DTA measure 2gyors Test Date: 20231017:1523 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.48 s Mass = 1402.000 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4194 -5.5225 434.8314 440.3538 420.1421 4.0176 -5.5331 434.8511 440.3842 420.1252 5.6165 -5.5388 434.8724 440.4112 420.1027 7.2305 -5.5460 434.9062 440.4522 420.0623 8.8445 -5.5514 434.9324 440.4838 419.9790 10.4435 -5.5591 434.9517 440.5108 419.9078 12.0575 -5.5682 434.9542 440.5224 419.7947 13.6565 -5.5768 434.9763 440.5531 419.6702 15.2555 -5.5823 434.9998 440.5821 419.5267 16.8843 -5.5882 435.0222 440.6104 419.3662 18.4839 -5.5948 435.0364 440.6312 419.2086 20.0981 -5.5971 435.0388 440.6359 419.0313 21.6981 -5.6028 435.0561 440.6589 418.8243 23.2978 -5.6084 435.0784 440.6867 418.6393 24.9116 -5.6139 435.0713 440.6852 418.4583 26.5255 -5.6160 435.0750 440.6910 418.2339 28.1191 -5.6185 435.0845 440.7030 418.0302 29.7244 -5.6188 435.0840 440.7028 417.8169 31.3166 -5.6220 435.0720 440.6941 417.6146 32.9231 -5.6263 435.0657 440.6921 417.3891 34.5309 -5.6288 435.0762 440.7050 417.1577 36.1398 -5.6322 435.0741 440.7063 416.9514 37.7378 -5.6329 435.0592 440.6922 416.7330 39.3368 -5.6357 435.0440 440.6797 416.5158 40.9506 -5.6361 435.0432 440.6793 416.2934 42.5649 -5.6359 435.0250 440.6610 416.0679 44.1636 -5.6343 435.0014 440.6357 415.8445 45.7775 -5.6363 434.9724 440.6087 415.6288 47.3765 -5.6374 434.9612 440.5986 415.4291 48.9905 -5.6366 434.9441 440.5807 415.2272 50.6045 -5.6372 434.9163 440.5535 415.0058 52.2185 -5.6350 434.8870 440.5220 414.7876 53.8175 -5.6371 434.8623 440.4994 414.6019 55.4165 -5.6400 434.8308 440.4707 414.4021 57.0450 -5.6371 434.8011 440.4382 414.1990 58.6595 -5.6387 434.7551 440.3938 414.0094 60.2534 -5.6387 434.7073 440.3460 413.8318 61.8448 -5.6401 434.6635 440.3036 413.6419 63.4524 -5.6399 434.6293 440.2692 413.4505 65.0746 -5.6389 434.5889 440.2279 413.2751 66.6693 -5.6425 434.5333 440.1758 413.1084 68.2664 -5.6418 434.4932 440.1350 412.9330 69.8794 -5.6411 434.4426 440.0837 412.7557 71.4781 -5.6400 434.3895 440.0295 412.5967 73.1070 -5.6382 434.3365 439.9747 412.3889 74.7058 -5.6382 434.2708 439.9091 412.2187 76.3048 -5.6405 434.2130 439.8535 412.0321 77.9214 -5.6407 434.1641 439.8048 411.8317 79.5128 -5.6400 434.1079 439.7479 411.6453 81.1426 -5.6404 434.0355 439.6759 411.4633 82.7428 -5.6387 433.9652 439.6040 411.2705 84.3569 -5.6412 433.9109 439.5521 411.0710 85.9566 -5.6364 433.8388 439.4753 410.8780 87.5555 -5.6388 433.7780 439.4168 410.7010 89.1746 -5.6415 433.6977 439.3391 410.4925 90.7874 -5.6396 433.6245 439.2641 410.3189 92.3781 -5.6388 433.5344 439.1733 410.1239 93.9700 -5.6422 433.4625 439.1047 409.9509 95.5760 -5.6423 433.3913 439.0336 409.7492 97.1680 -5.6410 433.3010 438.9420 409.5652 98.7929 -5.6387 433.2263 438.8650 409.3703 100.3905 -5.6392 433.1428 438.7820 409.1618 101.9895 -5.6392 433.0632 438.7024 408.9571 103.5885 -5.6393 432.9782 438.6175 408.7540 105.2025 -5.6393 432.8909 438.5302 408.5418 106.8165 -5.6390 432.8029 438.4418 408.3506 108.4305 -5.6370 432.7089 438.3459 408.1253 110.0295 -5.6321 432.6271 438.2592 407.9306 111.6284 -5.6294 432.5190 438.1484 407.7413 113.2421 -5.6293 432.4244 438.0536 407.5341 114.8559 -5.6238 432.3379 437.9617 407.3300 116.4699 -5.6240 432.2291 437.8531 407.1309 118.0688 -5.6239 432.1487 437.7725 406.9488 119.6833 -5.6233 432.0352 437.6584 406.7451 121.2826 -5.6236 431.9290 437.5526 406.5741 122.9109 -5.6224 431.8183 437.4407 406.3661 124.5030 -5.6205 431.7163 437.3368 406.1842 126.0941 -5.6185 431.6111 437.2295 405.9990 127.7000 -5.6170 431.5050 437.1219 405.8036 129.3075 -5.6165 431.3847 437.0012 405.6099 130.9160 -5.6181 431.2925 436.9106 405.4522 132.5129 -5.6144 431.1795 436.7940 405.2654 134.1266 -5.6151 431.0593 436.6744 405.0683 135.7256 -5.6127 430.9566 436.5692 404.8347 137.3398 -5.6095 430.8410 436.4506 404.6236 138.9538 -5.6084 430.7232 436.3316 404.3794 140.5526 -5.6083 430.6019 436.2102 404.1720 142.1668 -5.6067 430.4872 436.0938 403.9424 143.7656 -5.6050 430.3717 435.9768 403.7262 145.3645 -5.6041 430.2542 435.8583 403.5201 146.9935 -5.6020 430.1274 435.7295 403.2988 148.5925 -5.6003 430.0207 435.6210 403.0947 150.2069 -5.5979 429.8710 435.4688 402.8711 151.8065 -5.5992 429.7590 435.3582 402.6512 153.4065 -5.5973 429.6372 435.2345 402.4506 155.0360 -5.5907 429.5123 435.1030 402.2099 156.6321 -5.5905 429.3770 434.9675 402.0059 158.2238 -5.5876 429.2488 434.8364 401.8033 159.8310 -5.5857 429.1045 434.6902 401.6015 161.4233 -5.5843 428.9833 434.5676 401.3841 163.0461 -5.5822 428.8335 434.4157 401.1929 164.6408 -5.5785 428.7139 434.2924 401.0017 166.2383 -5.5784 428.5872 434.1656 400.7954 167.8518 -5.5768 428.4376 434.0144 400.6020 169.4510 -5.5752 428.2889 433.8640 400.4297 171.0649 -5.5718 428.1624 433.7343 400.2244 172.6789 -5.5675 428.0336 433.6011 400.0175 174.2778 -5.5672 427.8927 433.4599 399.8262 175.8768 -5.5648 427.7485 433.3134 399.6266 177.4906 -5.5607 427.5870 433.1477 399.4327 179.1198 -5.5605 427.4663 433.0267 399.2341 180.7070 -5.5568 427.3325 432.8894 399.0468 182.3285 -5.5557 427.1753 432.7310 398.8598 183.9275 -5.5517 427.0278 432.5795 398.6467 185.5271 -5.5489 426.8939 432.4428 398.4865 187.1573 -5.5466 426.7411 432.2877 398.2893 188.7518 -5.5429 426.5903 432.1333 398.0842 190.3589 -5.5421 426.4446 431.9866 397.8833 191.9504 -5.5316 426.3061 431.8377 397.6887 193.5590 -5.5184 426.1586 431.6770 397.4722 195.1818 -5.5226 425.9882 431.5108 397.2752 196.7770 -5.5256 425.8367 431.3623 397.0805 198.3755 -5.5222 425.6898 431.2119 396.8620 199.9745 -5.5185 425.5361 431.0546 396.6631 201.5885 -5.5175 425.3718 430.8893 396.4666 203.2025 -5.5157 425.2221 430.7378 396.2555 204.8165 -5.5150 425.0761 430.5911 396.0432 206.4155 -5.5106 424.9158 430.4264 395.8427 208.0140 -5.5085 424.7676 430.2761 395.6319 209.6129 -5.5066 424.6111 430.1177 395.4364 211.2426 -5.5035 424.4646 429.9681 395.2346 212.8569 -5.4996 424.2822 429.7819 395.0339 214.4558 -5.4925 424.1165 429.6090 394.8407 216.0548 -5.4895 423.9593 429.4489 394.6497 217.6541 -5.4904 423.7990 429.2894 394.4416 219.2836 -5.4849 423.6322 429.1171 394.2362 220.8835 -5.4800 423.4822 428.9621 394.0494 222.4825 -5.4763 423.3216 428.7978 393.8522 224.0969 -5.4729 423.1572 428.6301 393.6646 225.6970 -5.4706 422.9861 428.4568 393.4675 227.3115 -5.4684 422.8228 428.2912 393.2859 228.9264 -5.4654 422.6567 428.1221 393.0781 230.5250 -5.4592 422.4969 427.9561 392.8861 232.1429 -5.4563 422.3441 427.8004 392.6808 233.7443 -5.4554 422.1914 427.6468 392.4605 235.3376 -5.4541 422.0189 427.4730 392.2542 236.9406 -5.4490 421.8540 427.3030 392.0341 238.5480 -5.4416 421.7018 427.1434 391.8131 240.1395 -5.4387 421.5102 426.9489 391.6029 241.7316 -5.4343 421.3424 426.7767 391.3951 243.3386 -5.4317 421.1740 426.6057 391.1892 244.9471 -5.4282 421.0104 426.4386 390.9790 246.5578 -5.4233 420.8549 426.2782 390.7760 248.1558 -5.4212 420.6722 426.0934 390.5515 249.7548 -5.4158 420.5082 425.9241 390.3512 251.3688 -5.4159 420.3511 425.7670 390.1599 252.9849 -5.4119 420.1622 425.5741 389.9425 254.5998 -5.4047 419.9985 425.4032 389.7315 256.1986 -5.4029 419.8159 425.2188 389.5277 257.7976 -5.3999 419.6458 425.0457 389.3186 259.4115 -5.3930 419.4799 424.8728 389.1043 261.0263 -5.3901 419.3103 424.7004 388.9121 262.6414 -5.3869 419.1240 424.5109 388.7021 264.2408 -5.3823 418.9451 424.3274 388.4972 265.8409 -5.3803 418.7783 424.1586 388.3005 267.4555 -5.3765 418.5972 423.9737 388.1036 269.0639 -5.3703 418.4243 423.7946 387.8966 270.6706 -5.3657 418.2504 423.6162 387.7061 272.2619 -5.3607 418.0662 423.4269 387.5094 273.8538 -5.3596 417.8884 423.2479 387.3159 275.4624 -5.3559 417.7246 423.0805 387.1253 277.0729 -5.3522 417.5431 422.8953 386.9173 278.6865 -5.3448 417.3625 422.7073 386.7270 280.2855 -5.3409 417.1823 422.5232 386.5345 281.8855 -5.3408 417.0074 422.3482 386.3492 283.5068 -5.3349 416.8250 422.1599 386.1509 285.1080 -5.3315 416.6392 421.9707 385.9660 286.7220 -5.3270 416.4551 421.7821 385.7686 288.3208 -5.3248 416.2725 421.5973 385.5425 289.9200 -5.3209 416.1079 421.4288 385.3403 291.5348 -5.3155 415.9199 421.2354 385.1222 293.1338 -5.3099 415.7433 421.0532 384.9125 294.7476 -5.3042 415.5612 420.8654 384.6992 296.3616 -5.3016 415.3808 420.6824 384.4858 297.9605 -5.2964 415.2025 420.4989 384.2808 299.5595 -5.2911 415.0251 420.3162 384.0551 301.1679 -5.2868 414.8401 420.1269 383.8475 302.7750 -5.2836 414.6533 419.9370 383.6516 304.3819 -5.2762 414.4791 419.7552 383.4366 305.9733 -5.2715 414.2939 419.5654 383.2288 307.5809 -5.2690 414.1070 419.3760 383.0237 309.1915 -5.2650 413.9292 419.1942 382.8170 310.8046 -5.2606 413.7510 419.0116 382.6000 312.4035 -5.2542 413.5537 418.8079 382.3907 314.0025 -5.2480 413.3756 418.6236 382.1786 315.6165 -5.2432 413.1893 418.4325 381.9724 317.2305 -5.2402 413.0015 418.2417 381.7693 318.8445 -5.2350 412.8017 418.0368 381.5689 320.4435 -5.2319 412.6180 417.8499 381.3554 322.0575 -5.2279 412.4443 417.6722 381.1408 323.6624 -5.2210 412.2576 417.4786 380.9426 325.2630 -5.2162 412.0720 417.2882 380.7285 326.8926 -5.2142 411.8768 417.0910 380.5222 328.4928 -5.2116 411.6916 416.9032 380.3408 330.1068 -5.2066 411.5042 416.7108 380.1270 331.7051 -5.1973 411.3076 416.5049 379.9457 333.2971 -5.1934 411.1294 416.3228 379.7360 334.9183 -5.1875 410.9492 416.1367 379.5437 336.5093 -5.1841 410.7382 415.9223 379.3509 338.1164 -5.1771 410.5782 415.7553 379.1656 339.7101 -5.1729 410.3991 415.5720 378.9697 341.3058 -5.1696 410.1888 415.3584 378.7741 342.9349 -5.1657 409.9991 415.1648 378.5805 344.5339 -5.1594 409.8021 414.9615 378.3930 346.1328 -5.1562 409.6321 414.7883 378.1803 347.7466 -5.1502 409.4459 414.5961 377.9967 349.3456 -5.1460 409.2597 414.4057 377.7931 350.9446 -5.1422 409.0737 414.2159 377.5732 352.5739 -5.1376 408.8616 413.9992 377.3547 354.1739 -5.1346 408.6775 413.8121 377.1515 355.7815 -5.1272 408.4902 413.6174 376.9440 357.3805 -5.1233 408.2895 413.4128 376.7184 358.9800 -5.1181 408.1126 413.2307 376.4937 360.6095 -5.1159 407.9119 413.0278 376.2907 362.2085 -5.1071 407.7203 412.8274 376.0588 363.8215 -5.1022 407.5310 412.6333 375.8370 365.4141 -5.1000 407.3483 412.4483 375.6295 367.0069 -5.0938 407.1624 412.2562 375.4175 368.6289 -5.0894 406.9596 412.0489 375.2038 370.2228 -5.0839 406.7760 411.8599 374.9849 371.8314 -5.0793 406.5664 411.6457 374.7723 373.4266 -5.0741 406.3868 411.4610 374.5606 375.0255 -5.0713 406.2159 411.2872 374.3618 376.6545 -5.0653 406.0040 411.0693 374.1554 378.2535 -5.0599 405.8177 410.8776 373.9429 379.8523 -5.0558 405.6190 410.6748 373.7441 381.4659 -5.0508 405.4319 410.4827 373.5382 383.0650 -5.0433 405.2386 410.2819 373.3240 384.6798 -5.0385 405.0254 410.0639 373.1248 386.2939 -5.0354 404.8369 409.8723 372.9237 387.8928 -5.0277 404.6493 409.6770 372.7245 389.5066 -5.0229 404.4587 409.4816 372.5232 391.1061 -5.0158 404.2454 409.2613 372.3113 392.7364 -5.0123 404.0620 409.0743 372.1097 394.3366 -5.0069 403.8767 408.8836 371.9162 395.9519 -5.0007 403.6663 408.6671 371.7160 397.5486 -4.9961 403.4662 408.4623 371.5160 399.1399 -4.9913 403.2807 408.2720 371.3205 400.7456 -4.9861 403.0943 408.0804 371.1105 402.3549 -4.9746 402.8818 407.8564 370.9390 403.9514 -4.9696 402.7054 407.6750 370.7361 405.5556 -4.9679 402.5141 407.4820 370.5364 407.1544 -4.9637 402.2959 407.2596 370.3374 408.7545 -4.9567 402.1144 407.0711 370.1356 410.3835 -4.9550 401.9218 406.8767 369.9586 411.9830 -4.9504 401.7056 406.6560 369.7647 413.5825 -4.9460 401.5240 406.4701 369.5702 415.1835 -4.9383 401.3451 406.2834 369.3723 416.7975 -4.9325 401.1371 406.0696 369.1700 418.3979 -4.9245 400.9376 405.8621 368.9531 420.0274 -4.9091 400.7448 405.6539 368.7379 421.6259 -4.9033 400.5425 405.4458 368.5312 423.2250 -4.9047 400.3490 405.2537 368.3283 424.8256 -4.8958 400.1375 405.0333 368.1102 426.4411 -4.8905 399.9456 404.8361 367.8987 428.0563 -4.8844 399.7400 404.6243 367.6709 429.6535 -4.8788 399.5629 404.4417 367.4709 431.2594 -4.8769 399.3671 404.2439 367.2490 432.8510 -4.8712 399.1818 404.0530 367.0414 434.4433 -4.8669 399.0005 403.8675 366.8316 436.0661 -4.8600 398.7921 403.6521 366.6212 437.6738 -4.8528 398.5811 403.4339 366.4211 439.2709 -4.8494 398.3862 403.2356 366.2050 440.8698 -4.8434 398.2092 403.0526 366.0008 442.4688 -4.8408 397.9940 402.8348 365.7890 444.0983 -4.8354 397.7950 402.6304 365.6096 445.6979 -4.8239 397.5992 402.4231 365.3765 447.3043 -4.8188 397.3989 402.2177 365.1729 448.9096 -4.8118 397.2058 402.0176 364.9789 450.5096 -4.8041 396.9965 401.8006 364.7886 452.1085 -4.8025 396.8062 401.6088 364.5974 453.7375 -4.7971 396.5987 401.3957 364.3869 455.3515 -4.7938 396.4074 401.2012 364.1951 456.9504 -4.7875 396.1994 400.9869 363.9894 458.5499 -4.7824 396.0182 400.8006 363.8034 460.1489 -4.7776 395.8024 400.5801 363.5965 461.7744 -4.7742 395.6253 400.3995 363.3876 463.3655 -4.7730 395.4146 400.1876 363.1879 464.9734 -4.7722 395.2192 399.9914 362.9920 466.5660 -4.7695 395.0130 399.7825 362.7978 468.1711 -4.7733 394.8248 399.5981 362.6062 469.7685 -4.7719 394.6167 399.3885 362.4097 471.3975 -4.7592 394.4214 399.1806 362.2114 472.9964 -4.7492 394.2270 398.9762 362.0048 474.5955 -4.7552 394.0100 398.7651 361.7996 476.1940 -4.7513 393.8229 398.5742 361.6034 477.8080 -4.7463 393.6119 398.3582 361.3795 479.4219 -4.7405 393.4239 398.1644 361.1676 481.0359 -4.7335 393.2260 397.9595 360.9576 482.6348 -4.7297 393.0351 397.7648 360.7282 484.2338 -4.7283 392.8384 397.5666 360.5280 485.8478 -4.7285 392.6225 397.3510 360.3088 487.4616 -4.7122 392.4409 397.1531 360.0782 489.0786 -4.7100 392.2349 396.9449 359.8580 490.6775 -4.7078 392.0289 396.7367 359.6520 492.2765 -4.7028 391.8431 396.5459 359.4431 493.8860 -4.6962 391.6544 396.3505 359.2384 495.4920 -4.6906 391.4344 396.1250 359.0130 497.0840 -4.6859 391.2529 395.9388 358.7972 498.6914 -4.6783 391.0316 395.7098 358.5867 500.2864 -4.6740 390.8313 395.5053 358.3714 501.8828 -4.6672 390.6276 395.2948 358.1760 503.4965 -4.6636 390.4368 395.1004 357.9571 505.1105 -4.6587 390.2326 394.8913 357.7471 506.7096 -4.6533 390.0428 394.6962 357.5325 508.3093 -4.6472 389.8440 394.4912 357.3422 509.9095 -4.6416 389.6569 394.2985 357.1329 511.5085 -4.6382 389.4508 394.0890 356.9359 513.1375 -4.6321 389.2491 393.8811 356.7173 514.7373 -4.6252 389.0511 393.6763 356.5323 516.3514 -4.6211 388.8439 393.4651 356.3196 517.9503 -4.6123 388.6438 393.2560 356.1108 519.5498 -4.6089 388.4332 393.0421 355.9173 521.1639 -4.6038 388.2457 392.8495 355.7086 522.7788 -4.6003 388.0485 392.6488 355.4812 524.3776 -4.5938 387.8557 392.4496 355.2894 525.9908 -4.5887 387.6416 392.2304 355.0930 527.5830 -4.5826 387.4279 392.0106 354.8759 529.1900 -4.5744 387.2511 391.8254 354.6875 530.7971 -4.5699 387.0297 391.5996 354.4809 532.3891 -4.5658 386.8258 391.3915 354.2775 533.9984 -4.5581 386.6100 391.1682 354.0719 535.5968 -4.5538 386.4247 390.9785 353.8799 537.1958 -4.5501 386.2224 390.7725 353.6892 538.8098 -4.5434 386.0448 390.5882 353.5008 540.4239 -4.5384 385.8293 390.3676 353.2906 542.0228 -4.5334 385.6469 390.1803 353.1076 543.6216 -4.5290 385.4176 389.9466 352.8946 545.2205 -4.5227 385.2338 389.7565 352.6984 546.8495 -4.5202 385.0265 389.5468 352.5083 548.4485 -4.5151 384.8321 389.3472 352.3093 550.0625 -4.5068 384.6382 389.1450 352.0959 551.6619 -4.5024 384.4378 388.9402 351.8936 553.2615 -4.4980 384.2305 388.7285 351.6895 554.8903 -4.4887 384.0329 388.5215 351.4842 556.4899 -4.4840 383.8240 388.3080 351.2774 558.0876 -4.4801 383.6137 388.0938 351.0623 559.6948 -4.4759 383.4151 387.8911 350.8580 561.2874 -4.4713 383.2264 387.6977 350.6577 562.8951 -4.4644 383.0196 387.4840 350.4302 564.5035 -4.4592 382.8276 387.2867 350.2302 566.0984 -4.4557 382.6356 387.0913 350.0250 567.7098 -4.4500 382.4303 386.8803 349.8059 569.3076 -4.4438 382.2203 386.6641 349.5935 570.9061 -4.4387 382.0265 386.4653 349.4050 572.5206 -4.4349 381.8301 386.2649 349.1850 574.1349 -4.4281 381.6153 386.0434 348.9897 575.7339 -4.4220 381.4238 385.8459 348.7682 577.3328 -4.4178 381.2236 385.6414 348.5679 578.9474 -4.4115 381.0239 385.4354 348.3552 580.5618 -4.4070 380.8030 385.2100 348.1534 582.1609 -4.4025 380.6110 385.0135 347.9330 583.7746 -4.3945 380.4203 384.8148 347.7428 585.3735 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