DTA measure 1meres2 Test Date: 2024227:1329 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1152.81 s Mass = 1.000 mg data_number = 1429 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2660 -1.8850 204.2574 206.1424 251.1889 2.0875 -1.8805 204.4712 206.3517 251.1647 2.8780 -1.8775 204.6677 206.5452 251.1552 3.6988 -1.8726 204.8620 206.7346 251.1649 4.4883 -1.8687 205.0577 206.9264 251.1486 5.2860 -1.8635 205.2683 207.1318 251.1444 6.0705 -1.8597 205.4727 207.3324 251.1571 6.9205 -1.8558 205.6679 207.5236 251.1940 7.6815 -1.8508 205.8491 207.6999 251.2002 8.5028 -1.8487 206.0734 207.9220 251.2095 9.3225 -1.8443 206.2640 208.1084 251.2528 10.0828 -1.8411 206.4486 208.2897 251.2683 10.9343 -1.8353 206.6503 208.4856 251.3202 11.7238 -1.8323 206.8605 208.6929 251.3578 12.5148 -1.8286 207.0422 208.8708 251.4258 13.3365 -1.8221 207.2452 209.0674 251.4946 14.0970 -1.8191 207.4266 209.2456 251.5436 14.9478 -1.8127 207.6454 209.4581 251.6266 15.7393 -1.8126 207.8372 209.6499 251.6948 16.5295 -1.8107 208.0356 209.8463 251.7819 17.3510 -1.8068 208.2218 210.0287 251.8727 18.1125 -1.8051 208.3989 210.2040 251.9759 18.9650 -1.8008 208.6099 210.4107 252.0812 19.7260 -1.8002 208.8003 210.6006 252.1845 20.5470 -1.7970 208.9994 210.7964 252.2691 21.3670 -1.7934 209.1805 210.9739 252.3960 22.1285 -1.7934 209.3526 211.1460 252.5072 22.9808 -1.7915 209.5414 211.3328 252.6469 23.7418 -1.7894 209.7470 211.5365 252.7578 24.5630 -1.7863 209.9463 211.7325 252.8812 25.3840 -1.7807 210.1295 211.9102 253.0231 26.1640 -1.7756 210.3005 212.0761 253.1523 26.9748 -1.7750 210.5144 212.2894 253.2963 27.7655 -1.7752 210.7022 212.4774 253.4353 28.5855 -1.7739 210.8884 212.6623 253.5797 29.3458 -1.7732 211.0725 212.8457 253.7114 30.1973 -1.7718 211.2774 213.0492 253.8708 30.9868 -1.7677 211.4492 213.2168 254.0345 31.7783 -1.7650 211.6244 213.3894 254.1859 32.5985 -1.7625 211.8205 213.5830 254.3125 33.3603 -1.7611 211.9946 213.7557 254.4760 34.2113 -1.7586 212.1920 213.9506 254.6621 34.9708 -1.7590 212.3750 214.1340 254.8071 35.7918 -1.7524 212.5518 214.3041 254.9615 36.5853 -1.7437 212.7334 214.4771 255.1307 37.3975 -1.7386 212.9218 214.6604 255.2935 38.1888 -1.7372 213.0970 214.8342 255.4490 39.0095 -1.7412 213.2933 215.0345 255.6096 39.7708 -1.7453 213.4680 215.2133 255.7507 40.6220 -1.7505 213.6507 215.4012 255.9257 41.4123 -1.7510 213.8385 215.5895 256.0793 42.2030 -1.7521 214.0230 215.7750 256.2323 43.0240 -1.7524 214.2245 215.9769 256.3904 43.7845 -1.7526 214.3819 216.1344 256.5219 44.6368 -1.7507 214.5697 216.3204 256.6898 45.3978 -1.7518 214.7370 216.4888 256.8164 46.2215 -1.7552 214.9215 216.6767 256.9670 47.0283 -1.7526 215.1094 216.8620 257.0976 47.8200 -1.7503 215.2846 217.0348 257.2476 48.6110 -1.7453 215.4618 217.2070 257.3974 49.4330 -1.7441 215.6509 217.3951 257.5401 50.2230 -1.7454 215.8496 217.5950 257.6465 51.0440 -1.7454 216.0042 217.7496 257.7841 51.8348 -1.7455 216.1874 217.9329 257.8858 52.6258 -1.7470 216.3663 218.1133 258.0257 53.4475 -1.7452 216.5460 218.2912 258.1539 54.2095 -1.7459 216.7216 218.4676 258.2681 55.0615 -1.7437 216.9121 218.6558 258.3966 55.8518 -1.7453 217.0925 218.8378 258.5127 56.6610 -1.7475 217.2704 219.0180 258.6456 57.4508 -1.7506 217.4480 219.1986 258.7492 58.2705 -1.7503 217.6423 219.3926 258.8571 59.0318 -1.7523 217.7887 219.5410 258.9551 59.8833 -1.7536 217.9875 219.7411 259.0624 60.6445 -1.7526 218.1661 219.9187 259.1670 61.4660 -1.7544 218.3386 220.0930 259.2719 62.2575 -1.7542 218.5059 220.2601 259.3665 63.0488 -1.7539 218.6881 220.4420 259.4657 63.9003 -1.7530 218.8658 220.6188 259.5565 64.6615 -1.7514 219.0267 220.7781 259.6571 65.4828 -1.7520 219.2188 220.9709 259.7573 66.2735 -1.7542 219.4041 221.1583 259.8418 67.1035 -1.7556 219.5525 221.3081 259.9572 67.8730 -1.7535 219.7107 221.4642 260.0334 68.6943 -1.7533 219.9137 221.6670 260.1172 69.4550 -1.7522 220.0939 221.8462 260.2133 70.3070 -1.7550 220.2760 222.0310 260.2848 71.0990 -1.7540 220.4411 222.1951 260.3499 71.8890 -1.7547 220.6109 222.3656 260.4435 72.7090 -1.7526 220.7800 222.5326 260.5412 73.4690 -1.7508 220.9486 222.6994 260.6124 74.3208 -1.7552 221.1355 222.8907 260.6977 75.1098 -1.7550 221.3042 223.0592 260.7710 75.9000 -1.7556 221.4712 223.2268 260.8571 76.7218 -1.7520 221.6387 223.3908 260.9472 77.6340 -1.7501 221.8292 223.5793 261.0601 78.5373 -1.7488 222.0172 223.7660 261.1372 79.3278 -1.7475 222.1935 223.9410 261.2171 80.1190 -1.7483 222.3724 224.1207 261.3180 80.9395 -1.7437 222.5313 224.2750 261.4105 81.7005 -1.7457 222.6918 224.4375 261.4912 82.5523 -1.7456 222.8791 224.6247 261.5757 83.3418 -1.7459 223.0322 224.7781 261.6712 84.1335 -1.7460 223.2002 224.9462 261.7608 84.9545 -1.7493 223.3860 225.1353 261.8579 85.7158 -1.7457 223.5224 225.2682 261.9341 86.5725 -1.7458 223.6904 225.4362 262.0319 87.3338 -1.7499 223.8769 225.6267 262.1310 88.1545 -1.7499 224.0460 225.7959 262.2365 88.9453 -1.7487 224.2023 225.9510 262.3149 89.7350 -1.7519 224.3700 226.1219 262.4151 90.5855 -1.7481 224.5597 226.3078 262.5119 91.3465 -1.7426 224.7066 226.4492 262.6037 92.1670 -1.7435 224.8720 226.6154 262.7148 92.9870 -1.7426 225.0536 226.7962 262.8066 93.7483 -1.7458 225.2033 226.9491 262.9034 94.5993 -1.7437 225.3733 227.1170 263.0337 95.3600 -1.7464 225.5381 227.2845 263.1268 96.1813 -1.7489 225.6945 227.4434 263.2251 97.0020 -1.7489 225.8675 227.6164 263.3476 97.7620 -1.7468 226.0230 227.7697 263.4343 98.6130 -1.7470 226.2041 227.9512 263.5548 99.4040 -1.7494 226.3418 228.0912 263.6635 100.1950 -1.7486 226.5137 228.2623 263.7838 101.0178 -1.7491 226.6808 228.4299 263.8938 101.7798 -1.7509 226.8470 228.5979 264.0113 102.6313 -1.7494 227.0150 228.7644 264.1415 103.3925 -1.7520 227.1689 228.9209 264.2516 104.2145 -1.7528 227.3360 229.0888 264.3595 105.0365 -1.7503 227.4875 229.2378 264.4695 105.7965 -1.7532 227.6536 229.4068 264.5797 106.6455 -1.7534 227.8190 229.5724 264.6956 107.4365 -1.7528 227.9599 229.7127 264.8185 108.3613 -1.7527 228.1443 229.8971 264.9568 109.2563 -1.7522 228.3388 230.0910 265.0908 110.0468 -1.7528 228.4749 230.2276 265.2042 110.8378 -1.7557 228.6407 230.3964 265.3099 111.6595 -1.7567 228.7932 230.5499 265.4183 112.4210 -1.7586 228.9426 230.7011 265.5255 113.2725 -1.7592 229.1096 230.8688 265.6627 114.0365 -1.7628 229.2532 231.0160 265.7793 114.8615 -1.7613 229.4334 231.1948 265.8993 115.6835 -1.7614 229.5781 231.3395 266.0132 116.4455 -1.7640 229.7446 231.5086 266.1268 117.2968 -1.7631 229.9247 231.6878 266.2557 118.0580 -1.7644 230.0655 231.8299 266.3588 118.8803 -1.7632 230.2205 231.9837 266.4867 119.7020 -1.7639 230.3740 232.1380 266.5988 120.4628 -1.7663 230.5256 232.2919 266.7034 121.3148 -1.7651 230.7013 232.4665 266.8291 122.1050 -1.7661 230.8505 232.6166 266.9640 122.8955 -1.7696 231.0212 232.7908 267.0741 123.7180 -1.7702 231.1664 232.9365 267.1947 124.4785 -1.7743 231.3133 233.0875 267.3011 125.3308 -1.7747 231.4836 233.2583 267.4293 126.1210 -1.7743 231.6330 233.4073 267.5465 126.9118 -1.7751 231.7865 233.5617 267.6456 127.7335 -1.7730 231.9518 233.7248 267.7482 128.5383 -1.7752 232.1106 233.8858 267.8478 129.3110 -1.7776 232.2580 234.0356 267.9496 130.1613 -1.7802 232.4196 234.1998 268.0739 130.9218 -1.7820 232.5676 234.3497 268.1884 131.7430 -1.7844 232.7256 234.5100 268.3063 132.5345 -1.7885 232.8567 234.6452 268.3992 133.3263 -1.7863 233.0198 234.8060 268.4954 134.1775 -1.7893 233.2050 234.9944 268.6101 134.9388 -1.7905 233.3178 235.1083 268.7058 135.7608 -1.7935 233.4883 235.2818 268.8143 136.5525 -1.7989 233.6330 235.4319 268.9181 137.3430 -1.8011 233.8040 235.6051 269.0212 138.1935 -1.8011 233.9356 235.7367 269.1212 138.9875 -1.8006 234.0969 235.8974 269.2272 139.7690 -1.8002 234.2183 236.0185 269.3231 140.5905 -1.8037 234.3958 236.1995 269.4274 141.3815 -1.8060 234.5561 236.3621 269.5173 142.1730 -1.8087 234.7006 236.5093 269.6158 142.9953 -1.8126 234.8570 236.6697 269.7234 143.7845 -1.8119 235.0065 236.8184 269.8391 144.6055 -1.8121 235.1416 236.9537 269.9434 145.3963 -1.8120 235.2967 237.1088 270.0302 146.1868 -1.8132 235.4626 237.2757 270.1370 147.0378 -1.8138 235.6184 237.4322 270.2275 147.7978 -1.8182 235.7616 237.5797 270.3453 148.6195 -1.8175 235.8984 237.7159 270.4385 149.4265 -1.8166 236.0670 237.8835 270.5391 150.2163 -1.8176 236.2158 238.0334 270.6251 151.0068 -1.8204 236.3575 238.1779 270.7452 151.8285 -1.8233 236.4903 238.3136 270.8437 152.6200 -1.8253 236.6541 238.4794 270.9337 153.4410 -1.8241 236.8086 238.6327 271.0321 154.2315 -1.8250 236.9582 238.7832 271.1095 155.0235 -1.8277 237.0946 238.9222 271.2268 155.8455 -1.8286 237.2318 239.0604 271.3315 156.6353 -1.8288 237.3685 239.1974 271.4194 157.4565 -1.8310 237.5377 239.3687 271.5259 158.2478 -1.8341 237.6774 239.5115 271.5946 159.0595 -1.8372 237.8317 239.6689 271.6948 159.8535 -1.8376 237.9681 239.8057 271.7931 160.6455 -1.8375 238.1343 239.9719 271.8996 161.4373 -1.8414 238.2672 240.1087 272.0130 162.2883 -1.8371 238.4360 240.2730 272.1172 163.0485 -1.8386 238.5662 240.4048 272.2042 163.8698 -1.8405 238.7018 240.5423 272.3228 164.6593 -1.8414 238.8629 240.7043 272.4434 165.4498 -1.8447 239.0062 240.8509 272.5343 166.3003 -1.8421 239.1510 240.9931 272.6295 167.0608 -1.8416 239.2982 241.1398 272.7337 167.8815 -1.8448 239.4402 241.2850 272.8529 168.6733 -1.8457 239.5784 241.4241 272.9699 169.5033 -1.8490 239.7275 241.5765 273.0713 170.2705 -1.8489 239.8820 241.7309 273.1852 171.0920 -1.8483 240.0229 241.8712 273.2978 171.8513 -1.8502 240.1609 242.0111 273.4210 172.7030 -1.8481 240.2991 242.1472 273.5427 173.4950 -1.8492 240.4401 242.2893 273.6647 174.2853 -1.8527 240.6024 242.4551 273.7522 175.1070 -1.8555 240.7411 242.5966 273.8800 175.8673 -1.8553 240.8850 242.7404 274.0105 176.7188 -1.8601 241.0255 242.8856 274.1379 177.4788 -1.8581 241.1692 243.0274 274.2256 178.3000 -1.8616 241.3241 243.1857 274.3354 179.1205 -1.8642 241.4504 243.3146 274.4719 180.0335 -1.8652 241.6160 243.4812 274.5995 180.9353 -1.8666 241.7715 243.6381 274.7139 181.6955 -1.8654 241.9010 243.7664 274.8276 182.5168 -1.8643 242.0741 243.9385 274.9602 183.3075 -1.8705 242.2059 244.0763 275.0909 184.0980 -1.8695 242.3319 244.2014 275.1808 184.9485 -1.8688 242.4837 244.3526 275.3069 185.7098 -1.8659 242.6264 244.4923 275.4263 186.5315 -1.8664 242.7476 244.6140 275.5437 187.3223 -1.8680 242.9052 244.7732 275.6351 188.1123 -1.8706 243.0445 244.9151 275.7678 188.9335 -1.8751 243.2004 245.0755 275.8759 189.7238 -1.8809 243.3247 245.2056 275.9776 190.5453 -1.8837 243.4779 245.3615 276.0911 191.3348 -1.8869 243.6123 245.4992 276.2038 192.1258 -1.8925 243.7483 245.6408 276.3236 192.9473 -1.8927 243.8854 245.7781 276.4370 193.7365 -1.8932 244.0343 245.9275 276.5548 194.5570 -1.8921 244.1718 246.0640 276.6480 195.3480 -1.8972 244.3036 246.2008 276.7481 196.1388 -1.8982 244.4545 246.3527 276.8515 196.9600 -1.8985 244.6024 246.5010 276.9637 197.7200 -1.9007 244.7085 246.6092 277.0367 198.5720 -1.9031 244.8656 246.7688 277.1391 199.3633 -1.9034 245.0165 246.9199 277.2588 200.1545 -1.9047 245.1735 247.0782 277.3487 200.9758 -1.9046 245.3003 247.2049 277.4443 201.7353 -1.9071 245.4347 247.3418 277.5520 202.5865 -1.9061 245.5636 247.4697 277.6445 203.3768 -1.9085 245.7141 247.6225 277.7335 204.1680 -1.9114 245.8530 247.7644 277.8446 204.9895 -1.9154 245.9825 247.8978 277.9554 205.7498 -1.9134 246.1111 248.0245 278.0311 206.6005 -1.9157 246.2603 248.1760 278.1358 207.3905 -1.9178 246.4174 248.3352 278.2390 208.1815 -1.9199 246.5471 248.4670 278.3300 209.0015 -1.9213 246.7087 248.6300 278.4183 209.7620 -1.9200 246.8188 248.7388 278.5169 210.7543 -1.9168 246.9783 248.8951 278.6417 211.5925 -1.9192 247.1483 249.0674 278.7354 212.3830 -1.9179 247.2649 249.1827 278.8426 213.2335 -1.9184 247.3862 249.3047 278.9261 213.9945 -1.9215 247.5126 249.4341 279.0235 214.8163 -1.9243 247.6691 249.5933 279.1225 215.6075 -1.9252 247.8302 249.7554 279.2145 216.3988 -1.9276 247.9470 249.8746 279.3112 217.2205 -1.9290 248.0808 250.0098 279.4111 218.0105 -1.9300 248.2196 250.1496 279.4993 218.8310 -1.9317 248.3574 250.2891 279.6047 219.6223 -1.9313 248.4820 250.4132 279.7252 220.4130 -1.9343 248.6173 250.5516 279.8269 221.2343 -1.9342 248.7537 250.6879 279.9202 222.0243 -1.9374 248.9044 250.8418 280.0088 222.8458 -1.9366 249.0371 250.9738 280.1018 223.6380 -1.9396 249.1575 251.0971 280.2167 224.4288 -1.9442 249.2904 251.2346 280.3381 225.2508 -1.9451 249.4352 251.3803 280.4428 226.0413 -1.9419 249.5885 251.5305 280.5772 226.8628 -1.9447 249.7272 251.6719 280.6840 227.6548 -1.9475 249.8513 251.7988 280.7782 228.4463 -1.9484 249.9757 251.9241 280.8806 229.2675 -1.9513 250.1004 252.0517 280.9885 230.0278 -1.9522 250.2272 252.1794 281.0888 230.8795 -1.9538 250.3786 252.3325 281.2220 231.6715 -1.9541 250.5193 252.4734 281.3412 232.4618 -1.9554 250.6476 252.6030 281.4635 233.2835 -1.9583 250.7922 252.7505 281.5721 234.0433 -1.9597 250.9244 252.8841 281.6798 234.8943 -1.9612 251.0449 253.0061 281.7917 235.6855 -1.9640 251.1791 253.1431 281.9116 236.4765 -1.9648 251.3020 253.2669 282.0173 237.2975 -1.9644 251.4498 253.4142 282.1361 238.0880 -1.9685 251.5715 253.5400 282.2424 238.9095 -1.9714 251.7087 253.6801 282.3537 239.7015 -1.9725 251.8434 253.8159 282.4681 240.4928 -1.9752 251.9704 253.9456 282.5733 241.3145 -1.9773 252.1060 254.0833 282.6678 242.1055 -1.9772 252.2277 254.2049 282.7848 242.9273 -1.9816 252.3707 254.3523 282.8942 243.7195 -1.9833 252.4997 254.4830 283.0005 244.5105 -1.9875 252.6346 254.6221 283.1135 245.3323 -1.9884 252.7677 254.7561 283.2394 246.1215 -1.9889 252.8936 254.8826 283.3380 246.9423 -1.9907 253.0112 255.0018 283.4464 247.7340 -1.9962 253.1522 255.1484 283.5651 248.5248 -1.9959 253.2939 255.2898 283.6869 249.3470 -1.9969 253.4312 255.4280 283.7754 250.1113 -2.0007 253.5548 255.5555 283.8700 250.9648 -1.9997 253.6780 255.6777 284.0258 251.7548 -2.0027 253.8004 255.8031 284.1491 252.5453 -2.0045 253.9223 255.9268 284.2565 253.3668 -2.0096 254.0780 256.0876 284.3596 254.1578 -2.0126 254.2123 256.2249 284.4587 254.9790 -2.0156 254.3422 256.3578 284.5913 255.7705 -2.0171 254.4628 256.4799 284.7064 256.5625 -2.0189 254.5861 256.6049 284.8150 257.3845 -2.0209 254.7323 256.7532 284.9101 258.1765 -2.0199 254.8510 256.8709 285.0325 258.9985 -2.0197 254.9865 257.0062 285.1627 259.7895 -2.0221 255.1114 257.1335 285.3040 260.5810 -2.0231 255.2299 257.2529 285.3800 261.4518 -2.0248 255.3787 257.4034 285.5033 262.3960 -2.0292 255.5390 257.5682 285.6519 263.2170 -2.0292 255.6613 257.6906 285.7486 264.0085 -2.0320 255.7906 257.8225 285.8339 264.7998 -2.0353 255.9226 257.9579 285.9543 265.6215 -2.0362 256.0622 258.0984 286.0596 266.4113 -2.0369 256.1747 258.2116 286.1635 267.2325 -2.0401 256.3074 258.3475 286.2754 268.0238 -2.0435 256.4777 258.5212 286.3761 268.8153 -2.0467 256.5870 258.6337 286.4912 269.6373 -2.0497 256.7215 258.7713 286.5849 270.4275 -2.0508 256.8482 258.8990 286.6768 271.2480 -2.0500 256.9617 259.0117 286.7846 272.0380 -2.0522 257.0972 259.1495 286.8725 272.8283 -2.0559 257.2086 259.2645 286.9719 273.6798 -2.0571 257.3530 259.4101 287.0853 274.4408 -2.0567 257.4748 259.5315 287.1901 275.2625 -2.0622 257.5923 259.6545 287.2944 276.0540 -2.0620 257.7199 259.7819 287.3834 276.8443 -2.0615 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