DTA measure 3pd_updown3 Test Date: 2024220:1150 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.94 s Mass = 1383.2 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3935 -4.8841 430.2932 435.1773 423.9072 3.9925 -4.8910 430.4510 435.3420 423.9142 5.6065 -4.9002 430.6049 435.5051 423.9167 7.2205 -4.9061 430.7491 435.6553 423.8937 8.8195 -4.9154 430.8909 435.8063 423.8311 10.4335 -4.9233 431.0381 435.9614 423.7403 12.0323 -4.9312 431.1800 436.1111 423.6341 13.6309 -4.9397 431.3035 436.2432 423.4836 15.2596 -4.9459 431.4421 436.3879 423.3055 16.8588 -4.9519 431.5729 436.5248 423.1326 18.4726 -4.9585 431.7104 436.6688 422.9127 20.0720 -4.9659 431.8306 436.7966 422.6930 21.6855 -4.9707 431.9738 436.9445 422.4689 23.2920 -4.9684 432.0894 437.0578 422.2360 24.8983 -4.9648 432.2057 437.1705 421.9955 26.4909 -4.9709 432.3195 437.2904 421.7696 28.0840 -4.9742 432.4315 437.4057 421.5314 29.6931 -4.9790 432.5593 437.5383 421.2971 31.3038 -4.9817 432.6523 437.6340 421.0624 32.9178 -4.9858 432.7535 437.7393 420.8366 34.5166 -4.9899 432.8411 437.8310 420.6145 36.1156 -4.9899 432.9534 437.9432 420.3947 37.7296 -4.9930 433.0620 438.0550 420.1845 39.3436 -4.9941 433.1485 438.1426 419.9557 40.9429 -5.0002 433.2257 438.2259 419.7559 42.5575 -5.0017 433.3097 438.3114 419.5434 44.1565 -5.0043 433.3919 438.3962 419.3419 45.7705 -5.0096 433.4604 438.4700 419.1348 47.3845 -5.0139 433.5332 438.5471 418.9364 48.9994 -5.0158 433.6131 438.6289 418.7484 50.5988 -5.0205 433.6752 438.6957 418.5574 52.1984 -5.0242 433.7341 438.7583 418.3764 53.8110 -5.0276 433.7953 438.8230 418.1840 55.4173 -5.0319 433.8491 438.8810 418.0090 57.0245 -5.0349 433.9023 438.9372 417.8326 58.6166 -5.0421 433.9530 438.9951 417.6593 60.2091 -5.0461 434.0086 439.0547 417.4902 61.8189 -5.0499 434.0531 439.1031 417.3162 63.4315 -5.0581 434.1004 439.1585 417.1371 65.0455 -5.0631 434.1209 439.1839 416.9565 66.6450 -5.0689 434.1582 439.2271 416.7704 68.2441 -5.0733 434.1889 439.2622 416.5920 69.8430 -5.0770 434.2140 439.2910 416.3960 71.4719 -5.0827 434.2372 439.3198 416.2131 73.0709 -5.0874 434.2644 439.3517 416.0277 74.6861 -5.0922 434.2808 439.3730 415.8431 76.2826 -5.0984 434.3001 439.3985 415.6656 77.8971 -5.1038 434.3245 439.4282 415.4669 79.5125 -5.1100 434.3326 439.4425 415.2745 81.1268 -5.1129 434.3430 439.4559 415.0706 82.7265 -5.1160 434.3496 439.4657 414.8620 84.3405 -5.1207 434.3531 439.4738 414.6539 85.9370 -5.1242 434.3463 439.4705 414.4487 87.5430 -5.1316 434.3475 439.4791 414.2334 89.1500 -5.1367 434.3500 439.4867 414.0235 90.7424 -5.1410 434.3384 439.4793 413.8212 92.3504 -5.1474 434.3203 439.4676 413.6103 93.9445 -5.1519 434.3062 439.4581 413.4234 95.5715 -5.1557 434.3006 439.4564 413.2192 97.1705 -5.1598 434.2797 439.4395 413.0112 98.7695 -5.1652 434.2609 439.4261 412.8194 100.3835 -5.1701 434.2443 439.4144 412.6304 101.9825 -5.1742 434.1981 439.3722 412.4297 103.5965 -5.1798 434.1835 439.3633 412.2499 105.2105 -5.1837 434.1427 439.3264 412.0588 106.8095 -5.1887 434.1180 439.3067 411.8506 108.4234 -5.1935 434.0784 439.2718 411.6570 110.0229 -5.1977 434.0445 439.2421 411.4699 111.6370 -5.2039 433.9997 439.2036 411.2521 113.2518 -5.2066 433.9564 439.1630 411.0408 114.8508 -5.2153 433.9091 439.1245 410.8230 116.4660 -5.2155 433.8692 439.0847 410.6194 118.0655 -5.2205 433.8161 439.0366 410.4165 119.6741 -5.2227 433.7564 438.9791 410.2235 121.2804 -5.2261 433.7034 438.9294 410.0171 122.8720 -5.2300 433.6507 438.8807 409.8015 124.4790 -5.2339 433.5939 438.8278 409.5962 126.0728 -5.2385 433.5297 438.7683 409.3990 127.6838 -5.2427 433.4801 438.7228 409.2235 129.2979 -5.2459 433.4122 438.6581 409.0265 130.8966 -5.2508 433.3619 438.6127 408.8442 132.4956 -5.2546 433.2827 438.5374 408.6562 134.1096 -5.2591 433.2136 438.4727 408.4662 135.7086 -5.2615 433.1459 438.4074 408.2597 137.3236 -5.2644 433.0719 438.3363 408.0588 138.9378 -5.2684 433.0056 438.2740 407.8579 140.5366 -5.2706 432.9207 438.1913 407.6635 142.1355 -5.2715 432.8434 438.1150 407.4615 143.7495 -5.2763 432.7574 438.0337 407.2491 145.3635 -5.2771 432.6713 437.9484 407.0207 146.9775 -5.2806 432.5879 437.8685 406.8097 148.5765 -5.2840 432.4809 437.7648 406.6078 150.1749 -5.2876 432.4206 437.7081 406.4110 151.7671 -5.2893 432.3183 437.6077 406.1917 153.3889 -5.2907 432.2358 437.5265 405.9742 154.9808 -5.2951 432.1388 437.4339 405.7659 156.5883 -5.2987 432.0480 437.3467 405.5597 158.1811 -5.2998 431.9397 437.2395 405.3676 159.7923 -5.3028 431.8534 437.1562 405.1444 161.4055 -5.3041 431.7525 437.0567 404.9539 163.0045 -5.3042 431.6398 436.9440 404.7634 164.6035 -5.3087 431.5436 436.8523 404.5677 166.2173 -5.3107 431.4443 436.7551 404.3652 167.8161 -5.3128 431.3342 436.6470 404.1719 169.4299 -5.3126 431.2433 436.5560 403.9813 171.0439 -5.3168 431.1270 436.4438 403.7937 172.6426 -5.3187 431.0080 436.3267 403.5935 174.2566 -5.3203 430.9006 436.2209 403.4057 175.8556 -5.3231 430.7900 436.1131 403.1692 177.4696 -5.3261 430.6732 435.9992 402.9660 179.0846 -5.3254 430.5529 435.8782 402.7527 180.6835 -5.3276 430.4351 435.7628 402.5476 182.2968 -5.3279 430.3120 435.6399 402.3490 183.8898 -5.3279 430.2042 435.5321 402.1330 185.5110 -5.3269 430.0698 435.3967 401.9171 187.1020 -5.3297 429.9612 435.2909 401.7051 188.7086 -5.3300 429.8300 435.1600 401.4886 190.3020 -5.3307 429.7151 435.0458 401.2821 191.9135 -5.3335 429.5951 434.9286 401.0728 193.5266 -5.3334 429.4678 434.8012 400.8522 195.1405 -5.3326 429.3268 434.6595 400.6389 196.7395 -5.3320 429.2058 434.5378 400.4413 198.3385 -5.3331 429.0792 434.4122 400.2557 199.9525 -5.3333 428.9417 434.2750 400.0481 201.5665 -5.3327 428.7995 434.1322 399.8369 203.1805 -5.3337 428.6717 434.0054 399.6390 204.7795 -5.3335 428.5452 433.8787 399.4423 206.3785 -5.3328 428.4044 433.7372 399.2413 207.9925 -5.3332 428.2713 433.6046 399.0473 209.6211 -5.3340 428.1358 433.4698 398.8638 211.2196 -5.3353 427.9927 433.3280 398.6745 212.8186 -5.3339 427.8495 433.1834 398.4837 214.4319 -5.3334 427.7122 433.0455 398.2811 216.0390 -5.3339 427.5713 432.9052 398.0859 217.6463 -5.3359 427.4287 432.7646 397.8939 219.2400 -5.3332 427.2800 432.6132 397.6674 220.8496 -5.3309 427.1323 432.4632 397.4693 222.4439 -5.3319 426.9940 432.3259 397.2514 224.0559 -5.3313 426.8386 432.1700 397.0418 225.6698 -5.3315 426.7024 432.0339 396.8109 227.2688 -5.3315 426.5568 431.8883 396.6037 228.8836 -5.3290 426.4080 431.7370 396.3962 230.4836 -5.3288 426.2727 431.6016 396.1709 232.0826 -5.3289 426.1026 431.4314 395.9730 233.7118 -5.3257 425.9566 431.2823 395.7571 235.3106 -5.3257 425.8103 431.1361 395.5428 236.9096 -5.3242 425.6555 430.9796 395.3547 238.5236 -5.3238 425.4865 430.8104 395.1489 240.1386 -5.3225 425.3322 430.6547 394.9406 241.7534 -5.3208 425.1863 430.5072 394.7281 243.3525 -5.3194 425.0299 430.3492 394.5310 244.9669 -5.3176 424.8770 430.1946 394.3328 246.5665 -5.3164 424.7209 430.0374 394.1231 248.1923 -5.3138 424.5545 429.8683 393.9279 249.7839 -5.3101 424.3975 429.7077 393.7343 251.3753 -5.3082 424.2375 429.5457 393.5345 252.9824 -5.3068 424.0777 429.3846 393.3336 254.5745 -5.3051 423.9343 429.2394 393.1452 256.1983 -5.3063 423.7501 429.0564 392.9442 257.7939 -5.3050 423.5986 428.9036 392.7453 259.3951 -5.2996 423.4340 428.7336 392.5534 260.9995 -5.2986 423.2672 428.5659 392.3529 262.5985 -5.2963 423.0975 428.3938 392.1497 264.2125 -5.2939 422.9430 428.2369 391.9206 265.8274 -5.2917 422.7693 428.0610 391.7221 267.4260 -5.2902 422.6105 427.9006 391.4983 269.0399 -5.2850 422.4462 427.7312 391.2823 270.6386 -5.2823 422.2862 427.5686 391.0744 272.2376 -5.2824 422.1185 427.4008 390.8503 273.8674 -5.2811 421.9324 427.2135 390.6167 275.4668 -5.2772 421.7730 427.0503 390.4088 277.0806 -5.2752 421.6140 426.8892 390.1888 278.6800 -5.2724 421.4315 426.7039 389.9727 280.2760 -5.2693 421.2665 426.5358 389.7657 281.8820 -5.2651 421.0915 426.3567 389.5438 283.4889 -5.2610 420.9099 426.1709 389.3267 285.0960 -5.2582 420.7450 426.0032 389.1195 286.6880 -5.2574 420.5746 425.8320 388.9081 288.2968 -5.2542 420.4037 425.6580 388.6964 289.9110 -5.2500 420.2304 425.4804 388.4933 291.5135 -5.2446 420.0698 425.3144 388.2775 293.1126 -5.2418 419.8866 425.1284 388.0636 294.7116 -5.2388 419.7146 424.9534 387.8731 296.3255 -5.2360 419.5286 424.7646 387.6570 297.9245 -5.2317 419.3465 424.5781 387.4600 299.5535 -5.2270 419.1813 424.4082 387.2581 301.1450 -5.2236 419.0073 424.2309 387.0510 302.7595 -5.2224 418.8266 424.0490 386.8415 304.3589 -5.2201 418.6468 423.8669 386.6515 305.9585 -5.2149 418.4699 423.6848 386.4444 307.5876 -5.2106 418.2919 423.5025 386.2407 309.1868 -5.2085 418.1098 423.3182 386.0518 310.8008 -5.2043 417.9367 423.1411 385.8626 312.3960 -5.2001 417.7561 422.9562 385.6644 313.9884 -5.1947 417.5809 422.7757 385.4747 315.5953 -5.1926 417.3891 422.5817 385.2723 317.2014 -5.1917 417.2215 422.4132 385.0718 318.8098 -5.1852 417.0214 422.2067 384.8930 320.4038 -5.1821 416.8423 422.0244 384.7058 322.0029 -5.1793 416.6601 421.8394 384.5014 323.6319 -5.1749 416.4760 421.6509 384.2989 325.2310 -5.1703 416.2999 421.4702 384.0884 326.8446 -5.1666 416.1227 421.2892 383.8896 328.4436 -5.1626 415.9438 421.1064 383.6799 330.0426 -5.1596 415.7593 420.9189 383.4583 331.6716 -5.1559 415.5645 420.7204 383.2341 333.2708 -5.1516 415.3842 420.5358 383.0393 334.8855 -5.1492 415.1983 420.3475 382.8128 336.4850 -5.1431 415.0131 420.1562 382.6031 338.0845 -5.1380 414.8427 419.9807 382.4007 339.7144 -5.1352 414.6484 419.7836 382.1878 341.3144 -5.1310 414.4667 419.5977 381.9654 342.9284 -5.1289 414.2612 419.3901 381.7661 344.5218 -5.1241 414.0845 419.2086 381.5488 346.1136 -5.1173 413.9041 419.0214 381.3560 347.7358 -5.1147 413.7222 418.8369 381.1440 349.3438 -5.1125 413.5321 418.6446 380.9419 350.9366 -5.1069 413.3399 418.4468 380.7374 352.5478 -5.1006 413.1500 418.2506 380.5372 354.1465 -5.0974 412.9606 418.0580 380.3426 355.7605 -5.0943 412.7834 417.8777 380.1290 357.3745 -5.0908 412.5871 417.6779 379.9352 358.9735 -5.0852 412.3964 417.4816 379.7252 360.5725 -5.0788 412.1990 417.2778 379.5302 362.1884 -5.0754 412.0325 417.1079 379.3289 363.8031 -5.0703 411.8347 416.9051 379.1310 365.4174 -5.0679 411.6468 416.7147 378.9446 367.0158 -5.0622 411.4623 416.5246 378.7433 368.6146 -5.0575 411.2673 416.3247 378.5239 370.2286 -5.0541 411.0724 416.1265 378.3109 371.8586 -5.0479 410.8774 415.9253 378.0822 373.4578 -5.0462 410.6932 415.7394 377.8688 375.0576 -5.0414 410.4996 415.5411 377.6499 376.6703 -5.0376 410.3094 415.3470 377.4297 378.2624 -5.0354 410.1293 415.1647 377.2046 379.8690 -5.0301 409.9302 414.9603 376.9872 381.4750 -5.0257 409.7365 414.7622 376.7640 383.0668 -5.0176 409.5434 414.5610 376.5405 384.6748 -5.0122 409.3448 414.3570 376.3095 386.2694 -5.0092 409.1712 414.1804 376.0996 387.8966 -5.0053 408.9627 413.9680 375.8729 389.4956 -4.9995 408.7681 413.7676 375.6478 391.0946 -4.9962 408.5736 413.5698 375.4363 392.7131 -4.9940 408.3813 413.3752 375.2082 394.3006 -4.9869 408.1967 413.1836 374.9899 395.9296 -4.9814 407.9931 412.9745 374.7697 397.5435 -4.9761 407.8066 412.7828 374.5572 399.1425 -4.9702 407.6018 412.5720 374.3435 400.7415 -4.9662 407.4276 412.3938 374.1349 402.3555 -4.9601 407.2152 412.1753 373.9246 403.9701 -4.9579 407.0178 411.9757 373.7146 405.5840 -4.9532 406.8256 411.7789 373.4966 407.1828 -4.9495 406.6252 411.5747 373.2914 408.7803 -4.9455 406.4246 411.3701 373.0937 410.3729 -4.9395 406.2304 411.1700 372.8863 411.9951 -4.9348 406.0443 410.9791 372.6723 413.5876 -4.9295 405.8376 410.7671 372.4710 415.1948 -4.9246 405.6498 410.5744 372.2721 416.7879 -4.9197 405.4595 410.3792 372.0662 418.4006 -4.9167 405.2561 410.1729 371.8590 420.0141 -4.9112 405.0605 409.9718 371.6554 421.6129 -4.9080 404.8588 409.7668 371.4517 423.2266 -4.9020 404.6641 409.5661 371.2487 424.8258 -4.8976 404.4431 409.3408 371.0499 426.4246 -4.8907 404.2541 409.1448 370.8485 428.0536 -4.8890 404.0631 408.9521 370.6309 429.6540 -4.8833 403.8706 408.7539 370.4336 431.2536 -4.8795 403.6876 408.5672 370.2500 432.8680 -4.8717 403.4604 408.3321 370.0588 434.4675 -4.8672 403.2715 408.1387 369.8531 436.0823 -4.8643 403.0677 407.9320 369.6624 437.6975 -4.8594 402.8775 407.7369 369.4721 439.2965 -4.8566 402.6706 407.5272 369.2689 440.9085 -4.8511 402.4615 407.3126 369.0702 442.5000 -4.8477 402.2729 407.1206 368.8814 444.1060 -4.8415 402.0742 406.9157 368.6800 445.7120 -4.8359 401.8819 406.7178 368.4906 447.3053 -4.8321 401.6737 406.5058 368.3060 448.9160 -4.8298 401.4743 406.3041 368.1016 450.5136 -4.8247 401.2849 406.1096 367.8806 452.1126 -4.8183 401.0898 405.9081 367.6872 453.7415 -4.8138 400.8942 405.7080 367.4622 455.3405 -4.8082 400.6963 405.5045 367.2532 456.9395 -4.8028 400.5116 405.3145 367.0325 458.5385 -4.7931 400.2992 405.0923 366.8326 460.1525 -4.7819 400.0942 404.8761 366.6183 461.7664 -4.7897 399.8950 404.6847 366.3967 463.3800 -4.7906 399.6864 404.4769 366.1784 464.9799 -4.7860 399.4949 404.2809 365.9736 466.5796 -4.7841 399.2863 404.0704 365.7706 468.2388 -4.7755 399.0813 403.8568 365.5314 469.8526 -4.7705 398.8787 403.6492 365.3213 471.4666 -4.7652 398.6893 403.4545 365.1082 473.0779 -4.7577 398.4858 403.2435 364.9066 474.6841 -4.7527 398.2862 403.0389 364.6933 476.2754 -4.7477 398.0941 402.8418 364.4953 477.8825 -4.7447 397.8930 402.6377 364.2820 479.4749 -4.7373 397.6912 402.4285 364.0766 481.0998 -4.7332 397.4961 402.2293 363.8564 482.6980 -4.7276 397.2878 402.0155 363.6581 484.2989 -4.7222 397.0864 401.8085 363.4463 485.9056 -4.7154 396.8784 401.5938 363.2439 487.5046 -4.7117 396.6874 401.3991 363.0476 489.1186 -4.7017 396.4810 401.1827 362.8447 490.7326 -4.6909 396.2759 400.9668 362.6344 492.3466 -4.6895 396.0815 400.7710 362.4357 493.9455 -4.6876 395.8842 400.5718 362.2356 495.5450 -4.6817 395.6730 400.3546 362.0312 497.1595 -4.6769 395.4772 400.1541 361.8299 498.7735 -4.6710 395.2775 399.9485 361.6290 500.3876 -4.6658 395.0738 399.7396 361.4336 501.9874 -4.6623 394.8686 399.5309 361.2253 503.5861 -4.6572 394.6647 399.3219 361.0365 505.1998 -4.6511 394.4537 399.1048 360.8321 506.8081 -4.6458 394.2538 398.8996 360.6220 508.4148 -4.6409 394.0550 398.6959 360.4056 510.0059 -4.6353 393.8683 398.5035 360.2019 511.6133 -4.6321 393.6689 398.3010 359.9834 513.2215 -4.6248 393.4668 398.0916 359.7587 514.8326 -4.6170 393.2587 397.8757 359.5478 516.4313 -4.6124 393.0574 397.6699 359.3289 518.0453 -4.6080 392.8400 397.4480 359.1139 519.6439 -4.6021 392.6520 397.2541 358.9002 521.2426 -4.5960 392.4433 397.0394 358.7084 522.8720 -4.5926 392.2434 396.8360 358.4880 524.4706 -4.5843 392.0433 396.6276 358.2660 526.0683 -4.5786 391.8619 396.4405 358.0653 527.6916 -4.5736 391.6346 396.2082 357.8481 529.2906 -4.5690 391.4353 396.0043 357.6458 530.9051 -4.5635 391.2420 395.8055 357.4322 532.5216 -4.5587 391.0397 395.5984 357.2058 534.1205 -4.5526 390.8321 395.3846 357.0148 535.7345 -4.5469 390.6206 395.1675 356.8125 537.3333 -4.5410 390.4167 394.9577 356.5922 538.9409 -4.5358 390.2289 394.7647 356.3846 540.5470 -4.5326 390.0263 394.5589 356.1889 542.1531 -4.5233 389.8210 394.3442 355.9857 543.7470 -4.5160 389.6324 394.1485 355.7829 545.3426 -4.5078 389.4179 393.9258 355.5883 546.9705 -4.5027 389.2210 393.7237 355.3792 548.5688 -4.4983 389.0211 393.5194 355.1903 550.1825 -4.4933 388.8146 393.3079 354.9914 551.7815 -4.4859 388.6080 393.0939 354.7831 553.3805 -4.4840 388.4025 392.8865 354.5784 555.0095 -4.4829 388.1941 392.6769 354.3868 556.6085 -4.4775 387.9971 392.4747 354.1940 558.2225 -4.4741 387.7967 392.2708 353.9884 559.8214 -4.4673 387.5985 392.0658 353.7894 561.4203 -4.4656 387.3901 391.8557 353.6013 563.0489 -4.4595 387.1772 391.6367 353.3809 564.6628 -4.4534 386.9777 391.4311 353.1725 566.2618 -4.4467 386.7776 391.2243 352.9701 567.8610 -4.4411 386.5689 391.0099 352.7631 569.4755 -4.4364 386.3679 390.8043 352.5418 571.0833 -4.4300 386.1762 390.6063 352.3297 572.6893 -4.4251 385.9736 390.3988 352.1064 574.2818 -4.4200 385.7642 390.1842 351.8938 575.8754 -4.4142 385.5641 389.9783 351.6719 577.4863 -4.4101 385.3669 389.7770 351.4450 579.0998 -4.4026 385.1601 389.5627 351.2376 580.6999 -4.3966 384.9649 389.3615 351.0197 582.2988 -4.3859 384.7597 389.1455 350.7981 583.9126 -4.3785 384.5590 388.9376 350.5740 585.5116 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