DTA measure 1meres1 Test Date: 2024227:1114 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 890.07 s Mass = 1.000 mg data_number = 1104 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1120 -1.1443 257.6576 258.8019 264.1009 1.9033 -1.1357 257.7451 258.8809 264.0354 2.7553 -1.1374 257.6900 258.8274 264.0807 3.5163 -1.1418 257.6868 258.8286 263.8830 4.3373 -1.1404 257.6704 258.8108 263.9532 5.1278 -1.1202 257.6974 258.8176 263.9724 5.9195 -1.1227 257.7680 258.8908 263.9520 6.7415 -1.1287 257.8269 258.9556 263.9229 7.5098 -1.1210 257.8458 258.9668 263.8706 8.3695 -1.1280 257.8483 258.9763 263.8614 9.1308 -1.1261 257.8158 258.9419 263.9300 9.9510 -1.1178 257.9027 259.0205 263.8457 10.7425 -1.1229 257.8570 258.9799 263.8583 11.5330 -1.1119 257.8330 258.9448 263.8814 12.3535 -1.1110 257.9187 259.0297 263.8882 13.1448 -1.1223 257.9999 259.1222 263.9638 13.9663 -1.1332 257.9707 259.1039 264.0316 14.7575 -1.1181 257.9721 259.0902 264.0690 15.5495 -1.1353 257.9276 259.0629 264.1834 16.3715 -1.1171 257.9620 259.0791 264.1681 17.1335 -1.1087 257.9297 259.0384 264.3257 17.9853 -1.1084 257.9732 259.0816 264.3912 18.7758 -1.1100 258.0699 259.1799 264.4478 19.5653 -1.1186 258.0232 259.1418 264.4552 20.3870 -1.1075 258.0381 259.1456 264.5607 21.1475 -1.1121 258.0388 259.1509 264.5888 21.9988 -1.1074 258.1744 259.2818 264.7038 22.7598 -1.1215 258.1880 259.3096 264.9842 23.5810 -1.1228 258.1383 259.2610 264.9993 24.4010 -1.1275 258.1566 259.2842 265.0703 25.1608 -1.1252 258.2158 259.3411 265.2537 26.0125 -1.1251 258.2345 259.3595 265.3954 26.7723 -1.1329 258.2134 259.3463 265.6515 27.5960 -1.1402 258.2386 259.3788 265.7395 28.3633 -1.1311 258.3338 259.4649 265.9103 29.2143 -1.1432 258.2794 259.4226 266.0083 29.9738 -1.1403 258.3759 259.5163 266.1829 30.7948 -1.1387 258.4072 259.5458 266.2820 31.6145 -1.1335 258.4207 259.5541 266.4174 32.3763 -1.1272 258.4912 259.6185 266.5588 33.2275 -1.1338 258.4345 259.5683 266.8130 33.9883 -1.1322 258.3923 259.5246 267.0196 34.8085 -1.1306 258.5197 259.6502 267.0721 35.5995 -1.1270 258.5845 259.7115 267.2741 36.3900 -1.1356 258.4589 259.5945 267.5665 37.2405 -1.1477 258.5059 259.6536 267.6779 37.9915 -1.1536 258.5794 259.7330 267.8783 38.7865 -1.1461 258.6272 259.7733 268.0408 39.6375 -1.1450 258.6790 259.8240 268.1921 40.4268 -1.1530 258.7134 259.8664 268.3335 41.2178 -1.1586 258.7910 259.9496 268.4449 42.0375 -1.1664 258.7888 259.9553 268.6148 42.7990 -1.1659 258.8490 260.0150 268.8904 43.6498 -1.1723 258.7993 259.9716 269.2124 44.4098 -1.1739 258.8066 259.9806 269.3680 45.2310 -1.1750 258.7635 259.9384 269.4783 46.0533 -1.1895 258.8882 260.0777 269.6681 46.8125 -1.1782 258.9638 260.1420 269.8640 47.6640 -1.1869 258.8893 260.0762 270.0300 48.4370 -1.1789 258.9391 260.1180 270.0714 49.2405 -1.1915 258.9408 260.1323 270.3511 50.0618 -1.1851 259.0956 260.2807 270.6016 50.8530 -1.1945 259.1338 260.3283 270.6344 51.6430 -1.2073 259.1239 260.3312 270.7899 52.4640 -1.2087 259.1432 260.3519 271.0278 53.2233 -1.2037 259.1648 260.3686 271.0601 54.0748 -1.2069 259.1256 260.3325 271.3079 54.8655 -1.2105 259.2102 260.4207 271.4193 55.6570 -1.2256 259.3102 260.5358 271.5161 56.4775 -1.2340 259.3026 260.5365 271.7624 57.2380 -1.2265 259.3949 260.6215 271.8284 58.0893 -1.2289 259.4242 260.6531 271.9422 58.8790 -1.2323 259.4915 260.7238 272.1099 59.6605 -1.2265 259.5326 260.7591 272.2324 60.4825 -1.2315 259.5696 260.8011 272.3646 61.2735 -1.2373 259.5727 260.8100 272.4979 62.0643 -1.2368 259.5351 260.7718 272.6570 62.9155 -1.2253 259.6416 260.8668 272.6822 63.6765 -1.2283 259.6354 260.8638 272.8433 64.4983 -1.2384 259.6338 260.8722 272.9484 65.2895 -1.2373 259.6391 260.8765 273.0898 66.0815 -1.2466 259.7611 261.0076 273.2404 66.9035 -1.2376 259.8707 261.1083 273.3085 67.6940 -1.2620 259.8787 261.1408 273.4954 68.5150 -1.2759 259.8496 261.1254 273.5863 69.3253 -1.2721 259.9342 261.2062 273.7467 70.0865 -1.2778 259.9228 261.2006 273.9378 70.9073 -1.2875 259.9631 261.2506 274.0446 71.7283 -1.2946 259.9640 261.2586 274.1580 72.4890 -1.2927 260.0721 261.3648 274.2422 73.3410 -1.2814 260.0622 261.3436 274.3366 74.1010 -1.2814 260.1150 261.3964 274.3971 74.9223 -1.2928 260.2667 261.5596 274.4561 75.7440 -1.3126 260.2000 261.5127 274.6583 76.5033 -1.3179 260.2993 261.6172 274.7157 77.3540 -1.3212 260.2415 261.5627 274.8499 78.1433 -1.3130 260.4962 261.8092 274.8651 78.9538 -1.3157 260.4651 261.7807 274.9690 79.7430 -1.3174 260.5669 261.8843 275.1328 80.5338 -1.3127 260.5282 261.8409 275.2904 81.3240 -1.3098 260.5849 261.8947 275.3769 82.1745 -1.3131 260.6152 261.9283 275.6003 82.9348 -1.3283 260.6085 261.9368 275.7580 83.7560 -1.3284 260.7174 262.0458 275.7371 84.5475 -1.3171 260.7648 262.0819 275.7699 85.3388 -1.3277 260.7514 262.0791 276.0064 86.1905 -1.3352 260.8623 262.1975 276.1035 86.9520 -1.3304 260.9497 262.2801 276.0867 87.7735 -1.3304 260.9518 262.2822 276.1468 88.5645 -1.3445 260.8321 262.1766 276.4490 89.3953 -1.3447 261.0448 262.3895 276.5285 90.1665 -1.3456 261.1451 262.4908 276.6041 90.9885 -1.3571 261.0949 262.4520 276.7753 91.7505 -1.3639 261.2077 262.5715 276.7573 92.6025 -1.3598 261.2217 262.5815 276.9774 93.3645 -1.3753 261.2514 262.6267 277.1495 94.1858 -1.3619 261.3645 262.7264 277.1717 94.9765 -1.3661 261.3426 262.7087 277.2217 95.7675 -1.3556 261.3409 262.6964 277.4609 96.5893 -1.3659 261.4351 262.8010 277.5500 97.3785 -1.3621 261.5073 262.8694 277.6317 98.1990 -1.3746 261.6173 262.9919 277.7733 98.9900 -1.3941 261.5926 262.9868 277.9181 99.9283 -1.3892 261.5970 262.9862 278.0221 100.7990 -1.4123 261.6999 263.1122 278.1258 101.5898 -1.4105 261.7616 263.1722 278.3545 102.4115 -1.4020 261.8625 263.2645 278.4566 103.2030 -1.3990 261.8587 263.2576 278.6002 103.9938 -1.4004 261.9066 263.3069 278.7129 104.8160 -1.4038 261.8954 263.2992 278.8185 105.5763 -1.4099 261.9694 263.3792 278.9207 106.4265 -1.4259 262.0268 263.4527 278.9858 107.1858 -1.4341 262.0739 263.5080 279.2451 108.0068 -1.4365 262.1966 263.6331 279.3747 108.8265 -1.4149 262.3254 263.7403 279.4790 109.5875 -1.4192 262.2823 263.7015 279.5825 110.4438 -1.4189 262.4467 263.8655 279.7250 111.2043 -1.4197 262.4925 263.9122 279.8079 112.0250 -1.4396 262.5477 263.9873 279.9953 112.8155 -1.4312 262.4663 263.8975 280.1068 113.6060 -1.4285 262.4856 263.9141 280.2525 114.4258 -1.4325 262.6705 264.1030 280.2769 115.2160 -1.4379 262.6153 264.0533 280.4622 116.0373 -1.4353 262.7295 264.1647 280.5938 116.8275 -1.4519 262.7836 264.2355 280.6880 117.6180 -1.4456 262.9001 264.3457 280.7484 118.4385 -1.4515 262.9609 264.4123 280.9350 119.2295 -1.4534 263.0879 264.5413 281.2196 120.0510 -1.4700 263.0192 264.4891 281.2705 120.8405 -1.4702 263.0992 264.5694 281.3876 121.6313 -1.4777 263.2021 264.6799 281.5940 122.4533 -1.4718 263.1605 264.6323 281.7771 123.2425 -1.4706 263.3001 264.7707 281.7237 124.0638 -1.4719 263.3718 264.8437 281.7996 124.8560 -1.4753 263.4803 264.9556 281.9382 125.6468 -1.4865 263.5259 265.0125 282.0492 126.4695 -1.5035 263.4687 264.9722 282.3050 127.2310 -1.4862 263.6835 265.1697 282.3766 128.0820 -1.4979 263.7052 265.2031 282.4652 128.8408 -1.4987 263.7763 265.2750 282.5446 129.6610 -1.4978 263.8688 265.3666 282.7740 130.4810 -1.5060 264.0337 265.5397 282.9749 131.2410 -1.5190 263.9042 265.4231 283.1308 132.0923 -1.5154 264.0339 265.5493 283.2192 132.8528 -1.5235 264.0387 265.5622 283.3376 133.6738 -1.5086 264.1081 265.6167 283.3901 134.4945 -1.5112 264.1514 265.6626 283.5355 135.2565 -1.5214 264.2057 265.7271 283.6813 136.1083 -1.5126 264.3012 265.8138 283.8554 136.8678 -1.5331 264.3754 265.9085 284.0182 137.6895 -1.5490 264.4498 265.9987 284.1746 138.4805 -1.5581 264.4865 266.0446 284.2993 139.2718 -1.5453 264.5748 266.1201 284.3832 140.1233 -1.5437 264.7135 266.2572 284.5884 140.8828 -1.5393 264.7548 266.2941 284.7253 141.7035 -1.5522 264.7323 266.2845 284.8183 142.4955 -1.5484 264.8494 266.3978 284.8838 143.2860 -1.5512 264.8381 266.3894 285.0196 144.1365 -1.5729 264.8677 266.4406 285.2120 144.8985 -1.5771 265.0046 266.5817 285.3262 145.7193 -1.5699 265.1278 266.6977 285.5443 146.5095 -1.5747 265.1826 266.7573 285.5697 147.2995 -1.5804 265.3033 266.8837 285.6590 148.1213 -1.5862 265.3348 266.9210 285.8827 148.9105 -1.5776 265.4221 266.9997 285.9992 149.7310 -1.5805 265.4698 267.0503 286.0912 150.5220 -1.5815 265.5650 267.1464 286.1585 151.3123 -1.5923 265.6635 267.2558 286.3395 152.1340 -1.6078 265.6603 267.2681 286.5386 152.9240 -1.6031 265.7748 267.3780 286.6261 153.7455 -1.6070 265.7963 267.4032 286.7680 154.5370 -1.5969 265.9611 267.5580 286.8986 155.3273 -1.6109 266.1093 267.7202 286.9987 156.1490 -1.6127 266.1172 267.7299 287.1575 156.9400 -1.6164 266.1047 267.7212 287.3459 157.7618 -1.6165 266.2155 267.8320 287.4386 158.5525 -1.6124 266.3370 267.9494 287.4935 159.3440 -1.6162 266.3814 267.9976 287.5658 160.1655 -1.6185 266.4002 268.0187 287.8334 160.9300 -1.6351 266.4110 268.0461 288.0378 161.7875 -1.6326 266.5139 268.1465 288.1437 162.5478 -1.6448 266.5813 268.2262 288.3494 163.3688 -1.6491 266.5974 268.2465 288.3319 164.1895 -1.6465 266.7696 268.4162 288.4645 164.9510 -1.6466 266.8160 268.4626 288.5797 165.8023 -1.6508 266.9148 268.5656 288.6752 166.5625 -1.6472 266.9598 268.6070 288.9068 167.3838 -1.6596 267.1306 268.7902 288.9995 168.1743 -1.6648 267.1390 268.8038 289.0164 168.9653 -1.6480 267.2084 268.8564 289.1157 169.8163 -1.6777 267.3198 268.9975 289.3176 170.5765 -1.6852 267.5338 269.2190 289.4755 171.3980 -1.6849 267.5681 269.2530 289.6779 172.2193 -1.6859 267.5924 269.2783 289.8144 172.9793 -1.6755 267.6201 269.2956 290.0085 173.8308 -1.6653 267.7316 269.3969 290.1278 174.5923 -1.6810 267.8685 269.5495 290.2484 175.4130 -1.6930 267.8176 269.5106 290.3795 176.2035 -1.7031 267.8897 269.5928 290.4042 176.9945 -1.7035 268.0740 269.7776 290.5260 177.8468 -1.7014 268.2210 269.9224 290.7507 178.6070 -1.7122 268.1487 269.8609 290.8931 179.4288 -1.7082 268.2218 269.9301 290.8733 180.2198 -1.7103 268.3411 270.0514 290.9960 181.0095 -1.7184 268.4593 270.1777 291.0416 181.8265 -1.7250 268.5827 270.3077 291.2197 182.6243 -1.7241 268.6560 270.3801 291.3954 183.4455 -1.7239 268.7389 270.4628 291.6470 184.2063 -1.7332 268.6873 270.4206 291.7556 185.0573 -1.7354 268.8574 270.5928 291.8750 185.8470 -1.7201 268.9694 270.6895 291.9758 186.6378 -1.7251 269.0814 270.8065 292.0457 187.4595 -1.7349 269.0613 270.7962 292.2922 188.2200 -1.7432 269.1253 270.8685 292.3827 189.0713 -1.7299 269.2778 271.0077 292.4412 189.8318 -1.7204 269.3717 271.0921 292.5242 190.6530 -1.7332 269.4910 271.2243 292.5776 191.4735 -1.7347 269.6220 271.3567 292.7350 192.2353 -1.7273 269.6354 271.3627 292.8715 193.0855 -1.7323 269.8135 271.5458 293.0354 193.8748 -1.7615 269.7032 271.4647 293.1473 194.6665 -1.7745 269.8449 271.6194 293.4124 195.4885 -1.7781 269.8708 271.6489 293.4494 196.2498 -1.7762 270.0819 271.8582 293.5419 197.1015 -1.7661 270.2668 272.0329 293.5192 197.8625 -1.7779 270.3086 272.0865 293.6625 198.6838 -1.7805 270.3372 272.1177 293.8861 199.4750 -1.7962 270.3977 272.1939 294.0062 200.2663 -1.7901 270.4783 272.2684 294.0874 201.0880 -1.7844 270.4599 272.2443 294.3090 201.8573 -1.7910 270.7089 272.4999 294.4296 202.7078 -1.7930 270.7794 272.5724 294.5312 203.4678 -1.8087 270.8463 272.6550 294.7085 204.3198 -1.7974 270.9810 272.7784 294.7445 205.0790 -1.8037 271.1149 272.9186 294.8367 205.9000 -1.8022 271.0155 272.8177 295.0341 206.7193 -1.8104 271.0665 272.8769 295.2666 207.4800 -1.8148 271.2237 273.0385 295.2829 208.3318 -1.8427 271.3411 273.1837 295.4606 209.0928 -1.8364 271.3359 273.1723 295.6891 209.9145 -1.8301 271.5017 273.3319 295.7892 210.7055 -1.8171 271.5599 273.3770 295.8753 211.4973 -1.8304 271.6994 273.5298 296.0143 212.3185 -1.8387 271.8549 273.6937 296.1475 213.1083 -1.8392 271.8658 273.7050 296.3029 213.9285 -1.8515 271.9698 273.8213 296.4396 214.7198 -1.8443 271.9872 273.8314 296.6495 215.5105 -1.8464 272.0659 273.9123 296.7472 216.3315 -1.8526 272.2708 274.1234 296.9020 217.0918 -1.8466 272.4778 274.3245 296.9714 217.9435 -1.8587 272.4603 274.3190 297.2083 218.7338 -1.8580 272.5156 274.3737 297.3096 219.5250 -1.8631 272.6167 274.4798 297.4372 220.3465 -1.8697 272.6931 274.5628 297.5527 221.1063 -1.8795 272.6877 274.5671 297.6318 221.9575 -1.8882 272.9612 274.8493 297.7904 222.7200 -1.8702 272.9517 274.8219 297.9791 223.5533 -1.8816 272.9349 274.8165 298.1192 224.3135 -1.8810 273.1126 274.9936 298.2055 225.1650 -1.8776 273.3528 275.2304 298.3057 225.9260 -1.8840 273.3465 275.2306 298.3546 226.7475 -1.8985 273.3552 275.2537 298.6012 227.5685 -1.8990 273.5370 275.4360 298.7242 228.3285 -1.8979 273.6030 275.5008 298.6989 229.1808 -1.9093 273.6476 275.5570 298.7857 229.9418 -1.9045 273.7110 275.6154 298.9896 230.7638 -1.9112 273.8930 275.8042 299.1364 231.5558 -1.9150 274.0074 275.9224 299.2726 232.3460 -1.9130 274.0999 276.0129 299.3646 233.1580 -1.9194 274.1525 276.0720 299.5077 233.9788 -1.9111 274.3780 276.2890 299.5950 234.7400 -1.9354 274.3707 276.3061 299.7220 235.5915 -1.9356 274.4877 276.4233 299.8507 236.3518 -1.9419 274.5699 276.5119 299.9344 237.1730 -1.9347 274.6278 276.5626 300.1000 237.9935 -1.9457 274.7792 276.7249 300.1030 238.7550 -1.9516 274.8668 276.8184 300.3638 239.6058 -1.9466 275.0432 276.9898 300.5843 240.3675 -1.9483 275.0217 276.9699 300.6540 241.1888 -1.9466 275.1486 277.0952 300.7532 241.9795 -1.9592 275.2447 277.2039 300.8097 242.7923 -1.9710 275.3477 277.3187 301.0228 243.5770 -1.9541 275.4276 277.3818 301.1200 244.3985 -1.9530 275.5660 277.5190 301.3493 245.1895 -1.9649 275.6166 277.5815 301.4398 246.0108 -1.9635 275.8253 277.7888 301.6113 246.8015 -1.9713 275.7916 277.7629 301.6905 247.5935 -1.9699 275.9514 277.9214 301.8949 248.4155 -1.9836 276.0478 278.0314 302.0192 249.1775 -2.0010 276.1311 278.1321 302.1837 250.0290 -2.0004 276.1265 278.1268 302.1994 250.7923 -1.9944 276.3821 278.3765 302.2123 251.6145 -1.9926 276.4776 278.4702 302.3033 252.4350 -1.9899 276.5884 278.5783 302.5489 253.2320 -1.9845 276.7316 278.7161 302.7292 253.9988 -1.9862 276.8188 278.8049 302.8008 254.8510 -2.0012 276.9250 278.9261 302.9103 255.6128 -1.9959 276.9741 278.9700 302.9762 256.4335 -1.9901 277.0782 279.0683 303.1654 257.2260 -1.9970 277.1681 279.1651 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