DTA measure 1gyors Test Date: 20231017:1453 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.31 s Mass = 1402.000 mg data_number = 1269 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2715 0.4092 217.8921 217.4829 261.3498 2.1243 0.4091 218.1730 217.7639 261.3804 2.8865 0.4057 218.4444 218.0387 261.3967 3.7083 0.4047 218.7083 218.3036 261.4576 4.5248 0.4041 218.9812 218.5771 261.4844 5.2840 0.4034 219.2495 218.8461 261.5087 6.1320 0.4023 219.5359 219.1336 261.5520 6.8900 0.4017 219.7634 219.3617 261.5894 7.7080 0.4001 220.0499 219.6498 261.6460 8.5263 0.3985 220.3265 219.9280 261.6755 9.2850 0.3974 220.5800 220.1826 261.7427 10.1335 0.3984 220.8431 220.4448 261.7982 10.8955 0.3975 221.0840 220.6865 261.8536 11.7153 0.3946 221.3498 220.9552 261.9265 12.5360 0.3928 221.6108 221.2180 261.9959 13.2975 0.3934 221.8362 221.4428 262.0698 14.1500 0.3924 222.1158 221.7234 262.1648 14.9108 0.3908 222.3678 221.9770 262.2581 15.7328 0.3921 222.6408 222.2486 262.3689 16.5250 0.3885 222.8780 222.4895 262.4720 17.3165 0.3847 223.1291 222.7445 262.5612 18.1390 0.3840 223.3862 223.0022 262.6600 18.9305 0.3822 223.6277 223.2455 262.7750 19.7528 0.3814 223.8942 223.5128 262.9133 20.5448 0.3786 224.1463 223.7677 263.0297 21.3365 0.3779 224.3870 224.0091 263.1532 22.1588 0.3761 224.6427 224.2665 263.3022 22.9505 0.3728 224.8965 224.5238 263.4359 23.7725 0.3677 225.1374 224.7697 263.5879 24.5645 0.3666 225.3733 225.0067 263.7207 25.3565 0.3637 225.6336 225.2700 263.8513 26.1785 0.3648 225.8835 225.5188 263.9755 26.9405 0.3570 226.1201 225.7631 264.1377 27.7925 0.3577 226.3800 226.0223 264.2815 28.5845 0.3551 226.5986 226.2436 264.4405 29.3765 0.3501 226.8366 226.4865 264.5939 30.1985 0.3462 227.0985 226.7523 264.7313 30.9603 0.3434 227.3326 226.9892 264.8943 31.8125 0.3400 227.5936 227.2536 265.0678 32.6045 0.3364 227.8285 227.4921 265.1993 33.3968 0.3332 228.0530 227.7198 265.3386 34.2193 0.3262 228.3102 227.9840 265.4968 34.9818 0.3240 228.5389 228.2149 265.6369 35.8340 0.3207 228.8026 228.4819 265.7971 36.6258 0.3134 229.0271 228.7137 265.9636 37.4140 0.3122 229.2597 228.9475 266.1090 38.2323 0.3064 229.5068 229.2004 266.2636 38.9900 0.3031 229.7209 229.4178 266.4189 39.8383 0.2965 229.9683 229.6718 266.5759 40.6265 0.2911 230.2275 229.9364 266.7120 41.4150 0.2895 230.4512 230.1617 266.8514 42.2340 0.2823 230.6855 230.4032 267.0194 43.0225 0.2775 230.8952 230.6176 267.1573 43.8418 0.2734 231.1417 230.8683 267.2880 44.6308 0.2675 231.3634 231.0959 267.4060 45.4220 0.2620 231.5855 231.3235 267.5697 46.2435 0.2573 231.8309 231.5736 267.6952 47.0340 0.2531 232.0776 231.8245 267.8491 47.8560 0.2457 232.3122 232.0665 267.9980 48.6485 0.2419 232.5346 232.2926 268.1342 49.4398 0.2371 232.7422 232.5051 268.2670 50.2623 0.2305 232.9861 232.7556 268.3926 51.0538 0.2247 233.2202 232.9955 268.5234 51.8780 0.2188 233.4311 233.2123 268.6685 52.6700 0.2126 233.6518 233.4392 268.7893 53.4615 0.2071 233.8682 233.6612 268.9211 54.2840 0.2022 234.1174 233.9152 269.0514 55.0758 0.1971 234.3633 234.1662 269.1713 55.8978 0.1911 234.5912 234.4001 269.2998 56.6900 0.1834 234.7848 234.6014 269.4302 57.4815 0.1764 235.0186 234.8422 269.5644 58.3040 0.1708 235.2473 235.0765 269.6920 59.0958 0.1644 235.4699 235.3055 269.7972 59.9178 0.1574 235.7138 235.5564 269.9232 60.7098 0.1511 235.9203 235.7693 270.0594 61.5015 0.1447 236.1335 235.9887 270.1867 62.3543 0.1393 236.3606 236.2213 270.3148 63.1165 0.1327 236.6022 236.4695 270.4370 63.9388 0.1293 236.8208 236.6915 270.5721 64.7305 0.1240 237.0369 236.9130 270.6969 65.5225 0.1137 237.2290 237.1153 270.8190 66.3745 0.1100 237.4689 237.3589 270.9437 67.1365 0.1027 237.6692 237.5665 271.0844 67.9585 0.0949 237.8926 237.7976 271.2176 68.7783 0.0879 238.1188 238.0309 271.3239 69.5375 0.0819 238.3242 238.2423 271.4361 70.3860 0.0784 238.5526 238.4742 271.5859 71.1740 0.0760 238.7656 238.6896 271.7108 71.9620 0.0673 238.9825 238.9152 271.8138 72.7803 0.0569 239.2128 239.1559 271.9431 73.5390 0.0490 239.4223 239.3733 272.0632 74.3885 0.0428 239.6283 239.5856 272.1874 75.1470 0.0377 239.8335 239.7957 272.2920 75.9658 0.0327 240.0795 240.0468 272.4289 76.7843 0.0262 240.2863 240.2601 272.5647 77.5455 0.0185 240.4668 240.4483 272.6785 78.3975 0.0091 240.6954 240.6863 272.8060 79.1595 0.0029 240.9031 240.9002 272.9652 79.9815 -0.0036 241.1094 241.1129 273.0891 80.7735 -0.0125 241.3093 241.3219 273.1981 81.5655 -0.0188 241.5247 241.5436 273.3209 82.3908 -0.0229 241.7480 241.7709 273.4810 83.1845 -0.0331 241.9592 241.9922 273.6229 84.0065 -0.0351 242.1715 242.2066 273.7693 84.7985 -0.0426 242.3792 242.4218 273.9182 85.5905 -0.0485 242.5942 242.6427 274.0584 86.4125 -0.0580 242.8095 242.8674 274.2158 87.1745 -0.0648 243.0099 243.0747 274.3637 88.0265 -0.0691 243.2101 243.2792 274.5333 88.8185 -0.0776 243.4091 243.4866 274.6779 89.6105 -0.0872 243.6114 243.6986 274.8212 90.4323 -0.0916 243.8303 243.9218 274.9553 91.1943 -0.0962 244.0379 244.1341 275.0948 92.0460 -0.1047 244.2502 244.3550 275.2609 92.8380 -0.1145 244.4468 244.5613 275.4181 93.6295 -0.1188 244.6412 244.7600 275.5692 94.4520 -0.1238 244.8614 244.9852 275.7120 95.2135 -0.1320 245.0602 245.1923 275.8557 96.0733 -0.1433 245.2801 245.4234 276.0214 96.8358 -0.1489 245.4622 245.6110 276.1457 97.6578 -0.1556 245.6713 245.8269 276.2979 98.4498 -0.1644 245.8634 246.0278 276.4226 99.2415 -0.1717 246.0599 246.2316 276.5449 100.0943 -0.1769 246.2917 246.4687 276.6936 100.8558 -0.1851 246.4869 246.6720 276.8195 101.6740 -0.1901 246.6875 246.8776 276.9734 102.4620 -0.1963 246.8836 247.0799 277.0990 103.2500 -0.2059 247.0802 247.2862 277.2354 104.0980 -0.2123 247.2931 247.5053 277.3710 104.8563 -0.2196 247.4686 247.6882 277.4952 105.6755 -0.2247 247.6714 247.8961 277.6172 106.4643 -0.2323 247.8706 248.1029 277.7418 107.2530 -0.2401 248.0715 248.3116 277.8787 108.1018 -0.2496 248.2895 248.5391 278.0167 108.8613 -0.2546 248.4774 248.7319 278.1273 109.6818 -0.2627 248.6882 248.9509 278.2679 110.5040 -0.2710 248.8831 249.1541 278.4043 111.2655 -0.2787 249.0500 249.3286 278.5178 112.1178 -0.2841 249.2617 249.5458 278.6522 112.8810 -0.2934 249.4515 249.7450 278.7751 113.7055 -0.3005 249.6595 249.9600 278.9006 114.4978 -0.3087 249.8517 250.1604 279.0224 115.2895 -0.3162 250.0421 250.3583 279.1297 116.1120 -0.3225 250.2373 250.5598 279.2797 116.9035 -0.3258 250.4312 250.7570 279.3751 117.7258 -0.3360 250.6246 250.9607 279.5188 118.5178 -0.3430 250.8169 251.1599 279.6470 119.3095 -0.3479 251.0162 251.3641 279.7707 120.1320 -0.3548 251.2117 251.5664 279.9045 120.9235 -0.3629 251.4012 251.7641 280.0221 121.7455 -0.3702 251.6063 251.9765 280.1417 122.5375 -0.3781 251.8095 252.1876 280.2780 123.3295 -0.3838 252.0099 252.3937 280.3835 124.1815 -0.3923 252.2142 252.6065 280.5022 124.9435 -0.4002 252.3796 252.7798 280.6110 125.7655 -0.4077 252.5933 253.0011 280.7459 126.5575 -0.4139 252.7826 253.1965 280.8820 127.3495 -0.4201 252.9803 253.4004 280.9904 128.2015 -0.4265 253.1677 253.5942 281.1213 128.9635 -0.4347 253.3433 253.7780 281.2468 129.7863 -0.4445 253.5444 253.9889 281.3804 130.6083 -0.4532 253.7501 254.2033 281.5123 131.3695 -0.4595 253.9269 254.3864 281.6338 132.2225 -0.4633 254.1202 254.5835 281.7783 132.9833 -0.4678 254.2869 254.7548 281.8964 133.8010 -0.4751 254.4748 254.9499 282.0495 134.5893 -0.4850 254.6662 255.1512 282.1815 135.3770 -0.4881 254.8391 255.3272 282.3171 136.2258 -0.4917 255.0472 255.5389 282.4684 136.9838 -0.5016 255.2284 255.7300 282.6052 137.8030 -0.5082 255.4224 255.9306 282.7620 138.6210 -0.5137 255.6067 256.1204 282.9082 139.3790 -0.5212 255.7774 256.2986 283.0303 140.2285 -0.5293 255.9792 256.5086 283.1855 141.0188 -0.5361 256.1524 256.6885 283.3270 141.8105 -0.5444 256.3408 256.8852 283.4491 142.6325 -0.5503 256.5312 257.0815 283.6078 143.3940 -0.5566 256.6950 257.2516 283.7719 144.2455 -0.5607 256.9027 257.4634 283.9195 145.0373 -0.5726 257.1030 257.6755 284.0559 145.8288 -0.5774 257.2829 257.8603 284.1895 146.6515 -0.5855 257.4550 258.0405 284.3458 147.4125 -0.5928 257.6213 258.2141 284.4763 148.2650 -0.6026 257.8226 258.4251 284.6235 149.0270 -0.6101 257.9942 258.6044 284.7558 149.8488 -0.6171 258.1842 258.8013 284.8759 150.6710 -0.6231 258.3715 258.9946 285.0048 151.4325 -0.6263 258.5598 259.1861 285.1067 152.2850 -0.6340 258.7577 259.3917 285.2541 153.0468 -0.6428 258.9321 259.5749 285.3652 153.8688 -0.6479 259.0995 259.7474 285.4997 154.6910 -0.6544 259.2804 259.9347 285.6427 155.4528 -0.6600 259.4693 260.1293 285.7430 156.3053 -0.6651 259.6606 260.3257 285.8644 157.0675 -0.6756 259.8439 260.5196 285.9871 157.8898 -0.6833 260.0350 260.7183 286.1110 158.7118 -0.6910 260.2244 260.9153 286.2393 159.4735 -0.6951 260.3900 261.0851 286.3636 160.3265 -0.7018 260.5745 261.2763 286.4903 161.0895 -0.7072 260.7425 261.4498 286.5840 161.9145 -0.7108 260.9217 261.6325 286.7118 162.7065 -0.7212 261.0761 261.7973 286.8305 163.5048 -0.7284 261.2679 261.9964 286.9438 164.3185 -0.7348 261.4489 262.1837 287.0715 165.1105 -0.7420 261.6375 262.3796 287.1920 165.9300 -0.7450 261.8347 262.5796 287.3359 166.7168 -0.7533 261.9886 262.7419 287.4665 167.5358 -0.7601 262.1682 262.9283 287.5960 168.3245 -0.7653 262.3595 263.1248 287.7210 169.1130 -0.7736 262.5413 263.3150 287.8659 169.9610 -0.7799 262.7037 263.4836 288.0230 170.7190 -0.7867 262.8809 263.6676 288.1599 171.5385 -0.7919 263.0673 263.8593 288.2976 172.3280 -0.7973 263.2390 264.0364 288.4356 173.1180 -0.8039 263.4064 264.2102 288.5803 173.9678 -0.8079 263.5933 264.4012 288.7036 174.7270 -0.8185 263.7721 264.5907 288.8359 175.5473 -0.8262 263.9408 264.7670 288.9740 176.3375 -0.8308 264.1304 264.9612 289.1160 177.1295 -0.8391 264.3074 265.1465 289.2443 177.9815 -0.8481 264.4833 265.3315 289.3904 178.7435 -0.8563 264.6511 265.5073 289.5291 179.5655 -0.8646 264.8263 265.6909 289.6818 180.3580 -0.8715 265.0052 265.8767 289.8340 181.1515 -0.8763 265.1765 266.0528 289.9793 181.9735 -0.8807 265.3464 266.2271 290.1076 182.7655 -0.8825 265.5204 266.4029 290.2459 183.5875 -0.8911 265.7121 266.6032 290.3787 184.3795 -0.8936 265.8935 266.7871 290.5185 185.1715 -0.9034 266.0554 266.9588 290.6502 185.9935 -0.9109 266.2291 267.1401 290.7991 186.7850 -0.9181 266.3893 267.3074 290.9350 187.6073 -0.9214 266.5818 267.5033 291.0880 188.3995 -0.9283 266.7455 267.6738 291.2111 189.1905 -0.9365 266.9301 267.8666 291.3462 190.0130 -0.9453 267.1050 268.0502 291.4726 190.8048 -0.9504 267.2605 268.2108 291.6267 191.6268 -0.9575 267.4426 268.4002 291.7797 192.4190 -0.9632 267.6262 268.5893 291.9124 193.2105 -0.9698 267.7938 268.7636 292.0581 194.0380 -0.9763 267.9658 268.9421 292.1923 194.8295 -0.9826 268.1454 269.1280 292.3251 195.6525 -0.9859 268.3192 269.3051 292.4692 196.4448 -0.9913 268.4904 269.4817 292.6134 197.2365 -1.0009 268.6532 269.6541 292.7580 198.0588 -1.0065 268.8261 269.8326 292.9024 198.8505 -1.0124 269.0130 270.0254 293.0312 199.6735 -1.0174 269.1975 270.2149 293.1762 200.4655 -1.0241 269.3547 270.3788 293.3094 201.2575 -1.0319 269.5111 270.5430 293.4493 202.1095 -1.0388 269.6890 270.7278 293.5593 202.8715 -1.0442 269.8520 270.8962 293.6923 203.6943 -1.0511 270.0241 271.0751 293.8188 204.4865 -1.0545 270.1935 271.2481 293.9416 205.2795 -1.0607 270.3647 271.4254 294.0550 206.1315 -1.0642 270.5582 271.6224 294.1783 206.8935 -1.0732 270.7149 271.7880 294.2923 207.7163 -1.0805 270.8800 271.9605 294.4247 208.5380 -1.0819 271.0621 272.1440 294.5431 209.2995 -1.0883 271.2125 272.3008 294.6433 210.1520 -1.0934 271.3833 272.4767 294.7590 210.9138 -1.0978 271.5521 272.6499 294.8536 211.7365 -1.1032 271.7198 272.8230 294.9797 212.5593 -1.1058 271.9016 273.0074 295.1081 213.3215 -1.1123 272.0716 273.1840 295.2092 214.1740 -1.1177 272.2676 273.3853 295.3360 214.9358 -1.1258 272.4328 273.5586 295.4641 215.7578 -1.1276 272.5919 273.7195 295.5960 216.5800 -1.1366 272.7680 273.9045 295.7114 217.3425 -1.1412 272.9326 274.0738 295.8157 218.1953 -1.1463 273.0954 274.2417 295.9378 218.9598 -1.1542 273.2460 274.4002 296.0700 219.7825 -1.1584 273.4301 274.5885 296.2108 220.6050 -1.1663 273.5862 274.7525 296.3261 221.3675 -1.1730 273.7518 274.9247 296.4468 222.2200 -1.1801 273.9396 275.1197 296.5853 222.9825 -1.1885 274.0906 275.2791 296.7166 223.8053 -1.1907 274.2456 275.4364 296.8544 224.6275 -1.1949 274.4225 275.6174 296.9775 225.3895 -1.1995 274.5744 275.7739 297.1073 226.2420 -1.2065 274.7643 275.9708 297.2329 227.0045 -1.2128 274.9234 276.1362 297.3624 227.8258 -1.2163 275.0840 276.3003 297.4971 228.6183 -1.2238 275.2509 276.4747 297.6162 229.4108 -1.2285 275.4326 276.6610 297.7489 230.2545 -1.2347 275.5913 276.8260 297.8887 231.0095 -1.2406 275.7447 276.9853 298.0075 231.8210 -1.2455 275.9120 277.1576 298.1314 232.6065 -1.2533 276.0643 277.3175 298.2430 233.3940 -1.2571 276.2237 277.4808 298.3584 234.2403 -1.2624 276.3897 277.6521 298.5049 234.9978 -1.2622 276.5630 277.8252 298.6529 235.8160 -1.2646 276.7429 278.0074 298.7828 236.6040 -1.2704 276.8875 278.1578 298.9048 237.3920 -1.2767 277.0510 278.3277 299.0294 238.2108 -1.2815 277.2332 278.5147 299.1533 238.9993 -1.2840 277.3776 278.6615 299.2752 239.8180 -1.2869 277.5402 278.8271 299.4091 240.6065 -1.2965 277.7117 279.0082 299.5152 241.3950 -1.3021 277.8677 279.1698 299.6548 242.2443 -1.3079 278.0371 279.3450 299.7761 243.0040 -1.3129 278.1950 279.5079 299.8873 243.8245 -1.3186 278.3511 279.6696 300.0547 244.6160 -1.3237 278.5174 279.8411 300.1765 245.4075 -1.3278 278.7003 280.0281 300.2863 246.2600 -1.3322 278.8583 280.1905 300.4447 247.0218 -1.3382 279.0031 280.3413 300.5774 247.8438 -1.3436 279.1811 280.5248 300.7179 248.6360 -1.3509 279.3247 280.6755 300.8621 249.4275 -1.3543 279.4805 280.8348 301.0055 250.2500 -1.3613 279.6611 281.0224 301.1525 251.0415 -1.3665 279.8302 281.1967 301.3098 251.8638 -1.3705 279.9879 281.3584 301.4521 252.6558 -1.3748 280.1501 281.5250 301.5867 253.4475 -1.3828 280.3144 281.6972 301.7345 254.2698 -1.3877 280.4662 281.8539 301.8878 255.0615 -1.3895 280.6245 282.0141 302.0413 255.8838 -1.3937 280.7899 282.1836 302.1914 256.6755 -1.4002 280.9576 282.3578 302.3255 257.4675 -1.4049 281.1233 282.5282 302.4844 258.2895 -1.4077 281.2736 282.6813 302.6307 259.0815 -1.4121 281.4375 282.8497 302.7661 259.9035 -1.4170 281.5976 283.0145 302.9213 260.6955 -1.4244 281.7577 283.1821 303.0530 261.4875 -1.4298 281.9151 283.3449 303.1781 262.3395 -1.4345 282.0921 283.5266 303.3488 263.1015 -1.4392 282.2437 283.6829 303.4635 263.9235 -1.4441 282.3953 283.8395 303.6069 264.7458 -1.4496 282.5666 284.0162 303.7311 265.5080 -1.4558 282.7292 284.1850 303.8565 266.3600 -1.4601 282.8841 284.3442 304.0032 267.1218 -1.4645 283.0327 284.4973 304.1315 267.9445 -1.4689 283.2071 284.6760 304.2653 268.7673 -1.4747 283.3730 284.8477 304.3879 269.5298 -1.4809 283.5336 285.0145 304.5018 270.3835 -1.4902 283.6941 285.1844 304.6440 271.1458 -1.4924 283.8460 285.3384 304.7696 271.9685 -1.4967 283.9948 285.4915 304.9025 272.7913 -1.5020 284.1762 285.6781 305.0139 273.5535 -1.5070 284.3098 285.8168 305.1410 274.4063 -1.5105 284.4897 286.0002 305.2765 275.1685 -1.5145 284.6505 286.1649 305.4007 275.9915 -1.5214 284.8110 286.3324 305.5251 276.8135 -1.5258 284.9674 286.4932 305.6453 277.5755 -1.5278 285.1156 286.6434 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