DTA measure 1dta_pb3 Date: 2024326:1457 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 846.81 s Mass = 1094.800 mg data_number = 1054 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2420 0.0541 234.5876 234.5335 265.8655 2.0910 0.0374 234.7683 234.7309 265.8353 2.8793 0.0561 234.9258 234.8696 266.0011 3.6680 0.0546 235.0482 234.9936 265.9585 4.4875 0.0437 235.1061 235.0624 265.9699 5.2765 0.0595 235.3337 235.2743 266.0010 6.0970 0.0717 235.4764 235.4047 266.0623 6.8878 0.0542 235.6178 235.5636 266.0151 7.6828 0.0574 235.9080 235.8506 266.0821 8.5058 0.0594 236.1153 236.0559 266.1767 9.2990 0.0675 236.3921 236.3246 266.2749 10.1218 0.0770 236.5741 236.4971 266.4065 10.9203 0.0715 236.7530 236.6816 266.3946 11.7135 0.0596 236.9972 236.9376 266.4084 12.5355 0.0691 237.2615 237.1924 266.5970 13.2975 0.0798 237.5974 237.5176 266.5517 14.1540 0.0794 237.8343 237.7549 266.5681 14.9155 0.0943 238.0127 237.9184 266.7659 15.7378 0.0862 238.2041 238.1180 266.8914 16.5595 0.0955 238.3844 238.2889 266.9203 17.3228 0.0960 238.5388 238.4428 267.0629 18.1795 0.0796 238.7705 238.6910 267.2516 18.9415 0.0963 238.9309 238.8345 267.3683 19.7635 0.0932 239.0466 238.9534 267.6471 20.5598 0.1112 239.2039 239.0927 267.7399 21.3525 0.1129 239.4631 239.3502 267.8504 22.2005 0.0965 239.6073 239.5108 267.9714 22.9550 0.1045 239.7957 239.6912 268.1638 23.7718 0.1014 240.0795 239.9780 268.3808 24.5898 0.1020 240.2498 240.1478 268.4707 25.3480 0.1016 240.3616 240.2600 268.6427 26.1988 0.0919 240.6671 240.5752 268.8320 26.9580 0.1007 240.8521 240.7514 269.0558 27.7760 0.0963 241.0649 240.9686 269.1647 28.5940 0.0918 241.2765 241.1847 269.2649 29.3520 0.0988 241.5905 241.4916 269.3598 30.2000 0.1045 241.6859 241.5814 269.4985 30.9613 0.1117 241.8860 241.7743 269.6161 31.7850 0.1021 242.0633 241.9613 269.7185 32.6063 0.0907 242.2345 242.1439 269.9114 33.3685 0.1112 242.5230 242.4118 270.0850 34.2213 0.1090 242.7488 242.6398 270.1587 34.9803 0.1022 242.8831 242.7809 270.2556 35.8008 0.0969 243.1291 243.0322 270.3087 36.6228 0.1110 243.3403 243.2292 270.4586 37.3863 0.1115 243.5106 243.3992 270.5344 38.2385 0.1003 243.7198 243.6194 270.7243 39.0010 0.1030 243.9370 243.8339 270.8809 39.8248 0.1027 244.1400 244.0373 271.0365 40.6165 0.1026 244.3882 244.2855 271.1684 41.4085 0.0885 244.5345 244.4460 271.3443 42.2600 0.0946 244.7672 244.6726 271.5452 43.0253 0.0899 245.0644 244.9745 271.7545 43.8498 0.0953 245.3824 245.2871 271.9167 44.6493 0.0880 245.6255 245.5374 272.1103 45.4465 0.0786 245.9953 245.9167 272.4096 46.2690 0.0749 246.1511 246.0762 272.6399 47.0305 0.0936 246.2456 246.1520 272.6611 47.8828 0.0775 246.3868 246.3094 272.8691 48.6448 0.0794 246.5465 246.4670 272.9735 49.4705 0.0832 246.8764 246.7932 273.0541 50.2648 0.0851 247.0835 246.9984 273.3012 51.0565 0.0978 247.3505 247.2528 273.5074 51.9088 0.0900 247.6058 247.5158 273.5746 52.6705 0.0888 247.8079 247.7191 273.6749 53.4925 0.0817 247.9982 247.9166 273.8711 54.3068 0.0686 248.2377 248.1691 274.0704 55.0640 0.0706 248.3828 248.3122 274.1598 55.9105 0.1020 248.6117 248.5097 274.4615 56.6680 0.1078 248.6698 248.5620 274.5533 57.4860 0.0975 248.7993 248.7019 274.7521 58.3040 0.0864 248.9021 248.8158 274.9135 59.0620 0.0856 249.0568 248.9712 274.8584 59.9100 0.0804 249.1004 249.0201 275.0486 60.6985 0.0712 249.3049 249.2337 275.0981 61.4880 0.0764 249.5568 249.4804 275.2027 62.3060 0.0720 249.7192 249.6472 275.2105 63.0940 0.0664 249.9962 249.9298 275.3042 63.9133 0.0618 249.8207 249.7589 275.4105 64.7055 0.0699 250.1965 250.1266 275.4888 65.4950 0.0750 250.4997 250.4247 275.5326 66.3443 0.0706 250.4859 250.4152 275.6172 67.1030 0.0601 250.7019 250.6418 275.6215 67.9218 0.0717 250.7385 250.6667 275.8155 68.7408 0.0656 250.9815 250.9160 275.7724 69.5043 0.0646 251.1437 251.0791 275.8085 70.3625 0.0589 251.2968 251.2380 275.8324 71.1245 0.0412 251.3895 251.3484 275.9231 71.9465 0.0320 251.4559 251.4239 276.1430 72.7385 0.0316 251.6579 251.6262 276.1364 73.5305 0.0312 251.7125 251.6813 276.3459 74.3533 0.0304 251.8116 251.7813 276.3702 75.1455 0.0443 251.8548 251.8106 276.6740 75.9675 0.0451 252.0287 251.9836 276.8745 76.7595 0.0450 252.0722 252.0271 276.9115 77.5515 0.0355 252.2167 252.1812 277.1089 78.3743 0.0329 252.4542 252.4213 277.4207 79.1665 0.0321 252.5226 252.4905 277.7192 79.9885 0.0159 252.5895 252.5737 277.7358 80.7810 0.0170 252.8587 252.8416 277.8478 81.5745 0.0175 253.1367 253.1193 277.8710 82.3963 0.0151 253.2954 253.2802 278.0602 83.1880 0.0146 253.5452 253.5305 278.2546 84.0098 0.0197 253.8522 253.8325 278.2839 84.8023 0.0095 254.0075 253.9980 278.3366 85.5955 0.0011 254.2355 254.2345 278.3953 86.4178 0.0006 254.1968 254.1961 278.5293 87.2095 0.0019 254.4245 254.4227 278.7580 88.0318 -0.0077 254.6152 254.6229 278.9328 88.8238 -0.0063 254.8509 254.8572 279.0224 89.6165 -0.0042 255.1181 255.1224 279.2208 90.4388 -0.0064 255.3479 255.3543 279.3112 91.2305 -0.0041 255.5920 255.5961 279.5797 92.0528 -0.0226 255.8201 255.8427 279.7167 92.8483 -0.0189 255.8862 255.9050 279.8251 93.6405 -0.0229 256.1400 256.1629 280.0498 94.4625 -0.0365 256.2937 256.3302 280.0874 95.2245 -0.0344 256.3777 256.4121 280.3278 96.0775 -0.0251 256.6931 256.7182 280.4841 96.8695 -0.0269 256.7630 256.7898 280.7385 97.6615 -0.0426 256.9791 257.0217 280.9590 98.4835 -0.0465 257.0958 257.1423 281.1217 99.2455 -0.0623 257.2468 257.3091 281.3139 100.0975 -0.0637 257.4431 257.5068 281.3849 100.8905 -0.0648 257.5803 257.6450 281.4047 101.6813 -0.0614 257.7907 257.8521 281.5812 102.4958 -0.0779 257.8896 257.9675 281.7530 103.2513 -0.0684 258.0541 258.1225 281.8888 104.0965 -0.0694 258.3665 258.4359 282.1119 104.8565 -0.0702 258.4585 258.5287 282.2081 105.6735 -0.0928 258.6399 258.7327 282.4117 106.4895 -0.0836 258.8337 258.9173 282.3705 107.2470 -0.0946 258.9750 259.0696 282.4626 108.0965 -0.0979 259.2333 259.3312 282.5547 108.8553 -0.0940 259.3767 259.4707 282.6467 109.6730 -0.1055 259.6132 259.7188 282.7164 110.4918 -0.0917 259.8167 259.9085 282.8671 111.2513 -0.0987 260.0526 260.1513 282.9758 112.1040 -0.1081 260.2762 260.3843 283.0515 112.8623 -0.1227 260.4648 260.5875 283.0616 113.6805 -0.1139 260.5384 260.6524 283.2146 114.5003 -0.1194 260.7705 260.8899 283.4488 115.2598 -0.1431 260.8708 261.0139 283.6601 116.1080 -0.1221 261.0027 261.1248 283.4743 116.8973 -0.1187 261.2520 261.3707 283.6152 117.6870 -0.1221 261.3803 261.5024 283.9625 118.5060 -0.1241 261.6064 261.7305 283.8210 119.2943 -0.1407 261.8166 261.9573 284.0730 120.1185 -0.1484 261.9222 262.0705 284.3801 120.9178 -0.1594 262.1512 262.3106 284.4608 121.7095 -0.1532 262.2760 262.4293 284.5180 122.5320 -0.1693 262.4528 262.6222 284.6824 123.2935 -0.1631 262.5771 262.7402 284.7788 124.1500 -0.1690 262.7572 262.9262 284.9543 124.9115 -0.1650 262.9221 263.0870 285.0768 125.7338 -0.1720 263.0734 263.2455 285.3515 126.5558 -0.1812 263.2884 263.4696 285.6314 127.3175 -0.2083 263.4700 263.6783 285.7681 128.1698 -0.2001 263.7038 263.9039 285.6037 128.9315 -0.2134 263.8183 264.0317 285.8056 129.7543 -0.2078 263.8715 264.0793 285.9443 130.5485 -0.2049 264.1126 264.3175 285.9258 131.3405 -0.2090 264.2325 264.4415 285.9508 132.1925 -0.2094 264.4113 264.6207 286.0420 132.9560 -0.2064 264.6612 264.8676 286.0348 133.7773 -0.2094 264.7398 264.9492 286.1332 134.5625 -0.2180 264.9197 265.1377 286.2627 135.3495 -0.2175 265.0227 265.2403 286.4542 136.1945 -0.2245 265.3315 265.5559 286.7493 136.9520 -0.2175 265.4750 265.6925 286.8594 137.7705 -0.2150 265.6305 265.8455 286.9562 138.5648 -0.2176 265.7219 265.9395 287.1313 139.3560 -0.2314 265.8711 266.1024 287.1952 140.1758 -0.2325 266.0223 266.2548 287.3809 140.9643 -0.2421 266.1123 266.3545 287.5817 141.7830 -0.2281 266.2933 266.5214 287.7861 142.5735 -0.2457 266.5050 266.7506 287.9265 143.3663 -0.2587 266.7110 266.9696 288.1071 144.1883 -0.2660 266.8763 267.1423 288.4499 144.9518 -0.2531 267.0644 267.3176 288.6400 145.8005 -0.2575 267.1974 267.4549 288.8714 146.5890 -0.2635 267.3255 267.5890 289.2040 147.3780 -0.2654 267.4754 267.7409 289.4555 148.2265 -0.2589 267.6678 267.9266 289.5931 148.9865 -0.2751 267.9045 268.1796 289.7756 149.8110 -0.2671 268.0999 268.3670 289.8941 150.6035 -0.2857 268.3123 268.5980 289.9572 151.3998 -0.2913 268.3973 268.6886 290.1004 152.2290 -0.2959 268.5259 268.8218 290.1729 152.9928 -0.2955 268.7256 269.0211 290.2487 153.8495 -0.3082 268.8827 269.1909 290.3409 154.6140 -0.3085 268.9670 269.2755 290.4992 155.4388 -0.3196 269.1746 269.4942 290.6360 156.2338 -0.3200 269.3624 269.6825 290.7360 157.0275 -0.3188 269.4310 269.7498 290.8321 157.8583 -0.3252 269.6969 270.0221 290.9479 158.6228 -0.3319 269.8471 270.1789 290.9407 159.4813 -0.3596 270.0399 270.3995 291.0430 160.2430 -0.3677 270.0552 270.4230 291.1555 161.0650 -0.3596 270.2295 270.5891 291.2714 161.8613 -0.3514 270.5372 270.8886 291.4285 162.6570 -0.3567 270.7113 271.0680 291.5391 163.4808 -0.3493 270.8101 271.1594 291.7305 164.2725 -0.3578 270.9402 271.2979 291.8088 165.0948 -0.3470 271.0432 271.3902 291.9016 165.8835 -0.3488 271.2413 271.5902 291.9962 166.6695 -0.3494 271.4605 271.8099 291.9365 167.5158 -0.3675 271.6490 272.0165 292.0275 168.2738 -0.3770 271.7808 272.1578 292.1490 169.0920 -0.3903 271.9760 272.3664 292.3246 169.8810 -0.3917 272.1997 272.5915 292.5358 170.6720 -0.4001 272.4106 272.8107 292.8532 171.4900 -0.4035 272.6931 273.0966 292.8793 172.2533 -0.4019 272.9253 273.3273 292.9197 173.1035 -0.3965 273.0479 273.4443 292.9014 173.8915 -0.4103 273.1611 273.5714 293.1396 174.6800 -0.4135 273.4316 273.8451 293.2771 175.4983 -0.4073 273.6479 274.0552 293.5353 176.2868 -0.4020 273.7718 274.1738 293.7019 177.1070 -0.4044 273.9629 274.3673 293.7632 177.8958 -0.4241 274.1247 274.5488 293.9581 178.6850 -0.4310 274.2854 274.7164 294.0531 179.5358 -0.4295 274.5610 274.9905 294.3366 180.2940 -0.4268 274.7239 275.1506 294.4090 181.1145 -0.4380 274.7945 275.2325 294.6506 181.9348 -0.4337 275.1268 275.5605 294.6896 182.6965 -0.4511 275.3369 275.7880 294.7608 183.5500 -0.4557 275.5128 275.9686 294.9210 184.3138 -0.4534 275.6124 276.0658 295.0253 185.1378 -0.4653 275.6896 276.1548 295.1150 185.9298 -0.4673 275.7792 276.2466 295.2264 186.7215 -0.4673 275.9202 276.3875 295.3876 187.5735 -0.4529 276.0688 276.5217 295.6009 188.3368 -0.4574 276.1855 276.6429 295.7464 189.1625 -0.4432 276.4073 276.8504 295.8075 189.9585 -0.4597 276.5156 276.9753 295.9390 190.7515 -0.4693 276.7219 277.1912 296.0485 191.5740 -0.4780 276.7986 277.2766 296.2018 192.3395 -0.4847 276.7368 277.2215 296.3581 193.2013 -0.4740 276.9164 277.3903 296.4755 193.9638 -0.4710 277.1178 277.5888 296.6246 194.7855 -0.4941 277.2834 277.7775 296.7431 195.5785 -0.5069 277.5195 278.0264 296.8826 196.3715 -0.5038 277.6300 278.1339 296.9483 197.2235 -0.4951 277.8189 278.3140 297.0462 197.9855 -0.5070 277.9411 278.4481 297.2448 198.8028 -0.5050 277.8822 278.3872 297.3405 199.6183 -0.5185 278.1690 278.6875 297.5103 200.3720 -0.5285 278.3277 278.8561 297.6276 201.2195 -0.5187 278.5817 279.1005 297.8013 202.0080 -0.5305 278.6807 279.2112 297.8892 202.7985 -0.5372 278.7696 279.3068 297.9547 203.6170 -0.5435 278.8620 279.4056 298.0746 204.3750 -0.5374 279.1488 279.6862 298.2218 205.2230 -0.5395 279.2518 279.7913 298.3545 206.0110 -0.5334 279.3461 279.8796 298.5679 206.7990 -0.5454 279.5648 280.1103 298.7402 207.6170 -0.5525 279.6513 280.2037 298.7322 208.4050 -0.5498 279.7206 280.2704 298.8965 209.2238 -0.5474 279.8990 280.4465 299.0344 210.0120 -0.5486 280.1594 280.7080 299.1091 210.8010 -0.5710 280.3700 280.9410 299.2678 211.6495 -0.5596 280.3347 280.8943 299.4590 212.4083 -0.5711 280.5423 281.1134 299.5425 213.2288 -0.5724 280.7298 281.3022 299.6488 214.0478 -0.5764 280.7012 281.2776 299.7713 214.8070 -0.5854 280.9628 281.5483 299.8859 215.6583 -0.5843 281.0175 281.6018 300.0786 216.4203 -0.5913 281.2632 281.8545 300.2849 217.2418 -0.5909 281.5016 282.0926 300.4603 218.0678 -0.6067 281.5369 282.1436 300.6217 218.8315 -0.6130 281.7269 282.3399 300.7272 219.6575 -0.6153 281.9195 282.5347 300.8487 220.4485 -0.6153 282.1552 282.7706 300.9624 221.2708 -0.6122 282.1815 282.7936 301.0674 222.0628 -0.6167 282.3026 282.9193 301.2463 222.8545 -0.6180 282.3788 282.9968 301.4672 223.6778 -0.6240 282.5578 283.1818 301.5597 224.4720 -0.6323 282.7500 283.3823 301.7566 225.2998 -0.6364 282.8396 283.4760 301.8918 226.0918 -0.6538 283.0061 283.6598 301.8914 226.8835 -0.6614 283.2451 283.9065 302.0098 227.7055 -0.6521 283.4356 284.0877 302.1451 228.4710 -0.6618 283.4468 284.1086 302.3025 229.3225 -0.6689 283.6345 284.3034 302.4075 230.1145 -0.6665 283.9307 284.5972 302.5258 230.9065 -0.6628 284.0825 284.7453 302.6518 231.7295 -0.6733 284.3027 284.9760 302.7097 232.4915 -0.6830 284.4035 285.0865 303.0063 233.3435 -0.6772 284.4613 285.1385 303.1539 234.1075 -0.6775 284.5945 285.2720 303.1368 234.9333 -0.6840 284.7721 285.4562 303.2601 235.7275 -0.6924 284.7490 285.4414 303.4252 236.5195 -0.7040 284.8978 285.6018 303.5729 237.3715 -0.6777 285.2458 285.9236 303.6723 238.1330 -0.6889 285.4954 286.1843 303.8054 238.9570 -0.6997 285.4807 286.1804 303.8952 239.7508 -0.6987 285.6582 286.3569 304.0148 240.5425 -0.7120 285.7912 286.5032 304.1580 241.3950 -0.7202 285.9331 286.6533 304.3202 242.1600 -0.7157 286.0117 286.7274 304.3328 242.9818 -0.7217 286.0140 286.7357 304.5025 243.7758 -0.7091 285.9873 286.6964 304.7629 244.5720 -0.7175 286.2054 286.9229 305.0007 245.3975 -0.7226 286.3493 287.0719 305.1032 246.1855 -0.7191 286.4363 287.1554 305.2061 247.0005 -0.7323 286.4790 287.2114 305.4525 247.7843 -0.7483 286.6207 287.3690 305.5337 248.5695 -0.7482 286.9230 287.6712 305.6268 249.3878 -0.7423 286.8990 287.6413 305.7281 250.1503 -0.7604 287.0507 287.8111 305.9009 250.9983 -0.7578 287.2174 287.9752 306.1245 251.7560 -0.7728 287.4571 288.2299 306.1970 252.5740 -0.7674 287.4864 288.2538 306.3308 253.3920 -0.7853 287.6766 288.4619 306.4979 254.1515 -0.7971 287.8525 288.6497 306.5567 255.0000 -0.7799 288.0874 288.8673 306.6942 255.7585 -0.7865 288.3315 289.1180 306.8296 256.5830 -0.8107 288.4214 289.2320 306.9886 257.3800 -0.8135 288.4404 289.2540 307.1232 258.1680 -0.8190 288.6523 289.4712 307.1813 258.9903 -0.8141 288.7700 289.5841 307.3013 259.7790 -0.8099 289.0042 289.8141 307.4493 260.5978 -0.8329 289.2186 290.0515 307.4981 261.3860 -0.8370 289.4618 290.2988 307.6288 262.1750 -0.8388 289.6817 290.5205 307.7976 263.0243 -0.8416 289.9113 290.7529 308.0397 263.7845 -0.8418 290.0480 290.8898 308.1463 264.6060 -0.8337 290.2267 291.0604 308.1275 265.4268 -0.8307 290.4292 291.2599 308.3533 266.1898 -0.8403 290.4858 291.3261 308.5291 267.0448 -0.8390 290.6405 291.4795 308.5719 267.8065 -0.8403 290.8235 291.6638 308.7236 268.6285 -0.8536 290.9904 291.8440 308.8719 269.4205 -0.8590 291.1690 292.0280 308.9739 270.2125 -0.8528 291.2726 292.1253 309.1520 271.0645 -0.8620 291.4627 292.3247 309.2576 271.8265 -0.8645 291.6160 292.4805 309.3861 272.6505 -0.8704 291.8064 292.6767 309.5658 273.4425 -0.8786 291.9141 292.7928 309.7383 274.2345 -0.8735 292.1110 292.9845 309.8332 275.0868 -0.8760 292.3115 293.1875 310.0185 275.8495 -0.8928 292.5409 293.4337 310.0046 276.6708 -0.8864 292.7130 293.5994 310.1894 277.4628 -0.8957 292.8232 293.7189 310.3505 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