DTA measure 1pd_updown3 Test Date: 2024220:1120 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 938.25 s Mass = 1383.2 mg data_number = 1168 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1785 2.1586 227.2884 225.1299 265.6588 1.9670 2.1544 227.5395 225.3850 265.6786 2.7563 2.1528 227.8086 225.6558 265.6802 3.5778 2.1467 228.0730 225.9263 265.7083 4.3395 2.1410 228.3360 226.1950 265.7065 5.1915 2.1411 228.6011 226.4599 265.7398 5.9835 2.1371 228.8556 226.7185 265.7480 6.7755 2.1325 229.1221 226.9897 265.7739 7.5978 2.1326 229.3757 227.2431 265.8039 8.3595 2.1270 229.6102 227.4833 265.8420 9.2128 2.1230 229.9023 227.7793 265.8871 9.9745 2.1190 230.1350 228.0160 265.9226 10.7968 2.1151 230.3921 228.2770 265.9920 11.6188 2.1098 230.6480 228.5383 266.0653 12.3805 2.1069 230.8836 228.7767 266.1311 13.2328 2.1034 231.1559 229.0526 266.2444 13.9945 2.0979 231.4034 229.3055 266.3203 14.8168 2.0929 231.6609 229.5681 266.4188 15.6385 2.0860 231.9186 229.8326 266.5334 16.4005 2.0777 232.1489 230.0712 266.6530 17.2525 2.0741 232.4058 230.3317 266.7633 18.0145 2.0713 232.6351 230.5638 266.8971 18.8365 2.0682 232.8949 230.8267 267.0373 19.6585 2.0623 233.1575 231.0952 267.1842 20.4205 2.0543 233.3954 231.3411 267.2969 21.2725 2.0459 233.6302 231.5844 267.4695 22.0345 2.0416 233.8652 231.8236 267.5983 22.8560 2.0368 234.1240 232.0872 267.7568 23.6780 2.0297 234.3616 232.3319 267.9052 24.4395 2.0234 234.5968 232.5734 268.0521 25.2920 2.0165 234.8563 232.8398 268.2407 26.0535 2.0105 235.0777 233.0672 268.3996 26.8765 2.0032 235.3170 233.3138 268.5416 27.6980 1.9987 235.5581 233.5595 268.7056 28.4560 1.9952 235.7872 233.7920 268.8596 29.3043 1.9867 236.0208 234.0341 269.0271 30.0623 1.9802 236.2465 234.2663 269.1933 30.8803 1.9724 236.4931 234.5206 269.3557 31.6988 1.9649 236.7332 234.7682 269.5245 32.4570 1.9556 236.9600 235.0044 269.6921 33.3068 1.9489 237.2075 235.2586 269.8666 34.0953 1.9421 237.4251 235.4829 270.0258 34.8840 1.9334 237.6623 235.7289 270.1835 35.7033 1.9244 237.8905 235.9660 270.3450 36.4640 1.9176 238.1360 236.2184 270.4837 37.3160 1.9080 238.3825 236.4744 270.6559 38.1080 1.8969 238.5862 236.6893 270.8155 38.8998 1.8879 238.8028 236.9148 270.9566 39.7233 1.8841 239.0556 237.1715 271.1113 40.4855 1.8746 239.2763 237.4017 271.2783 41.3380 1.8642 239.5115 237.6473 271.4130 42.0998 1.8546 239.7325 237.8778 271.5470 42.9218 1.8463 239.9629 238.1166 271.6854 43.7438 1.8362 240.1735 238.3373 271.8145 44.5055 1.8279 240.3830 238.5551 271.9453 45.3585 1.8173 240.6358 238.8185 272.0798 46.1508 1.8084 240.8532 239.0448 272.1996 46.9425 1.7996 241.0798 239.2802 272.3293 47.7648 1.7919 241.3044 239.5125 272.4614 48.5265 1.7829 241.5206 239.7377 272.5733 49.3820 1.7724 241.7568 239.9845 272.7275 50.1475 1.7629 241.9804 240.2175 272.8458 50.9698 1.7525 242.1986 240.4461 272.9755 51.7918 1.7432 242.4313 240.6881 273.0964 52.5535 1.7343 242.6349 240.9006 273.2016 53.4058 1.7308 242.8725 241.1417 273.3256 54.1978 1.7192 243.0779 241.3587 273.4361 54.9905 1.7086 243.3036 241.5950 273.5411 55.8128 1.6983 243.5205 241.8222 273.6725 56.5755 1.6898 243.7240 242.0342 273.7771 57.4280 1.6796 243.9430 242.2634 273.9082 58.2205 1.6696 244.1804 242.5108 274.0102 59.0135 1.6583 244.3821 242.7239 274.1444 59.8348 1.6524 244.6112 242.9589 274.2657 60.5928 1.6439 244.8209 243.1770 274.3876 61.4410 1.6341 245.0490 243.4149 274.5199 62.2290 1.6224 245.2523 243.6299 274.6424 63.0170 1.6108 245.4467 243.8359 274.7752 63.8353 1.6020 245.6704 244.0684 274.9305 64.6240 1.5915 245.8861 244.2946 275.0600 65.4428 1.5827 246.1072 244.5245 275.1890 66.2313 1.5771 246.3148 244.7377 275.3294 67.0218 1.5653 246.5254 244.9601 275.4491 67.8420 1.5547 246.7294 245.1746 275.5949 68.6325 1.5436 246.9537 245.4101 275.7315 69.4545 1.5337 247.1559 245.6222 275.8766 70.2465 1.5233 247.3490 245.8257 276.0093 71.0385 1.5129 247.5619 246.0491 276.1410 71.8605 1.5037 247.8015 246.2978 276.2908 72.6525 1.4951 248.0052 246.5101 276.4285 73.4745 1.4850 248.2113 246.7264 276.5911 74.2665 1.4761 248.4163 246.9402 276.7182 75.0585 1.4653 248.6221 247.1567 276.8527 75.8805 1.4558 248.8352 247.3794 277.0002 76.6725 1.4457 249.0448 247.5991 277.1350 77.4945 1.4359 249.2571 247.8212 277.2656 78.2865 1.4274 249.4418 248.0144 277.4125 79.0785 1.4185 249.6444 248.2259 277.5631 79.9003 1.4097 249.8542 248.4445 277.7049 80.6935 1.4008 250.0474 248.6465 277.8493 81.5170 1.3882 250.2653 248.8770 277.9773 82.3093 1.3777 250.4775 249.0998 278.1310 83.1005 1.3694 250.6804 249.3110 278.2720 83.9535 1.3583 250.8809 249.5225 278.4219 84.7155 1.3517 251.0763 249.7246 278.5605 85.5385 1.3396 251.2936 249.9540 278.7022 86.3308 1.3282 251.5009 250.1727 278.8401 87.1225 1.3185 251.6822 250.3636 278.9643 87.9748 1.3066 251.9073 250.6007 279.1192 88.7365 1.2950 252.1059 250.8109 279.2541 89.5600 1.2858 252.2963 251.0104 279.3944 90.3528 1.2793 252.4911 251.2118 279.5300 91.1455 1.2661 252.6908 251.4247 279.6686 91.9960 1.2551 252.9131 251.6579 279.8124 92.7540 1.2455 253.1010 251.8555 279.9445 93.5720 1.2358 253.3021 252.0663 280.0791 94.3600 1.2265 253.4904 252.2638 280.1994 95.1480 1.2178 253.6799 252.4621 280.3374 95.9968 1.2050 253.8922 252.6872 280.4711 96.7550 1.1980 254.0905 252.8925 280.6042 97.5740 1.1869 254.2988 253.1119 280.7206 98.3925 1.1774 254.4871 253.3096 280.8275 99.1510 1.1687 254.6726 253.5040 280.9489 100.0005 1.1568 254.8775 253.7206 281.0638 100.7598 1.1453 255.0551 253.9098 281.1725 101.5808 1.1378 255.2588 254.1211 281.2944 102.4028 1.1280 255.4669 254.3389 281.4146 103.1645 1.1168 255.6476 254.5307 281.5288 104.0188 1.1057 255.8540 254.7483 281.6378 104.7805 1.0983 256.0344 254.9361 281.7553 105.6028 1.0900 256.2412 255.1512 281.9024 106.3948 1.0837 256.4325 255.3487 282.0092 107.1865 1.0761 256.6146 255.5385 282.1280 108.0388 1.0628 256.8193 255.7565 282.2820 108.8005 1.0533 257.0060 255.9527 282.4006 109.6228 1.0443 257.2113 256.1671 282.5262 110.4148 1.0351 257.4107 256.3756 282.6722 111.2075 1.0229 257.5954 256.5724 282.8066 112.0595 1.0146 257.8011 256.7865 282.9504 112.8215 1.0047 257.9817 256.9770 283.0805 113.6438 0.9938 258.1694 257.1756 283.2258 114.4355 0.9850 258.3616 257.3766 283.3490 115.2275 0.9776 258.5401 257.5625 283.4749 116.0495 0.9669 258.7459 257.7791 283.6169 116.8415 0.9587 258.9331 257.9744 283.7513 117.6635 0.9486 259.1277 258.1791 283.8864 118.4555 0.9406 259.3089 258.3684 284.0373 119.2475 0.9318 259.5025 258.5707 284.1456 120.0695 0.9233 259.6727 258.7494 284.2925 120.8620 0.9126 259.8736 258.9610 284.4290 121.6848 0.9024 260.0844 259.1820 284.5771 122.4770 0.8919 260.2599 259.3680 284.7224 123.2688 0.8826 260.4275 259.5449 284.8495 124.0888 0.8759 260.6239 259.7480 284.9919 124.8473 0.8678 260.8046 259.9368 285.1186 125.6958 0.8586 260.9958 260.1371 285.2728 126.4830 0.8478 261.1732 260.3255 285.4125 127.2718 0.8382 261.3672 260.5290 285.5382 128.0900 0.8276 261.5556 260.7280 285.6726 128.8490 0.8221 261.7277 260.9056 285.8115 129.6978 0.8124 261.9280 261.1157 285.9499 130.4860 0.8062 262.0995 261.2933 286.0807 131.2800 0.7923 262.2936 261.5013 286.2345 132.0815 0.7843 262.4865 261.7021 286.3482 132.8735 0.7747 262.6562 261.8815 286.4868 133.6955 0.7635 262.8375 262.0740 286.6217 134.4573 0.7565 263.0198 262.2633 286.7616 135.3093 0.7491 263.2052 262.4561 286.8929 136.1015 0.7405 263.3961 262.6556 287.0321 136.8930 0.7327 263.5599 262.8272 287.1627 137.7155 0.7242 263.7501 263.0260 287.2934 138.4770 0.7140 263.9224 263.2084 287.4300 139.3290 0.7054 264.1016 263.3962 287.5722 140.0910 0.6968 264.2822 263.5854 287.6971 140.9128 0.6878 264.4794 263.7917 287.8328 141.7348 0.6796 264.6591 263.9795 287.9687 142.4965 0.6702 264.8301 264.1599 288.0936 143.3490 0.6606 265.0279 264.3673 288.2263 144.1105 0.6537 265.2020 264.5483 288.3626 144.9328 0.6439 265.3846 264.7407 288.4952 145.7548 0.6366 265.5750 264.9384 288.6363 146.5165 0.6295 265.7470 265.1175 288.7679 147.3688 0.6209 265.9127 265.2918 288.9150 148.1305 0.6103 266.0906 265.4803 289.0398 148.9528 0.6011 266.2833 265.6822 289.1663 149.7748 0.5917 266.4715 265.8798 289.2984 150.5365 0.5863 266.6306 266.0443 289.4404 151.3893 0.5768 266.8240 266.2472 289.5881 152.1408 0.5692 266.9909 266.4217 289.6861 152.9995 0.5578 267.1937 266.6359 289.8374 153.7615 0.5485 267.3512 266.8027 289.9784 154.5835 0.5391 267.5442 267.0051 290.1084 155.3755 0.5284 267.7080 267.1797 290.2349 156.1675 0.5226 267.8775 267.3549 290.3660 157.0180 0.5136 268.0730 267.5593 290.4924 157.7758 0.5059 268.2446 267.7386 290.6278 158.5940 0.4984 268.4351 267.9367 290.7706 159.3820 0.4900 268.6098 268.1198 290.8782 160.1700 0.4796 268.7858 268.3062 291.0164 161.0180 0.4725 268.9558 268.4833 291.1538 161.7765 0.4661 269.1197 268.6536 291.2864 162.5958 0.4577 269.3086 268.8509 291.4239 163.4143 0.4469 269.4774 269.0305 291.5413 164.1743 0.4384 269.6434 269.2051 291.6553 165.0258 0.4305 269.8358 269.4053 291.8242 165.7863 0.4241 270.0040 269.5799 291.9247 166.6075 0.4156 270.1762 269.7606 292.0500 167.4285 0.4067 270.3597 269.9530 292.1966 168.1905 0.3987 270.5287 270.1300 292.3213 169.0425 0.3910 270.7135 270.3225 292.4557 169.8045 0.3842 270.8785 270.4943 292.5831 170.6265 0.3720 271.0588 270.6868 292.7074 171.4185 0.3635 271.2298 270.8663 292.8404 172.2105 0.3571 271.3723 271.0151 292.9649 173.0625 0.3473 271.5728 271.2255 293.0997 173.8245 0.3392 271.7423 271.4031 293.2325 174.6465 0.3338 271.9156 271.5819 293.3677 175.4385 0.3255 272.0852 271.7596 293.4883 176.2305 0.3151 272.2657 271.9506 293.6374 177.0825 0.3038 272.4462 272.1424 293.7509 177.8445 0.2956 272.6086 272.3129 293.8717 178.6660 0.2869 272.7800 272.4931 294.0174 179.4585 0.2819 272.9421 272.6602 294.1486 180.2500 0.2739 273.1189 272.8450 294.2635 181.1020 0.2644 273.3224 273.0580 294.4089 181.8635 0.2577 273.4757 273.2180 294.5360 182.6858 0.2493 273.6500 273.4007 294.6660 183.4778 0.2414 273.8204 273.5790 294.7753 184.2695 0.2339 273.9841 273.7502 294.9120 185.1218 0.2275 274.1639 273.9364 295.0523 185.8835 0.2193 274.3207 274.1014 295.1631 186.7065 0.2121 274.4966 274.2845 295.2971 187.4988 0.2059 274.6602 274.4543 295.4367 188.2905 0.1968 274.8177 274.6209 295.5526 189.1403 0.1878 274.9978 274.8100 295.6837 189.8990 0.1804 275.1685 274.9881 295.8151 190.7170 0.1731 275.3485 275.1753 295.9578 191.5053 0.1677 275.5144 275.3466 296.0805 192.2930 0.1593 275.6919 275.5326 296.1977 193.1418 0.1504 275.8444 275.6940 296.3269 193.9000 0.1440 276.0091 275.8650 296.4492 194.7218 0.1376 276.1821 276.0444 296.5716 195.5405 0.1340 276.3503 276.2163 296.7094 196.3013 0.1257 276.5132 276.3875 296.8259 197.1520 0.1184 276.6943 276.5759 296.9652 197.9140 0.1093 276.8650 276.7557 297.0928 198.7358 0.0999 277.0329 276.9330 297.2315 199.5278 0.0938 277.1841 277.0903 297.3592 200.3195 0.0853 277.3370 277.2517 297.5013 201.1718 0.0761 277.5131 277.4370 297.6479 201.9335 0.0690 277.7037 277.6346 297.8003 202.7558 0.0631 277.8601 277.7970 297.9370 203.5525 0.0561 278.0215 277.9653 298.0779 204.3748 0.0474 278.1917 278.1443 298.2206 205.1668 0.0403 278.3671 278.3268 298.3580 205.9585 0.0342 278.5208 278.4866 298.5148 206.7808 0.0268 278.6991 278.6722 298.6738 207.5725 0.0201 278.8560 278.8359 298.8112 208.3948 0.0109 279.0297 279.0187 298.9486 209.1868 0.0044 279.1756 279.1713 299.0970 209.9785 -0.0018 279.3443 279.3460 299.2373 210.8308 -0.0087 279.5123 279.5210 299.3780 211.5925 -0.0152 279.6788 279.6941 299.5225 212.4145 -0.0233 279.8483 279.8716 299.6573 213.2065 -0.0311 280.0185 280.0496 299.7765 213.9998 -0.0389 280.1848 280.2237 299.9224 214.8535 -0.0469 280.3575 280.4044 300.0618 215.6155 -0.0538 280.5105 280.5643 300.1775 216.4375 -0.0603 280.6789 280.7392 300.3074 217.2598 -0.0692 280.8563 280.9255 300.4352 218.0225 -0.0787 281.0086 281.0873 300.5510 218.8743 -0.0843 281.1846 281.2689 300.6955 219.6363 -0.0905 281.3246 281.4151 300.8278 220.4578 -0.0981 281.4914 281.5895 300.9282 221.2768 -0.1054 281.6724 281.7778 301.0629 222.0345 -0.1125 281.8343 281.9467 301.1643 222.8828 -0.1173 281.9945 282.1119 301.2958 223.6405 -0.1240 282.1319 282.2559 301.4186 224.4588 -0.1316 282.3051 282.4367 301.5424 225.2770 -0.1393 282.4905 282.6297 301.6606 226.0360 -0.1462 282.6403 282.7865 301.7832 226.8845 -0.1520 282.8021 282.9541 301.9146 227.6740 -0.1601 282.9545 283.1146 302.0252 228.4638 -0.1681 283.1321 283.3002 302.1528 229.2835 -0.1745 283.2842 283.4587 302.2841 230.0445 -0.1790 283.4372 283.6162 302.3972 230.8965 -0.1877 283.6068 283.7945 302.5381 231.6885 -0.1947 283.7730 283.9677 302.6635 232.4803 -0.2025 283.9227 284.1252 302.8043 233.3025 -0.2113 284.0884 284.2997 302.9410 234.0645 -0.2150 284.2290 284.4440 303.0728 234.9165 -0.2224 284.4067 284.6291 303.2152 235.7085 -0.2290 284.5702 284.7992 303.3565 236.5003 -0.2364 284.7318 284.9682 303.4969 237.3223 -0.2430 284.8961 285.1391 303.6369 238.0840 -0.2501 285.0478 285.2979 303.7676 238.9360 -0.2598 285.2303 285.4901 303.9089 239.7280 -0.2636 285.3900 285.6537 304.0530 240.5205 -0.2711 285.5373 285.8084 304.1889 241.3428 -0.2769 285.7112 285.9881 304.3290 242.1045 -0.2815 285.8572 286.1387 304.4517 242.9568 -0.2911 286.0266 286.3177 304.6091 243.7488 -0.2977 286.1782 286.4759 304.7482 244.5405 -0.3043 286.3257 286.6300 304.8784 245.3628 -0.3101 286.5076 286.8177 305.0428 246.1545 -0.3181 286.6669 286.9851 305.1739 246.9775 -0.3274 286.8235 287.1509 305.3125 247.7698 -0.3335 286.9797 287.3131 305.4507 248.5625 -0.3397 287.1522 287.4919 305.5891 249.3848 -0.3457 287.3169 287.6625 305.7393 250.1465 -0.3523 287.4537 287.8060 305.8735 250.9985 -0.3575 287.6261 287.9836 306.0106 251.7905 -0.3625 287.7747 288.1372 306.1362 252.5820 -0.3694 287.9328 288.3022 306.2716 253.4008 -0.3761 288.0982 288.4743 306.4276 254.1590 -0.3812 288.2388 288.6200 306.5611 255.0100 -0.3887 288.4117 288.8004 306.7023 255.7980 -0.3970 288.5664 288.9634 306.8459 256.5860 -0.4026 288.7238 289.1264 307.0062 257.4045 -0.4099 288.8875 289.2974 307.1294 258.1630 -0.4179 289.0361 289.4540 307.2597 259.0123 -0.4213 289.2081 289.6294 307.4087 259.8015 -0.4278 289.3558 289.7836 307.5272 260.5918 -0.4364 289.5170 289.9534 307.6411 261.4125 -0.4432 289.6754 290.1186 307.7644 262.1740 -0.4485 289.8082 290.2567 307.8926 263.0255 -0.4567 289.9954 290.4521 308.0179 263.7875 -0.4617 290.1530 290.6147 308.1231 264.6100 -0.4689 290.3116 290.7805 308.2405 265.4325 -0.4755 290.4651 290.9406 308.3575 266.1945 -0.4823 290.6199 291.1021 308.4625 267.0465 -0.4859 290.7868 291.2726 308.6083 267.8085 -0.4930 290.9406 291.4336 308.7029 268.6305 -0.4982 291.0900 291.5882 308.8201 269.4225 -0.5006 291.2620 291.7626 308.9327 270.2145 -0.5071 291.4177 291.9248 309.0704 271.0665 -0.5172 291.5597 292.0769 309.2154 271.8285 -0.5231 291.7192 292.2423 309.3427 272.6505 -0.5278 291.8773 292.4051 309.4646 273.4425 -0.5304 292.0341 292.5644 309.5740 274.2343 -0.5405 292.1835 292.7240 309.7062 275.0870 -0.5453 292.3746 292.9199 309.8540 275.8495 -0.5531 292.5185 293.0716 309.9837 276.6713 -0.5575 292.6635 293.2210 310.0990 277.4635 -0.5628 292.8244 293.3872 310.2295 278.2548 -0.5668 292.9753 293.5421 310.3690 279.0773 -0.5743 293.1409 293.7152 310.4911 279.8688 -0.5813 293.2908 293.8720 310.6324 280.6908 -0.5875 293.4418 294.0293 310.7777 281.4828 -0.5936 293.6106 294.2042 310.9092 282.2745 -0.6013 293.7575 294.3589 311.0245 283.0970 -0.6077 293.9065 294.5142 311.1661 283.8895 -0.6147 294.0706 294.6854 311.2938 284.7125 -0.6191 294.2199 294.8391 311.4408 285.5045 -0.6251 294.3818 295.0069 311.5711 286.2940 -0.6309 294.5482 295.1791 311.6993 287.1123 -0.6354 294.7056 295.3410 311.8401 287.8700 -0.6385 294.8614 295.4999 311.9597 288.7190 -0.6435 295.0121 295.6556 312.0963 289.5073 -0.6496 295.1479 295.7975 312.2344 290.2960 -0.6554 295.3127 295.9681 312.3822 291.1145 -0.6646 295.4670 296.1316 312.5236 291.8740 -0.6698 295.6105 296.2803 312.6391 292.7240 -0.6734 295.7793 296.4527 312.7683 293.5133 -0.6787 295.9410 296.6197 312.9031 294.3035 -0.6852 296.0866 296.7718 313.0171 295.1250 -0.6933 296.2476 296.9409 313.1591 295.8860 -0.6989 296.3957 297.0946 313.2804 296.7380 -0.7042 296.5525 297.2567 313.4155 297.4998 -0.7093 296.6933 297.4027 313.5286 298.3238 -0.7181 296.8510 297.5691 313.6792 299.1458 -0.7207 297.0324 297.7531 313.7978 299.9075 -0.7262 297.1820 297.9082 313.9264 300.7598 -0.7330 297.3280 298.0610 314.0661 301.5215 -0.7405 297.4756 298.2161 314.1992 302.3438 -0.7451 297.6253 298.3703 314.3267 303.1358 -0.7498 297.7751 298.5248 314.4529 303.9275 -0.7525 297.9325 298.6850 314.5745 304.7798 -0.7616 298.1222 298.8838 314.7134 305.5415 -0.7681 298.2569 299.0250 314.8254 306.3638 -0.7727 298.4055 299.1782 314.9615 307.1558 -0.7779 298.5469 299.3248 315.0994 307.9475 -0.7823 298.7184 299.5007 315.2268 308.7998 -0.7865 298.8750 299.6615 315.3578 309.5615 -0.7911 299.0265 299.8175 315.4742 310.3835 -0.7983 299.1734 299.9717 315.5944 311.1755 -0.8050 299.3355 300.1406 315.7354 311.9675 -0.8095 299.4801 300.2896 315.8484 312.8210 -0.8169 299.6352 300.4521 316.0038 313.5835 -0.8220 299.7763 300.5983 316.1365 314.4055 -0.8264 299.9263 300.7527 316.2674 315.1975 -0.8319 300.0910 300.9230 316.3812 315.9895 -0.8374 300.2495 301.0869 316.5113 316.8415 -0.8419 300.4044 301.2463 316.6732 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