DTA measure 3olom Date: 2024423:1122 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1432.17 s Mass = 953.800 mg data_number = 1783 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2080 -5.0166 392.0580 397.0746 418.3314 2.0290 -5.0119 392.2066 397.2185 418.3609 2.8200 -5.0079 392.3307 397.3387 418.3856 3.6418 -5.0035 392.4744 397.4780 418.4061 4.4330 -5.0026 392.6379 397.6406 418.4345 5.2235 -5.0005 392.7837 397.7842 418.4611 6.0450 -4.9998 392.9107 397.9104 418.4868 6.8348 -5.0007 393.0425 398.0432 418.5168 7.6568 -4.9977 393.1760 398.1737 418.5342 8.4475 -4.9988 393.3350 398.3339 418.5478 9.2380 -4.9945 393.4727 398.4672 418.5843 10.0898 -4.9919 393.6282 398.6201 418.5935 10.8515 -4.9908 393.7346 398.7254 418.6125 11.6733 -4.9891 393.8754 398.8645 418.6188 12.4635 -4.9869 394.0293 399.0162 418.6221 13.2555 -4.9865 394.1547 399.1412 418.6180 14.1073 -4.9817 394.2918 399.2736 418.5985 14.8685 -4.9787 394.4350 399.4137 418.5852 15.6903 -4.9782 394.5604 399.5387 418.5553 16.4815 -4.9773 394.7032 399.6805 418.5472 17.2725 -4.9736 394.8316 399.8053 418.4946 18.1235 -4.9742 394.9744 399.9486 418.4752 18.8845 -4.9681 395.1002 400.0682 418.4260 19.7075 -4.9635 395.2470 400.2104 418.3921 20.4985 -4.9631 395.3617 400.3249 418.3584 21.2903 -4.9602 395.4953 400.4554 418.3118 22.1115 -4.9567 395.6255 400.5822 418.2252 22.9035 -4.9526 395.7436 400.6963 418.1461 23.7253 -4.9487 395.8795 400.8282 418.0754 24.5175 -4.9461 396.0264 400.9724 417.9993 25.3075 -4.9459 396.1550 401.1009 417.9263 26.1590 -4.9394 396.2756 401.2149 417.8360 26.9203 -4.9360 396.4028 401.3388 417.7381 27.7418 -4.9318 396.5304 401.4622 417.6436 28.5340 -4.9263 396.6626 401.5889 417.5304 29.3248 -4.9191 396.7766 401.6958 417.4313 30.1760 -4.9162 396.9016 401.8178 417.3229 30.9378 -4.9120 397.0066 401.9186 417.2247 31.7598 -4.9063 397.1389 402.0451 417.1011 32.5520 -4.9020 397.2682 402.1702 416.9841 33.3435 -4.8983 397.3996 402.2978 416.9036 34.1958 -4.8922 397.5108 402.4030 416.7556 34.9565 -4.8869 397.6138 402.5007 416.6547 35.7788 -4.8805 397.7523 402.6328 416.5138 36.5755 -4.8756 397.8689 402.7445 416.4001 37.3725 -4.8706 397.9890 402.8596 416.2770 38.1945 -4.8640 398.0827 402.9467 416.1424 38.9565 -4.8570 398.1512 403.0082 416.0202 39.8078 -4.8488 398.3016 403.1504 415.9097 40.5985 -4.8449 398.4245 403.2695 415.7568 41.3905 -4.8409 398.5283 403.3692 415.6281 42.2125 -4.8341 398.6377 403.4719 415.5120 42.9745 -4.8254 398.7631 403.5886 415.3952 43.8265 -4.8190 398.8773 403.6963 415.2513 44.6168 -4.8135 398.9831 403.7965 415.1349 45.4075 -4.8087 399.0767 403.8854 414.9923 46.2285 -4.8011 399.1866 403.9877 414.8744 46.9910 -4.7924 399.2860 404.0784 414.7625 47.8435 -4.7860 399.3934 404.1793 414.6476 48.6355 -4.7827 399.5050 404.2877 414.5167 49.4268 -4.7764 399.6108 404.3872 414.3999 50.2473 -4.7670 399.7076 404.4746 414.2934 51.0088 -4.7621 399.7906 404.5527 414.1773 51.8610 -4.7582 399.9234 404.6816 414.0795 52.6520 -4.7546 400.0123 404.7669 413.9699 53.4433 -4.7460 400.1018 404.8477 413.8713 54.2640 -4.7359 400.2158 404.9517 413.7562 55.0255 -4.7317 400.3122 405.0439 413.6429 55.8780 -4.7245 400.3971 405.1216 413.5289 56.6398 -4.7181 400.4680 405.1861 413.4376 57.4618 -4.7109 400.5740 405.2849 413.3490 58.2843 -4.7028 400.6632 405.3660 413.2299 59.0443 -4.6963 400.7656 405.4619 413.1259 59.8955 -4.6892 400.8713 405.5605 413.0214 60.6565 -4.6867 400.9630 405.6496 412.9409 61.4785 -4.6841 401.0506 405.7347 412.8471 62.2995 -4.6740 401.1339 405.8079 412.7520 63.0615 -4.6685 401.1986 405.8671 412.6672 63.9135 -4.6602 401.3038 405.9641 412.5712 64.6755 -4.6561 401.3697 406.0257 412.4736 65.4970 -4.6484 401.4488 406.0972 412.3920 66.2893 -4.6439 401.5273 406.1711 412.3148 67.0805 -4.6394 401.6378 406.2772 412.2141 67.9083 -4.6329 401.7173 406.3503 412.1368 68.6683 -4.6252 401.7926 406.4177 412.0531 69.5195 -4.6160 401.8667 406.4827 411.9803 70.3103 -4.6120 401.9380 406.5499 411.8990 71.1008 -4.6064 402.0214 406.6278 411.8237 71.9215 -4.5995 402.1193 406.7188 411.7412 72.6833 -4.5960 402.1726 406.7685 411.6710 73.5345 -4.5906 402.2521 406.8427 411.5997 74.2965 -4.5863 402.3242 406.9106 411.4882 75.1183 -4.5790 402.4020 406.9811 411.4133 75.9405 -4.5725 402.4800 407.0525 411.3431 76.7003 -4.5661 402.5501 407.1162 411.2599 77.5500 -4.5554 402.6289 407.1843 411.1794 78.3103 -4.5539 402.7047 407.2587 411.0923 79.1310 -4.5475 402.7694 407.3170 410.9935 79.9510 -4.5397 402.8252 407.3649 410.9043 80.7123 -4.5365 402.9014 407.4379 410.8204 81.5640 -4.5271 402.9650 407.4921 410.7478 82.3240 -4.5206 403.0406 407.5612 410.6771 83.1440 -4.5128 403.1174 407.6303 410.6003 83.9340 -4.5116 403.1879 407.6995 410.5331 84.7240 -4.5075 403.2439 407.7513 410.4579 85.5750 -4.4984 403.2901 407.7884 410.3757 86.3365 -4.4905 403.3728 407.8633 410.2961 87.1585 -4.4853 403.4226 407.9079 410.2068 87.9270 -4.4804 403.4676 407.9480 410.1226 88.7553 -4.4767 403.5546 408.0313 410.0392 89.5758 -4.4696 403.6268 408.0965 409.9311 90.3368 -4.4666 403.6722 408.1388 409.8490 91.1883 -4.4601 403.7244 408.1845 409.7667 91.9495 -4.4491 403.7725 408.2217 409.6703 92.7708 -4.4384 403.8291 408.2675 409.5821 93.5905 -4.4361 403.8984 408.3346 409.5074 94.3518 -4.4314 403.9464 408.3778 409.4216 95.2018 -4.4249 404.0129 408.4378 409.3226 95.9618 -4.4208 404.0732 408.4940 409.2354 96.7830 -4.4151 404.1227 408.5378 409.1449 97.5735 -4.4088 404.1809 408.5897 409.0464 98.3653 -4.4021 404.2264 408.6285 408.9806 99.2175 -4.3957 404.2652 408.6609 408.8473 99.9788 -4.3922 404.3102 408.7024 408.7564 100.7985 -4.3848 404.3682 408.7530 408.6873 101.5895 -4.3791 404.4223 408.8013 408.5723 102.3795 -4.3739 404.4607 408.8346 408.4870 103.2303 -4.3649 404.5168 408.8816 408.3953 103.9910 -4.3576 404.5563 408.9140 408.2892 104.8128 -4.3512 404.6112 408.9624 408.1771 105.6050 -4.3444 404.6447 408.9891 408.0991 106.3950 -4.3387 404.6934 409.0321 408.0100 107.2160 -4.3357 404.7393 409.0750 407.8932 108.0060 -4.3277 404.7856 409.1132 407.7872 108.8270 -4.3180 404.8110 409.1290 407.6816 109.6160 -4.3128 404.8772 409.1900 407.5960 110.4065 -4.3078 404.9132 409.2210 407.5122 111.2580 -4.2991 404.9428 409.2420 407.4101 112.0188 -4.2951 404.9962 409.2913 407.2946 112.8403 -4.2916 405.0288 409.3204 407.1907 113.6305 -4.2804 405.0621 409.3425 407.1001 114.4213 -4.2708 405.1053 409.3761 407.0034 115.2425 -4.2667 405.1389 409.4056 406.9050 116.0323 -4.2622 405.1883 409.4505 406.7988 116.8528 -4.2567 405.2224 409.4790 406.6880 117.6425 -4.2494 405.2351 409.4845 406.5820 118.4338 -4.2441 405.2803 409.5244 406.5241 119.2550 -4.2333 405.3059 409.5392 406.4153 120.0460 -4.2282 405.3228 409.5510 406.3283 120.8675 -4.2223 405.3686 409.5909 406.2299 121.6595 -4.2160 405.4111 409.6270 406.1174 122.4508 -4.2101 405.4350 409.6451 406.0277 123.2725 -4.2077 405.4611 409.6689 405.9610 124.0333 -4.2012 405.4877 409.6889 405.8695 124.8855 -4.1950 405.5126 409.7076 405.7673 125.6745 -4.1892 405.5561 409.7453 405.6605 126.4663 -4.1855 405.5744 409.7599 405.5511 127.2873 -4.1765 405.5999 409.7764 405.4729 128.0480 -4.1723 405.6350 409.8073 405.3850 128.9003 -4.1709 405.6554 409.8263 405.2793 129.6913 -4.1636 405.6791 409.8427 405.1890 130.4825 -4.1578 405.6917 409.8495 405.0930 131.3040 -4.1503 405.7179 409.8682 404.9867 132.0640 -4.1414 405.7410 409.8824 404.9005 132.9158 -4.1382 405.7663 409.9045 404.7964 133.7063 -4.1345 405.7665 409.9010 404.6969 134.4963 -4.1281 405.7819 409.9100 404.5960 135.3170 -4.1242 405.7977 409.9220 404.4994 136.1065 -4.1146 405.8227 409.9373 404.3842 136.9275 -4.1087 405.8581 409.9668 404.2704 137.7168 -4.1016 405.8663 409.9680 404.1940 138.5085 -4.0987 405.8791 409.9778 404.1031 139.3305 -4.0926 405.8946 409.9873 404.0051 140.1203 -4.0903 405.8962 409.9865 403.9213 140.9415 -4.0825 405.9200 410.0025 403.8278 141.7318 -4.0764 405.9425 410.0189 403.7154 142.5228 -4.0704 405.9736 410.0440 403.6081 143.3445 -4.0671 405.9882 410.0553 403.5134 144.1355 -4.0622 405.9842 410.0464 403.4096 144.9565 -4.0550 405.9947 410.0496 403.3086 145.7485 -4.0512 405.9922 410.0434 403.2307 146.5405 -4.0472 406.0094 410.0566 403.1487 147.3615 -4.0399 406.0164 410.0563 403.0477 148.1520 -4.0327 406.0438 410.0765 402.9387 148.9733 -4.0269 406.0382 410.0651 402.8462 149.7625 -4.0210 406.0531 410.0741 402.7455 150.5528 -4.0163 406.0574 410.0737 402.6514 151.3745 -4.0146 406.0756 410.0903 402.5647 152.1665 -4.0093 406.0838 410.0931 402.4587 152.9883 -4.0021 406.0893 410.0914 402.3813 153.7803 -3.9973 406.0895 410.0868 402.2961 154.5713 -3.9932 406.0915 410.0846 402.1833 155.3933 -3.9891 406.0961 410.0852 402.1053 156.1538 -3.9868 406.0894 410.0762 402.0195 157.0060 -3.9758 406.1080 410.0838 401.9173 157.7970 -3.9683 406.0931 410.0614 401.8153 158.5883 -3.9660 406.0931 410.0590 401.7284 159.4100 -3.9597 406.1035 410.0632 401.6190 160.1710 -3.9556 406.1186 410.0741 401.5289 161.0230 -3.9497 406.1078 410.0575 401.4252 161.8143 -3.9472 406.0939 410.0411 401.3330 162.6055 -3.9419 406.0777 410.0196 401.2389 163.4278 -3.9340 406.0927 410.0267 401.1537 164.1895 -3.9308 406.0842 410.0151 401.0457 165.0413 -3.9233 406.0824 410.0058 400.9379 165.8318 -3.9158 406.0746 409.9904 400.8450 166.6233 -3.9119 406.0797 409.9916 400.7605 167.4445 -3.9108 406.0728 409.9836 400.6556 168.2343 -3.9059 406.0672 409.9731 400.5559 169.0555 -3.9000 406.0598 409.9598 400.4752 169.8455 -3.8931 406.0557 409.9488 400.3627 170.6358 -3.8886 406.0532 409.9418 400.2793 171.4560 -3.8850 406.0695 409.9545 400.1712 172.2458 -3.8804 406.0508 409.9312 400.0732 173.0670 -3.8774 406.0289 409.9063 399.9810 173.8585 -3.8743 406.0109 409.8852 399.9063 174.6505 -3.8697 406.0107 409.8804 399.8102 175.4725 -3.8631 406.0209 409.8840 399.6987 176.2645 -3.8579 405.9935 409.8513 399.5925 177.0865 -3.8564 405.9776 409.8340 399.5095 177.8775 -3.8512 405.9457 409.7969 399.4160 178.6695 -3.8450 405.9282 409.7732 399.3481 179.4913 -3.8377 405.9373 409.7751 399.2340 180.2813 -3.8342 405.9278 409.7619 399.1437 181.1015 -3.8314 405.9204 409.7518 399.0525 181.8920 -3.8253 405.8944 409.7197 398.9558 182.6823 -3.8199 405.8830 409.7029 398.8515 183.5040 -3.8153 405.8844 409.6997 398.7636 184.2935 -3.8121 405.8635 409.6756 398.6561 185.1148 -3.8081 405.8429 409.6510 398.5703 185.9070 -3.8022 405.8312 409.6334 398.4862 186.6975 -3.7970 405.8073 409.6043 398.3670 187.5190 -3.7919 405.7903 409.5822 398.2746 188.3098 -3.7875 405.7744 409.5619 398.1775 189.1310 -3.7845 405.7622 409.5466 398.0871 189.9205 -3.7808 405.7342 409.5150 397.9928 190.7123 -3.7778 405.7096 409.4874 397.9048 191.5635 -3.7728 405.6893 409.4621 397.7855 192.3245 -3.7647 405.6726 409.4373 397.6978 193.1465 -3.7611 405.6481 409.4093 397.5933 193.9373 -3.7555 405.6227 409.3783 397.5168 194.7275 -3.7496 405.6176 409.3672 397.4038 195.5488 -3.7463 405.5715 409.3178 397.3232 196.3390 -3.7411 405.5569 409.2980 397.2303 197.1603 -3.7385 405.5499 409.2884 397.1191 197.9515 -3.7319 405.5294 409.2613 397.0319 198.7425 -3.7180 405.4991 409.2171 396.9309 199.5645 -3.7120 405.4618 409.1739 396.8467 200.3565 -3.7168 405.4404 409.1572 396.7412 201.1783 -3.7133 405.4228 409.1361 396.6777 201.9698 -3.7091 405.4027 409.1118 396.5756 202.7620 -3.7070 405.3723 409.0793 396.4675 203.5835 -3.7017 405.3253 409.0270 396.3709 204.3445 -3.6953 405.3100 409.0052 396.2733 205.1958 -3.6869 405.2729 408.9598 396.1815 205.9863 -3.6824 405.2472 408.9297 396.0931 206.7775 -3.6824 405.2256 408.9081 395.9752 207.6000 -3.6799 405.1955 408.8754 395.8932 208.3600 -3.6759 405.1653 408.8412 395.8029 209.2120 -3.6701 405.1302 408.8003 395.7092 209.9738 -3.6657 405.0981 408.7638 395.6002 210.7958 -3.6590 405.0828 408.7418 395.5078 211.6180 -3.6560 405.0605 408.7165 395.4163 212.3783 -3.6533 405.0253 408.6786 395.3091 213.2298 -3.6474 404.9913 408.6387 395.2027 213.9888 -3.6456 404.9603 408.6059 395.1271 214.8090 -3.6413 404.9370 408.5783 395.0171 215.6308 -3.6345 404.8944 408.5289 394.8874 216.3918 -3.6327 404.8592 408.4919 394.8064 217.2435 -3.6301 404.8399 408.4700 394.6778 218.0038 -3.6212 404.8034 408.4245 394.5882 218.8250 -3.6206 404.7628 408.3834 394.5072 219.6458 -3.6142 404.7494 408.3636 394.4310 220.4065 -3.6111 404.6968 408.3080 394.3249 221.2585 -3.6058 404.6624 408.2682 394.2049 222.0188 -3.6019 404.6274 408.2294 394.1098 222.8405 -3.6007 404.5877 408.1884 394.0200 223.6325 -3.5970 404.5502 408.1471 393.9115 224.4238 -3.5912 404.5077 408.0989 393.8075 225.2445 -3.5896 404.4747 408.0644 393.7051 226.0358 -3.5850 404.4541 408.0392 393.6074 226.8575 -3.5778 404.4298 408.0076 393.5258 227.6495 -3.5731 404.3986 407.9717 393.4383 228.4415 -3.5684 404.3544 407.9227 393.3148 229.2633 -3.5669 404.3161 407.8830 393.2164 230.0245 -3.5665 404.2864 407.8529 393.1378 230.8758 -3.5618 404.2270 407.7888 393.0438 231.6650 -3.5592 404.1721 407.7313 392.9511 232.4555 -3.5538 404.1396 407.6934 392.8398 233.2773 -3.5487 404.1004 407.6491 392.7474 234.0380 -3.5467 404.0502 407.5969 392.6629 234.8900 -3.5425 403.9967 407.5392 392.5770 235.6508 -3.5379 403.9904 407.5283 392.4814 236.4728 -3.5336 403.9395 407.4731 392.3699 237.2940 -3.5270 403.8955 407.4225 392.2531 238.0555 -3.5252 403.8595 407.3846 392.1549 238.9078 -3.5195 403.8175 407.3370 392.0616 239.6690 -3.5139 403.7873 407.3012 391.9712 240.4905 -3.5139 403.7367 407.2506 391.8777 241.2808 -3.5108 403.6826 407.1934 391.7657 242.0710 -3.5055 403.6236 407.1291 391.6775 242.9215 -3.5023 403.6042 407.1065 391.5593 243.6828 -3.4982 403.5577 407.0559 391.4696 244.5038 -3.4929 403.4810 406.9738 391.3735 245.2935 -3.4913 403.4592 406.9505 391.2513 246.0840 -3.4883 403.4098 406.8981 391.1586 246.9343 -3.4828 403.3655 406.8483 391.0444 247.6943 -3.4806 403.3143 406.7948 390.9620 248.5153 -3.4760 403.2652 406.7412 390.8517 249.3063 -3.4687 403.2270 406.6957 390.7559 250.1000 -3.4657 403.1741 406.6398 390.6506 250.9508 -3.4641 403.1369 406.6010 390.5605 251.7103 -3.4590 403.0831 406.5420 390.4572 252.5305 -3.4580 403.0339 406.4919 390.3452 253.3225 -3.4560 402.9771 406.4331 390.2490 254.1143 -3.4470 402.9322 406.3793 390.1427 254.9355 -3.4448 402.8914 406.3362 390.0497 255.7253 -3.4418 402.8323 406.2741 389.9344 256.5470 -3.4418 402.7924 406.2343 389.8319 257.3395 -3.4386 402.7301 406.1687 389.7456 258.1305 -3.4318 402.6873 406.1192 389.6453 258.9530 -3.4270 402.6489 406.0759 389.5219 259.7425 -3.4209 402.5872 406.0081 389.4277 260.5628 -3.4146 402.5436 405.9582 389.3208 261.3550 -3.4130 402.4890 405.9020 389.2254 262.1465 -3.4158 402.4502 405.8660 389.1301 262.9690 -3.4112 402.3724 405.7836 389.0277 263.7585 -3.4085 402.3371 405.7456 388.9316 264.5793 -3.4068 402.3001 405.7069 388.8210 265.3710 -3.4011 402.2387 405.6398 388.7226 266.1628 -3.3982 402.1588 405.5570 388.6460 266.9848 -3.3951 402.1035 405.4986 388.5477 267.7465 -3.3913 402.0580 405.4493 388.4578 268.5985 -3.3838 401.9867 405.3706 388.3365 269.3898 -3.3796 401.9419 405.3215 388.2418 270.1800 -3.3749 401.8992 405.2742 388.1319 271.0015 -3.3698 401.8343 405.2041 388.0274 271.7630 -3.3686 401.7842 405.1527 387.9435 272.6145 -3.3628 401.7248 405.0876 387.8511 273.4058 -3.3589 401.6708 405.0296 387.7542 274.1973 -3.3521 401.6146 404.9667 387.6738 275.0175 -3.3534 401.5610 404.9144 387.5714 275.7773 -3.3526 401.5282 404.8809 387.4721 276.6285 -3.3502 401.4624 404.8126 387.3716 277.4193 -3.3479 401.4061 404.7539 387.2929 278.2100 -3.3455 401.3374 404.6829 387.2084 279.0300 -3.3387 401.2763 404.6150 387.0775 279.7910 -3.3365 401.2252 404.5617 386.9769 280.6443 -3.3336 401.1917 404.5252 386.8772 281.4365 -3.3303 401.1099 404.4402 386.7709 282.2270 -3.3227 401.0442 404.3669 386.6991 283.0458 -3.3165 400.9878 404.3042 386.5911 283.8053 -3.3149 400.9201 404.2349 386.4949 284.6578 -3.3109 400.8718 404.1827 386.3719 285.4493 -3.3084 400.8171 404.1255 386.2851 286.2405 -3.3062 400.7472 404.0534 386.1686 287.0630 -3.3014 400.7116 404.0131 386.0702 287.8245 -3.2983 400.6407 403.9390 385.9749 288.6768 -3.2941 400.5672 403.8613 385.8632 289.4678 -3.2906 400.5083 403.7989 385.7650 290.2580 -3.2876 400.4596 403.7472 385.6692 291.0800 -3.2836 400.3951 403.6787 385.5559 291.8405 -3.2835 400.3251 403.6086 385.4615 292.6925 -3.2764 400.2786 403.5549 385.3582 293.4818 -3.2730 400.2170 403.4900 385.2656 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