DTA measure 1pd_updown4_2het Test Date: 2024227:1241 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1273.85 s Mass = 1.000 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2503 2.4453 228.4234 225.9782 265.7963 2.0105 2.4316 228.7520 226.3203 265.7841 2.8628 2.4422 229.1129 226.6706 265.8376 3.6548 2.4338 229.4879 227.0541 265.8435 4.4465 2.4261 229.7175 227.2913 265.7928 5.2688 2.4176 229.9035 227.4860 265.8384 6.0305 2.4147 230.0909 227.6763 265.8380 6.8825 2.4016 230.3221 227.9205 265.8734 7.6445 2.3946 230.6445 228.2499 265.8797 8.4665 2.3804 230.9489 228.5685 265.8240 9.2888 2.3907 231.1498 228.7591 265.7786 10.0505 2.3926 231.5409 229.1483 265.7443 10.9028 2.3763 231.8305 229.4542 265.7280 11.6645 2.3633 232.1282 229.7649 265.7785 12.4865 2.3689 232.3689 230.0000 265.9255 13.3085 2.3721 232.8360 230.4639 266.0632 14.0705 2.3727 232.9907 230.6180 266.1695 14.9225 2.3686 233.2442 230.8757 266.2702 15.7145 2.3519 233.6341 231.2823 266.3991 16.5065 2.3358 233.8000 231.4642 266.4455 17.3285 2.3265 234.1304 231.8039 266.4974 18.0905 2.3173 234.3722 232.0549 266.5133 18.9425 2.3069 234.6072 232.3002 266.6643 19.7345 2.3137 234.7478 232.4341 266.8191 20.5265 2.3285 234.7707 232.4422 267.1024 21.3485 2.3189 234.9133 232.5944 267.2352 22.1098 2.3077 234.8876 232.5799 267.3473 22.9625 2.3026 234.9945 232.6919 267.4562 23.7550 2.2914 235.2401 232.9487 267.6603 24.5465 2.2738 235.3663 233.0925 267.7361 25.3688 2.2748 235.5740 233.2991 267.8940 26.1290 2.2676 235.7355 233.4679 268.0915 26.9795 2.2620 236.1642 233.9022 268.2836 27.7670 2.2488 236.3642 234.1154 268.3976 28.5550 2.2465 236.5090 234.2626 268.5693 29.3745 2.2342 236.9146 234.6805 268.6164 30.1625 2.2272 237.0540 234.8269 268.8067 30.9813 2.2119 237.3257 235.1138 268.8269 31.7708 2.2192 237.6945 235.4752 268.9283 32.5610 2.2042 237.9561 235.7519 269.0941 33.3813 2.2027 238.2021 235.9994 269.2328 34.1713 2.1985 238.4290 236.2306 269.3694 34.9930 2.1773 238.6194 236.4421 269.4651 35.7850 2.1752 238.7883 236.6131 269.6139 36.5768 2.1686 239.0079 236.8393 269.7936 37.3993 2.1638 239.1128 236.9490 269.9342 38.1910 2.1478 239.3321 237.1843 270.0207 39.0128 2.1426 239.5799 237.4373 270.1696 39.8048 2.1314 239.8185 237.6870 270.1563 40.5965 2.1010 239.9918 237.8908 270.1137 41.4190 2.1147 240.3307 238.2160 270.2984 42.2105 2.1001 240.4695 238.3693 270.4047 43.0328 2.0820 240.6831 238.6011 270.5737 43.8248 2.0653 240.8107 238.7455 270.5035 44.6165 2.0486 241.0100 238.9615 270.5738 45.4388 2.0548 241.3120 239.2572 270.8067 46.2005 2.0547 241.4951 239.4404 270.8426 47.0528 2.0244 241.8151 239.7907 271.0284 47.8448 2.0236 242.0850 240.0615 271.0831 48.6375 2.0172 242.3254 240.3082 271.1572 49.4598 2.0065 242.5416 240.5352 271.3179 50.2215 1.9968 242.7453 240.7485 271.3490 51.0738 1.9911 243.0077 241.0166 271.5137 51.8658 1.9733 243.3071 241.3338 271.7038 52.6585 1.9526 243.3768 241.4242 271.8037 53.4805 1.9380 243.6889 241.7509 271.9538 54.2425 1.9197 243.9714 242.0517 272.0627 55.0950 1.8990 244.1485 242.2496 272.2177 55.8575 1.8897 244.3917 242.5020 272.3226 56.6795 1.8788 244.6137 242.7350 272.3749 57.5018 1.8608 244.7944 242.9336 272.5459 58.2618 1.8652 244.9588 243.0937 272.7406 59.1100 1.8596 245.2892 243.4296 272.8870 59.8680 1.8523 245.6439 243.7916 272.9806 60.6858 1.8323 245.9496 244.1173 273.1810 61.5040 1.8108 246.3069 244.4961 273.3578 62.2620 1.8191 246.5441 244.7250 273.4580 63.1100 1.8070 246.5548 244.7479 273.7338 63.8690 1.8021 247.0005 245.1983 273.7884 64.6878 1.8028 247.1395 245.3368 273.9231 65.5070 1.8250 247.3807 245.5558 274.2743 66.2675 1.8056 247.5069 245.7014 274.0831 67.1185 1.7828 247.7881 246.0054 274.0683 67.8795 1.7847 247.9886 246.2039 274.1946 68.7015 1.7964 248.2892 246.4928 274.3435 69.5235 1.7805 248.3296 246.5492 274.4158 70.2855 1.7941 248.4500 246.6559 274.5736 71.1375 1.7788 248.6280 246.8492 274.5476 71.8995 1.7407 248.7236 246.9829 274.7541 72.7215 1.6937 248.8880 247.1943 274.8712 73.5143 1.6797 248.9640 247.2843 275.0316 74.3065 1.6671 249.2086 247.5415 275.0804 75.1585 1.6483 249.4200 247.7717 275.1953 75.9205 1.6546 249.6958 248.0412 275.1628 76.7425 1.6439 249.8415 248.1976 275.1647 77.5345 1.6342 249.8428 248.2086 275.3221 78.3263 1.6271 250.0828 248.4557 275.4188 79.1780 1.6216 250.1308 248.5092 275.4334 79.9400 1.6060 250.2982 248.6922 275.4120 80.7618 1.6023 250.5170 248.9147 275.3610 81.5540 1.6024 250.6540 249.0516 275.3548 82.3455 1.5859 250.7884 249.2024 275.3203 83.1978 1.5828 251.0182 249.4355 275.4369 83.9595 1.5682 251.2161 249.6479 275.3628 84.7818 1.5678 251.5105 249.9427 275.2980 85.6038 1.5663 251.5847 250.0185 275.1304 86.3655 1.5689 251.7960 250.2271 275.2563 87.2183 1.5508 251.7036 250.1528 275.3940 87.9805 1.5499 251.6803 250.1304 275.5649 88.8028 1.5389 251.6986 250.1597 275.6983 89.6248 1.5279 251.9077 250.3797 275.9835 90.3840 1.4937 252.0180 250.5243 276.2103 91.2320 1.5147 252.0695 250.5548 276.1828 91.9900 1.5119 252.2922 250.7803 276.4498 92.8080 1.4896 252.5953 251.1058 276.4873 93.6260 1.4847 252.7803 251.2957 276.5773 94.3840 1.4624 252.7714 251.3090 276.6942 95.2338 1.4419 252.8609 251.4189 276.8387 96.0223 1.4363 253.0485 251.6123 276.8892 96.8118 1.4235 253.2869 251.8634 277.1390 97.6320 1.4186 253.4680 252.0495 277.1035 98.3930 1.4114 253.7116 252.3002 277.2712 99.2448 1.4051 254.0252 252.6201 277.6083 100.0368 1.3914 254.3561 252.9647 277.7951 100.8285 1.3681 254.6370 253.2690 278.2047 101.6508 1.3614 254.9917 253.6303 278.3225 102.4125 1.3426 255.1828 253.8401 278.3993 103.2648 1.3425 255.2782 253.9357 278.5783 104.0568 1.3294 255.5469 254.2175 278.8826 104.8485 1.3166 255.7234 254.4067 278.9557 105.6708 1.3064 255.9813 254.6749 279.0356 106.4325 1.3059 256.1946 254.8887 279.2403 107.2848 1.2828 256.4163 255.1336 279.3405 108.0765 1.2659 256.4573 255.1914 279.3864 108.8685 1.2501 256.5111 255.2610 279.6155 109.6938 1.2496 256.6665 255.4170 279.7858 110.4565 1.2378 256.8676 255.6298 279.9096 111.3085 1.2316 257.1160 255.8843 279.8712 112.1005 1.2193 257.2960 256.0767 279.7655 112.8925 1.1983 257.4904 256.2921 279.9673 113.7145 1.1820 257.6666 256.4845 280.2379 114.4765 1.1780 257.7888 256.6108 280.4518 115.3285 1.1665 258.0353 256.8688 280.4541 116.1205 1.1468 258.1209 256.9741 280.6040 116.9135 1.1275 258.2178 257.0903 280.7050 117.7355 1.1169 258.4409 257.3239 280.6762 118.5273 1.1047 258.8071 257.7023 280.7536 119.3498 1.0958 259.0166 257.9208 280.6790 120.1425 1.0924 259.1311 258.0387 280.8213 120.9335 1.0822 259.2834 258.2012 280.8278 121.7558 1.0712 259.6453 258.5741 280.9406 122.5475 1.0580 259.7592 258.7012 280.9683 123.3673 1.0456 259.9264 258.8808 280.9638 124.1550 1.0406 260.1211 259.0805 281.0316 124.9430 1.0305 260.2741 259.2435 281.4293 125.7613 1.0249 260.4654 259.4405 281.5047 126.5493 1.0180 260.6608 259.6427 281.4956 127.3683 0.9894 260.8587 259.8693 281.5383 128.1568 0.9805 261.0390 260.0585 281.8486 128.9455 0.9679 261.2408 260.2729 281.9264 129.7645 0.9550 261.4144 260.4593 281.9224 130.5558 0.9516 261.5586 260.6070 281.9459 131.3765 0.9469 261.7269 260.7800 282.1414 132.1678 0.9484 261.9400 260.9916 282.2117 132.9585 0.9303 262.0017 261.0714 282.3932 133.7810 0.9162 262.1517 261.2355 282.3459 134.5728 0.9165 262.2031 261.2865 282.5332 135.3950 0.9050 262.4178 261.5127 282.6611 136.1873 0.8863 262.7065 261.8202 282.7978 136.9785 0.8674 262.7746 261.9072 282.9741 137.8010 0.8496 262.9262 262.0766 283.1308 138.5928 0.8332 263.1561 262.3229 283.2227 139.4148 0.8216 263.4171 262.5956 283.3436 140.2098 0.8207 263.4650 262.6443 283.3208 141.0055 0.8095 263.5320 262.7225 283.5477 141.8278 0.7971 263.8029 263.0058 283.5578 142.5895 0.7962 264.0695 263.2733 283.6808 143.4423 0.7762 264.1461 263.3699 283.9782 144.2045 0.7653 264.2822 263.5168 283.9756 145.0268 0.7660 264.3743 263.6083 284.0537 145.8488 0.7712 264.5704 263.7992 284.1774 146.6105 0.7396 264.8374 264.0979 284.3206 147.4628 0.7309 265.0957 264.3648 284.5016 148.2548 0.7301 265.1422 264.4121 284.6888 149.0465 0.7328 265.3985 264.6657 284.7825 149.8690 0.7195 265.5837 264.8643 284.7950 150.6315 0.7093 265.7431 265.0338 284.9499 151.4840 0.6962 265.8910 265.1948 284.7743 152.2465 0.6830 265.9814 265.2984 284.6940 153.0685 0.6799 266.1319 265.4520 285.0549 153.8908 0.6542 266.3555 265.7014 285.2536 154.6535 0.6505 266.5085 265.8580 285.3052 155.5023 0.6420 266.6005 265.9585 285.3334 156.2598 0.6233 266.7900 266.1666 285.4801 157.0780 0.6200 266.9381 266.3181 285.6257 157.8660 0.5968 267.1293 266.5325 285.7874 158.6540 0.5928 267.2959 266.7030 285.8968 159.5020 0.5940 267.3741 266.7801 285.8098 160.2600 0.5805 267.6476 267.0671 285.9221 161.0788 0.5719 267.8064 267.2345 285.8147 161.8670 0.5588 267.8278 267.2690 285.8846 162.6560 0.5582 268.0377 267.4795 285.9285 163.5048 0.5550 268.1694 267.6144 285.9811 164.2658 0.5657 268.3434 267.7777 285.9895 165.0875 0.5428 268.4151 267.8723 286.1133 165.8795 0.5479 268.6376 268.0897 286.2478 166.6715 0.5476 268.7884 268.2408 286.2139 167.5235 0.5335 268.9557 268.4221 286.3834 168.2855 0.5251 269.1592 268.6341 286.3912 169.1075 0.5196 269.3725 268.8530 286.7099 169.8995 0.5096 269.4689 268.9593 286.8667 170.6915 0.5074 269.6018 269.0943 287.0942 171.5135 0.5031 269.7781 269.2750 287.2808 172.3055 0.5022 269.9683 269.4660 287.4069 173.1275 0.4904 270.0178 269.5274 287.5526 173.9195 0.4848 270.1721 269.6873 287.6777 174.7110 0.4865 270.3334 269.8469 287.8560 175.5333 0.4822 270.4895 270.0074 288.0878 176.3250 0.4632 270.6886 270.2254 288.2341 177.1475 0.4464 270.8014 270.3549 288.4063 177.9395 0.4313 270.9686 270.5373 288.5327 178.7305 0.4191 271.1104 270.6913 288.8179 179.5530 0.4157 271.3085 270.8928 289.0253 180.3445 0.3950 271.4846 271.0896 289.2806 181.1668 0.3801 271.5197 271.1396 289.4226 181.9588 0.3675 271.8510 271.4836 289.6888 182.7505 0.3523 272.1098 271.7576 289.8158 183.5728 0.3512 272.1989 271.8477 289.8304 184.3345 0.3523 272.3267 271.9744 289.9000 185.1868 0.3307 272.5568 272.2261 289.8635 185.9788 0.3157 272.7175 272.4019 289.9921 186.7703 0.3043 272.9819 272.6775 290.0464 187.5893 0.3135 273.2384 272.9249 289.9936 188.3470 0.3114 273.5329 273.2215 290.2304 189.1950 0.3003 273.7329 273.4326 290.3567 189.9830 0.2925 273.7817 273.4892 290.4625 190.7710 0.2806 273.9367 273.6561 290.4910 191.5895 0.2623 274.1424 273.8801 290.6385 192.3780 0.2638 274.3886 274.1248 290.8802 193.1975 0.2611 274.4557 274.1946 291.0374 193.9865 0.2509 274.5586 274.3077 291.1757 194.7760 0.2277 274.7741 274.5464 291.2666 195.5960 0.2311 275.0351 274.8040 291.1269 196.3865 0.2298 275.1050 274.8752 291.1177 197.2088 0.2283 275.3564 275.1282 291.2554 198.0008 0.2315 275.4488 275.2173 291.1812 198.7925 0.2261 275.6221 275.3961 291.3697 199.6148 0.2119 275.6811 275.4693 291.4875 200.3765 0.2055 275.8160 275.6105 291.5701 201.2288 0.1890 275.8509 275.6619 291.6692 202.0208 0.1730 275.9354 275.7624 291.6917 202.8125 0.1617 276.0540 275.8922 291.6920 203.6348 0.1605 276.1608 276.0003 291.7861 204.3965 0.1746 276.2976 276.1230 291.7822 205.2488 0.1444 276.4676 276.3232 292.0070 206.0408 0.1402 276.5677 276.4275 292.0704 206.8325 0.1397 276.6730 276.5333 292.1389 207.6545 0.1458 276.7871 276.6413 292.1862 208.4165 0.1168 276.8994 276.7826 292.3501 209.2685 0.1065 276.9046 276.7981 292.5371 210.0605 0.0995 276.9393 276.8398 292.6757 210.8525 0.0925 277.0709 276.9784 292.7399 211.6745 0.0799 277.3389 277.2590 292.8796 212.4365 0.0720 277.4794 277.4074 292.9384 213.2885 0.0811 277.6156 277.5345 293.0642 214.0805 0.0721 277.8712 277.7991 293.0687 214.8723 0.0715 277.8770 277.8054 293.2519 215.6945 0.0640 277.9998 277.9358 293.4796 216.4565 0.0635 278.1861 278.1225 293.5951 217.3080 0.0614 278.3018 278.2404 293.7725 218.0998 0.0379 278.3793 278.3414 293.8414 218.8920 0.0212 278.4082 278.3870 293.9875 219.7105 0.0324 278.7434 278.7110 294.0430 220.4683 0.0186 278.9950 278.9764 294.0473 221.3170 0.0115 279.0415 279.0299 294.3736 222.1055 0.0174 279.1974 279.1800 294.4849 222.8935 0.0024 279.2754 279.2730 294.5399 223.7118 0.0026 279.4633 279.4607 294.6170 224.4998 -0.0100 279.5709 279.5809 294.7558 225.3178 -0.0167 279.7674 279.7841 294.8880 226.1068 -0.0106 280.0771 280.0877 295.0238 226.8978 -0.0343 280.1495 280.1837 295.0985 227.7195 -0.0600 280.1441 280.2042 295.2331 228.5108 -0.0578 280.3181 280.3759 295.2420 229.3325 -0.0542 280.4346 280.4887 295.3034 230.1235 -0.0457 280.5215 280.5672 295.4649 230.9153 -0.0611 280.7421 280.8031 295.5565 231.7375 -0.0615 280.8601 280.9217 295.5959 232.5293 -0.0729 280.9482 281.0211 295.7455 233.3518 -0.0817 281.1630 281.2447 295.8271 234.1445 -0.0948 281.2167 281.3114 295.8869 234.9355 -0.0959 281.5866 281.6825 295.8817 235.7580 -0.0975 281.5882 281.6857 296.0550 236.5495 -0.1144 281.6128 281.7272 296.1126 237.3718 -0.1257 281.8751 282.0008 296.2244 238.1638 -0.1211 281.8719 281.9930 296.3366 238.9555 -0.1299 282.0257 282.1556 296.5155 239.8078 -0.1426 282.3804 282.5230 296.6448 240.5695 -0.1472 282.4432 282.5904 296.7356 241.3918 -0.1586 282.3918 282.5504 296.7879 242.1838 -0.1535 282.6815 282.8350 296.9339 242.9755 -0.1520 283.1052 283.2572 297.0669 243.8278 -0.1695 282.9771 283.1467 297.2450 244.5895 -0.1646 283.0560 283.2206 297.3471 245.4125 -0.1666 283.2311 283.3977 297.4042 246.2048 -0.1836 283.2904 283.4741 297.4867 246.9965 -0.1933 283.5795 283.7728 297.5127 247.8488 -0.1917 283.7347 283.9263 297.7350 248.6105 -0.2089 283.7701 283.9790 297.8425 249.4325 -0.2127 284.0754 284.2881 297.9070 250.2548 -0.2165 284.0990 284.3155 298.0045 251.0175 -0.2078 284.2781 284.4858 298.1521 251.8688 -0.2169 284.4135 284.6304 298.1918 252.6268 -0.2324 284.3649 284.5973 298.4280 253.4450 -0.2296 284.4212 284.6508 298.4534 254.2628 -0.2438 284.7517 284.9955 298.5169 255.0210 -0.2311 284.7178 284.9489 298.6311 255.8695 -0.2474 284.9663 285.2137 298.7231 256.6280 -0.2420 285.0613 285.3032 298.8069 257.4468 -0.2570 285.3356 285.5926 298.8787 258.2653 -0.2670 285.5574 285.8244 299.1165 259.0250 -0.2933 285.5516 285.8450 299.1925 259.8753 -0.3018 285.5964 285.8982 299.2710 260.6353 -0.2995 285.7776 286.0771 299.3298 261.4565 -0.2925 285.9884 286.2808 299.4133 262.2785 -0.2882 286.2351 286.5233 299.5353 263.0405 -0.3044 286.2501 286.5545 299.6662 263.8925 -0.3131 286.0672 286.3803 299.8612 264.6545 -0.2984 286.1276 286.4260 300.0209 265.4765 -0.3126 286.1355 286.4480 300.0313 266.2985 -0.3208 286.2799 286.6006 300.1396 267.0605 -0.3180 286.2469 286.5649 300.3132 267.9125 -0.3397 286.3394 286.6791 300.4218 268.6745 -0.3345 286.3761 286.7107 300.6298 269.4965 -0.3399 286.4354 286.7752 300.7748 270.3185 -0.3529 286.4389 286.7918 300.8654 271.0805 -0.3608 286.6292 286.9900 301.0063 271.9325 -0.3705 286.8817 287.2522 301.1116 272.6945 -0.3744 286.9640 287.3385 301.2090 273.5175 -0.3884 287.1463 287.5347 301.3470 274.3395 -0.3805 287.1644 287.5449 301.4301 275.1013 -0.3925 287.4941 287.8866 301.4932 275.9530 -0.4011 287.6441 288.0452 301.5174 276.7148 -0.3873 287.9391 288.3263 301.6722 277.5368 -0.4061 287.9971 288.4032 301.6626 278.3598 -0.4023 288.0972 288.4995 301.7195 279.1225 -0.4120 288.3486 288.7607 301.7344 279.9748 -0.4401 288.3365 288.7766 301.8940 280.7365 -0.4391 288.4227 288.8618 301.9320 281.5595 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304.4843 300.0388 -0.5666 292.1198 292.6864 304.6311 300.8005 -0.5615 292.3010 292.8625 304.7613 301.6228 -0.5666 292.4907 293.0573 304.9085 302.4148 -0.5709 292.5758 293.1467 304.9855 303.2065 -0.5933 292.7619 293.3551 305.0951 304.0288 -0.5962 292.9650 293.5613 305.1362 304.8205 -0.5943 292.9923 293.5866 305.2413 305.6425 -0.6169 293.1802 293.7971 305.3043 306.4345 -0.6110 293.2865 293.8975 305.4723 307.2265 -0.6139 293.2917 293.9056 305.6398 308.0485 -0.6279 293.5209 294.1488 305.7131 308.8405 -0.6258 293.6930 294.3188 305.7470 309.6625 -0.6189 293.7654 294.3843 305.8115 310.4545 -0.6244 293.8978 294.5222 305.9229 311.2465 -0.6221 293.9555 294.5777 306.0312 312.0685 -0.6181 294.1185 294.7367 306.2088 312.8605 -0.6243 294.3190 294.9433 306.2391 313.6823 -0.6337 294.4286 295.0623 306.4233 314.4745 -0.6276 294.5465 295.1741 306.4058 315.2655 -0.6256 294.6765 295.3021 306.5329 316.0870 -0.6476 294.9364 295.5839 306.6555 316.8753 -0.6537 294.9833 295.6370 306.8232 317.6938 -0.6469 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