DTA measure 1pd_updown4 Test Date: 2024220:1215 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 835.26 s Mass = 1383.2 mg data_number = 1039 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1308 -0.1729 246.9711 247.1440 266.0965 1.8925 -0.1665 247.1099 247.2764 266.1230 2.7448 -0.1606 247.2769 247.4375 266.1517 3.5368 -0.1552 247.4416 247.5968 266.1498 4.3285 -0.1515 247.5934 247.7449 266.1708 5.1505 -0.1460 247.7564 247.9023 266.2018 5.9125 -0.1411 247.9086 248.0497 266.1937 6.7645 -0.1356 248.0694 248.2050 266.1990 7.5568 -0.1304 248.2095 248.3399 266.2257 8.3485 -0.1246 248.3774 248.5020 266.2664 9.1710 -0.1164 248.5386 248.6550 266.3030 9.9335 -0.1137 248.6775 248.7912 266.3398 10.7855 -0.1093 248.8399 248.9492 266.3801 11.5475 -0.1061 248.9732 249.0793 266.4353 12.3695 -0.0990 249.1566 249.2556 266.5046 13.1915 -0.0927 249.3096 249.4023 266.5640 13.9535 -0.0917 249.4485 249.5402 266.6260 14.8060 -0.0863 249.6114 249.6977 266.7081 15.5685 -0.0835 249.7530 249.8366 266.7983 16.3903 -0.0796 249.9037 249.9832 266.9015 17.2125 -0.0766 250.0571 250.1337 266.9909 17.9738 -0.0699 250.2017 250.2716 267.0764 18.8233 -0.0652 250.3574 250.4225 267.1910 19.5813 -0.0600 250.4952 250.5552 267.3032 20.4005 -0.0596 250.6407 250.7004 267.4153 21.2190 -0.0576 250.7900 250.8476 267.5162 21.9770 -0.0538 250.9396 250.9934 267.6329 22.8255 -0.0493 251.1084 251.1577 267.7324 23.5760 -0.0455 251.2454 251.2909 267.8370 24.4255 -0.0426 251.3952 251.4378 267.9594 25.1840 -0.0424 251.5244 251.5668 268.0914 26.0045 -0.0412 251.6778 251.7190 268.2108 26.8260 -0.0380 251.8208 251.8587 268.3252 27.5875 -0.0341 251.9557 251.9898 268.4566 28.4395 -0.0308 252.1182 252.1489 268.5916 29.2015 -0.0331 252.2517 252.2848 268.6976 30.0233 -0.0311 252.3922 252.4232 268.8134 30.8153 -0.0296 252.5416 252.5712 268.9604 31.6068 -0.0298 252.6980 252.7278 269.0784 32.4595 -0.0303 252.8396 252.8699 269.2014 33.2213 -0.0278 252.9724 253.0002 269.3254 34.0450 -0.0266 253.1252 253.1518 269.4379 34.8370 -0.0258 253.2817 253.3075 269.5753 35.6288 -0.0253 253.4269 253.4521 269.6972 36.4510 -0.0246 253.5685 253.5931 269.8238 37.2425 -0.0251 253.7079 253.7330 269.9543 38.0648 -0.0227 253.8399 253.8626 270.0798 38.8568 -0.0236 253.9934 254.0170 270.2035 39.6485 -0.0209 254.1355 254.1564 270.3121 40.4708 -0.0220 254.2949 254.3169 270.4422 41.2625 -0.0231 254.4418 254.4648 270.5719 42.0848 -0.0198 254.5755 254.5953 270.6882 42.8768 -0.0213 254.7119 254.7332 270.8057 43.6685 -0.0241 254.8665 254.8905 270.9115 44.4908 -0.0250 254.9965 255.0215 271.0286 45.2825 -0.0249 255.1258 255.1507 271.1293 46.1055 -0.0246 255.2726 255.2973 271.2361 46.8978 -0.0259 255.4007 255.4265 271.3488 47.6905 -0.0285 255.5418 255.5703 271.4550 48.5128 -0.0269 255.6869 255.7138 271.5662 49.3055 -0.0295 255.8327 255.8622 271.6721 50.1273 -0.0294 255.9834 256.0128 271.7748 50.9165 -0.0315 256.1093 256.1408 271.8776 51.7050 -0.0320 256.2381 256.2701 271.9769 52.5230 -0.0312 256.3946 256.4257 272.0778 53.3110 -0.0325 256.5340 256.5665 272.1860 54.1298 -0.0329 256.6760 256.7089 272.2860 54.9180 -0.0335 256.8270 256.8605 272.3860 55.7060 -0.0353 256.9581 256.9934 272.4890 56.5548 -0.0387 257.0974 257.1361 272.5974 57.3143 -0.0394 257.2340 257.2734 272.6770 58.1343 -0.0401 257.3682 257.4083 272.7902 58.9253 -0.0418 257.4989 257.5408 272.8881 59.7163 -0.0441 257.6376 257.6816 272.9759 60.5375 -0.0443 257.7722 257.8164 273.0767 61.3295 -0.0454 257.9089 257.9543 273.1883 62.1515 -0.0496 258.0518 258.1014 273.2759 62.9438 -0.0531 258.1971 258.2501 273.3644 63.7355 -0.0523 258.3364 258.3887 273.4635 64.5580 -0.0528 258.4678 258.5206 273.5740 65.3505 -0.0567 258.5978 258.6544 273.6663 66.1725 -0.0564 258.7476 258.8039 273.7649 66.9645 -0.0595 258.8847 258.9441 273.8630 67.7565 -0.0628 259.0303 259.0931 273.9631 68.5785 -0.0645 259.1678 259.2324 274.0616 69.3705 -0.0622 259.2879 259.3501 274.1579 70.1925 -0.0648 259.4382 259.5030 274.2547 70.9845 -0.0694 259.5701 259.6395 274.3381 71.7765 -0.0698 259.7022 259.7720 274.4521 72.6285 -0.0735 259.8434 259.9169 274.5686 73.3905 -0.0762 259.9768 260.0530 274.6504 74.2120 -0.0740 260.1239 260.1979 274.7641 75.0045 -0.0779 260.2482 260.3262 274.8730 75.7963 -0.0819 260.3744 260.4563 274.9911 76.6490 -0.0858 260.5194 260.6052 275.1024 77.4108 -0.0880 260.6455 260.7336 275.2105 78.2335 -0.0907 260.7840 260.8747 275.3303 79.0258 -0.0910 260.9251 261.0161 275.4493 79.8175 -0.0918 261.0575 261.1492 275.5751 80.6698 -0.0935 261.2091 261.3026 275.6878 81.4315 -0.0991 261.3210 261.4201 275.8017 82.2535 -0.0999 261.4542 261.5541 275.9002 83.0720 -0.1026 261.5885 261.6912 276.0245 83.8300 -0.1068 261.7158 261.8226 276.1377 84.6780 -0.1090 261.8632 261.9721 276.2763 85.4360 -0.1134 261.9838 262.0972 276.3909 86.2540 -0.1175 262.1256 262.2430 276.5025 87.0723 -0.1219 262.2554 262.3773 276.6316 87.8300 -0.1226 262.3795 262.5022 276.7481 88.6798 -0.1252 262.5113 262.6365 276.8695 89.4683 -0.1272 262.6440 262.7712 276.9875 90.2575 -0.1323 262.7817 262.9139 277.0746 91.0778 -0.1317 262.9181 263.0498 277.1697 91.8385 -0.1370 263.0454 263.1824 277.2670 92.6910 -0.1410 263.1889 263.3299 277.3776 93.4828 -0.1419 263.3167 263.4586 277.4775 94.2745 -0.1471 263.4466 263.5937 277.5911 95.0968 -0.1507 263.5825 263.7332 277.6866 95.8585 -0.1542 263.7113 263.8655 277.7783 96.7110 -0.1576 263.8472 264.0048 277.8816 97.5028 -0.1580 263.9752 264.1331 277.9656 98.2945 -0.1620 264.1038 264.2658 278.0570 99.1168 -0.1660 264.2511 264.4171 278.1539 99.8785 -0.1677 264.3701 264.5378 278.2472 100.7308 -0.1690 264.5110 264.6800 278.3550 101.5228 -0.1731 264.6412 264.8143 278.4325 102.3145 -0.1775 264.7650 264.9425 278.5233 103.1368 -0.1818 264.8991 265.0810 278.6262 103.8985 -0.1843 265.0176 265.2019 278.7085 104.7508 -0.1864 265.1469 265.3333 278.8120 105.5113 -0.1878 265.2799 265.4677 278.9257 106.3633 -0.1914 265.4232 265.6146 279.0273 107.1255 -0.1957 265.5501 265.7457 279.1257 107.9475 -0.1980 265.7006 265.8985 279.2262 108.7698 -0.2022 265.8309 266.0332 279.3291 109.5325 -0.2056 265.9445 266.1502 279.4522 110.3850 -0.2114 266.0762 266.2876 279.5644 111.1475 -0.2150 266.1965 266.4116 279.6694 111.9695 -0.2190 266.3304 266.5494 279.7826 112.7915 -0.2212 266.4543 266.6755 279.8978 113.5535 -0.2248 266.5768 266.8016 279.9975 114.4053 -0.2274 266.7197 266.9470 280.1308 115.1668 -0.2324 266.8298 267.0622 280.2360 115.9868 -0.2359 266.9700 267.2059 280.3550 116.8048 -0.2370 267.1013 267.3382 280.4803 117.5628 -0.2412 267.2249 267.4662 280.5771 118.4110 -0.2425 267.3542 267.5967 280.6925 119.1690 -0.2474 267.4722 267.7196 280.7978 119.9878 -0.2502 267.6142 267.8644 280.9190 120.8060 -0.2524 267.7526 268.0050 281.0312 121.5638 -0.2554 267.8564 268.1118 281.1409 122.4128 -0.2618 268.0003 268.2621 281.2697 123.1735 -0.2644 268.1129 268.3773 281.3731 123.9945 -0.2688 268.2358 268.5046 281.4856 124.8165 -0.2713 268.3691 268.6404 281.5969 125.5963 -0.2760 268.5059 268.7819 281.7109 126.4065 -0.2826 268.6353 268.9179 281.8280 127.1980 -0.2858 268.7625 269.0482 281.9339 128.0195 -0.2895 268.9032 269.1927 282.0755 128.7815 -0.2927 269.0230 269.3157 282.1840 129.6333 -0.2951 269.1650 269.4601 282.2978 130.3953 -0.2974 269.2691 269.5665 282.3945 131.2173 -0.3007 269.4019 269.7026 282.5091 132.0395 -0.3056 269.5296 269.8353 282.6286 132.8005 -0.3091 269.6538 269.9629 282.7332 133.6530 -0.3135 269.7815 270.0949 282.8330 134.4145 -0.3187 269.8983 270.2170 282.9249 135.2370 -0.3219 270.0424 270.3643 283.0209 136.0590 -0.3252 270.1700 270.4951 283.1061 136.8208 -0.3301 270.2962 270.6262 283.2086 137.6728 -0.3333 270.4237 270.7569 283.3114 138.4345 -0.3367 270.5338 270.8706 283.4000 139.2568 -0.3405 270.6666 271.0071 283.4844 140.0788 -0.3386 270.7926 271.1312 283.5685 140.8405 -0.3372 270.9112 271.2484 283.6498 141.6933 -0.3408 271.0636 271.4044 283.7562 142.4555 -0.3521 271.1765 271.5287 283.8444 143.2778 -0.3568 271.3043 271.6610 283.9476 144.0998 -0.3592 271.4396 271.7988 284.0329 144.8615 -0.3623 271.5453 271.9076 284.1264 145.7135 -0.3670 271.6801 272.0471 284.2291 146.4755 -0.3699 271.7977 272.1676 284.3329 147.2973 -0.3719 271.9319 272.3038 284.4326 148.1160 -0.3783 272.0706 272.4489 284.5343 148.8740 -0.3833 272.1836 272.5669 284.6471 149.7220 -0.3881 272.3301 272.7182 284.7559 150.4800 -0.3898 272.4397 272.8296 284.8525 151.2980 -0.3932 272.5632 272.9563 284.9505 152.1163 -0.3964 272.6927 273.0890 285.0595 152.8758 -0.4012 272.8017 273.2030 285.1641 153.7245 -0.4047 272.9315 273.3362 285.2821 154.4845 -0.4079 273.0615 273.4693 285.4052 155.3053 -0.4134 273.1806 273.5941 285.5094 156.1263 -0.4171 273.3156 273.7326 285.6273 156.8865 -0.4208 273.4321 273.8529 285.7216 157.7388 -0.4236 273.5622 273.9858 285.8372 158.5005 -0.4283 273.6772 274.1055 285.9389 159.3228 -0.4290 273.7972 274.2262 286.0550 160.1148 -0.4318 273.9229 274.3546 286.1569 160.9065 -0.4369 274.0625 274.4994 286.2570 161.7585 -0.4390 274.1902 274.6292 286.3874 162.5205 -0.4426 274.2990 274.7417 286.4803 163.3425 -0.4462 274.4177 274.8640 286.5894 164.1345 -0.4528 274.5328 274.9856 286.6966 164.9265 -0.4583 274.6576 275.1159 286.8010 165.7485 -0.4613 274.7810 275.2423 286.8998 166.5155 -0.4646 274.8989 275.3635 287.0044 167.3805 -0.4698 275.0391 275.5089 287.1297 168.1425 -0.4735 275.1600 275.6335 287.2317 168.9645 -0.4776 275.2717 275.7493 287.3543 169.7565 -0.4799 275.4079 275.8878 287.4482 170.5485 -0.4848 275.5082 275.9930 287.5451 171.4005 -0.4882 275.6520 276.1402 287.6544 172.1623 -0.4937 275.7867 276.2804 287.7610 172.9845 -0.4977 275.9084 276.4061 287.8789 173.7763 -0.4996 276.0114 276.5110 287.9793 174.5680 -0.5035 276.1353 276.6389 288.0979 175.4198 -0.5065 276.2513 276.7578 288.1986 176.1818 -0.5084 276.3976 276.9060 288.3007 177.0045 -0.5127 276.5209 277.0336 288.4066 177.7968 -0.5179 276.6312 277.1492 288.5201 178.5885 -0.5206 276.7577 277.2784 288.6313 179.4405 -0.5220 276.8976 277.4196 288.7379 180.1993 -0.5273 277.0119 277.5392 288.8528 181.0175 -0.5304 277.1407 277.6711 288.9496 181.8053 -0.5349 277.2588 277.7937 289.0626 182.5930 -0.5371 277.3704 277.9076 289.1686 183.4413 -0.5416 277.5056 278.0472 289.2686 184.1993 -0.5454 277.6123 278.1576 289.3757 185.0190 -0.5475 277.7405 278.2880 289.5003 185.8383 -0.5543 277.8628 278.4171 289.5901 186.5973 -0.5573 277.9819 278.5393 289.6835 187.4483 -0.5601 278.1109 278.6711 289.8156 188.2090 -0.5653 278.2353 278.8007 289.9059 189.0298 -0.5701 278.3554 278.9255 290.0287 189.8518 -0.5724 278.4899 279.0623 290.1407 190.6135 -0.5783 278.5879 279.1662 290.2389 191.4660 -0.5792 278.7319 279.3111 290.3675 192.2278 -0.5840 278.8290 279.4131 290.4452 193.0498 -0.5878 278.9601 279.5480 290.5540 193.8418 -0.5909 279.0803 279.6713 290.6526 194.6335 -0.5943 279.2030 279.7973 290.7609 195.4863 -0.5991 279.3303 279.9294 290.8747 196.2485 -0.6039 279.4506 280.0545 290.9701 197.0708 -0.6066 279.5997 280.2062 291.0795 197.8628 -0.6076 279.6959 280.3036 291.1848 198.6545 -0.6111 279.8020 280.4131 291.3047 199.5065 -0.6177 279.9303 280.5479 291.3995 200.2693 -0.6233 280.0492 280.6725 291.4997 201.0918 -0.6223 280.1742 280.7965 291.6100 201.8838 -0.6237 280.2918 280.9155 291.7036 202.6755 -0.6283 280.4078 281.0361 291.8107 203.5283 -0.6325 280.5491 281.1816 291.8996 204.2913 -0.6345 280.6612 281.2957 292.0175 205.1145 -0.6366 280.8048 281.4414 292.1124 205.9065 -0.6416 280.9279 281.5695 292.2125 206.6985 -0.6466 281.0333 281.6799 292.3257 207.5510 -0.6483 281.1603 281.8087 292.4109 208.3135 -0.6525 281.2757 281.9282 292.5276 209.1355 -0.6555 281.3883 282.0438 292.6278 209.9275 -0.6585 281.5129 282.1713 292.7180 210.7205 -0.6629 281.6335 282.2964 292.8215 211.5715 -0.6651 281.7765 282.4416 292.9409 212.3295 -0.6690 281.8736 282.5426 293.0206 213.1485 -0.6679 282.0009 282.6688 293.1161 213.9373 -0.6738 282.1292 282.8030 293.2140 214.7270 -0.6793 282.2306 282.9099 293.2977 215.5755 -0.6834 282.3718 283.0552 293.3994 216.3340 -0.6861 282.4838 283.1699 293.4883 217.1528 -0.6895 282.5978 283.2873 293.5941 217.9720 -0.6907 282.7455 283.4362 293.7032 218.7313 -0.6938 282.8567 283.5505 293.8000 219.5805 -0.6987 282.9786 283.6773 293.9109 220.3415 -0.7044 283.0846 283.7889 294.0181 221.1635 -0.7079 283.2136 283.9215 294.1229 221.9855 -0.7101 283.3332 284.0434 294.2209 222.7475 -0.7134 283.4420 284.1554 294.3269 223.5995 -0.7166 283.5625 284.2791 294.4376 224.3615 -0.7205 283.6749 284.3954 294.5545 225.1835 -0.7224 283.8001 284.5225 294.6591 225.9755 -0.7261 283.9106 284.6367 294.7716 226.7675 -0.7291 284.0558 284.7849 294.8862 227.6195 -0.7314 284.1807 284.9121 295.0076 228.3815 -0.7357 284.2797 285.0154 295.1291 229.2033 -0.7404 284.4012 285.1416 295.2446 229.9955 -0.7456 284.5269 285.2725 295.3526 230.7873 -0.7466 284.6282 285.3748 295.4667 231.6393 -0.7481 284.7489 285.4969 295.5898 232.4010 -0.7522 284.8635 285.6157 295.7018 233.2228 -0.7581 285.0008 285.7589 295.8273 234.0150 -0.7617 285.1100 285.8717 295.9318 234.8065 -0.7646 285.2174 285.9820 296.0597 235.6593 -0.7679 285.3473 286.1152 296.1743 236.4215 -0.7713 285.4703 286.2416 296.2822 237.2445 -0.7753 285.6023 286.3776 296.3962 238.0368 -0.7791 285.7167 286.4958 296.5059 238.8285 -0.7821 285.8300 286.6120 296.6222 239.6813 -0.7840 285.9487 286.7327 296.7293 240.4435 -0.7891 286.0699 286.8590 296.8307 241.2658 -0.7910 286.1896 286.9806 296.9219 242.0878 -0.7986 286.3080 287.1066 297.0489 242.8495 -0.7993 286.4218 287.2211 297.1346 243.7015 -0.8022 286.5436 287.3458 297.2253 244.4628 -0.8069 286.6630 287.4699 297.3170 245.2810 -0.8119 286.7846 287.5965 297.4173 246.0990 -0.8142 286.9120 287.7262 297.5114 246.8570 -0.8167 287.0262 287.8428 297.6025 247.7050 -0.8199 287.1490 287.9690 297.6984 248.4630 -0.8216 287.2588 288.0804 297.7944 249.2818 -0.8228 287.3767 288.1995 297.8793 250.1000 -0.8290 287.5075 288.3365 297.9745 250.8580 -0.8326 287.6274 288.4600 298.0480 251.7085 -0.8373 287.7502 288.5875 298.1568 252.4688 -0.8399 287.8502 288.6902 298.2641 253.2908 -0.8439 287.9824 288.8263 298.3559 254.0825 -0.8463 288.0982 288.9444 298.4500 254.8745 -0.8501 288.2180 289.0680 298.5472 255.7268 -0.8540 288.3226 289.1766 298.6627 256.4885 -0.8584 288.4478 289.3062 298.7673 257.3108 -0.8620 288.5570 289.4191 298.8732 258.1028 -0.8625 288.6766 289.5391 298.9838 258.9063 -0.8665 288.7892 289.6558 299.0851 259.7325 -0.8700 288.9301 289.8002 299.2018 260.4945 -0.8736 289.0423 289.9158 299.2985 261.3465 -0.8768 289.1799 290.0567 299.4306 262.1085 -0.8798 289.2774 290.1572 299.5194 262.9305 -0.8855 289.3898 290.2753 299.6407 263.7525 -0.8893 289.5068 290.3961 299.7373 264.5145 -0.8921 289.6401 290.5322 299.8487 265.3665 -0.8958 289.7604 290.6563 299.9718 266.1285 -0.9003 289.8622 290.7625 300.0704 266.9505 -0.9010 289.9880 290.8890 300.1675 267.7725 -0.9066 290.1160 291.0225 300.2918 268.5345 -0.9113 290.2302 291.1416 300.4098 269.3865 -0.9130 290.3517 291.2646 300.5293 270.1485 -0.9154 290.4694 291.3848 300.6424 270.9700 -0.9175 290.5869 291.5044 300.7553 271.7923 -0.9216 290.6999 291.6215 300.8540 272.5545 -0.9249 290.8055 291.7303 300.9748 273.4070 -0.9308 290.9311 291.8619 301.0923 274.1685 -0.9328 291.0527 291.9856 301.1785 274.9908 -0.9313 291.1626 292.0939 301.2967 275.8130 -0.9337 291.2800 292.2137 301.3987 276.5740 -0.9408 291.4030 292.3438 301.5129 277.4220 -0.9456 291.5336 292.4792 301.6201 278.1800 -0.9501 291.6416 292.5917 301.7286 278.9985 -0.9539 291.7629 292.7168 301.8411 279.7868 -0.9503 291.8721 292.8225 301.9641 280.5750 -0.9551 291.9975 292.9526 302.0724 281.4250 -0.9621 292.1181 293.0801 302.1865 282.1835 -0.9655 292.2258 293.1913 302.2881 283.0038 -0.9681 292.3495 293.3176 302.3949 283.8233 -0.9717 292.4666 293.4382 302.5088 284.5830 -0.9749 292.5907 293.5656 302.6133 285.4350 -0.9774 292.7226 293.7000 302.7296 286.1960 -0.9816 292.8044 293.7860 302.8190 287.0178 -0.9820 292.9210 293.9031 302.9357 287.8100 -0.9867 293.0432 294.0300 303.0307 288.6015 -0.9914 293.1556 294.1470 303.1276 289.4318 -0.9948 293.2789 294.2736 303.2505 290.2005 -0.9996 293.3886 294.3882 303.3636 291.0528 -1.0054 293.5188 294.5241 303.4855 291.8145 -1.0095 293.6367 294.6462 303.5911 292.6368 -1.0100 293.7589 294.7689 303.6844 293.4288 -1.0123 293.8621 294.8744 303.7871 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