DTA measure 1dta_pb4 Date: 2024326:1553 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1119.64 s Mass = 1094.800 mg data_number = 1391 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1695 -0.5536 247.8090 248.3626 266.2953 2.0258 -0.5618 247.8916 248.4534 266.3280 2.7900 -0.5573 248.0805 248.6378 266.2889 3.7120 -0.5527 248.1800 248.7327 266.3706 4.7160 -0.5509 248.2351 248.7860 266.4017 5.5678 -0.5391 248.4374 248.9765 266.3841 6.3295 -0.5295 248.7089 249.2384 266.2606 7.1518 -0.5562 248.6911 249.2472 266.3317 7.9773 -0.5338 248.9343 249.4681 266.3643 8.7418 -0.5255 248.8826 249.4081 266.3796 9.5975 -0.5274 249.0775 249.6049 266.3765 10.3608 -0.5258 249.2283 249.7540 266.4366 11.1865 -0.5147 249.2960 249.8108 266.4663 11.9785 -0.5176 249.4337 249.9514 266.5168 12.7705 -0.5074 249.5577 250.0651 266.5868 13.6225 -0.5032 249.7074 250.2107 266.7071 14.3845 -0.5054 249.9156 250.4210 266.7711 15.2085 -0.5059 249.9123 250.4182 266.8135 16.0005 -0.4856 249.9190 250.4045 266.9089 16.7925 -0.4788 250.2228 250.7016 267.0857 17.6445 -0.4843 250.2071 250.6914 267.1274 18.4078 -0.4795 250.3217 250.8012 267.2115 19.2310 -0.4746 250.4085 250.8830 267.3260 20.0270 -0.4788 250.4625 250.9414 267.3702 20.8175 -0.4742 250.7430 251.2171 267.5078 21.6698 -0.4767 250.8734 251.3501 267.6481 22.4315 -0.4840 251.0650 251.5489 267.7779 23.2558 -0.4676 251.0693 251.5369 267.9033 24.0478 -0.4703 251.2226 251.6929 268.0071 24.8395 -0.4682 251.3576 251.8258 268.2436 25.6918 -0.4658 251.4324 251.8982 268.2474 26.4533 -0.4540 251.4859 251.9399 268.4777 27.2758 -0.4366 251.5754 252.0121 268.5819 28.0685 -0.4308 251.6995 252.1303 268.6392 28.8605 -0.4315 251.7538 252.1853 268.8342 29.7040 -0.4174 251.8088 252.2262 269.0522 30.4603 -0.4171 251.8813 252.2984 269.1983 31.2735 -0.4103 251.9058 252.3162 269.2682 32.0875 -0.4190 251.9900 252.4090 269.2466 32.8413 -0.4156 252.1412 252.5568 269.3403 33.6863 -0.4149 252.2103 252.6252 269.6080 34.4730 -0.4191 252.2600 252.6791 269.7288 35.2610 -0.4278 252.3999 252.8276 269.7847 36.0798 -0.4298 252.4791 252.9088 269.9774 36.8380 -0.4348 252.5732 253.0081 270.1190 37.6860 -0.4321 252.7072 253.1392 270.1968 38.4765 -0.4160 252.8287 253.2447 270.2374 39.2670 -0.4100 252.9911 253.4011 270.3997 40.0860 -0.4027 253.1348 253.5375 270.5720 40.8475 -0.4015 253.2957 253.6973 270.6603 41.6980 -0.4205 253.4667 253.8872 270.7704 42.4860 -0.4253 253.6082 254.0335 270.8521 43.2750 -0.4271 253.8886 254.3157 270.8859 44.0933 -0.4248 253.9420 254.3668 271.0535 44.8820 -0.4287 253.9392 254.3679 271.1068 45.7008 -0.4287 254.1865 254.6152 271.1615 46.4945 -0.4383 254.4099 254.8483 271.3100 47.2840 -0.4277 254.5922 255.0199 271.4282 48.1335 -0.4312 254.8162 255.2474 271.5519 48.8943 -0.4388 255.0389 255.4777 271.7176 49.7145 -0.4310 255.1981 255.6291 271.8698 50.5365 -0.4122 255.3231 255.7353 271.9326 51.2985 -0.4326 255.4730 255.9056 272.0316 52.1505 -0.4310 255.7639 256.1949 272.1300 52.9425 -0.4308 255.8144 256.2452 272.3088 53.7345 -0.4263 255.9585 256.3847 272.2925 54.5595 -0.4388 256.0691 256.5079 272.4510 55.3215 -0.4379 256.2462 256.6841 272.5742 56.1785 -0.4474 256.4507 256.8981 272.7623 57.0305 -0.4231 256.5764 256.9995 272.9666 57.8520 -0.4284 256.5891 257.0175 273.2181 58.6135 -0.4371 256.7958 257.2329 273.2502 59.4658 -0.4348 256.8620 257.2969 273.2884 60.2578 -0.4341 256.9801 257.4142 273.2591 61.1168 -0.4172 257.2324 257.6495 273.4639 61.9085 -0.4168 257.2931 257.7099 273.5463 62.7573 -0.4215 257.4196 257.8411 273.6472 63.5090 -0.4384 257.5714 258.0098 273.9197 64.3258 -0.4184 257.6289 258.0473 273.9840 65.1428 -0.4166 257.8015 258.2181 274.1141 65.9000 -0.4095 258.0177 258.4272 274.2366 66.7480 -0.3942 258.0467 258.4408 274.2594 67.5068 -0.4009 258.3237 258.7246 274.1914 68.3270 -0.3925 258.4546 258.8470 274.3060 69.1450 -0.3950 258.5327 258.9277 274.3983 69.9030 -0.3949 258.7084 259.1033 274.5144 70.7525 -0.4050 258.8145 259.2195 274.6221 71.5405 -0.3972 259.0688 259.4660 274.6996 72.3293 -0.4293 259.1508 259.5801 274.7393 73.1515 -0.4416 259.2817 259.7233 274.9500 73.9400 -0.4348 259.3016 259.7363 274.9696 74.7590 -0.4436 259.4510 259.8946 275.1465 75.5473 -0.4487 259.5145 259.9631 275.1674 76.3360 -0.4463 259.7416 260.1879 275.2284 77.1863 -0.4467 259.8775 260.3242 275.2021 77.9753 -0.4538 260.0950 260.5489 275.2677 78.7645 -0.4462 260.1863 260.6325 275.3036 79.5845 -0.4302 260.3757 260.8059 275.4133 80.3755 -0.4370 260.5623 260.9992 275.5491 81.1978 -0.4324 260.6335 261.0658 275.5873 81.9905 -0.4238 260.7622 261.1860 275.6407 82.7845 -0.4327 260.8859 261.3185 275.7643 83.6068 -0.4257 260.9833 261.4090 275.9311 84.3713 -0.4170 261.1564 261.5734 275.9340 85.2235 -0.4306 261.2771 261.7077 276.2010 85.9860 -0.4348 261.4260 261.8608 276.3259 86.8105 -0.4339 261.5815 262.0154 276.3873 87.6040 -0.4625 261.7141 262.1765 276.5019 88.3965 -0.4667 261.8347 262.3013 276.6235 89.2485 -0.4729 261.9777 262.4506 276.7833 90.0125 -0.4700 262.0075 262.4775 276.9064 90.8380 -0.4711 262.2309 262.7021 276.8862 91.6305 -0.4650 262.2861 262.7511 276.8489 92.4225 -0.4593 262.3824 262.8417 276.9339 93.2753 -0.4443 262.5592 263.0035 277.1358 94.0360 -0.4654 262.6734 263.1388 277.3133 94.8585 -0.4658 262.7886 263.2544 277.4700 95.6243 -0.4600 262.9407 263.4007 277.6845 96.5085 -0.4621 263.0856 263.5477 277.6701 97.2990 -0.4707 263.1502 263.6209 277.7963 98.1178 -0.4693 263.2370 263.7063 277.9477 98.9060 -0.4729 263.3771 263.8500 278.1732 99.7240 -0.4820 263.6297 264.1118 278.3012 100.5163 -0.4785 263.7587 264.2371 278.3253 101.3060 -0.4844 263.9016 264.3860 278.2583 102.1240 -0.4822 263.9304 264.4126 278.5291 102.9120 -0.4753 264.0819 264.5572 278.6891 103.7300 -0.4735 264.1839 264.6575 278.6937 104.5228 -0.4862 264.2377 264.7239 278.8618 105.3120 -0.4791 264.2925 264.7716 278.9998 106.1605 -0.4904 264.4715 264.9619 279.1738 106.9190 -0.5047 264.6655 265.1702 279.1796 107.7378 -0.5050 264.8240 265.3290 279.4197 108.5563 -0.5135 264.8746 265.3881 279.5793 109.3178 -0.5040 264.9771 265.4811 279.5608 110.1695 -0.5033 265.1734 265.6767 279.6511 110.9595 -0.5031 265.3085 265.8116 279.6443 111.7515 -0.5124 265.3085 265.8209 279.7154 112.5735 -0.5118 265.5662 266.0780 280.0070 113.3348 -0.5096 265.7764 266.2860 280.1067 114.1890 -0.5186 265.8396 266.3583 280.3718 114.9813 -0.5136 265.8856 266.3993 280.4031 115.7725 -0.5185 266.0008 266.5193 280.4403 116.5960 -0.5225 266.1542 266.6767 280.5628 117.3585 -0.5214 266.2917 266.8131 280.5915 118.2108 -0.5267 266.4086 266.9352 280.7211 119.0028 -0.5346 266.5784 267.1130 280.8088 119.7945 -0.5388 266.6277 267.1665 280.8966 120.6198 -0.5397 266.8665 267.4062 280.8579 121.3825 -0.5267 266.9543 267.4810 280.9088 122.2360 -0.5129 267.1161 267.6290 281.0166 122.9985 -0.5285 267.2564 267.7850 281.0527 123.8208 -0.5299 267.4197 267.9496 281.4757 124.6425 -0.5378 267.4870 268.0247 281.4787 125.4045 -0.5282 267.5814 268.1096 281.5131 126.2558 -0.5466 267.5954 268.1420 281.5791 127.0090 -0.5511 267.7641 268.3152 281.7548 127.8253 -0.5440 267.8383 268.3824 281.8908 128.6408 -0.5494 268.0078 268.5572 281.8507 129.3980 -0.5481 268.1284 268.6766 282.0464 130.2460 -0.5588 268.2679 268.8267 282.1003 131.0045 -0.5810 268.4149 268.9958 282.3931 131.8240 -0.5607 268.5953 269.1560 282.4621 132.6420 -0.5707 268.6305 269.2012 282.5619 133.4000 -0.5782 268.7702 269.3484 282.7758 134.2480 -0.5821 268.9083 269.4904 282.8521 135.0360 -0.5765 269.1456 269.7221 283.0193 135.8240 -0.5791 269.2111 269.7901 283.1541 136.6423 -0.5963 269.2962 269.8925 283.2037 137.4318 -0.5840 269.4717 270.0557 283.3189 138.2518 -0.5719 269.5138 270.0857 283.3393 139.0425 -0.5846 269.6271 270.2117 283.6004 139.8320 -0.5875 269.8724 270.4599 283.6364 140.6828 -0.6035 270.0354 270.6388 283.6989 141.4440 -0.6003 270.0308 270.6311 283.7848 142.2660 -0.6143 270.0905 270.7048 283.9809 143.0598 -0.6179 270.1902 270.8081 284.0435 143.8525 -0.6123 270.3485 270.9608 284.2119 144.6750 -0.6057 270.5387 271.1444 284.1116 145.4375 -0.6007 270.7030 271.3037 284.1608 146.2895 -0.6075 270.8197 271.4272 284.4249 147.0820 -0.6052 270.8583 271.4636 284.4331 147.8755 -0.6173 270.9147 271.5320 284.5326 148.6975 -0.6166 270.9864 271.6030 284.5190 149.4608 -0.6009 271.1410 271.7419 284.4438 150.3145 -0.6132 271.2980 271.9112 284.7726 151.0765 -0.6115 271.5284 272.1398 284.8593 151.8985 -0.6076 271.5840 272.1915 284.9470 152.6940 -0.6045 271.7622 272.3667 285.1827 153.4848 -0.6014 271.8258 272.4272 285.2860 154.3370 -0.6191 272.0667 272.6858 285.3536 155.0993 -0.6203 272.2185 272.8388 285.5638 155.9228 -0.6158 272.3570 272.9728 285.5859 156.7150 -0.6261 272.5666 273.1927 285.7722 157.5078 -0.6239 272.7109 273.3348 285.8661 158.3320 -0.6291 272.9521 273.5813 285.8580 159.1248 -0.6427 273.1173 273.7599 286.1586 159.9488 -0.6407 273.2390 273.8797 286.1316 160.7408 -0.6490 273.3554 274.0043 286.2219 161.5325 -0.6646 273.4528 274.1174 286.0776 162.3558 -0.6668 273.7047 274.3715 286.1010 163.1185 -0.6569 273.7352 274.3921 286.0402 163.9705 -0.6605 273.7748 274.4353 286.0380 164.7625 -0.6349 273.9707 274.6057 286.2753 165.5558 -0.6402 274.0097 274.6499 286.3780 166.3825 -0.6411 274.3327 274.9738 286.5281 167.1458 -0.6430 274.5257 275.1686 286.9304 167.9995 -0.6676 274.6227 275.2903 287.2391 168.7615 -0.6550 274.8211 275.4761 287.3074 169.5835 -0.6598 274.9466 275.6064 287.5019 170.4055 -0.6705 275.0445 275.7150 287.3411 171.1675 -0.6819 275.1277 275.8095 287.4052 172.0203 -0.6802 275.3738 276.0540 287.6285 172.7843 -0.6843 275.3807 276.0650 287.8579 173.6070 -0.6757 275.4629 276.1387 288.0668 174.4233 -0.6770 275.4622 276.1392 288.3431 175.1813 -0.6768 275.6093 276.2861 288.4249 176.0210 -0.6957 275.9013 276.5970 288.7114 176.7748 -0.6914 276.0633 276.7548 288.8622 177.5910 -0.6935 275.9133 276.6068 289.0765 178.4053 -0.7094 276.1575 276.8669 289.3107 179.1625 -0.7102 276.2235 276.9337 289.4544 180.0130 -0.7090 276.4058 277.1148 289.5328 180.7720 -0.7042 276.4970 277.2012 289.6566 181.5900 -0.7040 276.5701 277.2741 289.8694 182.4080 -0.7026 276.6918 277.3944 289.9425 183.1660 -0.7169 276.7398 277.4567 289.9650 184.0140 -0.7257 276.7328 277.4585 289.9773 184.8023 -0.7210 276.9330 277.6540 289.9726 185.5900 -0.7234 276.9151 277.6386 290.0448 186.4083 -0.7265 276.9157 277.6422 290.0060 187.1963 -0.7296 277.0723 277.8020 290.0733 188.0150 -0.7272 277.3454 278.0727 290.1675 188.8038 -0.7319 277.2714 278.0033 290.2286 189.5940 -0.7336 277.4172 278.1508 290.3794 190.4428 -0.7334 277.6488 278.3822 290.4659 191.2010 -0.7237 277.8060 278.5297 290.5347 192.0210 -0.7287 277.8915 278.6202 290.5647 192.8408 -0.7289 278.0455 278.7744 290.6388 193.6015 -0.7355 278.1653 278.9008 290.8941 194.4538 -0.7330 278.2730 279.0060 290.8451 195.2155 -0.7318 278.3562 279.0880 290.9590 196.0378 -0.7601 278.4929 279.2530 291.0654 196.8613 -0.7581 278.6337 279.3918 291.0676 197.6235 -0.7788 278.7134 279.4923 291.2856 198.4760 -0.7802 278.7017 279.4819 291.3676 199.2375 -0.7899 278.6904 279.4804 291.5179 200.0598 -0.7759 278.9839 279.7598 291.6027 200.8818 -0.7912 279.0716 279.8628 291.7643 201.6435 -0.7851 279.4497 280.2348 291.8041 202.4998 -0.7768 279.4567 280.2335 291.8028 203.2615 -0.7808 279.7648 280.5456 291.9268 204.0835 -0.7936 279.7958 280.5894 292.0911 204.8793 -0.7815 279.8090 280.5905 292.1908 205.6753 -0.8011 279.7865 280.5876 292.2891 206.5008 -0.7946 279.9186 280.7132 292.3788 207.2568 -0.7889 280.1635 280.9524 292.5608 208.1018 -0.7973 280.1783 280.9755 292.5633 208.8898 -0.8089 280.3498 281.1587 292.6776 209.6770 -0.7871 280.5442 281.3314 292.8283 210.4950 -0.7885 280.6302 281.4187 292.9680 211.2830 -0.8027 280.6983 281.5010 293.0591 212.1010 -0.8011 280.7941 281.5952 293.1211 212.8928 -0.7938 280.8994 281.6932 293.1510 213.6820 -0.8153 281.1314 281.9467 293.3776 214.5003 -0.8158 281.2347 282.0505 293.4083 215.2890 -0.8097 281.1793 281.9890 293.6130 216.1078 -0.8073 281.2937 282.1010 293.7717 216.8960 -0.8139 281.4386 282.2525 293.9188 217.6858 -0.8089 281.6077 282.4166 293.9924 218.5345 -0.8188 281.6697 282.4886 294.1035 219.2930 -0.8155 281.8472 282.6627 294.2186 220.1128 -0.8326 281.8997 282.7323 294.3782 220.9325 -0.8300 282.0935 282.9235 294.4196 221.6920 -0.8286 282.1453 282.9738 294.5957 222.5425 -0.8286 282.2570 283.0856 294.7115 223.3355 -0.8360 282.4652 283.3012 294.7738 224.1285 -0.8382 282.5587 283.3969 294.8232 224.9505 -0.8416 282.8072 283.6488 294.9137 225.7125 -0.8451 282.7644 283.6095 295.0659 226.5645 -0.8411 282.9932 283.8343 295.2170 227.3310 -0.8348 283.1939 284.0286 295.2773 228.1575 -0.8582 283.2873 284.1455 295.3654 228.9495 -0.8535 283.2827 284.1362 295.4680 229.7413 -0.8656 283.4122 284.2778 295.5179 230.5965 -0.8772 283.5924 284.4696 295.6569 231.3575 -0.8788 283.7580 284.6368 295.7130 232.1798 -0.8632 283.7992 284.6624 295.7733 232.9720 -0.8590 283.9061 284.7651 295.9018 233.7635 -0.8689 284.1102 284.9790 295.9854 234.5908 -0.8810 284.0668 284.9478 296.1626 235.3825 -0.8731 284.1265 284.9996 296.3131 236.2048 -0.8891 284.2292 285.1183 296.3871 237.0008 -0.8846 284.5920 285.4766 296.3762 237.7935 -0.8990 284.6220 285.5209 296.4653 238.6110 -0.9061 284.6347 285.5408 296.7547 239.3965 -0.8905 284.8232 285.7137 296.8706 240.2118 -0.8766 284.9372 285.8138 296.9275 241.0015 -0.8743 284.9224 285.7967 296.9473 241.7913 -0.8805 285.0854 285.9660 297.0102 242.6090 -0.8995 285.2811 286.1806 297.1273 243.3983 -0.8977 285.3110 286.2087 297.3053 244.2200 -0.9024 285.4212 286.3236 297.4088 245.0080 -0.9061 285.5067 286.4127 297.4284 245.7960 -0.9000 285.6693 286.5693 297.5800 246.6140 -0.9004 285.7937 286.6942 297.7081 247.4020 -0.8930 285.8524 286.7454 297.8626 248.2200 -0.9101 286.0620 286.9721 297.9894 249.0080 -0.9084 285.9946 286.9030 298.0701 249.7970 -0.8959 286.1937 287.0895 298.1761 250.6468 -0.9185 286.1859 287.1044 298.3069 251.4053 -0.9155 286.1669 287.0823 298.4369 252.2250 -0.9186 286.1800 287.0986 298.5396 253.0435 -0.9171 286.2588 287.1759 298.7310 253.8023 -0.9135 286.3604 287.2738 298.8521 254.6518 -0.9231 286.4663 287.3894 298.9673 255.4425 -0.9168 286.5348 287.4516 298.9905 256.2335 -0.9134 286.8000 287.7134 299.1651 257.0555 -0.9114 286.8339 287.7453 299.2826 257.8475 -0.9340 286.8998 287.8338 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