DTA measure 1fazis1 Test Date: 20231025:136 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.59 s Mass = 909.500 mg data_number = 1269 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2870 0.5159 222.3660 221.8501 261.5459 2.1355 0.5138 222.6106 222.0968 261.5654 2.8948 0.5157 222.8457 222.3300 261.5892 3.7148 0.5141 223.1056 222.5915 261.6159 4.5340 0.5162 223.3553 222.8392 261.6046 5.2955 0.5154 223.5906 223.0752 261.6239 6.1475 0.5125 223.8549 223.3424 261.6439 6.9088 0.5122 224.0817 223.5694 261.6850 7.7305 0.5121 224.3234 223.8113 261.7366 8.5525 0.5138 224.5639 224.0501 261.7747 9.3145 0.5117 224.7950 224.2833 261.8183 10.1665 0.5124 225.0487 224.5364 261.8846 10.9285 0.5124 225.2789 224.7665 261.9535 11.7505 0.5122 225.5241 225.0119 262.0190 12.5425 0.5117 225.7596 225.2479 262.0814 13.3345 0.5086 225.9877 225.4791 262.1641 14.1865 0.5068 226.2507 225.7439 262.2395 14.9485 0.5060 226.4699 225.9639 262.3218 15.7703 0.5037 226.7110 226.2073 262.4139 16.5623 0.5031 226.9264 226.4233 262.5208 17.3538 0.5034 227.1466 226.6432 262.6305 18.1763 0.5035 227.3851 226.8816 262.7366 18.9680 0.5002 227.6252 227.1250 262.8639 19.7905 0.4968 227.8705 227.3737 262.9818 20.5830 0.4962 228.0751 227.5789 263.1156 21.3745 0.4947 228.3084 227.8137 263.2401 22.1970 0.4922 228.5457 228.0534 263.3764 22.9888 0.4889 228.7674 228.2785 263.5032 23.8108 0.4891 229.0099 228.5208 263.6524 24.6030 0.4892 229.2301 228.7409 263.7876 25.3945 0.4848 229.4558 228.9710 263.9166 26.2468 0.4826 229.6977 229.2152 264.1013 27.0085 0.4809 229.8980 229.4171 264.2399 27.8320 0.4772 230.1285 229.6513 264.3950 28.6280 0.4760 230.3677 229.8916 264.5463 29.4160 0.4731 230.5939 230.1208 264.7058 30.2340 0.4725 230.8125 230.3400 264.8577 30.9920 0.4709 231.0251 230.5543 265.0146 31.8400 0.4637 231.2681 230.8044 265.1777 32.6288 0.4570 231.4812 231.0242 265.3309 33.4188 0.4537 231.6965 231.2428 265.5032 34.2378 0.4497 231.8979 231.4482 265.6539 35.0260 0.4472 232.1304 231.6832 265.8168 35.8455 0.4442 232.3553 231.9112 265.9795 36.6355 0.4401 232.5842 232.1441 266.1150 37.4265 0.4355 232.7965 232.3611 266.2648 38.2480 0.4293 233.0200 232.5907 266.4101 39.0395 0.4248 233.2241 232.7993 266.5701 39.8618 0.4204 233.4401 233.0196 266.7062 40.6538 0.4204 233.6528 233.2325 266.8739 41.4455 0.4159 233.8674 233.4515 267.0030 42.2680 0.4100 234.0915 233.6816 267.1370 43.0595 0.4046 234.2939 233.8893 267.2813 43.8818 0.3985 234.5169 234.1184 267.4106 44.6738 0.3928 234.7378 234.3450 267.5383 45.4655 0.3878 234.9517 234.5639 267.6799 46.2878 0.3821 235.1645 234.7824 267.8218 47.0795 0.3768 235.3777 235.0009 267.9446 47.9015 0.3716 235.5915 235.2199 268.0827 48.6935 0.3664 235.8039 235.4375 268.2129 49.4855 0.3625 236.0091 235.6466 268.3537 50.3075 0.3563 236.2275 235.8712 268.4857 51.0995 0.3497 236.4479 236.0983 268.6132 51.9215 0.3426 236.6498 236.3071 268.7369 52.7135 0.3372 236.8549 236.5177 268.8630 53.5055 0.3317 237.0567 236.7250 268.9976 54.3575 0.3280 237.2975 236.9695 269.1386 55.1195 0.3211 237.4768 237.1557 269.2561 55.9415 0.3142 237.6900 237.3758 269.4123 56.7335 0.3096 237.8960 237.5864 269.5434 57.5245 0.3080 238.1087 237.8007 269.6561 58.3775 0.2991 238.3253 238.0262 269.7815 59.1473 0.2925 238.5295 238.2369 269.8997 59.9698 0.2846 238.7596 238.4749 270.0407 60.7615 0.2793 238.9508 238.6715 270.1751 61.5500 0.2756 239.1609 238.8853 270.3035 62.3685 0.2698 239.3649 239.0951 270.4370 63.1560 0.2670 239.5532 239.2862 270.5723 63.9743 0.2611 239.7737 239.5125 270.6974 64.7625 0.2538 239.9711 239.7174 270.8131 65.5510 0.2450 240.1669 239.9219 270.9357 66.4000 0.2391 240.3796 240.1406 271.1013 67.1585 0.2323 240.5735 240.3411 271.2094 67.9780 0.2241 240.7775 240.5534 271.3321 68.7670 0.2184 240.9840 240.7656 271.4584 69.5560 0.2149 241.1697 240.9548 271.5822 70.4060 0.2060 241.3672 241.1612 271.7233 71.1658 0.1986 241.5660 241.3675 271.8550 71.9878 0.1912 241.7857 241.5946 271.9847 72.8103 0.1852 241.9932 241.8080 272.1158 73.5718 0.1806 242.1688 241.9883 272.2389 74.4240 0.1756 242.3777 242.2022 272.3578 75.1858 0.1669 242.5726 242.4058 272.4962 76.0078 0.1594 242.7650 242.6056 272.6260 76.8300 0.1519 242.9766 242.8246 272.7534 77.5915 0.1460 243.1810 243.0350 272.8725 78.4440 0.1406 243.3955 243.2550 273.0044 79.2360 0.1340 243.5740 243.4401 273.1432 80.0275 0.1256 243.7682 243.6426 273.2778 80.8500 0.1200 243.9825 243.8624 273.4126 81.6125 0.1137 244.1657 244.0520 273.5163 82.4650 0.1109 244.3785 244.2676 273.6778 83.2568 0.1059 244.5635 244.4576 273.7880 84.0485 0.0989 244.7464 244.6475 273.8964 84.8710 0.0884 244.9481 244.8597 274.0264 85.6335 0.0813 245.1262 245.0449 274.1431 86.4858 0.0763 245.3291 245.2528 274.3054 87.2775 0.0683 245.5273 245.4590 274.4266 88.0695 0.0614 245.7292 245.6679 274.5376 88.8915 0.0563 245.9318 245.8756 274.6617 89.6663 0.0510 246.1085 246.0575 274.7960 90.5240 0.0449 246.3122 246.2673 274.9351 91.2865 0.0358 246.5063 246.4705 275.0603 92.1085 0.0285 246.7004 246.6719 275.1743 92.8970 0.0218 246.8732 246.8514 275.3017 93.6860 0.0148 247.0608 247.0460 275.4338 94.5348 0.0079 247.2738 247.2659 275.5637 95.2930 0.0018 247.4538 247.4520 275.6745 96.1118 -0.0043 247.6392 247.6435 275.7949 96.9000 -0.0106 247.8186 247.8292 275.9221 97.6890 -0.0201 248.0086 248.0287 276.0495 98.5375 -0.0280 248.2186 248.2467 276.1976 99.2965 -0.0344 248.3815 248.4159 276.3103 100.1160 -0.0415 248.5996 248.6411 276.4478 100.9358 -0.0480 248.7838 248.8318 276.5825 101.6970 -0.0520 248.9696 249.0216 276.7172 102.5485 -0.0620 249.1561 249.2181 276.8686 103.3105 -0.0708 249.3354 249.4063 277.0101 104.1325 -0.0772 249.5319 249.6091 277.1560 104.9245 -0.0854 249.7152 249.8006 277.2912 105.7165 -0.0916 249.8903 249.9818 277.4339 106.5685 -0.0967 250.0943 250.1909 277.5755 107.3305 -0.1047 250.2718 250.3765 277.7047 108.1525 -0.1111 250.4562 250.5674 277.8612 108.9445 -0.1217 250.6380 250.7598 278.0058 109.7440 -0.1289 250.8234 250.9523 278.1517 110.5595 -0.1319 251.0253 251.1572 278.2962 111.3515 -0.1359 251.2010 251.3368 278.4451 112.1735 -0.1454 251.3965 251.5419 278.6010 112.9648 -0.1512 251.5719 251.7231 278.7511 113.7873 -0.1584 251.7567 251.9151 278.8979 114.5793 -0.1666 251.9500 252.1166 279.0422 115.3705 -0.1735 252.1207 252.2942 279.1574 116.1930 -0.1797 252.3008 252.4805 279.2883 116.9848 -0.1873 252.4909 252.6781 279.4340 117.8075 -0.1948 252.7001 252.8949 279.5742 118.6000 -0.2069 252.8844 253.0913 279.6978 119.3925 -0.2126 253.0504 253.2630 279.8208 120.2150 -0.2190 253.2297 253.4487 279.9684 121.0065 -0.2259 253.4033 253.6292 280.1051 121.8295 -0.2328 253.5933 253.8261 280.2291 122.6218 -0.2409 253.7765 254.0174 280.3396 123.4170 -0.2474 253.9558 254.2031 280.4690 124.2420 -0.2542 254.1396 254.3938 280.6014 125.0030 -0.2606 254.3104 254.5711 280.7345 125.8500 -0.2685 254.5019 254.7704 280.8754 126.6093 -0.2752 254.6668 254.9420 281.0084 127.4270 -0.2815 254.8581 255.1396 281.1327 128.2453 -0.2870 255.0588 255.3458 281.2366 129.0040 -0.2953 255.2197 255.5150 281.3631 129.8528 -0.3016 255.3977 255.6993 281.4731 130.6113 -0.3089 255.5796 255.8885 281.6006 131.4310 -0.3157 255.7632 256.0788 281.7235 132.2495 -0.3223 255.9460 256.2683 281.8507 133.0085 -0.3303 256.1069 256.4372 281.9688 133.8613 -0.3389 256.2951 256.6340 282.1103 134.6238 -0.3440 256.4681 256.8121 282.2217 135.4458 -0.3499 256.6546 257.0046 282.3349 136.2378 -0.3538 256.8165 257.1703 282.4570 137.0295 -0.3614 256.9909 257.3523 282.5817 137.8518 -0.3708 257.1842 257.5549 282.6856 138.6435 -0.3764 257.3658 257.7422 282.8192 139.4658 -0.3844 257.5443 257.9287 282.9640 140.2578 -0.3909 257.7174 258.1083 283.0830 141.0495 -0.3992 257.8863 258.2855 283.2075 141.8718 -0.4053 258.0719 258.4772 283.3466 142.6335 -0.4130 258.2278 258.6409 283.4782 143.4858 -0.4194 258.4172 258.8367 283.6277 144.2775 -0.4260 258.6055 259.0315 283.7650 145.0695 -0.4330 258.7730 259.2060 283.9039 145.8918 -0.4411 258.9445 259.3856 284.0485 146.6545 -0.4482 259.1026 259.5507 284.1878 147.5065 -0.4535 259.3014 259.7549 284.3439 148.2685 -0.4567 259.4626 259.9193 284.4869 149.0905 -0.4658 259.6321 260.0979 284.6125 149.9128 -0.4703 259.8085 260.2789 284.7792 150.6755 -0.4757 259.9762 260.4519 284.9123 151.5280 -0.4803 260.1791 260.6595 285.0555 152.2905 -0.4886 260.3392 260.8278 285.1852 153.1118 -0.4945 260.5183 261.0128 285.3536 153.9340 -0.5015 260.6972 261.1988 285.4931 154.6955 -0.5087 260.8531 261.3618 285.6234 155.5485 -0.5146 261.0224 261.5370 285.7659 156.3108 -0.5221 261.1870 261.7091 285.9001 157.1310 -0.5278 261.3763 261.9041 286.0665 157.9195 -0.5339 261.5638 262.0977 286.2070 158.7070 -0.5404 261.7161 262.2565 286.3559 159.5560 -0.5488 261.8963 262.4451 286.5081 160.3143 -0.5540 262.0609 262.6149 286.6321 161.1325 -0.5607 262.2611 262.8218 286.7548 161.9210 -0.5686 262.4178 262.9864 286.8919 162.7100 -0.5776 262.5735 263.1511 287.0206 163.5595 -0.5835 262.7721 263.3556 287.1573 164.3188 -0.5902 262.9265 263.5166 287.2797 165.1398 -0.5969 263.0956 263.6926 287.4117 165.9315 -0.6040 263.2738 263.8778 287.5235 166.7225 -0.6122 263.4468 264.0590 287.6442 167.5450 -0.6201 263.6274 264.2474 287.7713 168.3368 -0.6255 263.7846 264.4101 287.8785 169.1588 -0.6312 263.9566 264.5878 288.0149 169.9513 -0.6351 264.1223 264.7574 288.1263 170.7425 -0.6416 264.2848 264.9264 288.2296 171.5650 -0.6499 264.4658 265.1157 288.3636 172.3568 -0.6566 264.6391 265.2957 288.4764 173.1788 -0.6627 264.8054 265.4681 288.5895 173.9710 -0.6698 264.9702 265.6400 288.7060 174.7625 -0.6748 265.1365 265.8112 288.8433 175.5850 -0.6790 265.3066 265.9856 288.9729 176.3768 -0.6862 265.4715 266.1577 289.0849 177.1990 -0.6906 265.6522 266.3428 289.2029 177.9910 -0.6970 265.8198 266.5168 289.3344 178.7825 -0.7030 265.9945 266.6974 289.4752 179.6048 -0.7083 266.1461 266.8544 289.6026 180.3965 -0.7171 266.2970 267.0142 289.7243 181.2195 -0.7235 266.4921 267.2155 289.8675 182.0065 -0.7281 266.6568 267.3848 290.0065 182.8295 -0.7323 266.8293 267.5616 290.1645 183.6218 -0.7395 266.9950 267.7345 290.2630 184.4145 -0.7473 267.1599 267.9072 290.4047 185.2365 -0.7530 267.3175 268.0706 290.5539 186.0285 -0.7554 267.4995 268.2549 290.6961 186.8513 -0.7604 267.6778 268.4383 290.8194 187.6435 -0.7688 267.8298 268.5986 290.9630 188.4355 -0.7736 267.9814 268.7550 291.1097 189.2583 -0.7772 268.1760 268.9532 291.2477 190.0485 -0.7830 268.3425 269.1256 291.3794 190.8678 -0.7894 268.5153 269.3047 291.5135 191.6560 -0.7956 268.6643 269.4598 291.6682 192.4440 -0.8005 268.8167 269.6172 291.8087 193.2623 -0.8067 268.9841 269.7908 291.9435 194.0508 -0.8120 269.1561 269.9681 292.0784 194.8698 -0.8192 269.3381 270.1573 292.1982 195.6580 -0.8248 269.5028 270.3276 292.3541 196.4470 -0.8316 269.6445 270.4761 292.4829 197.2958 -0.8390 269.8302 270.6693 292.6261 198.0568 -0.8444 269.9849 270.8294 292.7570 198.8775 -0.8507 270.1578 271.0085 292.9098 199.6695 -0.8570 270.3325 271.1895 293.0505 200.4615 -0.8637 270.4716 271.3353 293.1692 201.3135 -0.8724 270.6510 271.5234 293.3095 202.0755 -0.8747 270.8180 271.6926 293.4522 202.8975 -0.8832 270.9805 271.8636 293.5866 203.6895 -0.8877 271.1303 272.0180 293.7084 204.4815 -0.8922 271.2916 272.1839 293.8389 205.3335 -0.9003 271.4648 272.3651 294.0042 206.0955 -0.9042 271.6195 272.5237 294.1139 206.9175 -0.9089 271.7832 272.6922 294.2505 207.7095 -0.9157 271.9512 272.8669 294.3878 208.5010 -0.9220 272.1115 273.0335 294.5249 209.3533 -0.9270 272.2817 273.2087 294.6712 210.1155 -0.9353 272.4482 273.3835 294.7947 210.9368 -0.9427 272.6186 273.5613 294.9182 211.7593 -0.9473 272.7698 273.7171 295.0624 212.5215 -0.9512 272.9257 273.8769 295.1983 213.3740 -0.9562 273.0903 274.0466 295.3429 214.1358 -0.9600 273.2658 274.2258 295.4704 214.9585 -0.9652 273.4396 274.4047 295.5941 215.7810 -0.9715 273.5974 274.5689 295.7263 216.5425 -0.9782 273.7556 274.7338 295.8326 217.3948 -0.9821 273.9363 274.9184 295.9913 218.1870 -0.9883 274.0820 275.0703 296.1231 218.9785 -0.9938 274.2442 275.2381 296.2491 219.8013 -0.9985 274.4157 275.4141 296.3785 220.5635 -1.0019 274.5506 275.5525 296.5136 221.4158 -1.0114 274.7279 275.7393 296.6399 222.2038 -1.0161 274.8980 275.9141 296.7735 222.9930 -1.0233 275.0651 276.0885 296.9117 223.8115 -1.0283 275.2157 276.2441 297.0486 224.6000 -1.0327 275.3731 276.4059 297.1634 225.4188 -1.0375 275.5338 276.5713 297.3012 226.2070 -1.0428 275.7182 276.7610 297.4338 226.9960 -1.0478 275.8659 276.9137 297.5867 227.8160 -1.0534 276.0193 277.0727 297.7204 228.6050 -1.0574 276.1792 277.2366 297.8499 229.4245 -1.0627 276.3295 277.3923 297.9549 230.2160 -1.0685 276.4892 277.5578 298.0906 231.0073 -1.0720 276.6652 277.7372 298.2242 231.8288 -1.0776 276.8279 277.9054 298.3461 232.6205 -1.0841 276.9791 278.0632 298.4796 233.4428 -1.0924 277.1330 278.2254 298.6124 234.2350 -1.0969 277.2940 278.3909 298.7573 235.0265 -1.1003 277.4645 278.5647 298.8891 235.8493 -1.1043 277.6285 278.7327 299.0124 236.6415 -1.1083 277.7897 278.8981 299.1475 237.4638 -1.1143 277.9589 279.0732 299.2798 238.2558 -1.1208 278.1097 279.2305 299.4064 239.0475 -1.1232 278.2727 279.3959 299.5493 239.8695 -1.1304 278.4247 279.5551 299.6744 240.6615 -1.1315 278.5841 279.7156 299.7980 241.4835 -1.1385 278.7464 279.8849 299.9314 242.2755 -1.1455 278.9027 280.0482 300.0582 243.0675 -1.1519 279.0489 280.2008 300.1807 243.8895 -1.1586 279.2224 280.3810 300.3088 244.6815 -1.1658 279.3714 280.5373 300.4399 245.5043 -1.1710 279.5444 280.7154 300.5692 246.2965 -1.1755 279.7134 280.8889 300.7016 247.0885 -1.1793 279.8709 281.0501 300.8247 247.9405 -1.1833 280.0331 281.2165 300.9709 248.7025 -1.1886 280.1735 281.3621 301.0976 249.5245 -1.1936 280.3234 281.5170 301.2176 250.3173 -1.1974 280.4772 281.6746 301.3467 251.1085 -1.2043 280.6474 281.8517 301.4718 251.9615 -1.2075 280.8259 282.0333 301.5879 252.7238 -1.2133 280.9689 282.1822 301.7160 253.5463 -1.2168 281.1194 282.3362 301.8520 254.3340 -1.2244 281.2684 282.4928 301.9702 255.1230 -1.2306 281.4377 282.6683 302.0931 255.9418 -1.2322 281.6113 282.8435 302.2105 256.7303 -1.2366 281.7563 282.9929 302.3339 257.5483 -1.2413 281.9199 283.1613 302.4638 258.3365 -1.2466 282.0664 283.3129 302.5685 259.1260 -1.2505 282.2184 283.4689 302.6993 259.9448 -1.2563 282.3795 283.6358 302.8395 260.7345 -1.2618 282.5408 283.8026 302.9477 261.5548 -1.2646 282.7123 283.9769 303.1001 262.3455 -1.2686 282.8780 284.1466 303.2164 263.1365 -1.2749 283.0228 284.2977 303.3357 263.9593 -1.2792 283.1662 284.4455 303.4682 264.7205 -1.2842 283.3031 284.5873 303.5880 265.5730 -1.2880 283.4620 284.7500 303.7095 266.3348 -1.2939 283.6255 284.9194 303.8364 267.1568 -1.2999 283.7753 285.0751 303.9566 267.9790 -1.3058 283.9469 285.2527 304.0787 268.7405 -1.3128 284.0857 285.3985 304.1952 269.5930 -1.3154 284.2647 285.5801 304.3226 270.3548 -1.3193 284.4179 285.7372 304.4420 271.1768 -1.3250 284.5825 285.9075 304.5811 271.9990 -1.3308 284.7329 286.0637 304.7000 272.7605 -1.3332 284.8866 286.2199 304.8252 273.6128 -1.3396 285.0386 286.3782 304.9885 274.3745 -1.3453 285.1863 286.5316 305.1233 275.1968 -1.3485 285.3433 286.6917 305.2744 275.9898 -1.3524 285.5023 286.8547 305.4086 276.7815 -1.3590 285.6495 287.0086 305.5614 277.6343 -1.3643 285.8175 287.1818 305.7149 278.3965 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