DTA measure 3dta_pb3 Date: 2024326:1527 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.09 s Mass = 1094.800 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2846 -4.2366 423.2753 427.5119 423.6513 3.8890 -4.2355 423.5139 427.7494 423.6834 5.4903 -4.2437 423.8428 428.0866 423.5837 7.1033 -4.2527 424.0085 428.2612 423.5971 8.6940 -4.2512 424.1952 428.4464 423.5124 10.3144 -4.2499 424.4228 428.6727 423.4177 11.9050 -4.2575 424.6643 428.9218 423.3503 13.5114 -4.2827 424.9035 429.1862 423.2292 15.1028 -4.2680 425.0758 429.3438 423.0138 16.7235 -4.2656 425.2976 429.5632 422.8345 18.3309 -4.2746 425.5129 429.7875 422.5742 19.9321 -4.2826 425.7087 429.9913 422.4376 21.5309 -4.2968 425.9328 430.2295 422.2011 23.1353 -4.2744 426.1011 430.3755 421.9356 24.7506 -4.2870 426.3214 430.6085 421.7517 26.3719 -4.2761 426.5423 430.8184 421.5338 27.9771 -4.2784 426.7533 431.0317 421.2585 29.5780 -4.2796 426.8511 431.1307 421.0876 31.1776 -4.2641 427.1647 431.4288 420.8682 32.7916 -4.2284 427.3130 431.5414 420.6304 34.4055 -4.2346 427.4565 431.6911 420.4249 36.0195 -4.2489 427.6232 431.8721 420.1675 37.6185 -4.2620 427.6993 431.9613 419.9049 39.2196 -4.2857 427.8495 432.1352 419.7618 40.8236 -4.2885 428.0967 432.3851 419.5564 42.4313 -4.2766 428.2019 432.4784 419.4044 44.0380 -4.3013 428.3872 432.6885 419.1762 45.6371 -4.2818 428.5404 432.8222 419.0743 47.2268 -4.2836 428.6502 432.9339 418.9023 48.8364 -4.2950 428.7518 433.0469 418.6779 50.4546 -4.2959 428.9841 433.2801 418.5207 52.0649 -4.2920 429.0687 433.3606 418.3619 53.6760 -4.2758 429.2368 433.5126 418.1298 55.2724 -4.2880 429.3697 433.6578 417.9086 56.8725 -4.2839 429.4939 433.7778 417.8266 58.4875 -4.3057 429.5629 433.8686 417.5905 60.1015 -4.2856 429.5857 433.8713 417.3235 61.7033 -4.2927 429.8478 434.1406 417.2211 63.3083 -4.3054 429.9631 434.2685 417.0393 64.9218 -4.3064 429.8930 434.1994 416.8321 66.5216 -4.3045 430.0448 434.3493 416.5955 68.1374 -4.3121 430.1003 434.4124 416.4201 69.7528 -4.2913 430.2217 434.5130 416.1728 71.3598 -4.3005 430.2960 434.5966 415.9185 72.9613 -4.2810 430.3949 434.6759 415.8132 74.5605 -4.2918 430.4792 434.7710 415.6506 76.1895 -4.3061 430.5619 434.8681 415.5116 77.7885 -4.3152 430.6310 434.9462 415.2833 79.3904 -4.3152 430.6837 434.9990 415.0421 81.0044 -4.3161 430.7413 435.0574 414.8205 82.6043 -4.3115 430.7992 435.1106 414.6191 84.2068 -4.3062 430.8842 435.1903 414.4157 85.8410 -4.3068 430.8925 435.1993 414.3196 87.4385 -4.3092 430.8708 435.1800 414.0925 89.0284 -4.2980 430.9795 435.2774 413.9731 90.6224 -4.3177 431.0808 435.3985 413.6908 92.2151 -4.3100 431.0341 435.3441 413.4444 93.8216 -4.2868 431.1299 435.4167 413.3629 95.4320 -4.3111 431.1257 435.4369 413.0830 97.0230 -4.3244 431.1378 435.4622 412.9034 98.6205 -4.3355 431.1844 435.5199 412.7872 100.2339 -4.3091 431.1721 435.4811 412.5467 101.8579 -4.3224 431.2634 435.5858 412.4093 103.4568 -4.3258 431.2700 435.5958 412.1619 105.0585 -4.3320 431.2460 435.5780 411.8972 106.6719 -4.3316 431.3119 435.6435 411.6712 108.2705 -4.3147 431.2081 435.5228 411.5107 109.8695 -4.3032 431.2832 435.5864 411.3334 111.5005 -4.3296 431.2474 435.5771 411.1562 113.0998 -4.3360 431.3231 435.6591 411.0276 114.6995 -4.3406 431.3363 435.6769 410.7708 116.3135 -4.3577 431.3219 435.6796 410.5159 117.9136 -4.3400 431.3523 435.6923 410.3388 119.5385 -4.3746 431.2935 435.6681 410.2203 121.1290 -4.3805 431.2779 435.6584 409.9772 122.7216 -4.3884 431.2405 435.6289 409.7825 124.3289 -4.3773 431.1706 435.5479 409.4793 125.9268 -4.3765 431.0917 435.4683 409.2701 127.5810 -4.4009 431.1758 435.5766 409.0838 129.2191 -4.4038 431.0851 435.4890 408.9378 130.8331 -4.3809 431.0842 435.4651 408.7052 132.4325 -4.3867 431.1191 435.5057 408.5075 134.0410 -4.4067 431.0735 435.4802 408.3683 135.6358 -4.4194 431.0393 435.4587 408.1435 137.2645 -4.4027 430.9340 435.3367 407.8790 138.8635 -4.4128 430.8487 435.2615 407.7407 140.4636 -4.4203 430.8748 435.2951 407.4911 142.0778 -4.4072 430.7558 435.1630 407.3182 143.6773 -4.4113 430.7448 435.1561 407.1009 145.2916 -4.4061 430.6907 435.0968 406.9931 146.9058 -4.4051 430.6967 435.1018 406.7456 148.5046 -4.4057 430.6076 435.0133 406.5840 150.1185 -4.4094 430.5526 434.9620 406.3269 151.7149 -4.4430 430.4724 434.9154 406.2344 153.3064 -4.4354 430.4186 434.8540 405.9923 154.9253 -4.4240 430.3444 434.7685 405.7252 156.5208 -4.4156 430.2686 434.6842 405.5893 158.1173 -4.4308 430.1818 434.6126 405.3460 159.7110 -4.4396 430.1654 434.6049 405.1198 161.3186 -4.4470 430.0829 434.5299 404.8376 162.9433 -4.4328 430.0029 434.4357 404.7113 164.5371 -4.4383 429.9112 434.3495 404.5383 166.1455 -4.4569 429.9244 434.3813 404.3006 167.7416 -4.4526 429.7292 434.1819 404.0808 169.3561 -4.4564 429.7002 434.1566 403.9386 170.9695 -4.4714 429.6244 434.0958 403.7256 172.5835 -4.4714 429.5135 433.9849 403.4934 174.1830 -4.4454 429.4303 433.8756 403.2848 175.7831 -4.4646 429.3595 433.8241 403.0968 177.3891 -4.4478 429.3010 433.7488 402.9419 179.0203 -4.4618 429.1977 433.6595 402.7878 180.6189 -4.4690 429.0067 433.4758 402.5371 182.2186 -4.4541 429.0534 433.5076 402.3518 183.8281 -4.4618 428.8586 433.3204 402.1304 185.4163 -4.4627 428.7715 433.2343 401.9217 187.0370 -4.4840 428.6912 433.1752 401.7748 188.6285 -4.4914 428.6369 433.1283 401.5486 190.2200 -4.4881 428.5294 433.0175 401.3028 191.8263 -4.4868 428.2295 432.7163 401.0199 193.4330 -4.4720 428.2032 432.6753 400.8553 195.0440 -4.4791 428.1221 432.6011 400.6788 196.6455 -4.4672 428.0568 432.5240 400.4820 198.2541 -4.4908 427.9393 432.4301 400.2275 199.8498 -4.4778 427.8436 432.3214 400.0854 201.4645 -4.4720 427.7027 432.1747 399.8450 203.0793 -4.4814 427.6199 432.1013 399.6451 204.6828 -4.4758 427.4546 431.9304 399.4926 206.2879 -4.4962 427.3929 431.8891 399.3200 207.8875 -4.4909 427.2692 431.7602 399.0515 209.5015 -4.4622 427.1199 431.5821 398.8480 211.1173 -4.4806 427.0610 431.5416 398.6393 212.7315 -4.4620 426.8718 431.3337 398.4039 214.3310 -4.4791 426.7340 431.2132 398.1670 215.9315 -4.4845 426.6205 431.1050 397.9815 217.5373 -4.4765 426.4823 430.9588 397.8055 219.1519 -4.4943 426.4362 430.9305 397.6425 220.7660 -4.4946 426.2353 430.7299 397.5290 222.3656 -4.4911 426.1383 430.6294 397.2308 223.9796 -4.4934 426.0468 430.5402 396.9862 225.5809 -4.5010 425.8715 430.3725 396.8138 227.1859 -4.4870 425.7881 430.2751 396.5796 228.8036 -4.4826 425.7119 430.1945 396.3709 230.4175 -4.5040 425.5028 430.0068 396.2338 232.0088 -4.4593 425.3661 429.8254 396.0240 233.5965 -4.4727 425.2049 429.6776 395.8472 235.1831 -4.4873 425.0675 429.5548 395.6197 236.8040 -4.4791 424.9617 429.4408 395.4572 238.3998 -4.4876 424.7167 429.2043 395.1628 239.9981 -4.4885 424.5645 429.0530 394.9881 241.6050 -4.4934 424.5158 429.0093 394.8194 243.1960 -4.4794 424.3105 428.7898 394.6028 244.8178 -4.4856 424.2266 428.7122 394.4117 246.4250 -4.4584 424.0579 428.5163 394.2430 248.0173 -4.4580 423.8543 428.3122 393.9983 249.6159 -4.4650 423.7593 428.2242 393.8181 251.2281 -4.4493 423.6849 428.1341 393.5761 252.8435 -4.4692 423.5078 427.9769 393.4213 254.4574 -4.4624 423.3289 427.7914 393.1987 256.0575 -4.4683 423.1958 427.6641 393.0091 257.6579 -4.4761 423.0002 427.4763 392.7865 259.2586 -4.4675 422.8133 427.2808 392.5894 260.8899 -4.4656 422.7983 427.2639 392.3903 262.4908 -4.4503 422.5908 427.0412 392.1686 264.0854 -4.4462 422.3791 426.8253 391.9116 265.6893 -4.4430 422.2831 426.7262 391.7542 267.2844 -4.4293 422.1465 426.5758 391.5789 268.8926 -4.4344 422.0296 426.4640 391.2701 270.5031 -4.4479 421.7529 426.2007 391.0638 272.0945 -4.4559 421.6295 426.0853 390.9533 273.7045 -4.4389 421.5506 425.9895 390.7003 275.3004 -4.4146 421.3881 425.8026 390.4512 276.9249 -4.4301 421.2003 425.6303 390.2645 278.5333 -4.4245 421.0969 425.5214 390.0168 280.1321 -4.4105 420.9187 425.3292 389.7840 281.7316 -4.4381 420.7984 425.2365 389.6574 283.3456 -4.4136 420.5753 424.9889 389.4428 284.9631 -4.4265 420.3410 424.7674 389.1751 286.5699 -4.4047 420.2613 424.6659 389.0367 288.1760 -4.4217 420.0707 424.4923 388.8134 289.7776 -4.4120 419.8592 424.2712 388.5778 291.3785 -4.4120 419.7788 424.1908 388.4379 292.9925 -4.4122 419.5911 424.0033 388.1474 294.6080 -4.4169 419.5200 423.9369 388.0979 296.2126 -4.3905 419.2938 423.6843 387.8464 297.7991 -4.3953 419.0890 423.4843 387.6419 299.3944 -4.3929 418.8146 423.2075 387.3931 301.0029 -4.3899 418.7837 423.1736 387.2535 302.6240 -4.3879 418.6078 422.9957 387.0535 304.2195 -4.3936 418.3846 422.7782 386.7774 305.8370 -4.3877 418.2596 422.6473 386.6317 307.4295 -4.3932 418.0892 422.4824 386.4659 309.0516 -4.3787 417.9415 422.3202 386.1790 310.6651 -4.3690 417.7446 422.1136 386.0099 312.2686 -4.3812 417.5495 421.9307 385.7621 313.8625 -4.3926 417.3757 421.7682 385.5094 315.4646 -4.3856 417.3106 421.6962 385.3392 317.0786 -4.3651 417.0177 421.3829 385.0611 318.6950 -4.3619 416.7945 421.1565 384.9056 320.3108 -4.3585 416.6708 421.0293 384.7178 321.9096 -4.3468 416.4753 420.8220 384.4944 323.5236 -4.3446 416.2088 420.5534 384.1909 325.1226 -4.3597 416.0832 420.4429 383.9917 326.7515 -4.3082 416.0405 420.3487 383.8631 328.3480 -4.3423 415.7796 420.1219 383.6875 329.9376 -4.3433 415.6111 419.9544 383.5492 331.5429 -4.3455 415.4525 419.7981 383.3300 333.1361 -4.3416 415.2764 419.6180 383.1228 334.7614 -4.3428 415.1253 419.4681 382.8808 336.3595 -4.3033 414.8605 419.1638 382.6967 337.9545 -4.3290 414.6573 418.9863 382.5459 339.5635 -4.3236 414.5075 418.8311 382.3722 341.1735 -4.3021 414.3789 418.6810 382.1235 342.7809 -4.3165 414.2981 418.6146 381.9680 344.3905 -4.3275 414.0204 418.3479 381.7266 345.9921 -4.3289 413.7958 418.1247 381.5316 347.5921 -4.3214 413.6753 417.9966 381.2166 349.1951 -4.3201 413.4189 417.7390 381.0389 350.8245 -4.3194 413.2915 417.6108 380.8795 352.4235 -4.3183 413.1187 417.4370 380.5758 354.0369 -4.3236 412.9578 417.2814 380.3623 355.6363 -4.3171 412.7765 417.0936 380.2907 357.2395 -4.3036 412.5822 416.8858 380.0567 358.8688 -4.3098 412.3332 416.6430 379.8327 360.4645 -4.2999 412.2189 416.5188 379.6701 362.0705 -4.3108 411.9021 416.2129 379.3739 363.6538 -4.3048 411.8682 416.1730 379.1973 365.2606 -4.2862 411.6119 415.8981 378.9519 366.8720 -4.3023 411.4992 415.8014 378.7211 368.4780 -4.3104 411.2857 415.5961 378.4771 370.0721 -4.3130 411.0576 415.3706 378.2895 371.6796 -4.3051 410.9064 415.2116 378.1144 373.2868 -4.3027 410.7175 415.0202 377.9262 374.8946 -4.3039 410.5133 414.8172 377.7136 376.5073 -4.3048 410.3090 414.6138 377.4705 378.1116 -4.2652 410.1219 414.3871 377.2744 379.7125 -4.2666 409.9473 414.2139 377.1020 381.3181 -4.2412 409.7468 413.9880 376.8142 382.9388 -4.2573 409.4966 413.7539 376.6213 384.5448 -4.3031 409.3579 413.6610 376.3995 386.1518 -4.3078 409.1378 413.4456 376.2066 387.7650 -4.2762 409.0366 413.3128 376.0030 389.3805 -4.2990 408.8057 413.1046 375.8185 390.9808 -4.2929 408.5916 412.8845 375.6366 392.6101 -4.2827 408.5199 412.8026 375.4534 394.2105 -4.2788 408.3351 412.6139 375.2400 395.8116 -4.2838 408.0347 412.3185 374.9678 397.4123 -4.2736 407.8703 412.1438 374.8229 399.0183 -4.2626 407.5778 411.8404 374.6438 400.6486 -4.2432 407.5273 411.7705 374.4103 402.2486 -4.2327 407.3040 411.5367 374.2670 403.8645 -4.2477 407.1345 411.3823 374.0584 405.4648 -4.2705 406.8988 411.1693 373.8800 407.0638 -4.2689 406.7532 411.0221 373.6484 408.6515 -4.2374 406.5152 410.7526 373.4374 410.2690 -4.2349 406.2995 410.5344 373.1575 411.8543 -4.2358 406.1991 410.4349 373.0377 413.4583 -4.2335 406.0227 410.2562 372.7631 415.0513 -4.2353 405.7992 410.0346 372.5271 416.6730 -4.2286 405.5912 409.8198 372.2558 418.2790 -4.2480 405.3372 409.5852 372.0671 419.8875 -4.2265 405.1316 409.3581 371.8598 421.4805 -4.2162 404.9217 409.1379 371.6303 423.1098 -4.2054 404.7792 408.9846 371.4761 424.7040 -4.1932 404.5618 408.7550 371.2111 426.3165 -4.1941 404.4740 408.6681 371.0929 427.9181 -4.2022 404.3060 408.5082 370.9055 429.5178 -4.2059 404.0256 408.2315 370.7942 431.1195 -4.2041 403.8381 408.0422 370.4945 432.7370 -4.1908 403.6977 407.8885 370.3685 434.3429 -4.1900 403.4734 407.6635 370.1057 435.9476 -4.1686 403.2338 407.4024 369.8413 437.5616 -4.1461 402.9362 407.0823 369.6541 439.1620 -4.1245 402.8717 406.9962 369.5116 440.7715 -4.1319 402.7234 406.8554 369.3357 442.3715 -4.1804 402.4887 406.6691 369.1330 443.9613 -4.1685 402.2752 406.4437 368.8710 445.5690 -4.1193 402.0829 406.2022 368.6735 447.1750 -4.1016 401.8676 405.9692 368.4042 448.7960 -4.1025 401.7152 405.8177 368.2431 450.3900 -4.1112 401.4690 405.5802 367.9605 451.9995 -4.0762 401.2966 405.3729 367.8062 453.5925 -4.0935 401.0831 405.1767 367.6781 455.2148 -4.0609 400.8508 404.9117 367.4789 456.8226 -4.1086 400.7072 404.8157 367.2387 458.4268 -4.0834 400.5713 404.6547 367.0119 460.0265 -4.0986 400.3160 404.4147 366.7339 461.6405 -4.1065 400.1233 404.2298 366.6325 463.2556 -4.1107 399.9452 404.0558 366.3821 464.8695 -4.0958 399.7326 403.8284 366.1665 466.4685 -4.0910 399.5945 403.6855 366.0060 468.0669 -4.0815 399.3672 403.4486 365.8897 469.6808 -4.0927 399.1760 403.2687 365.5822 471.3099 -4.0914 399.0288 403.1202 365.4078 472.9014 -4.0604 398.7275 402.7879 365.1705 474.5033 -4.0432 398.5401 402.5834 364.9901 476.0930 -4.0487 398.3049 402.3536 364.7599 477.6864 -4.0502 398.1087 402.1589 364.5844 479.3120 -4.0608 397.9579 402.0187 364.4146 480.9194 -4.0469 397.7616 401.8085 364.1464 482.5169 -4.0298 397.5760 401.6058 363.9054 484.1108 -4.0481 397.4310 401.4791 363.6990 485.7330 -4.0431 397.1436 401.1867 363.4094 487.3326 -4.0373 396.9856 401.0229 363.1732 488.9480 -4.0177 396.7313 400.7491 362.9296 490.5466 -4.0103 396.5562 400.5665 362.6703 492.1456 -4.0063 396.3139 400.3202 362.5075 493.7598 -3.9855 396.1733 400.1587 362.2771 495.3756 -3.9536 395.9149 399.8685 361.9691 496.9790 -3.9542 395.7862 399.7404 361.8811 498.5825 -3.9694 395.5556 399.5250 361.7370 500.1965 -3.9702 395.3057 399.2759 361.4386 501.8106 -3.9636 395.1116 399.0752 361.2115 503.4320 -3.9600 395.0792 399.0392 361.0795 505.0298 -3.9332 394.9040 398.8372 360.9269 506.6174 -3.9201 394.5751 398.4952 360.6680 508.2239 -3.9199 394.3520 398.2719 360.3810 509.8200 -3.9166 394.1581 398.0747 360.3113 511.4450 -3.9058 394.0042 397.9100 360.0448 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