DTA measure 1pd_updown4_2 Test Date: 2024220:1415 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 792.41 s Mass = 1.000 mg data_number = 1972 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.5200 0.3862 240.8571 240.4709 265.9787 0.9440 0.3879 240.9523 240.5644 265.9974 1.3680 0.3896 241.0464 240.6568 266.0031 1.7320 0.3920 241.1435 240.7516 266.0094 2.1560 0.3941 241.2417 240.8476 266.0038 2.5805 0.3973 241.3371 240.9398 266.0045 2.9450 0.3987 241.4264 241.0277 266.0044 3.3090 0.4022 241.5089 241.1067 266.0268 3.7940 0.4040 241.6097 241.2057 266.0382 4.1600 0.4061 241.6889 241.2828 266.0377 4.5250 0.4072 241.7811 241.3739 266.0596 4.9490 0.4098 241.8908 241.4810 266.0762 5.3735 0.4125 241.9773 241.5648 266.0862 5.7385 0.4148 242.0646 241.6498 266.0937 6.1630 0.4176 242.1664 241.7487 266.0999 6.5875 0.4195 242.2600 241.8404 266.1018 6.9530 0.4227 242.3307 241.9079 266.1053 7.3185 0.4242 242.4127 241.9886 266.1230 7.8040 0.4280 242.5313 242.1034 266.1526 8.1705 0.4292 242.6329 242.2038 266.1820 8.5365 0.4299 242.7162 242.2863 266.1980 8.9625 0.4312 242.8076 242.3765 266.2064 9.3885 0.4324 242.9030 242.4706 266.2260 9.7545 0.4327 242.9890 242.5563 266.2442 10.1205 0.4356 243.0847 242.6491 266.2696 10.6065 0.4392 243.1903 242.7511 266.2802 10.9725 0.4403 243.2749 242.8346 266.3109 11.3385 0.4418 243.3655 242.9238 266.3342 11.8245 0.4460 243.4728 243.0268 266.3779 12.1905 0.4497 243.5478 243.0981 266.4082 12.5565 0.4491 243.6188 243.1697 266.4410 12.9875 0.4494 243.7130 243.2636 266.4563 13.4135 0.4518 243.7973 243.3455 266.4891 13.7795 0.4528 243.8960 243.4433 266.5215 14.1480 0.4563 243.9868 243.5306 266.5584 14.6365 0.4599 244.0984 243.6385 266.6196 15.0015 0.4618 244.1837 243.7220 266.6513 15.3680 0.4621 244.2520 243.7899 266.6848 15.7990 0.4640 244.3489 243.8848 266.7461 16.2250 0.4652 244.4509 243.9857 266.7873 16.5905 0.4697 244.5358 244.0661 266.8192 16.9590 0.4696 244.6075 244.1379 266.8606 17.4485 0.4733 244.7062 244.2329 266.9318 17.8135 0.4716 244.7904 244.3188 266.9812 18.1795 0.4729 244.8728 244.3998 267.0203 18.6065 0.4763 244.9640 244.4877 267.0822 19.0340 0.4766 245.0677 244.5911 267.1445 19.3995 0.4773 245.1449 244.6677 267.1885 19.7655 0.4782 245.2296 244.7514 267.2415 20.2520 0.4812 245.3403 244.8591 267.3225 20.6180 0.4814 245.4158 244.9344 267.3750 20.9835 0.4818 245.4940 245.0123 267.4320 21.4745 0.4835 245.5909 245.1074 267.5022 21.8405 0.4845 245.6655 245.1810 267.5664 22.2065 0.4838 245.7519 245.2680 267.6257 22.6325 0.4854 245.8610 245.3756 267.6878 23.0590 0.4883 245.9721 245.4838 267.7573 23.4245 0.4881 246.0494 245.5613 267.8275 23.7905 0.4878 246.1120 245.6243 267.8819 24.2780 0.4885 246.2180 245.7295 267.9679 24.6450 0.4923 246.2988 245.8064 268.0361 25.0130 0.4906 246.3742 245.8836 268.0897 25.4395 0.4886 246.4676 245.9790 268.1583 25.8660 0.4905 246.5695 246.0790 268.2322 26.2315 0.4918 246.6466 246.1548 268.2888 26.5975 0.4929 246.7187 246.2258 268.3469 27.0835 0.4923 246.8200 246.3277 268.4399 27.4495 0.4922 246.9008 246.4086 268.5006 27.8155 0.4937 246.9856 246.4919 268.5588 28.3015 0.4944 247.0812 246.5867 268.6240 28.6670 0.4948 247.1636 246.6688 268.6948 29.0310 0.4950 247.2450 246.7500 268.7538 29.4575 0.4959 247.3327 246.8367 268.8309 29.8830 0.4962 247.4217 246.9256 268.9035 30.2470 0.4944 247.5001 247.0057 268.9608 30.6110 0.4953 247.5762 247.0810 269.0314 31.0965 0.4948 247.6750 247.1802 269.1052 31.4620 0.4927 247.7666 247.2739 269.1716 31.8260 0.4925 247.8467 247.3543 269.2204 32.2500 0.4974 247.9355 247.4381 269.2766 32.6740 0.4981 248.0248 247.5267 269.3269 33.0390 0.4957 248.1067 247.6110 269.3873 33.4630 0.4939 248.1853 247.6913 269.4691 33.8875 0.4930 248.2745 247.7815 269.5383 34.2520 0.4938 248.3675 247.8738 269.6085 34.6160 0.4942 248.4400 247.9458 269.6692 35.1030 0.4924 248.5481 248.0557 269.7518 35.4680 0.4915 248.6158 248.1243 269.7986 35.8320 0.4931 248.6851 248.1920 269.8404 36.2560 0.4932 248.7674 248.2742 269.9027 36.6810 0.4941 248.8610 248.3669 269.9770 37.0460 0.4936 248.9504 248.4568 270.0339 37.4700 0.4942 249.0305 248.5362 270.1001 38.0360 0.4912 249.1407 248.6495 270.2047 38.4620 0.4930 249.2291 248.7362 270.2641 38.8870 0.4911 249.3271 248.8360 270.3180 39.2515 0.4908 249.4046 248.9138 270.3595 39.6775 0.4904 249.5022 249.0118 270.4111 40.1025 0.4912 249.5871 249.0959 270.4573 40.4685 0.4899 249.6726 249.1827 270.5064 40.8370 0.4913 249.7414 249.2502 270.5622 41.3260 0.4892 249.8380 249.3488 270.6196 41.6915 0.4885 249.9111 249.4225 270.6639 42.0575 0.4887 249.9840 249.4953 270.7155 42.4890 0.4835 250.0713 249.5879 270.7891 42.9145 0.4821 250.1534 249.6713 270.8357 43.2805 0.4826 250.2391 249.7565 270.8816 43.6490 0.4821 250.3308 249.8487 270.9432 44.1375 0.4818 250.4136 249.9318 271.0009 44.5035 0.4812 250.4954 250.0143 271.0396 44.8695 0.4813 250.5753 250.0940 271.0869 45.2955 0.4806 250.6641 250.1835 271.1455 45.7235 0.4780 250.7458 250.2678 271.1851 46.0895 0.4743 250.8269 250.3526 271.2306 46.4555 0.4746 250.9167 250.4421 271.2859 46.9415 0.4751 251.0128 250.5377 271.3533 47.3075 0.4736 251.0798 250.6062 271.3915 47.6735 0.4722 251.1534 250.6812 271.4379 48.1010 0.4733 251.2471 250.7738 271.4933 48.5275 0.4740 251.3271 250.8531 271.5524 48.8935 0.4727 251.3976 250.9249 271.5907 49.3195 0.4713 251.4908 251.0195 271.6402 49.7455 0.4712 251.5805 251.1094 271.6948 50.1115 0.4680 251.6408 251.1728 271.7394 50.4775 0.4656 251.7246 251.2590 271.8007 50.9680 0.4660 251.8255 251.3595 271.8599 51.3335 0.4672 251.9025 251.4353 271.8976 51.6995 0.4668 251.9738 251.5070 271.9310 52.1255 0.4659 252.0643 251.5984 271.9855 52.5515 0.4636 252.1508 251.6872 272.0421 52.9175 0.4642 252.2252 251.7609 272.0818 53.3435 0.4626 252.3184 251.8559 272.1312 53.7695 0.4628 252.3949 251.9321 272.1759 54.1355 0.4594 252.4652 252.0058 272.2183 54.5035 0.4584 252.5449 252.0866 272.2599 54.9925 0.4566 252.6418 252.1853 272.3157 55.3575 0.4524 252.7128 252.2604 272.3629 55.7235 0.4523 252.7980 252.3457 272.4142 56.1500 0.4506 252.8812 252.4306 272.4784 56.5780 0.4492 252.9561 252.5069 272.5300 56.9435 0.4481 253.0195 252.5713 272.5716 57.3150 0.4477 253.0939 252.6462 272.6072 57.8050 0.4463 253.2043 252.7580 272.6591 58.1695 0.4468 253.2929 252.8461 272.6946 58.5355 0.4459 253.3760 252.9301 272.7437 58.9615 0.4438 253.4609 253.0172 272.7972 59.3880 0.4424 253.5400 253.0977 272.8378 59.7535 0.4401 253.6062 253.1661 272.8876 60.1795 0.4391 253.6828 253.2437 272.9438 60.6060 0.4377 253.7723 253.3346 272.9987 60.9705 0.4360 253.8409 253.4049 273.0440 61.3365 0.4358 253.9127 253.4768 273.0850 61.8230 0.4340 254.0101 253.5761 273.1421 62.1875 0.4309 254.0891 253.6582 273.1840 62.5510 0.4310 254.1492 253.7182 273.2329 62.9770 0.4283 254.2358 253.8075 273.2861 63.4020 0.4270 254.3221 253.8951 273.3294 63.7670 0.4274 254.3971 253.9697 273.3743 64.1300 0.4277 254.4646 254.0369 273.4081 64.6150 0.4241 254.5603 254.1362 273.4756 64.9790 0.4215 254.6278 254.2064 273.5252 65.3425 0.4199 254.6904 254.2704 273.5788 65.7665 0.4173 254.7783 254.3610 273.6537 66.1910 0.4173 254.8779 254.4607 273.7088 66.5560 0.4146 254.9443 254.5296 273.7476 66.9815 0.4127 255.0189 254.6062 273.7895 67.4085 0.4108 255.1040 254.6931 273.8517 67.7730 0.4090 255.1771 254.7682 273.9126 68.1375 0.4063 255.2386 254.8323 273.9717 68.5810 0.4071 255.3269 254.9199 274.0302 69.0065 0.4044 255.4190 255.0146 274.0986 69.3725 0.4018 255.4940 255.0922 274.1422 69.7360 0.4006 255.5632 255.1626 274.1865 70.2215 0.3991 255.6534 255.2544 274.2605 70.5875 0.3971 255.7243 255.3272 274.3062 70.9525 0.3965 255.7983 255.4018 274.3589 71.4380 0.3954 255.9028 255.5074 274.4204 71.8030 0.3926 255.9607 255.5681 274.4726 72.1685 0.3915 256.0361 255.6446 274.5302 72.5940 0.3877 256.1166 255.7289 274.5879 73.0200 0.3880 256.2088 255.8208 274.6527 73.3855 0.3869 256.2752 255.8882 274.7153 73.8120 0.3845 256.3575 255.9729 274.7803 74.2380 0.3846 256.4462 256.0616 274.8466 74.6040 0.3826 256.5187 256.1361 274.9000 74.9695 0.3781 256.5899 256.2118 274.9566 75.4560 0.3775 256.6836 256.3061 275.0241 75.8215 0.3753 256.7381 256.3628 275.0874 76.1875 0.3739 256.8042 256.4303 275.1405 76.6160 0.3726 256.8889 256.5163 275.2003 77.0450 0.3692 256.9589 256.5897 275.2657 77.4105 0.3664 257.0588 256.6924 275.3167 77.7765 0.3646 257.1202 256.7555 275.3729 78.2675 0.3623 257.2097 256.8474 275.4492 78.6335 0.3617 257.2818 256.9201 275.5049 78.9995 0.3615 257.3486 256.9871 275.5541 79.4255 0.3590 257.4239 257.0649 275.6244 79.8520 0.3588 257.5083 257.1495 275.6865 80.2175 0.3537 257.5779 257.2242 275.7389 80.5835 0.3512 257.6543 257.3031 275.7982 81.0700 0.3472 257.7632 257.4159 275.8791 81.4355 0.3462 257.8302 257.4840 275.9270 81.8015 0.3434 257.9003 257.5569 275.9690 82.2880 0.3419 257.9815 257.6396 276.0369 82.6535 0.3389 258.0486 257.7098 276.0790 83.0195 0.3368 258.1195 257.7827 276.1243 83.4455 0.3356 258.1909 257.8554 276.1804 83.8720 0.3345 258.2803 257.9459 276.2420 84.2375 0.3332 258.3442 258.0111 276.2892 84.6635 0.3299 258.4351 258.1052 276.3456 85.0900 0.3307 258.5146 258.1839 276.4042 85.4555 0.3301 258.5729 258.2427 276.4421 85.8215 0.3263 258.6476 258.3213 276.4759 86.3120 0.3234 258.7502 258.4268 276.5399 86.6775 0.3230 258.8224 258.4994 276.5983 87.0435 0.3213 258.8777 258.5563 276.6451 87.4695 0.3179 258.9614 258.6435 276.6956 87.8955 0.3151 259.0221 258.7070 276.7620 88.2615 0.3129 259.0955 258.7826 276.7988 88.6875 0.3102 259.1763 258.8662 276.8456 89.1135 0.3104 259.2636 258.9532 276.9103 89.4795 0.3070 259.3261 259.0191 276.9400 89.8455 0.3054 259.3994 259.0940 276.9875 90.3330 0.3016 259.5004 259.1988 277.0486 90.7005 0.2998 259.5524 259.2526 277.1152 91.0665 0.2987 259.6251 259.3264 277.1435 91.4925 0.2972 259.7217 259.4245 277.1879 91.9185 0.2960 259.8183 259.5222 277.2413 92.2845 0.2933 259.8819 259.5886 277.2770 92.7105 0.2899 259.9573 259.6675 277.3270 93.1365 0.2882 260.0374 259.7492 277.3647 93.5025 0.2854 260.1026 259.8172 277.4304 93.8665 0.2837 260.1531 259.8695 277.4721 94.3560 0.2825 260.2471 259.9647 277.5301 94.7200 0.2799 260.3154 260.0355 277.5789 95.0840 0.2767 260.3816 260.1048 277.6179 95.5125 0.2756 260.4671 260.1915 277.6708 95.9375 0.2730 260.5575 260.2845 277.7249 96.3020 0.2701 260.6232 260.3531 277.7688 96.6660 0.2702 260.6840 260.4138 277.8021 97.1500 0.2699 260.7614 260.4915 277.8581 97.5140 0.2674 260.8299 260.5625 277.9033 97.8780 0.2658 260.9134 260.6476 277.9500 98.3620 0.2613 260.9947 260.7334 278.0029 98.7270 0.2577 261.0608 260.8031 278.0451 99.0910 0.2571 261.1204 260.8632 278.0827 99.5150 0.2559 261.1863 260.9304 278.1455 99.9420 0.2540 261.2720 261.0181 278.1945 100.3060 0.2494 261.3450 261.0956 278.2423 100.7325 0.2463 261.4415 261.1952 278.2876 101.1585 0.2435 261.5202 261.2767 278.3447 101.5230 0.2407 261.5823 261.3416 278.3777 101.8870 0.2397 261.6552 261.4155 278.4308 102.3710 0.2390 261.7320 261.4930 278.4993 102.7360 0.2356 261.8034 261.5679 278.5614 103.1005 0.2321 261.8660 261.6338 278.6058 103.5260 0.2292 261.9337 261.7045 278.6597 103.9505 0.2294 262.0077 261.7783 278.7176 104.3150 0.2281 262.0797 261.8516 278.7751 104.7405 0.2253 262.1596 261.9343 278.8249 105.1665 0.2211 262.2378 262.0167 278.8737 105.5310 0.2193 262.3078 262.0885 278.9244 105.8965 0.2148 262.3678 262.1530 278.9780 106.3825 0.2112 262.4483 262.2371 279.0491 106.7485 0.2086 262.5278 262.3192 279.0944 107.1145 0.2082 262.5882 262.3800 279.1589 107.5405 0.2065 262.6682 262.4618 279.2244 107.9665 0.2029 262.7321 262.5292 279.2891 108.3325 0.2022 262.8102 262.6080 279.3339 108.7585 0.1993 262.8819 262.6826 279.4039 109.1845 0.1969 262.9506 262.7537 279.4495 109.5505 0.1940 263.0126 262.8186 279.5045 109.9165 0.1912 263.0803 262.8891 279.5548 110.4025 0.1883 263.1761 262.9877 279.6383 110.7685 0.1842 263.2575 263.0733 279.6864 111.1345 0.1823 263.3301 263.1477 279.7423 111.5605 0.1807 263.4235 263.2428 279.7837 111.9865 0.1792 263.4903 263.3111 279.8488 112.3515 0.1781 263.5444 263.3663 279.8996 112.7780 0.1767 263.6250 263.4483 279.9568 113.2040 0.1733 263.6961 263.5228 280.0248 113.5695 0.1696 263.7694 263.5998 280.0819 113.9355 0.1674 263.8365 263.6691 280.1329 114.4220 0.1647 263.9282 263.7635 280.2092 114.7880 0.1610 263.9892 263.8282 280.2510 115.1535 0.1601 264.0680 263.9080 280.3124 115.6400 0.1564 264.1480 263.9916 280.3753 116.0055 0.1558 264.2032 264.0474 280.4290 116.3715 0.1535 264.2628 264.1093 280.4769 116.8000 0.1494 264.3395 264.1901 280.5393 117.2265 0.1480 264.4131 264.2651 280.6166 117.5925 0.1469 264.4804 264.3335 280.6656 117.9585 0.1431 264.5527 264.4095 280.7292 118.4450 0.1408 264.6399 264.4991 280.7935 118.8105 0.1377 264.7111 264.5734 280.8399 119.1765 0.1356 264.7708 264.6353 280.8817 119.6630 0.1320 264.8580 264.7260 280.9538 120.0285 0.1317 264.9265 264.7949 281.0031 120.3945 0.1310 264.9870 264.8560 281.0565 120.8230 0.1270 265.0705 264.9435 281.1140 121.2500 0.1247 265.1403 265.0156 281.1788 121.6155 0.1245 265.2196 265.0951 281.2281 121.9815 0.1195 265.2891 265.1696 281.2676 122.4680 0.1161 265.3648 265.2486 281.3325 122.8335 0.1163 265.4215 265.3052 281.3912 123.1995 0.1138 265.4903 265.3766 281.4388 123.6860 0.1094 265.5748 265.4654 281.4909 124.0515 0.1072 265.6392 265.5320 281.5287 124.4175 0.1044 265.6966 265.5922 281.5945 124.8435 0.1038 265.7600 265.6561 281.6455 125.2715 0.0978 265.8549 265.7571 281.6915 125.6370 0.0962 265.9328 265.8366 281.7473 126.0055 0.0943 265.9979 265.9036 281.7715 126.4890 0.0925 266.0709 265.9783 281.8254 126.8530 0.0899 266.1338 266.0439 281.8780 127.2170 0.0848 266.1946 266.1098 281.9353 127.6410 0.0830 266.2655 266.1825 281.9816 128.0650 0.0812 266.3494 266.2682 282.0297 128.4290 0.0803 266.4171 266.3368 282.0612 128.8530 0.0784 266.4892 266.4109 282.1072 129.2780 0.0753 266.5654 266.4901 282.1530 129.6420 0.0709 266.6321 266.5612 282.2024 130.0060 0.0706 266.6940 266.6234 282.2464 130.4905 0.0689 266.7767 266.7077 282.3078 130.8550 0.0661 266.8475 266.7814 282.3479 131.2190 0.0635 266.9066 266.8431 282.3824 131.7035 0.0600 266.9961 266.9361 282.4493 132.0685 0.0568 267.0550 266.9981 282.4857 132.4330 0.0545 267.1197 267.0652 282.5251 132.8570 0.0533 267.2028 267.1495 282.5622 133.2815 0.0514 267.2740 267.2226 282.6229 133.6460 0.0479 267.3350 267.2871 282.6770 134.0700 0.0457 267.4079 267.3622 282.7217 134.4950 0.0434 267.4785 267.4352 282.7812 134.8605 0.0400 267.5475 267.5075 282.8172 135.2290 0.0386 267.6070 267.5684 282.8763 135.7165 0.0359 267.7006 267.6647 282.9237 136.0815 0.0341 267.7544 267.7203 282.9713 136.4475 0.0332 267.8320 267.7989 283.0339 136.8775 0.0321 267.9014 267.8693 283.0949 137.3030 0.0291 267.9761 267.9470 283.1459 137.6680 0.0267 268.0365 268.0098 283.1950 138.0335 0.0235 268.0922 268.0687 283.2564 138.5200 0.0210 268.1865 268.1655 283.3080 138.8855 0.0185 268.2446 268.2261 283.3548 139.2515 0.0167 268.3030 268.2862 283.4134 139.6775 0.0132 268.3846 268.3714 283.4704 140.1040 0.0104 268.4580 268.4476 283.5240 140.4690 0.0087 268.5199 268.5112 283.5870 140.8945 0.0054 268.5880 268.5826 283.6455 141.3210 0.0030 268.6604 268.6573 283.6969 141.6865 0.0011 268.7243 268.7232 283.7452 142.0525 -0.0013 268.7830 268.7843 283.8084 142.5390 -0.0035 268.8587 268.8622 283.8756 142.9045 -0.0066 268.9262 268.9328 283.9358 143.2705 -0.0099 268.9932 269.0031 283.9818 143.7565 -0.0133 269.0867 269.1000 284.0376 144.1225 -0.0152 269.1501 269.1653 284.0931 144.4885 -0.0158 269.2043 269.2201 284.1275 144.9195 -0.0170 269.2750 269.2920 284.1860 145.3455 -0.0224 269.3576 269.3799 284.2498 145.7115 -0.0236 269.4267 269.4503 284.3107 146.0775 -0.0253 269.4982 269.5235 284.3742 146.5635 -0.0284 269.5825 269.6109 284.4398 146.9295 -0.0317 269.6296 269.6613 284.4845 147.2955 -0.0323 269.6887 269.7209 284.5389 147.7215 -0.0350 269.7739 269.8089 284.6099 148.1475 -0.0377 269.8508 269.8885 284.6689 148.5135 -0.0405 269.9008 269.9413 284.7178 148.9445 -0.0439 269.9625 270.0063 284.7724 149.3705 -0.0459 270.0436 270.0895 284.8291 149.7365 -0.0496 270.1190 270.1686 284.8833 150.1025 -0.0541 270.1821 270.2362 284.9380 150.5895 -0.0533 270.2620 270.3153 285.0064 150.9565 -0.0554 270.3174 270.3728 285.0479 151.3225 -0.0589 270.3839 270.4428 285.1118 151.7485 -0.0608 270.4580 270.5188 285.1770 152.1745 -0.0626 270.5227 270.5853 285.2458 152.5400 -0.0674 270.5894 270.6567 285.2852 152.9660 -0.0706 270.6656 270.7362 285.3467 153.3920 -0.0699 270.7528 270.8227 285.4003 153.7575 -0.0728 270.8145 270.8873 285.4607 154.1240 -0.0760 270.8610 270.9370 285.5108 154.6100 -0.0773 270.9458 271.0231 285.5953 154.9755 -0.0804 271.0100 271.0904 285.6506 155.3415 -0.0832 271.0668 271.1500 285.7017 155.8280 -0.0886 271.1362 271.2247 285.7487 156.1935 -0.0892 271.1940 271.2831 285.8055 156.5595 -0.0900 271.2688 271.3587 285.8621 156.9905 -0.0922 271.3566 271.4488 285.9190 157.4170 -0.0952 271.4293 271.5246 285.9804 157.7820 -0.0964 271.4897 271.5861 286.0385 158.1450 -0.0980 271.5417 271.6396 286.0920 158.6330 -0.1006 271.6384 271.7391 286.1519 158.9980 -0.1052 271.7065 271.8116 286.2101 159.3615 -0.1050 271.7540 271.8591 286.2550 159.7880 -0.1072 271.8178 271.9250 286.3176 160.2145 -0.1115 271.8950 272.0065 286.3784 160.5885 -0.1147 271.9548 272.0695 286.4228 160.9650 -0.1196 272.0259 272.1455 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