DTA measure 1olom Date: 2024423:1056 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 853.21 s Mass = 953.800 mg data_number = 1062 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3465 -1.9544 229.1842 231.1386 262.6188 2.1703 -1.9480 229.3287 231.2767 262.6340 2.9615 -1.9452 229.4842 231.4293 262.6573 3.7525 -1.9439 229.6493 231.5932 262.6630 4.6035 -1.9379 229.8354 231.7734 262.6658 5.3655 -1.9332 229.9602 231.8934 262.6866 6.1860 -1.9293 230.1071 232.0365 262.6919 6.9775 -1.9257 230.2524 232.1780 262.7276 7.7688 -1.9216 230.4028 232.3244 262.7302 8.6205 -1.9174 230.5633 232.4807 262.7336 9.3815 -1.9139 230.7032 232.6171 262.7251 10.2025 -1.9105 230.8646 232.7751 262.7602 10.9945 -1.9060 230.9975 232.9035 262.7696 11.7843 -1.9018 231.1437 233.0455 262.7947 12.6360 -1.8986 231.3172 233.2158 262.8272 13.3970 -1.8954 231.4592 233.3545 262.8638 14.2170 -1.8924 231.6069 233.4993 262.8900 15.0370 -1.8903 231.7382 233.6285 262.9696 15.7985 -1.8866 231.8730 233.7597 263.0026 16.6510 -1.8808 232.0183 233.8991 263.0838 17.4123 -1.8800 232.1685 234.0485 263.1547 18.2333 -1.8801 232.3407 234.2208 263.2148 19.0540 -1.8783 232.4792 234.3574 263.2827 19.8145 -1.8729 232.6184 234.4913 263.3559 20.6668 -1.8628 232.7539 234.6167 263.4545 21.4278 -1.8607 232.9021 234.7627 263.5377 22.2493 -1.8586 233.0305 234.8892 263.6376 23.0408 -1.8600 233.1710 235.0310 263.7298 23.8310 -1.8571 233.3078 235.1649 263.8477 24.6815 -1.8541 233.4668 235.3210 263.9832 25.4428 -1.8500 233.6072 235.4572 264.0709 26.2630 -1.8460 233.7271 235.5731 264.1803 27.0835 -1.8436 233.8848 235.7284 264.3132 27.8448 -1.8440 234.0016 235.8456 264.4584 28.6958 -1.8436 234.1559 235.9995 264.6284 29.4575 -1.8462 234.2845 236.1307 264.7514 30.2790 -1.8427 234.4209 236.2636 264.9005 31.0990 -1.8369 234.5634 236.4003 265.0622 31.8583 -1.8375 234.6987 236.5362 265.2221 32.7095 -1.8342 234.8419 236.6761 265.3643 33.4715 -1.8362 234.9714 236.8076 265.5188 34.2933 -1.8364 235.1050 236.9414 265.7123 35.1135 -1.8315 235.2378 237.0693 265.8622 35.8735 -1.8326 235.3820 237.2146 266.0121 36.7248 -1.8291 235.5313 237.3604 266.1891 37.5143 -1.8274 235.6569 237.4843 266.3690 38.3050 -1.8284 235.7858 237.6143 266.5409 39.1270 -1.8284 235.9090 237.7374 266.6961 39.8880 -1.8304 236.0231 237.8535 266.8738 40.7388 -1.8283 236.1636 237.9919 267.0435 41.5293 -1.8288 236.2918 238.1206 267.2246 42.3198 -1.8230 236.4254 238.2484 267.4154 43.1400 -1.8210 236.5807 238.4017 267.5891 43.9000 -1.8250 236.7176 238.5426 267.7483 44.7518 -1.8259 236.8434 238.6693 267.9290 45.5413 -1.8235 236.9849 238.8084 268.1165 46.3325 -1.8263 237.1000 238.9263 268.3033 47.1545 -1.8254 237.2450 239.0704 268.4529 47.9158 -1.8270 237.3734 239.2004 268.5848 48.7683 -1.8252 237.5062 239.3314 268.7642 49.5578 -1.8268 237.6388 239.4656 268.9436 50.3488 -1.8268 237.7537 239.5805 269.1263 51.1685 -1.8256 237.9105 239.7361 269.2863 51.9300 -1.8295 238.0335 239.8631 269.4258 52.7815 -1.8317 238.1654 239.9971 269.6279 53.5428 -1.8338 238.2947 240.1285 269.7735 54.3643 -1.8366 238.4124 240.2490 269.9160 55.1845 -1.8385 238.5488 240.3873 270.0757 55.9458 -1.8383 238.6700 240.5083 270.2216 56.7965 -1.8416 238.8021 240.6436 270.3793 57.5573 -1.8418 238.9310 240.7728 270.5400 58.3785 -1.8443 239.0574 240.9017 270.7002 59.1695 -1.8421 239.2103 241.0524 270.8427 59.9605 -1.8458 239.3343 241.1800 270.9880 60.8115 -1.8436 239.4537 241.2972 271.1269 61.5728 -1.8468 239.5802 241.4270 271.2630 62.3930 -1.8473 239.7278 241.5750 271.3917 63.1840 -1.8421 239.8530 241.6951 271.5366 63.9730 -1.8405 239.9783 241.8188 271.6740 64.7943 -1.8438 240.1023 241.9461 271.7866 65.5858 -1.8474 240.2201 242.0675 271.9102 66.4078 -1.8477 240.3536 242.2013 272.0264 67.1993 -1.8527 240.4975 242.3502 272.1638 67.9898 -1.8550 240.6182 242.4732 272.2783 68.8120 -1.8544 240.7392 242.5936 272.4155 69.5735 -1.8551 240.8454 242.7005 272.5273 70.4260 -1.8538 240.9853 242.8391 272.6497 71.1870 -1.8515 241.1330 242.9845 272.7670 72.0080 -1.8511 241.2594 243.1106 272.8929 72.8268 -1.8541 241.3812 243.2354 273.0044 73.5873 -1.8551 241.4914 243.3465 273.0874 74.4383 -1.8606 241.6271 243.4877 273.2197 75.1978 -1.8568 241.7383 243.5951 273.3350 76.0190 -1.8563 241.8917 243.7480 273.4627 76.8095 -1.8608 242.0005 243.8613 273.5574 77.6013 -1.8660 242.1206 243.9866 273.6525 78.4525 -1.8664 242.2684 244.1347 273.7583 79.2130 -1.8716 242.3804 244.2519 273.8614 80.0345 -1.8746 242.4949 244.3696 273.9813 80.8258 -1.8737 242.6342 244.5080 274.0859 81.6168 -1.8728 242.7585 244.6313 274.2087 82.4685 -1.8740 242.8856 244.7596 274.3368 83.2288 -1.8742 243.0193 244.8935 274.4234 84.0503 -1.8750 243.1444 245.0195 274.5323 84.8405 -1.8753 243.2704 245.1457 274.6307 85.6318 -1.8764 243.3762 245.2526 274.7570 86.4825 -1.8769 243.5176 245.3944 274.8656 87.2430 -1.8769 243.6258 245.5027 274.9617 88.0638 -1.8808 243.7745 245.6553 275.0756 88.8545 -1.8828 243.8902 245.7729 275.2023 89.6448 -1.8853 244.0236 245.9089 275.3289 90.4960 -1.8860 244.1359 246.0220 275.4552 91.2570 -1.8863 244.2520 246.1383 275.5458 92.0788 -1.8836 244.3718 246.2554 275.6741 92.8700 -1.8828 244.5033 246.3860 275.8143 93.6603 -1.8818 244.6245 246.5064 275.9176 94.5120 -1.8810 244.7606 246.6416 276.0428 95.2725 -1.8842 244.8669 246.7512 276.1539 96.0935 -1.8883 244.9880 246.8763 276.2673 96.8850 -1.8924 245.1312 247.0236 276.4045 97.6750 -1.8937 245.2525 247.1462 276.5173 98.5245 -1.8926 245.3850 247.2776 276.6578 99.2838 -1.8966 245.5175 247.4141 276.7692 100.1055 -1.8977 245.6191 247.5168 276.9352 100.8975 -1.8992 245.7254 247.6246 277.0446 101.6888 -1.9019 245.8482 247.7501 277.1699 102.5395 -1.9004 246.0079 247.9083 277.3019 103.2998 -1.9045 246.1098 248.0143 277.4420 104.1215 -1.9089 246.2370 248.1459 277.5672 104.9135 -1.9090 246.3681 248.2771 277.7136 105.7055 -1.9110 246.4661 248.3771 277.8571 106.5275 -1.9119 246.5946 248.5065 277.9914 107.2910 -1.9114 246.7102 248.6216 278.1128 108.1445 -1.9160 246.8400 248.7559 278.2658 108.9358 -1.9155 246.9666 248.8821 278.4282 109.7273 -1.9157 247.0711 248.9868 278.5278 110.5485 -1.9179 247.2233 249.1412 278.6531 111.3105 -1.9201 247.3305 249.2506 278.7941 112.1620 -1.9236 247.4443 249.3680 278.9260 112.9528 -1.9251 247.5835 249.5085 279.0861 113.7488 -1.9273 247.7217 249.6490 279.2207 114.5443 -1.9279 247.8222 249.7501 279.3590 115.3348 -1.9294 247.9467 249.8761 279.4824 116.1860 -1.9306 248.0888 250.0194 279.6372 116.9460 -1.9342 248.2040 250.1382 279.7733 117.7673 -1.9350 248.3190 250.2541 279.9133 118.5880 -1.9365 248.4411 250.3776 280.0628 119.3495 -1.9383 248.5604 250.4987 280.2183 120.2020 -1.9438 248.6824 250.6262 280.3201 120.9640 -1.9441 248.7887 250.7329 280.4493 121.7853 -1.9462 248.9122 250.8584 280.6041 122.6063 -1.9470 249.0502 250.9972 280.7338 123.3663 -1.9530 249.1646 251.1176 280.8794 124.2175 -1.9528 249.2896 251.2425 281.0220 124.9778 -1.9538 249.4189 251.3726 281.1477 125.7990 -1.9549 249.5249 251.4798 281.2943 126.6185 -1.9564 249.6650 251.6214 281.4292 127.3798 -1.9591 249.7769 251.7359 281.5561 128.2315 -1.9621 249.9017 251.8639 281.7181 128.9935 -1.9623 250.0345 251.9967 281.8432 129.8148 -1.9675 250.1443 252.1118 281.9785 130.6355 -1.9686 250.2694 252.2380 282.1331 131.3975 -1.9722 250.3732 252.3455 282.2643 132.2495 -1.9747 250.5028 252.4775 282.3993 133.0115 -1.9777 250.6080 252.5857 282.5315 133.8330 -1.9783 250.7224 252.7007 282.6748 134.6258 -1.9785 250.8507 252.8292 282.8268 135.4485 -1.9796 251.0124 252.9920 282.9633 136.2395 -1.9838 251.1192 253.1031 283.0948 137.0313 -1.9845 251.2298 253.2144 283.2260 137.8525 -1.9877 251.3530 253.3407 283.3564 138.6130 -1.9914 251.4745 253.4659 283.4793 139.4643 -1.9921 251.6038 253.5959 283.6170 140.2553 -1.9953 251.7101 253.7053 283.7580 141.0463 -1.9979 251.8495 253.8474 283.9030 141.8683 -1.9982 251.9624 253.9606 284.0412 142.6293 -2.0017 252.0739 254.0755 284.1722 143.4810 -2.0012 252.1868 254.1881 284.3345 144.2723 -2.0038 252.3042 254.3079 284.4499 145.0625 -2.0040 252.4246 254.4286 284.5625 145.8840 -2.0101 252.5460 254.5561 284.6987 146.6745 -2.0124 252.6903 254.7027 284.8379 147.4953 -2.0119 252.8277 254.8397 284.9750 148.2870 -2.0150 252.9496 254.9646 285.1135 149.0783 -2.0188 253.0716 255.0904 285.2143 149.8998 -2.0194 253.1969 255.2163 285.3479 150.6610 -2.0227 253.3081 255.3307 285.4835 151.5128 -2.0261 253.4380 255.4641 285.6334 152.3028 -2.0259 253.5604 255.5863 285.7329 153.0943 -2.0274 253.6792 255.7066 285.8519 153.9158 -2.0302 253.7922 255.8224 285.9995 154.6945 -2.0329 253.9314 255.9643 286.1273 155.5338 -2.0328 254.0420 256.0748 286.2550 156.2950 -2.0368 254.1687 256.2055 286.3790 157.1463 -2.0399 254.3152 256.3551 286.5047 157.9068 -2.0418 254.4086 256.4504 286.6189 158.7283 -2.0460 254.5339 256.5799 286.7563 159.5495 -2.0407 254.6616 256.7023 286.9041 160.3123 -2.0292 254.7777 256.8068 287.0267 161.1695 -2.0298 254.9148 256.9447 287.1586 161.9620 -2.0293 255.0212 257.0505 287.2745 162.7555 -2.0423 255.1506 257.1928 287.4027 163.5775 -2.0477 255.2732 257.3210 287.5068 164.3383 -2.0502 255.4030 257.4531 287.6315 165.1893 -2.0527 255.5176 257.5704 287.7486 165.9805 -2.0530 255.6430 257.6961 287.8779 166.7715 -2.0551 255.7654 257.8205 288.0120 167.5940 -2.0478 255.8808 257.9286 288.1297 168.3538 -2.0413 255.9914 258.0327 288.2501 169.2038 -2.0445 256.1185 258.1630 288.3877 169.9950 -2.0576 256.2502 258.3078 288.4989 170.7868 -2.0605 256.3660 258.4265 288.6075 171.6090 -2.0593 256.4995 258.5589 288.7405 172.3698 -2.0656 256.6385 258.7041 288.8607 173.2195 -2.0651 256.7513 258.8163 288.9900 174.0103 -2.0768 256.8586 258.9354 289.1197 174.8005 -2.0852 256.9823 259.0675 289.2134 175.6218 -2.0834 257.1253 259.2086 289.3538 176.3820 -2.0894 257.2180 259.3074 289.4590 177.2335 -2.0906 257.3543 259.4449 289.5800 177.9948 -2.0961 257.4679 259.5640 289.6875 178.8165 -2.1013 257.5862 259.6875 289.8017 179.6385 -2.1032 257.7189 259.8222 289.9585 180.3993 -2.1065 257.8231 259.9296 290.0639 181.2505 -2.1066 257.9711 260.0777 290.1712 182.0125 -2.1087 258.0812 260.1898 290.3030 182.8340 -2.1097 258.2053 260.3150 290.4306 183.6555 -2.1130 258.3270 260.4401 290.5482 184.4175 -2.1125 258.4463 260.5588 290.6545 185.2695 -2.1148 258.5904 260.7052 290.7820 186.0315 -2.1175 258.6983 260.8158 290.9221 186.8530 -2.1212 258.8138 260.9350 291.0692 187.6435 -2.1232 258.9387 261.0619 291.2016 188.4353 -2.1273 259.0623 261.1896 291.3229 189.2565 -2.1296 259.1969 261.3265 291.4718 190.0475 -2.1322 259.3152 261.4474 291.5976 190.8680 -2.1351 259.4420 261.5771 291.7382 191.6585 -2.1352 259.5572 261.6924 291.8651 192.4485 -2.1358 259.6745 261.8103 291.9810 193.2703 -2.1376 259.7965 261.9341 292.1197 194.0618 -2.1393 259.9342 262.0735 292.2510 194.8835 -2.1386 260.0522 262.1908 292.3886 195.6750 -2.1439 260.1972 262.3411 292.5376 196.4660 -2.1471 260.3107 262.4578 292.6626 197.2860 -2.1475 260.4333 262.5808 292.7919 198.0460 -2.1509 260.5323 262.6832 292.9240 198.8978 -2.1504 260.6841 262.8346 293.0919 199.6880 -2.1545 260.8005 262.9550 293.1980 200.4793 -2.1585 260.9183 263.0767 293.3254 201.3008 -2.1545 261.0455 263.2000 293.4774 202.0625 -2.1508 261.1525 263.3033 293.6202 202.9148 -2.1622 261.2710 263.4332 293.7697 203.6775 -2.1682 261.3966 263.5648 293.8823 204.4990 -2.1698 261.5281 263.6978 294.0194 205.2920 -2.1725 261.6603 263.8328 294.1715 206.0848 -2.1770 261.7866 263.9636 294.3113 206.9065 -2.1798 261.8907 264.0705 294.4305 207.6963 -2.1747 262.0265 264.2012 294.5693 208.5175 -2.1827 262.1414 264.3241 294.7217 209.3088 -2.1876 262.2746 264.4622 294.8354 210.0995 -2.1892 262.3947 264.5839 294.9629 210.9200 -2.1925 262.5088 264.7013 295.1140 211.7093 -2.1947 262.6468 264.8415 295.2398 212.5300 -2.1956 262.7541 264.9497 295.3830 213.3205 -2.1981 262.8764 265.0745 295.4949 214.1125 -2.2017 263.0069 265.2086 295.6240 214.9345 -2.2060 263.1465 265.3526 295.7653 215.6960 -2.2049 263.2333 265.4382 295.8785 216.5473 -2.2069 263.3782 265.5850 296.0153 217.3385 -2.2080 263.5047 265.7127 296.1695 218.1290 -2.2118 263.6311 265.8429 296.3233 218.9503 -2.2147 263.7473 265.9620 296.4686 219.7105 -2.2171 263.8982 266.1153 296.5816 220.5620 -2.2203 264.0071 266.2274 296.7206 221.3220 -2.2203 264.1152 266.3355 296.8431 222.1438 -2.2232 264.2543 266.4775 296.9752 222.9660 -2.2264 264.3873 266.6137 297.1135 223.7270 -2.2319 264.4979 266.7298 297.2463 224.5790 -2.2334 264.6229 266.8563 297.3839 225.3400 -2.2349 264.7657 267.0006 297.5066 226.1610 -2.2372 264.8805 267.1176 297.6440 226.9520 -2.2353 264.9834 267.2187 297.7655 227.7430 -2.2389 265.1084 267.3473 297.9152 228.5958 -2.2434 265.2511 267.4945 298.0570 229.3558 -2.2478 265.3732 267.6209 298.1751 230.1775 -2.2521 265.4865 267.7386 298.3133 230.9695 -2.2536 265.6212 267.8748 298.4303 231.7610 -2.2526 265.7529 268.0056 298.5654 232.5820 -2.2570 265.8791 268.1362 298.7043 233.3718 -2.2624 265.9959 268.2583 298.8359 234.1933 -2.2637 266.1219 268.3856 298.9686 234.9835 -2.2629 266.2507 268.5135 299.0870 235.7740 -2.2666 266.3840 268.6506 299.2176 236.6245 -2.2682 266.5131 268.7813 299.3661 237.3860 -2.2724 266.6341 268.9065 299.4850 238.2070 -2.2718 266.7745 269.0463 299.6163 238.9958 -2.2742 266.8892 269.1633 299.7396 239.7868 -2.2795 267.0174 269.2969 299.8798 240.6375 -2.2826 267.1607 269.4434 300.0110 241.3983 -2.2836 267.2718 269.5553 300.1216 242.2188 -2.2869 267.3932 269.6800 300.2375 243.0095 -2.2895 267.5117 269.8012 300.3821 243.7998 -2.2889 267.6336 269.9225 300.5159 244.6210 -2.2913 267.7740 270.0653 300.6345 245.4128 -2.2910 267.8938 270.1848 300.7599 246.2348 -2.2942 268.0162 270.3104 300.8797 247.0260 -2.2988 268.1173 270.4161 301.0020 247.8163 -2.2973 268.2652 270.5625 301.1288 248.6380 -2.3024 268.3855 270.6878 301.2556 249.4283 -2.3063 268.4976 270.8038 301.3957 250.2495 -2.3051 268.6370 270.9420 301.5293 251.0403 -2.3063 268.7863 271.0926 301.6518 251.8305 -2.3082 268.9035 271.2117 301.7706 252.6520 -2.3110 269.0302 271.3413 301.8901 253.4428 -2.3140 269.1453 271.4593 302.0119 254.2645 -2.3193 269.2746 271.5939 302.1402 255.0558 -2.3203 269.4032 271.7235 302.2598 255.8460 -2.3218 269.5137 271.8354 302.3771 256.6668 -2.3235 269.6349 271.9584 302.5026 257.4570 -2.3267 269.7682 272.0949 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