378.8916 345.2219 -2.5245 397.6165 400.1410 378.6681 346.8651 -2.5169 397.4350 399.9520 378.4592 348.4785 -2.5106 397.2691 399.7797 378.2513 350.0761 -2.5071 397.1074 399.6145 378.0616 351.6883 -2.5048 396.9448 399.4496 377.8464 353.3015 -2.4989 396.7808 399.2797 377.6530 354.8991 -2.4930 396.6085 399.1016 377.4501 356.5115 -2.4861 396.4402 398.9263 377.2546 358.1103 -2.4829 396.2719 398.7548 377.0681 359.7221 -2.4767 396.1093 398.5860 376.8719 361.3334 -2.4699 395.9553 398.4252 376.6807 362.9300 -2.4662 395.7549 398.2211 376.4816 364.5424 -2.4580 395.6013 398.0592 376.2896 366.1398 -2.4532 395.4333 397.8865 376.1094 367.7371 -2.4512 395.2822 397.7334 375.9127 369.3645 -2.4446 395.1159 397.5605 375.7151 370.9621 -2.4401 394.9295 397.3696 375.5322 372.5596 -2.4376 394.7635 397.2011 375.3316 374.1720 -2.4309 394.5847 397.0155 375.1069 375.7765 -2.4216 394.4181 396.8398 374.9159 377.3894 -2.4167 394.2407 396.6574 374.7364 378.9856 -2.4154 394.0788 396.4942 374.5146 380.5963 -2.4086 393.8997 396.3083 374.3155 382.1938 -2.4025 393.7254 396.1279 374.1156 383.7903 -2.3979 393.5527 395.9506 373.9126 385.4175 -2.3964 393.3992 395.7956 373.6786 387.0158 -2.3862 393.2036 395.5898 373.4822 388.6136 -2.3842 393.0452 395.4294 373.2774 390.2103 -2.3807 392.8644 395.2451 373.0802 391.8219 -2.3757 392.6987 395.0744 372.8671 393.4199 -2.3677 392.5188 394.8865 372.6655 395.0330 -2.3653 392.3603 394.7255 372.4609 396.8413 -2.3599 392.1522 394.5122 372.2327 398.4396 -2.3544 391.9721 394.3265 372.0380 400.0365 -2.3503 391.8167 394.1670 371.8256 401.6476 -2.3463 391.6258 393.9721 371.6314 403.2591 -2.3411 391.4404 393.7815 371.4162 404.8713 -2.3354 391.2734 393.6088 371.2229 406.4670 -2.3314 391.1077 393.4391 371.0051 408.0645 -2.3266 390.9266 393.2531 370.7938 409.6773 -2.3206 390.7469 393.0676 370.5896 411.2891 -2.3156 390.5735 392.8891 370.3828 412.8996 -2.3123 390.4149 392.7273 370.2092 414.4960 -2.3059 390.2209 392.5268 369.9986 416.1069 -2.3014 390.0344 392.3358 369.8092 417.7029 -2.2970 389.8548 392.1518 369.6087 419.3294 -2.2924 389.6930 391.9854 369.4038 420.9271 -2.2870 389.5012 391.7882 369.2107 422.5229 -2.2831 389.3114 391.5945 369.0094 424.1356 -2.2807 389.1567 391.4373 368.7789 425.7324 -2.2778 388.9710 391.2487 368.5779 427.3603 -2.2746 388.7860 391.0606 368.3662 428.9561 -2.2704 388.6085 390.8789 368.1655 430.5524 -2.2642 388.4329 390.6971 367.9694 432.1645 -2.2636 388.2619 390.5255 367.7665 433.7623 -2.2565 388.0641 390.3206 367.5323 435.3901 -2.2547 387.8844 390.1392 367.3072 436.9866 -2.2479 387.7153 389.9632 367.1073 438.5830 -2.2441 387.5304 389.7745 366.9170 440.1949 -2.2424 387.3451 389.5875 366.6935 441.7918 -2.2378 387.1599 389.3977 366.4860 443.4040 -2.2298 386.9814 389.2111 366.2709 445.0153 -2.2259 386.8033 389.0292 366.0641 446.6118 -2.2210 386.6214 388.8424 365.8642 448.2096 -2.2135 386.4392 388.6527 365.6496 449.8219 -2.2110 386.2451 388.4562 365.4387 451.4336 -2.2056 386.0582 388.2638 365.2305 453.0305 -2.2009 385.8943 388.0952 365.0272 454.6420 -2.1950 385.7102 387.9052 364.8219 456.2393 -2.1890 385.5145 387.7035 364.6223 457.8488 -2.1839 385.3301 387.5141 364.4160 459.4611 -2.1801 385.1560 387.3361 364.1966 461.0718 -2.1716 384.9630 387.1346 364.0128 462.6676 -2.1668 384.7843 386.9511 363.8032 464.2661 -2.1616 384.5963 386.7580 363.6055 465.8771 -2.1561 384.4106 386.5667 363.3965 467.4895 -2.1537 384.2260 386.3796 363.2124 469.1005 -2.1485 384.0389 386.1875 363.0105 470.6973 -2.1441 383.8414 385.9854 362.8338 472.2938 -2.1383 383.6658 385.8041 362.6132 473.9053 -2.1352 383.4798 385.6150 362.4256 475.5174 -2.1295 383.2953 385.4247 362.2340 477.1264 -2.1209 383.1113 385.2322 362.0344 478.7216 -2.1189 382.9206 385.0395 361.8263 480.3183 -2.1149 382.7405 384.8554 361.6342 481.9293 -2.1068 382.5689 384.6756 361.4463 483.5421 -2.1034 382.3512 384.4546 361.2506 485.1545 -2.0988 382.1731 384.2719 361.0533 486.7519 -2.0917 381.9784 384.0701 360.8537 488.3550 -2.0853 381.8093 383.8947 360.6700 489.9574 -2.0810 381.6276 383.7086 360.4523 491.5694 -2.0792 381.4399 383.5191 360.2418 493.1811 -2.0714 381.2261 383.2974 360.0348 494.7783 -2.0693 381.0418 383.1111 359.8314 496.3884 -2.0635 380.8577 382.9212 359.6309 497.9846 -2.0560 380.6917 382.7477 359.4306 499.5968 -2.0491 380.4947 382.5438 359.2157 501.2093 -2.0466 380.3063 382.3529 358.9914 502.8069 -2.0437 380.1224 382.1661 358.7923 504.4040 -2.0398 379.9102 381.9500 358.5954 506.0174 -2.0312 379.7290 381.7602 358.3731 507.6135 -2.0289 379.5554 381.5844 358.1590 509.2395 -2.0219 379.3456 381.3675 357.9305 510.8360 -2.0141 379.1750 381.1891 357.7298 512.4328 -2.0101 378.9857 380.9958 357.5385 514.0435 -2.0045 378.8038 380.8083 357.3411 515.6391 -1.9995 378.6069 380.6064 357.1250 517.2649 -1.9955 378.4243 380.4198 356.9114 518.8643 -1.9891 378.2425 380.2316 356.7166 520.4626 -1.9853 378.0540 380.0393 356.5120 522.0604 -1.9790 377.8683 379.8474 356.3161 523.6583 -1.9766 377.6915 379.6680 356.1086 525.2848 -1.9711 377.4774 379.4485 355.8992 526.8965 -1.9648 377.2798 379.2446 355.6918 528.4929 -1.9591 377.0942 379.0532 355.4921 530.0895 -1.9534 376.9010 378.8544 355.2937 531.7001 -1.9489 376.7289 378.6777 355.1190 533.3119 -1.9458 376.5388 378.4846 354.9127 534.9243 -1.9424 376.3491 378.2915 354.7228 536.5199 -1.9395 376.1603 378.0998 354.5134 538.1185 -1.9377 375.9592 377.8970 354.3171 539.7295 -1.9307 375.7556 377.6864 354.1096 541.3421 -1.9322 375.5753 377.5075 353.9188 542.9523 -1.9231 375.4010 377.3240 353.7339 544.5488 -1.9181 375.2142 377.1322 353.5241 546.1446 -1.9135 375.0062 376.9197 353.3204 547.7550 -1.9111 374.8176 376.7286 353.1211 549.3693 -1.9053 374.6274 376.5327 352.9108 550.9679 -1.9028 374.4258 376.3286 352.7014 552.5818 -1.8938 374.2283 376.1221 352.4761 554.1775 -1.8881 374.0490 375.9371 352.2616 555.7754 -1.8821 373.8613 375.7434 352.0586 557.3865 -1.8815 373.6547 375.5362 351.8631 558.9979 -1.8779 373.4604 375.3383 351.6531 560.5949 -1.8735 373.2662 375.1396 351.4321 562.2073 -1.8700 373.0829 374.9529 351.2148 563.8054 -1.8656 372.8982 374.7638 351.0112 565.4176 -1.8609 372.7036 374.5645 350.7918 567.0298 -1.8555 372.5110 374.3665 350.5904 568.6270 -1.8519 372.3204 374.1723 350.3680 570.2314 -1.8478 372.1349 373.9827 350.1767 571.8433 -1.8406 371.9432 373.7838 349.9460 573.4398 -1.8368 371.7433 373.5800 349.7256 575.0378 -1.8369 371.5405 373.3774 349.5304 576.6670 -1.8296 371.3579 373.1874 349.3422 578.2775 -1.8237 371.1609 372.9845 349.1295 579.8728 -1.8185 370.9687 372.7873 348.9070 581.4696 -1.8164 370.7975 372.6139 348.6947 583.0819 -1.8142 370.5914 372.4057 348.5017 584.6940 -1.8085 370.3852 372.1937 348.2962 586.2908 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