DTA measure 1fazis02 Test Date: 20231025:1418 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1274.05 s Mass = 909.500 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2568 0.0512 226.8659 226.8147 261.5554 2.0788 0.0544 227.0987 227.0443 261.5707 2.8710 0.0570 227.3430 227.2861 261.5968 3.6625 0.0599 227.5509 227.4910 261.6030 4.5150 0.0599 227.8002 227.7403 261.6300 5.2765 0.0592 227.9977 227.9385 261.6521 6.0988 0.0615 228.2261 228.1646 261.6790 6.8908 0.0630 228.4387 228.3757 261.7171 7.6835 0.0678 228.6729 228.6051 261.7497 8.5358 0.0682 228.8940 228.8258 261.7810 9.2975 0.0685 229.1125 229.0440 261.8098 10.1205 0.0719 229.3327 229.2608 261.8627 10.9128 0.0754 229.5547 229.4793 261.9130 11.7055 0.0747 229.7792 229.7044 261.9594 12.5575 0.0759 230.0043 229.9284 262.0252 13.3195 0.0771 230.1930 230.1160 262.0866 14.1415 0.0774 230.4291 230.3518 262.1599 14.9333 0.0772 230.6254 230.5482 262.2274 15.7225 0.0780 230.8483 230.7703 262.3145 16.5415 0.0790 231.0675 230.9885 262.3861 17.3300 0.0782 231.2838 231.2056 262.4764 18.1493 0.0776 231.4842 231.4066 262.5576 18.9393 0.0800 231.6869 231.6069 262.6401 19.7285 0.0809 231.8939 231.8130 262.7257 20.5480 0.0793 232.1180 232.0386 262.8296 21.3370 0.0801 232.3436 232.2635 262.9229 22.1563 0.0828 232.5540 232.4712 263.0436 22.9468 0.0789 232.7592 232.6803 263.1427 23.7375 0.0778 232.9647 232.8868 263.2626 24.5595 0.0763 233.1875 233.1112 263.3672 25.3515 0.0761 233.4085 233.3324 263.4829 26.1738 0.0746 233.6070 233.5325 263.6053 26.9655 0.0740 233.8285 233.7546 263.7321 27.7575 0.0747 234.0255 233.9508 263.8615 28.5795 0.0709 234.2259 234.1550 263.9819 29.3715 0.0713 234.4157 234.3444 264.1044 30.1935 0.0695 234.6326 234.5632 264.2471 30.9855 0.0683 234.8383 234.7700 264.3701 31.7775 0.0671 235.0342 234.9671 264.4983 32.5998 0.0640 235.2312 235.1672 264.6302 33.3625 0.0631 235.4308 235.3677 264.7689 34.2145 0.0619 235.6496 235.5877 264.9024 35.0065 0.0603 235.8655 235.8052 265.0214 35.7995 0.0594 236.0722 236.0128 265.1456 36.6215 0.0540 236.2574 236.2034 265.2715 37.3835 0.0522 236.4576 236.4053 265.3950 38.2365 0.0524 236.6657 236.6133 265.5219 39.0290 0.0501 236.8552 236.8051 265.6466 39.8205 0.0452 237.0424 236.9972 265.7588 40.6433 0.0430 237.2484 237.2054 265.8645 41.4055 0.0413 237.4426 237.4012 265.9828 42.2580 0.0381 237.6631 237.6250 266.1253 43.0500 0.0355 237.8550 237.8195 266.2260 43.8425 0.0322 238.0515 238.0193 266.3359 44.6648 0.0326 238.2503 238.2177 266.4513 45.4265 0.0291 238.4569 238.4278 266.5685 46.2788 0.0251 238.6447 238.6197 266.6829 47.0705 0.0203 238.8372 238.8170 266.8058 47.8600 0.0178 239.0267 239.0090 266.9072 48.6785 0.0157 239.2323 239.2166 267.0246 49.4383 0.0125 239.4223 239.4098 267.1300 50.2878 0.0089 239.6349 239.6260 267.2484 51.0470 0.0046 239.7939 239.7893 267.3573 51.8670 0.0003 239.9958 239.9956 267.4650 52.6865 -0.0025 240.1932 240.1957 267.5831 53.4470 -0.0055 240.3729 240.3783 267.7006 54.2990 -0.0088 240.5801 240.5889 267.8065 55.0608 -0.0119 240.7612 240.7731 267.9201 55.8828 -0.0177 240.9497 240.9673 268.0119 56.6750 -0.0229 241.1303 241.1532 268.1414 57.4665 -0.0268 241.3135 241.3403 268.2598 58.3190 -0.0291 241.5361 241.5651 268.3561 59.0808 -0.0331 241.7081 241.7412 268.4522 59.9028 -0.0377 241.8979 241.9356 268.5848 60.6948 -0.0422 242.0782 242.1204 268.6782 61.4865 -0.0446 242.2678 242.3125 268.7887 62.3388 -0.0502 242.4614 242.5115 268.8982 63.1005 -0.0548 242.6467 242.7015 268.9997 63.9228 -0.0589 242.8403 242.8993 269.1242 64.7445 -0.0627 243.0285 243.0912 269.2390 65.5065 -0.0673 243.2106 243.2780 269.3261 66.3588 -0.0713 243.4025 243.4738 269.4515 67.1205 -0.0756 243.5793 243.6549 269.5349 67.9425 -0.0814 243.7846 243.8660 269.6433 68.7645 -0.0861 243.9548 244.0410 269.7414 69.5265 -0.0915 244.1297 244.2213 269.8309 70.3790 -0.0949 244.3233 244.4182 269.9511 71.1415 -0.0994 244.5134 244.6128 270.0321 71.9643 -0.1042 244.6785 244.7827 270.1194 72.7868 -0.1118 244.8658 244.9776 270.2166 73.5495 -0.1157 245.0322 245.1479 270.3009 74.4018 -0.1206 245.2246 245.3452 270.3950 75.1940 -0.1255 245.4115 245.5370 270.4735 75.9855 -0.1303 245.5927 245.7230 270.5557 76.8085 -0.1344 245.7719 245.9063 270.6528 77.5705 -0.1418 245.9562 246.0980 270.7359 78.4245 -0.1481 246.1450 246.2931 270.8340 79.2163 -0.1525 246.3022 246.4547 270.9388 80.0055 -0.1593 246.4886 246.6479 271.0381 80.8240 -0.1649 246.6641 246.8291 271.1369 81.5835 -0.1717 246.8343 247.0061 271.2233 82.4325 -0.1748 247.0277 247.2025 271.3267 83.2205 -0.1800 247.2003 247.3803 271.4212 84.0115 -0.1864 247.3799 247.5663 271.5291 84.8320 -0.1889 247.5649 247.7538 271.6468 85.5920 -0.1951 247.7350 247.9302 271.7490 86.4415 -0.2000 247.9031 248.1030 271.8585 87.2020 -0.2057 248.0798 248.2855 271.9420 88.0245 -0.2090 248.2512 248.4602 272.0506 88.8455 -0.2150 248.4371 248.6521 272.1557 89.6065 -0.2213 248.5989 248.8202 272.2687 90.4593 -0.2275 248.7904 249.0179 272.3800 91.2210 -0.2326 248.9599 249.1925 272.4946 92.0428 -0.2375 249.1388 249.3763 272.6071 92.8650 -0.2422 249.3107 249.5529 272.6954 93.6265 -0.2476 249.4571 249.7047 272.8030 94.4790 -0.2557 249.6464 249.9021 272.9305 95.2408 -0.2602 249.8222 250.0824 273.0232 96.0635 -0.2683 249.9893 250.2577 273.1322 96.8860 -0.2741 250.1727 250.4467 273.2377 97.6475 -0.2794 250.3240 250.6033 273.3374 98.5000 -0.2828 250.5131 250.7958 273.4595 99.2618 -0.2882 250.6668 250.9550 273.5682 100.0838 -0.2965 250.8399 251.1364 273.6825 100.9060 -0.3030 251.0114 251.3144 273.8078 101.6685 -0.3080 251.1830 251.4909 273.8979 102.5213 -0.3122 251.3759 251.6880 274.0168 103.3138 -0.3192 251.5367 251.8558 274.1185 104.1055 -0.3239 251.6938 252.0177 274.2221 104.9275 -0.3273 251.8747 252.2020 274.3239 105.6895 -0.3351 252.0333 252.3684 274.4204 106.5423 -0.3401 252.2006 252.5408 274.5529 107.3345 -0.3491 252.3609 252.7100 274.6659 108.1275 -0.3554 252.5336 252.8890 274.7609 108.9495 -0.3599 252.6997 253.0596 274.8787 109.7115 -0.3655 252.8555 253.2211 274.9904 110.5640 -0.3701 253.0253 253.3954 275.0973 111.3565 -0.3764 253.2052 253.5816 275.2083 112.1478 -0.3808 253.3630 253.7439 275.3145 112.9665 -0.3861 253.5250 253.9110 275.4286 113.7248 -0.3944 253.6901 254.0846 275.5377 114.5743 -0.4020 253.8600 254.2620 275.6543 115.3333 -0.4071 254.0141 254.4212 275.7368 116.1528 -0.4139 254.1824 254.5964 275.8495 116.9713 -0.4177 254.3466 254.7642 275.9737 117.7313 -0.4235 254.5096 254.9331 276.0723 118.5820 -0.4295 254.6803 255.1099 276.2032 119.3418 -0.4345 254.8430 255.2775 276.2913 120.1635 -0.4407 255.0091 255.4498 276.4051 120.9555 -0.4459 255.1643 255.6102 276.5122 121.7475 -0.4505 255.3129 255.7634 276.6314 122.5995 -0.4597 255.4923 255.9520 276.7396 123.3615 -0.4625 255.6423 256.1047 276.8286 124.1835 -0.4675 255.8226 256.2902 276.9362 124.9755 -0.4726 255.9675 256.4401 277.0557 125.7675 -0.4774 256.1247 256.6021 277.1581 126.5895 -0.4833 256.2952 256.7785 277.2549 127.3815 -0.4898 256.4406 256.9303 277.3759 128.2035 -0.4972 256.6018 257.0991 277.4916 128.9955 -0.5022 256.7608 257.2630 277.5912 129.7868 -0.5098 256.9277 257.4375 277.6817 130.6095 -0.5134 257.0973 257.6107 277.8106 131.4013 -0.5175 257.2419 257.7594 277.9219 132.2228 -0.5251 257.4137 257.9387 278.0362 133.0150 -0.5335 257.5581 258.0917 278.1405 133.8065 -0.5393 257.7302 258.2695 278.2377 134.6290 -0.5466 257.8840 258.4307 278.3569 135.3905 -0.5537 258.0357 258.5894 278.4521 136.2435 -0.5577 258.1869 258.7446 278.5840 137.0058 -0.5639 258.3464 258.9104 278.6753 137.8278 -0.5690 258.5001 259.0691 278.7866 138.6498 -0.5741 258.6633 259.2374 278.8903 139.4115 -0.5783 258.8148 259.3931 279.0015 140.2643 -0.5838 258.9606 259.5444 279.1138 141.0265 -0.5910 259.1235 259.7144 279.2172 141.8495 -0.5962 259.2893 259.8854 279.3135 142.6720 -0.6055 259.4591 260.0646 279.4271 143.4345 -0.6121 259.6000 260.2120 279.5349 144.2845 -0.6174 259.7654 260.3829 279.6478 145.0440 -0.6234 259.9018 260.5252 279.7601 145.8620 -0.6281 260.0558 260.6839 279.8557 146.6500 -0.6315 260.2035 260.8350 279.9682 147.4380 -0.6381 260.3673 261.0055 280.0807 148.2860 -0.6448 260.5304 261.1752 280.1786 149.0440 -0.6508 260.6721 261.3230 280.2732 149.8633 -0.6541 260.8180 261.4720 280.3820 150.6540 -0.6588 260.9844 261.6432 280.4920 151.4445 -0.6650 261.1268 261.7918 280.5868 152.2660 -0.6697 261.2827 261.9524 280.7023 153.0575 -0.6762 261.4373 262.1135 280.8082 153.8798 -0.6855 261.5913 262.2768 280.9205 154.6718 -0.6918 261.7358 262.4276 281.0407 155.4635 -0.6980 261.8791 262.5771 281.1334 156.2858 -0.7047 262.0432 262.7479 281.2333 157.0475 -0.7066 262.1877 262.8943 281.3304 157.9018 -0.7167 262.3573 263.0740 281.4467 158.6635 -0.7229 262.4889 263.2118 281.5559 159.4855 -0.7274 262.6342 263.3616 281.6565 160.3075 -0.7353 262.7835 263.5188 281.7738 161.0695 -0.7388 262.9247 263.6635 281.8574 161.9215 -0.7454 263.1005 263.8459 281.9896 162.6835 -0.7521 263.2311 263.9832 282.0945 163.5055 -0.7596 263.3803 264.1399 282.1989 164.2985 -0.7632 263.5315 264.2947 282.2954 165.0905 -0.7661 263.6691 264.4352 282.4031 165.9425 -0.7720 263.8426 264.6146 282.5211 166.7045 -0.7795 263.9923 264.7718 282.6140 167.5265 -0.7848 264.1536 264.9384 282.7362 168.3185 -0.7890 264.2841 265.0731 282.8326 169.1113 -0.7944 264.4240 265.2184 282.9269 169.9630 -0.8003 264.5734 265.3737 283.0387 170.7248 -0.8035 264.7244 265.5279 283.1489 171.5468 -0.8104 264.8664 265.6768 283.2622 172.3403 -0.8172 265.0405 265.8577 283.3670 173.1325 -0.8227 265.1784 266.0011 283.4565 173.9850 -0.8286 265.3386 266.1673 283.5581 174.7468 -0.8333 265.4711 266.3044 283.6560 175.5688 -0.8383 265.6142 266.4525 283.7609 176.3598 -0.8422 265.7716 266.6138 283.8847 177.1490 -0.8467 265.9108 266.7576 284.0040 177.9978 -0.8513 266.0591 266.9104 284.1063 178.7553 -0.8569 266.1934 267.0503 284.2089 179.5740 -0.8608 266.3354 267.1961 284.3116 180.3625 -0.8673 266.4824 267.3496 284.4043 181.1518 -0.8762 266.6428 267.5191 284.5078 182.0018 -0.8838 266.8076 267.6914 284.6284 182.7628 -0.8876 266.9178 267.8055 284.7311 183.5848 -0.8925 267.0741 267.9666 284.8390 184.3760 -0.8948 267.2134 268.1082 284.9401 185.1680 -0.9006 267.3418 268.2423 285.0542 185.9903 -0.9061 267.5148 268.4209 285.1527 186.7820 -0.9128 267.6444 268.5572 285.2524 187.6038 -0.9196 267.7871 268.7067 285.3590 188.3960 -0.9234 267.9268 268.8501 285.4885 189.1875 -0.9287 268.0749 269.0036 285.5849 190.0100 -0.9359 268.2130 269.1489 285.6738 190.8018 -0.9389 268.3611 269.3000 285.7722 191.6238 -0.9446 268.5098 269.4544 285.8888 192.4160 -0.9505 268.6579 269.6085 285.9919 193.2075 -0.9560 268.7847 269.7407 286.0889 194.0328 -0.9619 268.9393 269.9012 286.1826 194.8255 -0.9664 269.0905 270.0569 286.2955 195.6478 -0.9708 269.2355 270.2062 286.3812 196.4398 -0.9740 269.3732 270.3472 286.4804 197.2325 -0.9807 269.5118 270.4925 286.5890 198.0550 -0.9857 269.6528 270.6385 286.7133 198.8475 -0.9881 269.7732 270.7613 286.8035 199.6695 -0.9947 269.9192 270.9139 286.9090 200.4618 -1.0014 270.0699 271.0713 286.9981 201.2545 -1.0056 270.1982 271.2039 287.0952 202.0770 -1.0093 270.3604 271.3698 287.2016 202.8695 -1.0159 270.4895 271.5054 287.3146 203.6918 -1.0199 270.6340 271.6539 287.4189 204.4845 -1.0257 270.7704 271.7961 287.5148 205.2775 -1.0296 270.9033 271.9329 287.6207 206.1300 -1.0376 271.0506 272.0883 287.7334 206.8925 -1.0434 271.1764 272.2198 287.8217 207.7150 -1.0472 271.3165 272.3637 287.9389 208.5053 -1.0524 271.4737 272.5261 288.0355 209.2938 -1.0557 271.6056 272.6613 288.1377 210.1420 -1.0603 271.7618 272.8221 288.2301 210.9000 -1.0674 271.8857 272.9531 288.3315 211.7185 -1.0715 272.0213 273.0928 288.4385 212.5073 -1.0761 272.1576 273.2336 288.5425 213.2973 -1.0822 272.3076 273.3898 288.6522 214.1465 -1.0849 272.4472 273.5321 288.7331 214.9068 -1.0879 272.5804 273.6683 288.8200 215.7275 -1.0941 272.7151 273.8092 288.9259 216.5495 -1.0991 272.8650 273.9641 289.0210 217.3108 -1.1048 272.9939 274.0988 289.1182 218.1625 -1.1073 273.1380 274.2452 289.2261 218.9245 -1.1138 273.2586 274.3725 289.3167 219.7465 -1.1166 273.4048 274.5214 289.4230 220.5385 -1.1210 273.5390 274.6600 289.5225 221.3305 -1.1258 273.6737 274.7994 289.6368 222.1825 -1.1334 273.8158 274.9492 289.7397 222.9445 -1.1392 273.9391 275.0783 289.8411 223.7660 -1.1436 274.1009 275.2444 289.9692 224.5583 -1.1474 274.2401 275.3874 290.0727 225.3505 -1.1506 274.3685 275.5191 290.1742 226.2025 -1.1557 274.4951 275.6508 290.2881 226.9638 -1.1606 274.6253 275.7859 290.4080 227.7860 -1.1660 274.7741 275.9401 290.5443 228.6083 -1.1701 274.9131 276.0832 290.6451 229.3705 -1.1754 275.0428 276.2182 290.7613 230.2235 -1.1808 275.1737 276.3545 290.8774 230.9858 -1.1830 275.3124 276.4954 291.0035 231.8085 -1.1877 275.4547 276.6425 291.1209 232.6313 -1.1941 275.5787 276.7729 291.2732 233.3935 -1.1978 275.7097 276.9075 291.3833 234.2460 -1.2033 275.8531 277.0563 291.5003 235.0378 -1.2078 275.9768 277.1846 291.6201 235.8295 -1.2136 276.1195 277.3331 291.7459 236.6520 -1.2161 276.2595 277.4755 291.8745 237.4145 -1.2217 276.3872 277.6090 291.9891 238.2673 -1.2251 276.5332 277.7584 292.0798 239.0595 -1.2324 276.6500 277.8824 292.1884 239.8525 -1.2371 276.7852 278.0224 292.3025 240.6748 -1.2416 276.9200 278.1616 292.4267 241.4360 -1.2474 277.0481 278.2955 292.5208 242.2840 -1.2502 277.1960 278.4462 292.6282 243.0720 -1.2533 277.3249 278.5783 292.7250 243.8605 -1.2589 277.4590 278.7179 292.8291 244.6795 -1.2666 277.6078 278.8744 292.9347 245.4385 -1.2707 277.7260 278.9967 293.0238 246.2880 -1.2711 277.8744 279.1454 293.1284 247.0780 -1.2742 278.0075 279.2817 293.2223 247.8683 -1.2808 278.1310 279.4118 293.3284 248.6875 -1.2847 278.2769 279.5617 293.4395 249.4485 -1.2899 278.3857 279.6755 293.5437 250.3005 -1.2957 278.5266 279.8223 293.6400 251.0918 -1.3004 278.6540 279.9543 293.7195 251.8825 -1.3026 278.8138 280.1164 293.8331 252.7045 -1.3049 278.9341 280.2390 293.9297 253.4685 -1.3112 279.0512 280.3624 294.0119 254.3205 -1.3153 279.1946 280.5099 294.1278 255.1725 -1.3221 279.3232 280.6454 294.2280 255.9345 -1.3284 279.4484 280.7768 294.3271 256.7565 -1.3312 279.5819 280.9131 294.4114 257.5485 -1.3390 279.7074 281.0464 294.5097 258.3405 -1.3406 279.8457 281.1863 294.6261 259.1925 -1.3425 280.0081 281.3506 294.7286 259.9545 -1.3467 280.1172 281.4638 294.8039 260.8968 -1.3505 280.2514 281.6018 294.9297 261.7493 -1.3583 280.4013 281.7596 295.0362 262.5715 -1.3620 280.5464 281.9084 295.1348 263.3333 -1.3671 280.6740 282.0411 295.2302 264.1853 -1.3711 280.7967 282.1678 295.3309 264.9770 -1.3753 280.9354 282.3107 295.4391 265.7685 -1.3796 281.0523 282.4318 295.5596 266.5910 -1.3851 281.1852 282.5703 295.6605 267.3828 -1.3895 281.3145 282.7040 295.7571 268.2055 -1.3957 281.4494 282.8450 295.8629 268.9980 -1.3994 281.5814 282.9808 295.9916 269.7905 -1.4043 281.7120 283.1163 296.1024 270.6133 -1.4066 281.8435 283.2501 296.2221 271.4055 -1.4127 281.9565 283.3692 296.3320 272.2285 -1.4159 282.0944 283.5103 296.4375 273.0203 -1.4199 282.2222 283.6421 296.5542 273.8090 -1.4260 282.3446 283.7705 296.6776 274.6558 -1.4310 282.4852 283.9162 296.7878 275.4150 -1.4321 282.6121 284.0441 296.9020 276.2330 -1.4354 282.7477 284.1831 297.0287 277.0213 -1.4396 282.8719 284.3115 297.1339 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