DTA measure 3fazis1 Test Date: 20231025:1335 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.67 s Mass = 909.500 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3696 -5.3625 429.5384 434.9009 419.9070 3.9688 -5.3738 429.6287 435.0025 419.9041 5.5826 -5.3853 429.7135 435.0989 419.9002 7.1975 -5.3946 429.7967 435.1912 419.8461 8.8119 -5.4046 429.8811 435.2857 419.7809 10.4115 -5.4108 429.9751 435.3859 419.7123 12.0105 -5.4191 430.0583 435.4774 419.6120 13.6405 -5.4287 430.1398 435.5685 419.4750 15.2339 -5.4349 430.2163 435.6512 419.3475 16.8413 -5.4432 430.2888 435.7320 419.1897 18.4341 -5.4507 430.3672 435.8178 419.0108 20.0285 -5.4584 430.4582 435.9166 418.8276 21.6531 -5.4641 430.5150 435.9791 418.6284 23.2511 -5.4712 430.5695 436.0407 418.4250 24.8645 -5.4785 430.6389 436.1174 418.2154 26.4635 -5.4852 430.7076 436.1928 418.0118 28.0625 -5.4904 430.7532 436.2436 417.7906 29.6915 -5.4944 430.8260 436.3204 417.5783 31.2905 -5.4989 430.8814 436.3803 417.3726 32.9041 -5.5048 430.9366 436.4415 417.1579 34.5031 -5.5105 430.9812 436.4917 416.9519 36.1168 -5.5147 431.0348 436.5494 416.7380 37.7309 -5.5200 431.0741 436.5941 416.5284 39.3449 -5.5257 431.1248 436.6505 416.3447 40.9438 -5.5264 431.1609 436.6873 416.1127 42.5576 -5.5326 431.1931 436.7257 415.9311 44.1640 -5.5380 431.2292 436.7672 415.7386 45.7653 -5.5398 431.2498 436.7896 415.5477 47.3880 -5.5444 431.2767 436.8211 415.3745 48.9794 -5.5474 431.2963 436.8437 415.1881 50.5714 -5.5513 431.3347 436.8861 415.0181 52.1790 -5.5545 431.3514 436.9059 414.8261 53.7789 -5.5582 431.3639 436.9221 414.6458 55.3938 -5.5602 431.3622 436.9224 414.4613 57.0076 -5.5625 431.3877 436.9502 414.2448 58.6066 -5.5647 431.3861 436.9508 414.0414 60.2055 -5.5668 431.3928 436.9597 413.8477 61.8046 -5.5682 431.4021 436.9703 413.6576 63.4335 -5.5698 431.4076 436.9774 413.4486 65.0325 -5.5730 431.4015 436.9745 413.2503 66.6465 -5.5753 431.3915 436.9668 413.0683 68.2455 -5.5778 431.3926 436.9704 412.8733 69.8445 -5.5796 431.3766 436.9563 412.6828 71.4735 -5.5834 431.3626 436.9460 412.4975 73.0725 -5.5842 431.3518 436.9360 412.3181 74.6858 -5.5888 431.3548 436.9436 412.1262 76.2848 -5.5906 431.3332 436.9238 411.9315 77.8825 -5.5929 431.3065 436.8995 411.7521 79.5053 -5.5938 431.2859 436.8797 411.5586 81.0965 -5.5973 431.2513 436.8486 411.3609 82.7049 -5.6018 431.2256 436.8274 411.1509 84.2968 -5.6024 431.1947 436.7971 410.9595 85.8906 -5.6041 431.1680 436.7721 410.7653 87.5155 -5.6109 431.1169 436.7277 410.5416 89.1139 -5.6119 431.0842 436.6960 410.3515 90.7278 -5.6147 431.0496 436.6643 410.1483 92.3268 -5.6194 431.0016 436.6210 409.9532 93.9264 -5.6220 430.9551 436.5771 409.7499 95.5459 -5.6248 430.9120 436.5368 409.5583 97.1599 -5.6272 430.8533 436.4805 409.3631 98.7586 -5.6317 430.8108 436.4425 409.1688 100.3730 -5.6316 430.7554 436.3870 408.9716 101.9726 -5.6361 430.7067 436.3428 408.7812 103.5866 -5.6405 430.6336 436.2741 408.5965 105.2015 -5.6429 430.5852 436.2282 408.4208 106.8006 -5.6429 430.5089 436.1518 408.2485 108.4155 -5.6459 430.4616 436.1075 408.0534 110.0184 -5.6503 430.3945 436.0447 407.8696 111.6126 -5.6515 430.3356 435.9871 407.6666 113.2329 -5.6526 430.2674 435.9200 407.4596 114.8251 -5.6532 430.2035 435.8568 407.2578 116.4326 -5.6552 430.1169 435.7721 407.0487 118.0265 -5.6590 430.0529 435.7119 406.8546 119.6371 -5.6599 429.9677 435.6276 406.6476 121.2505 -5.6609 429.8993 435.5601 406.4414 122.8495 -5.6644 429.8291 435.4936 406.2458 124.4485 -5.6643 429.7436 435.4078 406.0247 126.0624 -5.6670 429.6573 435.3242 405.8232 127.6614 -5.6676 429.5900 435.2576 405.6279 129.2759 -5.6661 429.4937 435.1598 405.4249 130.8925 -5.6663 429.4115 435.0778 405.2288 132.4919 -5.6673 429.3243 434.9916 405.0423 134.0954 -5.6685 429.2356 434.9041 404.8337 135.6958 -5.6729 429.1342 434.8072 404.6397 137.3248 -5.6766 429.0439 434.7204 404.4416 138.9246 -5.6774 428.9403 434.6177 404.2513 140.5260 -5.6784 428.8441 434.5225 404.0457 142.1424 -5.6793 428.7544 434.4337 403.8582 143.7388 -5.6792 428.6488 434.3280 403.6799 145.3300 -5.6782 428.5537 434.2319 403.4967 146.9511 -5.6776 428.4518 434.1293 403.2757 148.5445 -5.6778 428.3470 434.0248 403.0840 150.1378 -5.6833 428.2491 433.9324 402.8851 151.7455 -5.6843 428.1361 433.8204 402.6809 153.3401 -5.6913 428.0300 433.7214 402.4784 154.9576 -5.6904 427.9176 433.6080 402.2659 156.5725 -5.6910 427.8044 433.4954 402.0505 158.1715 -5.6929 427.6929 433.3858 401.8567 159.7735 -5.6884 427.5734 433.2617 401.6494 161.3765 -5.6921 427.4703 433.1624 401.4509 163.0063 -5.6892 427.3490 433.0382 401.2287 164.6084 -5.6869 427.2445 432.9313 401.0311 166.2225 -5.6876 427.1156 432.8032 400.8371 167.8223 -5.6873 427.0114 432.6986 400.6311 169.4213 -5.6867 426.8727 432.5594 400.4358 171.0503 -5.6869 426.7547 432.4416 400.2340 172.6518 -5.6913 426.6272 432.3185 400.0415 174.2505 -5.6936 426.4958 432.1894 399.8416 175.8614 -5.6893 426.3974 432.0867 399.6274 177.4658 -5.6911 426.2645 431.9556 399.4324 179.0723 -5.6884 426.1108 431.7992 399.2497 180.6811 -5.6892 425.9969 431.6861 399.0579 182.2773 -5.6889 425.8787 431.5677 398.8723 183.8758 -5.6896 425.7345 431.4241 398.6710 185.4888 -5.6878 425.5995 431.2873 398.4763 187.0878 -5.6886 425.4703 431.1589 398.3037 188.7019 -5.6859 425.3315 431.0174 398.1081 190.3159 -5.6871 425.2029 430.8901 397.9060 191.9148 -5.6854 425.0716 430.7570 397.6956 193.5138 -5.6834 424.9223 430.6057 397.4756 195.1276 -5.6828 424.7970 430.4798 397.2716 196.7416 -5.6807 424.6512 430.3319 397.0655 198.3578 -5.6721 424.5148 430.1868 396.8544 199.9575 -5.6699 424.3825 430.0524 396.6449 201.5565 -5.6698 424.2377 429.9075 396.4184 203.1711 -5.6723 424.0960 429.7682 396.2162 204.8005 -5.6701 423.9469 429.6170 396.0056 206.4000 -5.6687 423.7980 429.4666 395.8097 207.9926 -5.6664 423.6643 429.3307 395.6006 209.5986 -5.6656 423.5163 429.1819 395.3762 211.2050 -5.6622 423.3818 429.0440 395.1881 212.8116 -5.6600 423.2237 428.8837 394.9942 214.4060 -5.6635 423.0823 428.7458 394.8027 216.0028 -5.6602 422.9423 428.6025 394.5816 217.6165 -5.6549 422.7935 428.4485 394.3838 219.2155 -5.6539 422.6377 428.2916 394.1970 220.8445 -5.6552 422.4879 428.1430 393.9961 222.4434 -5.6552 422.3403 427.9955 393.7908 224.0419 -5.6543 422.1917 427.8460 393.5959 225.6559 -5.6530 422.0427 427.6957 393.4122 227.2548 -5.6480 421.8756 427.5237 393.2185 228.8840 -5.6468 421.7149 427.3618 393.0310 230.4828 -5.6432 421.5652 427.2084 392.8433 232.0818 -5.6404 421.4005 427.0408 392.6569 233.6961 -5.6407 421.2490 426.8898 392.4506 235.2971 -5.6384 421.0999 426.7383 392.2295 236.9274 -5.6349 420.9398 426.5748 392.0367 238.5270 -5.6317 420.7721 426.4038 391.8267 240.1226 -5.6265 420.6097 426.2362 391.6041 241.7295 -5.6247 420.4497 426.0744 391.4009 243.3210 -5.6204 420.2950 425.9154 391.1808 244.9300 -5.6196 420.1410 425.7606 390.9773 246.5383 -5.6149 419.9701 425.5850 390.7517 248.1316 -5.6103 419.8045 425.4148 390.5485 249.7436 -5.6033 419.6349 425.2382 390.3444 251.3426 -5.6013 419.4847 425.0860 390.1367 252.9565 -5.5981 419.3190 424.9171 389.9253 254.5709 -5.5927 419.1631 424.7558 389.7174 256.1706 -5.5902 418.9975 424.5877 389.5063 257.7695 -5.5877 418.8270 424.4147 389.2863 259.3835 -5.5849 418.6583 424.2431 389.0910 260.9983 -5.5776 418.4858 424.0633 388.8774 262.6125 -5.5740 418.3278 423.9019 388.6688 264.2116 -5.5707 418.1588 423.7295 388.4678 265.8111 -5.5678 418.0040 423.5718 388.2754 267.4264 -5.5651 417.8215 423.3866 388.0714 269.0409 -5.5614 417.6483 423.2097 387.8697 270.6549 -5.5570 417.4803 423.0373 387.6731 272.2521 -5.5547 417.3095 422.8642 387.4818 273.8431 -5.5483 417.1481 422.6963 387.2724 275.4368 -5.5469 416.9653 422.5122 387.0749 277.0601 -5.5457 416.8065 422.3522 386.8900 278.6548 -5.5391 416.6324 422.1714 386.6763 280.2638 -5.5341 416.4501 421.9842 386.4949 281.8608 -5.5341 416.2748 421.8089 386.2994 283.4598 -5.5309 416.1008 421.6318 386.1008 285.0745 -5.5271 415.9311 421.4582 385.9142 286.6888 -5.5236 415.7588 421.2824 385.7207 288.2878 -5.5174 415.5752 421.0926 385.5080 289.8866 -5.5098 415.4115 420.9213 385.3047 291.5006 -5.5092 415.2361 420.7453 385.0874 293.0995 -5.5078 415.0630 420.5707 384.8656 294.7285 -5.5047 414.8756 420.3803 384.6503 296.3276 -5.5020 414.7032 420.2053 384.4374 297.9275 -5.4984 414.5355 420.0339 384.2097 299.5269 -5.4918 414.3489 419.8408 384.0055 301.1424 -5.4889 414.1646 419.6535 383.8021 302.7559 -5.4894 413.9932 419.4825 383.5583 304.3528 -5.4838 413.8173 419.3012 383.3481 305.9486 -5.4745 413.6353 419.1098 383.1212 307.5569 -5.4712 413.4530 418.9242 382.9169 309.1493 -5.4692 413.2788 418.7480 382.7129 310.7576 -5.4672 413.0951 418.5622 382.4959 312.3670 -5.4633 412.9221 418.3854 382.2643 313.9638 -5.4609 412.7275 418.1884 382.0700 315.5625 -5.4531 412.5534 418.0064 381.8585 317.1763 -5.4456 412.3706 417.8162 381.6421 318.7751 -5.4420 412.1950 417.6370 381.4261 320.3925 -5.4392 412.0006 417.4398 381.2211 322.0069 -5.4348 411.8376 417.2723 381.0141 323.6058 -5.4320 411.6423 417.0742 380.7922 325.2048 -5.4268 411.4579 416.8847 380.5876 326.8188 -5.4237 411.2783 416.7020 380.3964 328.4328 -5.4215 411.1023 416.5239 380.1821 330.0318 -5.4158 410.9222 416.3380 379.9721 331.6466 -5.4098 410.7304 416.1402 379.7615 333.2455 -5.4093 410.5434 415.9527 379.5507 334.8450 -5.4047 410.3401 415.7448 379.3547 336.4710 -5.3997 410.1648 415.5645 379.1484 338.0620 -5.3968 409.9732 415.3700 378.9468 339.6683 -5.3933 409.8023 415.1957 378.7572 341.2600 -5.3868 409.6067 414.9934 378.5517 342.8515 -5.3802 409.4267 414.8069 378.3619 344.4751 -5.3775 409.2250 414.6025 378.1691 346.0878 -5.3704 409.0385 414.4089 377.9789 347.6865 -5.3658 408.8573 414.2230 377.7739 349.2855 -5.3628 408.6794 414.0422 377.5904 350.8845 -5.3578 408.5015 413.8593 377.4105 352.5135 -5.3569 408.3015 413.6584 377.2223 354.1275 -5.3529 408.1153 413.4682 377.0336 355.7265 -5.3473 407.9373 413.2846 376.8445 357.3254 -5.3435 407.7437 413.0872 376.6619 358.9393 -5.3392 407.5552 412.8945 376.4739 360.5545 -5.3352 407.3628 412.6980 376.2704 362.1749 -5.3332 407.1741 412.5073 376.0830 363.7738 -5.3248 406.9904 412.3152 375.8836 365.3726 -5.3182 406.7938 412.1121 375.6666 366.9868 -5.3132 406.6062 411.9194 375.4579 368.6149 -5.3080 406.4240 411.7320 375.2653 370.2070 -5.3077 406.2261 411.5338 375.0316 371.8030 -5.3001 406.0366 411.3368 374.8238 373.3963 -5.2934 405.8509 411.1443 374.6137 375.0048 -5.2934 405.6707 410.9641 374.4154 376.6273 -5.2916 405.4678 410.7595 374.1923 378.2231 -5.2836 405.2756 410.5593 373.9777 379.8215 -5.2831 405.0959 410.3790 373.7798 381.4205 -5.2776 404.9000 410.1777 373.5652 383.0346 -5.2727 404.7065 409.9791 373.3602 384.6503 -5.2694 404.5149 409.7843 373.1366 386.2648 -5.2636 404.3258 409.5895 372.9409 387.8635 -5.2561 404.1342 409.3903 372.7347 389.4626 -5.2523 403.9578 409.2100 372.5258 391.0801 -5.2449 403.7539 408.9987 372.3355 392.6945 -5.2451 403.5540 408.7991 372.1262 394.2935 -5.2396 403.3807 408.6202 371.9348 395.9080 -5.2353 403.1752 408.4105 371.7259 397.5090 -5.2271 402.9901 408.2172 371.5289 399.1088 -5.2270 402.8037 408.0308 371.3460 400.7374 -5.2222 402.5945 407.8167 371.1261 402.3299 -5.2143 402.4036 407.6179 370.9414 403.9225 -5.2083 402.2031 407.4114 370.7401 405.5294 -5.2047 402.0119 407.2166 370.5598 407.1235 -5.1989 401.8252 407.0240 370.3486 408.7316 -5.1956 401.6466 406.8422 370.1441 410.3420 -5.1944 401.4379 406.6323 369.9542 411.9419 -5.1886 401.2393 406.4279 369.7743 413.5440 -5.1843 401.0589 406.2432 369.5652 415.1579 -5.1794 400.8701 406.0495 369.3674 416.7568 -5.1741 400.6780 405.8521 369.1599 418.3725 -5.1673 400.4790 405.6464 368.9547 419.9798 -5.1610 400.2849 405.4459 368.7491 421.5946 -5.1575 400.0914 405.2490 368.5075 423.1936 -5.1534 399.8931 405.0464 368.3026 424.7931 -5.1474 399.6966 404.8440 368.0976 426.4228 -5.1393 399.5002 404.6395 367.8739 428.0235 -5.1363 399.3056 404.4419 367.6647 429.6225 -5.1342 399.1219 404.2561 367.4480 431.2369 -5.1272 398.9187 404.0460 367.2291 432.8350 -5.1204 398.7302 403.8506 367.0384 434.4410 -5.1140 398.5389 403.6529 366.8236 436.0480 -5.1085 398.3366 403.4451 366.6026 437.6401 -5.1052 398.1501 403.2553 366.3937 439.2490 -5.1002 397.9544 403.0546 366.1742 440.8459 -5.0944 397.7612 402.8557 365.9834 442.4525 -5.0847 397.5662 402.6510 365.7691 444.0505 -5.0803 397.3798 402.4601 365.5615 445.6800 -5.0764 397.1787 402.2551 365.3655 447.2799 -5.0701 396.9771 402.0472 365.1595 448.8795 -5.0671 396.7823 401.8494 364.9636 450.4785 -5.0655 396.5885 401.6540 364.7564 452.0923 -5.0581 396.3825 401.4406 364.5474 453.7064 -5.0559 396.1808 401.2367 364.3492 455.3243 -5.0504 395.9909 401.0414 364.1439 456.9240 -5.0477 395.8024 400.8501 363.9490 458.5238 -5.0405 395.5990 400.6394 363.7406 460.1378 -5.0330 395.3922 400.4252 363.5419 461.7518 -5.0292 395.2047 400.2339 363.3689 463.3659 -5.0220 394.9936 400.0155 363.1557 464.9636 -5.0190 394.8149 399.8339 362.9625 466.5545 -5.0139 394.6165 399.6305 362.7617 468.1626 -5.0123 394.4124 399.4247 362.5777 469.7704 -5.0034 394.2020 399.2054 362.3674 471.3790 -4.9951 394.0260 399.0210 362.1871 472.9703 -4.9909 393.8307 398.8216 361.9803 474.5791 -4.9877 393.6300 398.6177 361.7867 476.1766 -4.9870 393.4274 398.4144 361.5773 477.8045 -4.9824 393.2387 398.2212 361.3645 479.4036 -4.9786 393.0499 398.0285 361.1494 481.0026 -4.9729 392.8439 397.8168 360.9358 482.6165 -4.9712 392.6478 397.6190 360.7176 484.2155 -4.9708 392.4429 397.4138 360.5095 485.8445 -4.9645 392.2452 397.2097 360.2898 487.4435 -4.9575 392.0553 397.0128 360.0666 489.0425 -4.9520 391.8537 396.8057 359.8450 490.6565 -4.9470 391.6478 396.5948 359.6251 492.2705 -4.9431 391.4675 396.4106 359.4079 493.8848 -4.9370 391.2639 396.2009 359.1842 495.4838 -4.9315 391.0614 395.9928 358.9669 497.0826 -4.9247 390.8424 395.7672 358.7540 498.6878 -4.9171 390.6531 395.5702 358.5485 500.2800 -4.9137 390.4760 395.3897 358.3396 501.9024 -4.9082 390.2674 395.1756 358.1232 503.4959 -4.9047 390.0661 394.9708 357.8893 505.0908 -4.8959 389.8772 394.7731 357.6717 506.6888 -4.8921 389.6752 394.5673 357.4821 508.3011 -4.8884 389.4688 394.3572 357.2536 509.9150 -4.8815 389.2740 394.1555 357.0465 511.5139 -4.8796 389.0644 393.9440 356.8447 513.1278 -4.8745 388.8766 393.7511 356.6373 514.8320 -4.8664 388.6519 393.5184 356.4088 516.4309 -4.8614 388.4623 393.3237 356.2092 518.0308 -4.8576 388.2694 393.1269 355.9970 519.6598 -4.8546 388.0518 392.9064 355.7819 521.2596 -4.8492 387.8578 392.7071 355.5817 522.8735 -4.8426 387.6732 392.5157 355.3904 524.4725 -4.8392 387.4609 392.3001 355.1890 526.0715 -4.8348 387.2571 392.0919 354.9738 527.7005 -4.8271 387.0603 391.8874 354.7574 529.2994 -4.8231 386.8664 391.6894 354.5794 530.9080 -4.8182 386.6697 391.4878 354.3732 532.4994 -4.8111 386.4564 391.2675 354.1625 534.0918 -4.8061 386.2512 391.0573 353.9645 535.6900 -4.8038 386.0766 390.8804 353.7637 537.3166 -4.7990 385.8429 390.6419 353.5716 538.9150 -4.7968 385.6526 390.4494 353.3619 540.5125 -4.7899 385.4619 390.2519 353.1706 542.1115 -4.7837 385.2542 390.0379 352.9814 543.7128 -4.7793 385.0618 389.8411 352.7853 545.3424 -4.7738 384.8614 389.6352 352.6018 546.9433 -4.7666 384.6557 389.4223 352.3899 548.5453 -4.7597 384.4636 389.2232 352.2069 550.1459 -4.7597 384.2552 389.0149 352.0142 551.7604 -4.7556 384.0689 388.8245 351.8187 553.3611 -4.7474 383.8624 388.6098 351.6273 554.9759 -4.7473 383.6582 388.4055 351.4205 556.5898 -4.7410 383.4622 388.2032 351.2239 558.1886 -4.7381 383.2685 388.0066 351.0428 559.7884 -4.7304 383.0546 387.7850 350.8228 561.4029 -4.7274 382.8501 387.5776 350.6104 563.0105 -4.7197 382.6622 387.3819 350.4041 564.6021 -4.7170 382.4736 387.1907 350.2049 566.2090 -4.7093 382.2575 386.9668 349.9944 567.8006 -4.7037 382.0497 386.7533 349.7956 569.3959 -4.7028 381.8668 386.5696 349.5760 571.0235 -4.6987 381.6538 386.3525 349.3591 572.6228 -4.6920 381.4504 386.1423 349.1493 574.2216 -4.6861 381.2501 385.9361 348.9483 575.8205 -4.6826 381.0609 385.7435 348.7470 577.4346 -4.6798 380.8508 385.5305 348.5335 579.0335 -4.6726 380.6439 385.3165 348.3171 580.6475 -4.6654 380.4536 385.1190 348.1155 582.2618 -4.6598 380.2447 384.9045 347.9057 583.8615 -4.6571 380.0462 384.7033 347.7209 585.4755 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