DTA measure 1olom4 Date: 2024423:1143 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1033.05 s Mass = 953.800 mg data_number = 1286 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2505 -1.3597 250.2120 251.5717 262.9099 2.1013 -1.3599 250.2368 251.5967 262.8861 2.8605 -1.3606 250.2708 251.6313 262.8484 3.6845 -1.3568 250.3247 251.6815 262.8227 4.4770 -1.3571 250.3476 251.7047 262.7956 5.2670 -1.3576 250.3747 251.7323 262.7763 6.1178 -1.3599 250.3995 251.7594 262.7704 6.8643 -1.3630 250.4498 251.8127 262.7765 7.7153 -1.3598 250.4859 251.8457 262.7650 8.5055 -1.3600 250.5406 251.9006 262.7649 9.2975 -1.3588 250.5609 251.9196 262.7568 10.1185 -1.3597 250.5890 251.9487 262.7634 10.8798 -1.3613 250.6369 251.9983 262.7902 11.7313 -1.3620 250.6698 252.0318 262.8128 12.5225 -1.3610 250.7011 252.0621 262.8181 13.3145 -1.3620 250.7414 252.1034 262.8559 14.1360 -1.3612 250.7640 252.1252 262.8874 14.8965 -1.3605 250.7992 252.1598 262.9492 15.7473 -1.3588 250.8326 252.1914 262.9900 16.5378 -1.3615 250.8740 252.2355 263.0493 17.3280 -1.3599 250.9222 252.2820 263.1068 18.1485 -1.3620 250.9431 252.3051 263.1718 18.9390 -1.3620 250.9887 252.3507 263.2329 19.7605 -1.3616 251.0368 252.3985 263.3073 20.5515 -1.3612 251.0732 252.4344 263.3866 21.3420 -1.3607 251.1241 252.4848 263.4833 22.1633 -1.3657 251.1481 252.5138 263.5833 22.9523 -1.3658 251.1788 252.5445 263.6884 23.7728 -1.3675 251.2211 252.5886 263.7834 24.5638 -1.3664 251.2645 252.6309 263.8926 25.3530 -1.3658 251.2919 252.6577 264.0036 26.2040 -1.3699 251.3335 252.7035 264.1162 26.9678 -1.3690 251.3744 252.7434 264.2270 27.7908 -1.3670 251.4090 252.7760 264.3384 28.5820 -1.3690 251.4469 252.8159 264.4765 29.3733 -1.3728 251.4993 252.8721 264.6235 30.1950 -1.3752 251.5383 252.9135 264.7543 30.9863 -1.3761 251.5805 252.9565 264.9012 31.8070 -1.3808 251.6149 252.9956 265.0265 32.5963 -1.3862 251.6459 253.0321 265.1667 33.3873 -1.3874 251.7043 253.0917 265.2970 34.2385 -1.3853 251.7272 253.1125 265.4395 34.9983 -1.3854 251.7564 253.1418 265.6056 35.8190 -1.3878 251.8087 253.1965 265.7428 36.6095 -1.3893 251.8653 253.2546 265.9008 37.4008 -1.3903 251.8974 253.2877 266.0483 38.2505 -1.3901 251.9331 253.3232 266.2005 39.0115 -1.3938 251.9771 253.3709 266.3415 39.8330 -1.3929 252.0331 253.4260 266.5166 40.6245 -1.3971 252.0547 253.4518 266.6472 41.4158 -1.3976 252.1043 253.5020 266.7911 42.2663 -1.4008 252.1645 253.5653 266.9537 43.0275 -1.4040 252.2070 253.6110 267.0874 43.8490 -1.4041 252.2487 253.6528 267.2358 44.6405 -1.4065 252.3146 253.7210 267.3880 45.4318 -1.4113 252.3377 253.7491 267.5466 46.2835 -1.4148 252.3790 253.7937 267.6731 47.0455 -1.4182 252.4164 253.8346 267.8285 47.8665 -1.4171 252.4818 253.8989 267.9724 48.6575 -1.4196 252.5259 253.9455 268.0972 49.4483 -1.4212 252.5557 253.9768 268.2336 50.3000 -1.4213 252.6187 254.0400 268.3533 51.0608 -1.4279 252.6400 254.0679 268.4867 51.8823 -1.4340 252.6935 254.1275 268.6268 52.6730 -1.4355 252.7402 254.1757 268.7530 53.4633 -1.4388 252.7827 254.2215 268.8932 54.3150 -1.4391 252.8564 254.2955 269.0072 55.0768 -1.4428 252.8944 254.3372 269.1318 55.8985 -1.4445 252.9408 254.3853 269.2467 56.6890 -1.4454 252.9946 254.4400 269.3532 57.4903 -1.4488 253.0382 254.4870 269.4608 58.2808 -1.4514 253.0956 254.5470 269.5811 59.1020 -1.4528 253.1314 254.5842 269.6876 59.9235 -1.4534 253.1963 254.6496 269.7903 60.6850 -1.4591 253.2442 254.7032 269.8846 61.5373 -1.4595 253.2878 254.7473 270.0080 62.2978 -1.4623 253.3341 254.7964 270.1033 63.1190 -1.4629 253.3834 254.8463 270.2121 63.9395 -1.4647 253.4349 254.8996 270.3035 64.7005 -1.4683 253.4821 254.9504 270.4005 65.5518 -1.4684 253.5632 255.0315 270.5023 66.3125 -1.4744 253.5881 255.0625 270.5839 67.1335 -1.4761 253.6486 255.1246 270.6990 67.9245 -1.4783 253.6987 255.1769 270.7941 68.7163 -1.4794 253.7266 255.2061 270.8802 69.5675 -1.4815 253.8049 255.2864 270.9674 70.3283 -1.4815 253.8569 255.3385 271.0486 71.1495 -1.4861 253.9226 255.4086 271.1456 71.9415 -1.4876 253.9599 255.4475 271.2280 72.7330 -1.4885 253.9990 255.4876 271.3145 73.5843 -1.4917 254.0637 255.5553 271.4080 74.3453 -1.4956 254.1288 255.6243 271.4956 75.1663 -1.4982 254.1736 255.6718 271.5935 75.9583 -1.5016 254.2376 255.7392 271.6526 76.7485 -1.5014 254.2911 255.7925 271.7447 77.6000 -1.5012 254.3316 255.8328 271.8195 78.3618 -1.5028 254.3864 255.8893 271.8904 79.1828 -1.5050 254.4493 255.9543 272.0030 79.9738 -1.5093 254.5110 256.0202 272.0806 80.7645 -1.5129 254.5725 256.0854 272.1350 81.5870 -1.5172 254.6064 256.1235 272.2352 82.3778 -1.5183 254.6504 256.1687 272.3176 83.1995 -1.5202 254.7224 256.2426 272.4095 83.9905 -1.5247 254.7667 256.2914 272.4897 84.7820 -1.5257 254.8330 256.3586 272.5866 85.6025 -1.5198 254.8888 256.4086 272.6651 86.3645 -1.5230 254.9442 256.4672 272.7372 87.2165 -1.5275 254.9979 256.5254 272.8433 87.9775 -1.5293 255.0370 256.5663 272.9298 88.8073 -1.5331 255.1019 256.6350 273.0140 89.6005 -1.5382 255.1688 256.7069 273.0979 90.3923 -1.4925 255.2304 256.7229 273.1972 91.2153 -1.4774 255.2887 256.7661 273.2745 91.9770 -1.4867 255.3392 256.8259 273.3754 92.8305 -1.4855 255.3868 256.8723 273.4614 93.6215 -1.4861 255.4752 256.9614 273.5761 94.4135 -1.4937 255.5508 257.0445 273.6789 95.2355 -1.5055 255.6054 257.1109 273.7848 95.9963 -1.5303 255.6399 257.1702 273.8647 96.8473 -1.5366 255.7120 257.2486 273.9605 97.6075 -1.5385 255.7584 257.2969 274.0482 98.4288 -1.5286 255.8100 257.3386 274.1643 99.2505 -1.5315 255.8852 257.4167 274.2673 100.0118 -1.5359 255.9187 257.4546 274.3716 100.8623 -1.5329 256.0111 257.5440 274.4538 101.6238 -1.5362 256.0604 257.5966 274.5706 102.4458 -1.5405 256.1270 257.6675 274.6979 103.2680 -1.5466 256.1746 257.7212 274.8043 104.0290 -1.5456 256.2306 257.7762 274.8934 104.8823 -1.5505 256.3048 257.8553 275.0200 105.6440 -1.5557 256.3765 257.9322 275.1268 106.4660 -1.5661 256.4327 257.9989 275.2179 107.2580 -1.5662 256.4955 258.0617 275.3352 108.0488 -1.5622 256.5630 258.1252 275.4266 108.8743 -1.5676 256.6101 258.1778 275.5390 109.6650 -1.5678 256.6724 258.2401 275.6655 110.4860 -1.5743 256.7168 258.2911 275.7614 111.2778 -1.5725 256.7884 258.3608 275.8729 112.0688 -1.5693 256.8736 258.4429 275.9602 112.8905 -1.5756 256.9273 258.5029 276.0887 113.6815 -1.5793 256.9901 258.5693 276.2237 114.5035 -1.5560 257.0445 258.6005 276.3124 115.2968 -1.5303 257.1072 258.6375 276.4233 116.0883 -1.5275 257.1765 258.7041 276.5362 116.9085 -1.5313 257.2301 258.7614 276.6466 117.6700 -1.5335 257.2876 258.8211 276.7299 118.5215 -1.5344 257.3731 258.9075 276.8551 119.2838 -1.5335 257.4311 258.9646 276.9626 120.1065 -1.5291 257.4840 259.0131 277.0761 120.9275 -1.5435 257.5669 259.1105 277.1872 121.6890 -1.5853 257.6464 259.2317 277.2847 122.5405 -1.6098 257.6797 259.2894 277.4070 123.3018 -1.6138 257.7509 259.3647 277.5137 124.1223 -1.6191 257.8144 259.4335 277.6243 124.9423 -1.6212 257.8694 259.4906 277.7255 125.7020 -1.6267 257.9553 259.5821 277.8291 126.5530 -1.6355 258.0201 259.6557 277.9511 127.3140 -1.6364 258.0813 259.7177 278.0419 128.1358 -1.6307 258.1563 259.7870 278.1518 128.9580 -1.6203 258.2062 259.8266 278.2607 129.7195 -1.6227 258.2562 259.8789 278.3585 130.5703 -1.6238 258.3341 259.9579 278.4700 131.3310 -1.6351 258.4023 260.0375 278.5843 132.1513 -1.6360 258.4626 260.0987 278.7055 132.9713 -1.6350 258.5463 260.1813 278.8065 133.7320 -1.6341 258.6463 260.2805 278.8909 134.5840 -1.6337 258.6901 260.3238 279.0190 135.3448 -1.6319 258.7495 260.3815 279.1160 136.1658 -1.6230 258.8424 260.4654 279.2082 136.9865 -1.6156 258.8846 260.5002 279.3291 137.7485 -1.6333 258.9465 260.5799 279.4309 138.6005 -1.6464 259.0236 260.6700 279.5188 139.3608 -1.6548 259.1021 260.7568 279.6321 140.1835 -1.6594 259.1910 260.8504 279.7359 140.9763 -1.6570 259.2319 260.8889 279.8456 141.7698 -1.6562 259.2853 260.9416 279.9490 142.6215 -1.6541 259.3608 261.0149 280.0533 143.3835 -1.6640 259.4352 261.0992 280.1243 144.2055 -1.6542 259.5114 261.1656 280.2468 144.9963 -1.6570 259.5842 261.2412 280.3493 145.7868 -1.6672 259.6634 261.3306 280.4520 146.6383 -1.6748 259.7285 261.4033 280.5499 147.3995 -1.6782 259.7810 261.4592 280.6611 148.2215 -1.6782 259.8669 261.5451 280.7678 149.0125 -1.6798 259.9315 261.6112 280.8712 149.8033 -1.6782 260.0081 261.6862 280.9612 150.6535 -1.6875 260.0886 261.7761 281.0600 151.4145 -1.6912 260.1371 261.8284 281.1748 152.2358 -1.6952 260.2150 261.9102 281.2628 153.0280 -1.6906 260.2861 261.9767 281.3503 153.8188 -1.7052 260.3709 262.0761 281.4523 154.6708 -1.6984 260.4453 262.1437 281.5880 155.4318 -1.6930 260.4953 262.1883 281.6633 156.2538 -1.6796 260.5898 262.2693 281.7438 157.0460 -1.6800 260.6645 262.3445 281.8452 157.8375 -1.6909 260.7303 262.4212 281.9501 158.6900 -1.6947 260.7898 262.4845 282.0714 159.4518 -1.7086 260.8598 262.5684 282.1356 160.2730 -1.7096 260.9464 262.6561 282.2238 161.0635 -1.7207 261.0253 262.7460 282.3194 161.8543 -1.7236 261.0987 262.8223 282.4300 162.7055 -1.7290 261.1592 262.8882 282.5324 163.4675 -1.7379 261.2315 262.9694 282.6329 164.2895 -1.7373 261.3176 263.0549 282.7229 165.0815 -1.7339 261.3943 263.1282 282.8240 165.8735 -1.7411 261.4439 263.1850 282.9150 166.7253 -1.7415 261.5261 263.2676 283.0249 167.4865 -1.6843 261.6068 263.2911 283.1081 168.3085 -1.6469 261.6980 263.3449 283.1863 169.1005 -1.6856 261.7626 263.4481 283.2733 169.8925 -1.7437 261.8464 263.5901 283.3801 170.6845 -1.7471 261.9066 263.6538 283.4643 171.5155 -1.7080 261.9804 263.6884 283.5578 172.3075 -1.6873 262.0632 263.7505 283.6552 173.0988 -1.6748 262.1329 263.8077 283.7389 173.9205 -1.6612 262.2045 263.8657 283.8645 174.7125 -1.6588 262.2750 263.9338 283.9799 175.5338 -1.6590 262.3423 264.0013 284.0690 176.3235 -1.6596 262.4327 264.0923 284.1851 177.1143 -1.6627 262.5267 264.1894 284.2864 177.9363 -1.6613 262.6102 264.2715 284.3943 178.7260 -1.6644 262.6834 264.3478 284.5044 179.5475 -1.6657 262.7672 264.4329 284.6149 180.3420 -1.6694 262.8336 264.5030 284.7364 181.1438 -1.7059 262.9068 264.6128 284.8202 181.9360 -1.7482 262.9723 264.7204 284.9192 182.7263 -1.7773 263.0454 264.8227 285.0317 183.5783 -1.7817 263.1357 264.9174 285.1488 184.4295 -1.7349 263.2089 264.9438 285.2521 185.2860 -1.6941 263.3001 264.9941 285.3688 186.0780 -1.6879 263.3719 265.0598 285.4769 186.8695 -1.6895 263.4651 265.1546 285.5870 187.6920 -1.6795 263.5281 265.2075 285.6952 188.4525 -1.6805 263.5915 265.2720 285.7975 189.3043 -1.6877 263.6748 265.3625 285.9086 190.0655 -1.6919 263.7493 265.4412 286.0253 190.8870 -1.7015 263.8514 265.5529 286.1385 191.7085 -1.7034 263.9272 265.6306 286.2440 192.4698 -1.7041 263.9835 265.6876 286.3357 193.3215 -1.7072 264.0825 265.7897 286.4533 194.0818 -1.7091 264.1761 265.8852 286.5598 194.9035 -1.7074 264.2543 265.9617 286.6795 195.6955 -1.7170 264.3239 266.0409 286.7972 196.4863 -1.7175 264.4046 266.1221 286.8983 197.3375 -1.7225 264.4755 266.1979 286.9958 198.0980 -1.7266 264.5733 266.2999 287.0880 198.9180 -1.7280 264.6404 266.3684 287.2027 199.7085 -1.7251 264.7276 266.4526 287.3326 200.4998 -1.7306 264.7952 266.5258 287.4455 201.3505 -1.7344 264.8826 266.6170 287.5636 202.1108 -1.7389 264.9565 266.6954 287.6571 202.9318 -1.7407 265.0439 266.7846 287.7505 203.7230 -1.7418 265.1078 266.8496 287.8635 204.5140 -1.7435 265.1883 266.9318 287.9833 205.3360 -1.7433 265.2809 267.0241 288.0796 206.1278 -1.7498 265.3579 267.1078 288.2040 206.9498 -1.7547 265.4485 267.2032 288.2892 207.7413 -1.7566 265.5266 267.2832 288.3839 208.5328 -1.7573 265.5946 267.3519 288.4843 209.3550 -1.7591 265.6878 267.4469 288.6121 210.1160 -1.7570 265.7756 267.5326 288.7159 210.9678 -1.7523 265.8526 267.6050 288.8098 211.7620 -1.7534 265.9227 267.6762 288.9244 212.5563 -1.7562 265.9970 267.7532 289.0093 213.4075 -1.7665 266.1116 267.8782 289.1268 214.1695 -1.7768 266.1869 267.9637 289.2192 214.9910 -1.7761 266.2632 268.0393 289.3180 215.7815 -1.7797 266.3493 268.1290 289.4149 216.5725 -1.7835 266.4381 268.2217 289.5236 217.3935 -1.7865 266.5107 268.2972 289.6208 218.1840 -1.7871 266.5732 268.3603 289.7381 219.0055 -1.7905 266.6630 268.4536 289.8402 219.7975 -1.7925 266.7522 268.5447 289.9429 220.5893 -1.7958 266.8513 268.6471 290.0479 221.4105 -1.7975 266.9264 268.7239 290.1521 222.2018 -1.7965 266.9980 268.7945 290.2614 223.0235 -1.7969 267.0966 268.8936 290.3676 223.8138 -1.8025 267.1941 268.9967 290.4486 224.6053 -1.8062 267.2885 269.0947 290.5646 225.4265 -1.8071 267.3496 269.1567 290.6675 226.1873 -1.8111 267.4487 269.2598 290.7679 227.0378 -1.8105 267.5346 269.3450 290.8757 227.8285 -1.8127 267.5929 269.4056 290.9657 228.6195 -1.8160 267.6820 269.4980 291.0703 229.4423 -1.8167 267.7689 269.5856 291.1676 230.2035 -1.8195 267.8627 269.6822 291.2801 231.0560 -1.8232 267.9443 269.7675 291.3745 231.8183 -1.8230 268.0285 269.8514 291.4705 232.6415 -1.8270 268.1191 269.9461 291.5807 233.4625 -1.8265 268.2098 270.0363 291.6793 234.2228 -1.8291 268.2817 270.1108 291.7794 235.0748 -1.8302 268.3597 270.1900 291.8790 235.8358 -1.8359 268.4553 270.2912 291.9803 236.6575 -1.8390 268.5438 270.3828 292.0813 237.4488 -1.8412 268.6129 270.4541 292.1695 238.2403 -1.8433 268.7102 270.5534 292.2555 239.0915 -1.8428 268.8093 270.6522 292.3784 239.8525 -1.8430 268.8909 270.7339 292.4520 240.6745 -1.8460 268.9826 270.8286 292.5761 241.4665 -1.8496 269.0763 270.9259 292.6593 242.2583 -1.8534 269.1567 271.0101 292.7747 243.0795 -1.8564 269.2469 271.1033 292.8792 243.8415 -1.8596 269.3255 271.1851 292.9525 244.6933 -1.8556 269.4128 271.2684 293.0594 245.4838 -1.8555 269.4841 271.3396 293.1569 246.2753 -1.8638 269.5723 271.4361 293.2208 247.0955 -1.8714 269.6594 271.5308 293.3314 247.8575 -1.8743 269.7332 271.6076 293.4711 248.7095 -1.8763 269.8332 271.7095 293.5645 249.5008 -1.8745 269.9345 271.8089 293.6537 250.2920 -1.8766 270.0163 271.8929 293.7669 251.1135 -1.8790 270.0891 271.9681 293.8543 251.8748 -1.8815 270.1809 272.0624 293.9513 252.7265 -1.8833 270.2843 272.1676 294.0588 253.4883 -1.8836 270.3849 272.2685 294.1588 254.3103 -1.8854 270.4615 272.3470 294.2576 255.1323 -1.8845 270.5251 272.4096 294.3849 255.8948 -1.8754 270.6242 272.4996 294.5032 256.7460 -1.8793 270.7186 272.5979 294.6338 257.5058 -1.8708 270.7989 272.6696 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382.2044 928.7125 -3.8207 358.2516 362.0723 382.3261 929.4735 -3.8239 358.3648 362.1887 382.4278 930.3255 -3.8206 358.4628 362.2834 382.5177 931.1148 -3.8448 358.5914 362.4362 382.6309 931.9065 -3.8516 358.6925 362.5441 382.7417 932.7280 -3.8489 358.8276 362.6764 382.8388 933.4888 -3.8571 358.9367 362.7938 382.9425 934.3395 -3.8506 359.0320 362.8826 383.0581 935.1283 -3.8473 359.1335 362.9808 383.1521 935.9195 -3.8448 359.2516 363.0964 383.2772 936.7405 -3.8444 359.3615 363.2059 383.3720 937.5010 -3.8458 359.4742 363.3201 383.4776 938.3515 -3.8573 359.6052 363.4624 383.5881 939.1405 -3.8590 359.7195 363.5785 383.7163 939.9313 -3.8496 359.8199 363.6696 383.8189 940.7515 -3.8494 359.9298 363.7792 383.9326 941.5428 -3.8524 360.0720 363.9244 384.0447 942.3645 -3.8494 360.1651 364.0144 384.1598 943.1565 -3.8473 360.2714 364.1186 384.2450 943.9485 -3.8484 360.3730 364.2214 384.3665 944.7700 -3.8410 360.5024 364.3434 384.4997 945.5310 -3.8435 360.6073 364.4509 384.5884 946.3818 -3.8517 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964.8505 -3.9492 363.3104 367.2596 387.3400 965.6110 -3.9904 363.4179 367.4083 387.4510 966.4608 -3.9999 363.5495 367.5494 387.5559 967.2518 -4.0046 363.6491 367.6537 387.6439 968.0428 -4.0141 363.7518 367.7660 387.7291 968.8638 -3.9712 363.8811 367.8523 387.8439 969.6258 -3.9373 363.9721 367.9094 387.9380 970.4775 -3.9304 364.0993 368.0298 388.0430 971.2393 -3.9327 364.2074 368.1401 388.1315 972.0605 -3.9347 364.3269 368.2616 388.2153 972.8810 -3.9359 364.4310 368.3670 388.3033 973.6425 -3.9396 364.5325 368.4721 388.3948 974.4940 -3.9394 364.6512 368.5906 388.5013 975.2540 -3.9318 364.7699 368.7017 388.5836 976.0753 -3.9487 364.8684 368.8171 388.6754 976.8965 -4.0058 364.9874 368.9933 388.7788 977.6565 -4.0205 365.0803 369.1007 388.8542 978.5088 -4.0281 365.1998 369.2279 388.9566 979.2700 -4.0266 365.3107 369.3373 389.0464 980.0928 -3.9763 365.4442 369.4205 389.1511 980.8848 -3.9563 365.5403 369.4966 389.2478 981.6750 -3.9385 365.6258 369.5643 389.3616 982.5255 -3.9421 365.7675 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