DTA measure 1olom3 Test Date: 20231121:1128 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.42 s Mass = 1147 mg data_number = 1269 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1615 -1.6435 270.4860 272.1295 260.0766 1.9840 -1.6246 270.3455 271.9701 259.9146 2.7455 -1.6283 270.4533 272.0815 259.9415 3.5980 -1.6356 270.3962 272.0318 260.0575 4.3900 -1.6405 270.4846 272.1252 260.0749 5.1815 -1.6410 270.5612 272.2022 260.0752 6.0038 -1.6347 270.5510 272.1856 260.0912 6.7955 -1.6361 270.5481 272.1843 260.2028 7.6178 -1.6411 270.5467 272.1878 260.1713 8.4095 -1.6258 270.4684 272.0942 260.1866 9.2015 -1.6380 270.4371 272.0751 260.0781 10.0235 -1.6351 270.4296 272.0648 260.0983 10.8155 -1.6487 270.3681 272.0168 260.1492 11.6383 -1.6516 270.4798 272.1315 260.2805 12.4305 -1.6439 270.5468 272.1907 260.3096 13.2233 -1.6380 270.5030 272.1410 260.3196 14.0415 -1.6393 270.5000 272.1393 260.3629 14.8300 -1.6333 270.5189 272.1522 260.4080 15.6478 -1.6279 270.4704 272.0983 260.5251 16.4360 -1.6288 270.4118 272.0406 260.5807 17.2240 -1.6491 270.4460 272.0951 260.5651 18.0728 -1.6305 270.5143 272.1448 260.6354 18.8320 -1.6347 270.4837 272.1184 260.8051 19.6508 -1.6458 270.4704 272.1162 260.8399 20.4393 -1.6534 270.4820 272.1354 260.9899 21.2303 -1.6524 270.4750 272.1274 261.0218 22.0818 -1.6468 270.5617 272.2085 261.1128 22.8435 -1.6474 270.4661 272.1135 261.2769 23.6655 -1.6432 270.3832 272.0265 261.3055 24.4575 -1.6436 270.4850 272.1286 261.4350 25.2495 -1.6395 270.4105 272.0500 261.5673 26.1025 -1.6375 270.4978 272.1353 261.7682 26.8645 -1.6590 270.6238 272.2828 261.9115 27.6865 -1.6642 270.5562 272.2204 261.9746 28.4785 -1.6634 270.5584 272.2218 262.1244 29.2705 -1.6614 270.5563 272.2177 262.2031 30.1225 -1.6643 270.6504 272.3147 262.3317 30.8845 -1.6658 270.6170 272.2828 262.5552 31.7065 -1.6627 270.5438 272.2065 262.6333 32.4985 -1.6610 270.5285 272.1895 262.8635 33.2905 -1.6584 270.5446 272.2030 263.0106 34.1425 -1.6651 270.5824 272.2475 263.0580 34.9040 -1.6712 270.5755 272.2467 263.2340 35.7263 -1.6723 270.5695 272.2418 263.4164 36.5183 -1.6767 270.6204 272.2971 263.6050 37.3095 -1.6793 270.6045 272.2839 263.6981 38.1625 -1.6784 270.6844 272.3629 263.7217 38.9248 -1.6877 270.6737 272.3614 263.8141 39.7475 -1.6807 270.6341 272.3148 264.0288 40.5400 -1.6991 270.6677 272.3669 264.1421 41.3315 -1.6986 270.6730 272.3715 264.2189 42.1845 -1.6862 270.7338 272.4199 264.4261 42.9468 -1.6957 270.7031 272.3988 264.4720 43.7695 -1.6958 270.7164 272.4122 264.6575 44.5618 -1.6981 270.7373 272.4353 264.7646 45.3528 -1.6876 270.7096 272.3972 264.9073 46.2010 -1.6950 270.6717 272.3667 265.1002 46.9590 -1.6920 270.6821 272.3741 265.3292 47.7770 -1.6951 270.6965 272.3917 265.3939 48.5700 -1.7071 270.7153 272.4224 265.5411 49.3580 -1.7048 270.6856 272.3904 265.6674 50.1765 -1.6862 270.7709 272.4571 265.6954 50.9653 -1.6967 270.7594 272.4562 265.8858 51.7840 -1.7108 270.8010 272.5118 266.0287 52.5733 -1.7183 270.8558 272.5741 266.2297 53.3640 -1.7169 270.9033 272.6202 266.3496 54.1855 -1.7085 270.8848 272.5933 266.5329 54.9755 -1.7253 270.8761 272.6014 266.5019 55.7970 -1.7174 270.7949 272.5123 266.5230 56.5890 -1.7105 270.8227 272.5332 266.6997 57.3805 -1.7194 270.8913 272.6107 266.9166 58.2033 -1.7233 270.9750 272.6982 266.9815 58.9655 -1.7078 270.8500 272.5578 267.2010 59.8178 -1.7190 270.9612 272.6802 267.2620 60.6098 -1.7339 270.8954 272.6293 267.3632 61.4015 -1.7310 270.9729 272.7040 267.4969 62.2238 -1.7361 271.0320 272.7681 267.6642 62.9855 -1.7386 270.9830 272.7217 267.8413 63.8378 -1.7316 271.0217 272.7533 267.9405 64.5995 -1.7302 271.0493 272.7795 268.0715 65.4218 -1.7291 271.1224 272.8515 268.0997 66.2435 -1.7443 271.0813 272.8256 268.3008 67.0055 -1.7443 271.1056 272.8499 268.3740 67.8575 -1.7455 271.1245 272.8700 268.5156 68.6195 -1.7421 271.1371 272.8792 268.6987 69.4415 -1.7405 271.1657 272.9062 268.7808 70.2635 -1.7440 271.1957 272.9397 268.8350 71.0255 -1.7412 271.2585 272.9996 268.9255 71.8775 -1.7508 271.2305 272.9813 269.0997 72.6395 -1.7494 271.2412 272.9906 269.2243 73.4615 -1.7425 271.2372 272.9797 269.3370 74.2535 -1.7528 271.3408 273.0936 269.3938 75.0445 -1.7525 271.3467 273.0992 269.4991 75.8975 -1.7475 271.3999 273.1474 269.7131 76.6600 -1.7555 271.3974 273.1530 269.8304 77.4818 -1.7610 271.4367 273.1978 269.8959 78.2690 -1.7547 271.4820 273.2367 270.0206 79.0580 -1.7596 271.4672 273.2269 270.1618 79.8775 -1.7524 271.5877 273.3401 270.2412 80.6663 -1.7607 271.6243 273.3850 270.3633 81.4855 -1.7520 271.5730 273.3250 270.5817 82.2738 -1.7638 271.5152 273.2790 270.6854 83.0628 -1.7745 271.6492 273.4237 270.7087 83.8825 -1.7725 271.6705 273.4431 270.8054 84.6713 -1.7765 271.6801 273.4566 270.9277 85.4925 -1.7760 271.6768 273.4528 271.0777 86.2825 -1.7695 271.7842 273.5537 271.2339 87.0745 -1.7731 271.7484 273.5215 271.4485 87.8963 -1.7670 271.8075 273.5744 271.5647 88.6583 -1.7715 271.9026 273.6741 271.7177 89.5105 -1.7661 271.9290 273.6951 271.6964 90.3020 -1.7716 271.9307 273.7023 271.8324 91.0938 -1.7753 271.9206 273.6959 271.9540 91.9165 -1.7774 271.9272 273.7046 272.0095 92.6778 -1.7890 271.9677 273.7567 272.2425 93.5300 -1.7723 272.1294 273.9017 272.3091 94.2918 -1.7802 272.1037 273.8839 272.4185 95.1138 -1.7814 272.1194 273.9008 272.6534 95.9360 -1.7814 272.0745 273.8559 272.7332 96.6975 -1.7744 272.1779 273.9523 272.8416 97.5500 -1.7832 272.2589 274.0421 273.0789 98.3118 -1.7774 272.2920 274.0694 273.1421 99.1338 -1.7781 272.3115 274.0896 273.2477 99.9558 -1.7824 272.2768 274.0592 273.3436 100.7175 -1.7922 272.3863 274.1786 273.5644 101.5698 -1.7821 272.4213 274.2034 273.6963 102.3315 -1.7800 272.3900 274.1700 273.7626 103.1538 -1.7862 272.4500 274.2362 273.8558 103.9760 -1.7769 272.5315 274.3084 274.0416 104.7385 -1.7958 272.6066 274.4024 274.0955 105.5905 -1.7937 272.5526 274.3463 274.1833 106.3525 -1.7913 272.6135 274.4048 274.3744 107.1753 -1.7820 272.6653 274.4473 274.5548 107.9975 -1.7869 272.6423 274.4292 274.6366 108.7595 -1.7855 272.8273 274.6128 274.8392 109.6103 -1.7795 272.8885 274.6680 274.9486 110.3690 -1.7767 272.8650 274.6418 275.0898 111.1878 -1.7907 272.8393 274.6300 275.2076 112.0063 -1.7884 272.9789 274.7673 275.3215 112.7650 -1.7886 272.9677 274.7563 275.3989 113.6130 -1.7848 273.0438 274.8286 275.6584 114.3710 -1.7917 273.0305 274.8222 275.7227 115.1898 -1.7882 273.0438 274.8320 275.8330 116.0083 -1.7720 273.0629 274.8348 276.0068 116.7680 -1.7876 273.1016 274.8892 276.1211 117.6168 -1.7953 273.2208 275.0160 276.2654 118.4078 -1.7952 273.3305 275.1257 276.4351 119.1995 -1.7884 273.2763 275.0647 276.6572 120.0215 -1.7966 273.2740 275.0707 276.6877 120.7825 -1.8086 273.4094 275.2180 276.8454 121.6345 -1.8013 273.5543 275.3556 277.1108 122.4265 -1.7936 273.6704 275.4640 277.1250 123.2185 -1.7957 273.6738 275.4695 277.1526 124.0405 -1.7898 273.6466 275.4364 277.3483 124.8025 -1.7920 273.7111 275.5031 277.4478 125.6545 -1.7973 273.8410 275.6383 277.5161 126.4465 -1.7933 273.8540 275.6472 277.6068 127.2385 -1.7925 273.8255 275.6180 277.7018 128.0605 -1.7861 273.9346 275.7207 277.8557 128.8225 -1.7785 274.0068 275.7853 278.0915 129.6745 -1.7864 274.0559 275.8424 278.2194 130.4660 -1.8051 274.1101 275.9153 278.3607 131.2580 -1.8055 274.1810 275.9865 278.5781 132.0800 -1.7976 274.1895 275.9871 278.6983 132.8415 -1.7835 274.1122 275.8956 278.7171 133.6945 -1.7880 274.2639 276.0519 278.7518 134.4870 -1.8054 274.3093 276.1147 278.9090 135.2785 -1.8072 274.4732 276.2804 278.9919 136.1010 -1.8104 274.6153 276.4257 279.1713 136.8928 -1.8163 274.6551 276.4714 279.3769 137.7155 -1.7981 274.6098 276.4080 279.4854 138.5080 -1.7883 274.6528 276.4411 279.5933 139.3005 -1.7900 274.7366 276.5266 279.6307 140.1228 -1.7974 274.6403 276.4377 279.7788 140.9145 -1.7926 274.7795 276.5722 279.8976 141.7375 -1.8021 274.8534 276.6555 280.1027 142.5273 -1.7980 274.9797 276.7777 280.1920 143.3160 -1.7928 275.0271 276.8199 280.3555 144.1348 -1.7959 275.0736 276.8696 280.4171 144.9230 -1.8006 275.1677 276.9683 280.5893 145.7420 -1.7907 275.2417 277.0324 280.6123 146.5305 -1.7840 275.2585 277.0425 280.7123 147.3190 -1.7921 275.3002 277.0923 280.7560 148.1678 -1.7755 275.4341 277.2096 280.9648 148.9273 -1.7800 275.4739 277.2539 281.1649 149.7470 -1.7937 275.5454 277.3391 281.2852 150.5668 -1.8091 275.5631 277.3722 281.3499 151.3268 -1.8118 275.5522 277.3640 281.4722 152.1790 -1.7984 275.6776 277.4760 281.5941 152.9408 -1.7924 275.7394 277.5318 281.7721 153.7628 -1.7873 275.7983 277.5856 281.8651 154.5848 -1.7914 275.9136 277.7050 281.9326 155.3465 -1.7941 275.9952 277.7893 282.1142 156.1990 -1.7936 276.0505 277.8441 282.2535 156.9605 -1.7938 276.1314 277.9253 282.4307 157.7828 -1.7921 276.1609 277.9530 282.5523 158.6048 -1.7953 276.2297 278.0250 282.7169 159.3665 -1.7926 276.4102 278.2028 282.7905 160.2205 -1.7885 276.4109 278.1994 282.9697 160.9825 -1.7927 276.4799 278.2727 283.0322 161.8045 -1.7838 276.5019 278.2856 283.1060 162.6265 -1.7889 276.5985 278.3873 283.3092 163.3885 -1.7954 276.6301 278.4255 283.5015 164.2405 -1.8061 276.7457 278.5519 283.5509 165.0325 -1.7906 276.7919 278.5825 283.7367 165.8250 -1.7903 276.8948 278.6852 283.9381 166.6475 -1.7920 276.8815 278.6736 284.0037 167.4095 -1.8000 276.9684 278.7684 284.1542 168.2615 -1.7936 277.0512 278.8448 284.2958 169.0535 -1.8011 277.1961 278.9972 284.3895 169.8448 -1.8002 277.2343 279.0344 284.5700 170.6673 -1.7968 277.4098 279.2066 284.6551 171.4588 -1.7906 277.4520 279.2426 284.8252 172.2815 -1.7858 277.3885 279.1743 284.9573 173.0740 -1.7823 277.4118 279.1941 285.0496 173.8665 -1.7884 277.5127 279.3011 285.2147 174.6883 -1.7873 277.6030 279.3903 285.2787 175.4470 -1.7826 277.6728 279.4554 285.3878 176.2975 -1.7872 277.7623 279.5495 285.5973 177.0865 -1.7936 277.8626 279.6562 285.7512 177.8753 -1.8010 277.9273 279.7283 285.8353 178.6940 -1.7937 277.9947 279.7884 286.0518 179.4530 -1.7928 278.1487 279.9415 286.1449 180.3028 -1.7880 278.1291 279.9171 286.2697 181.0915 -1.7809 278.2059 279.9868 286.3947 181.8818 -1.7831 278.2906 280.0737 286.5581 182.7015 -1.7846 278.3317 280.1163 286.6475 183.4623 -1.7856 278.3689 280.1545 286.7772 184.3140 -1.7751 278.5061 280.2812 286.9217 185.0760 -1.7859 278.5645 280.3503 287.1064 185.8978 -1.7842 278.6322 280.4164 287.1103 186.7200 -1.7946 278.7451 280.5396 287.3240 187.4815 -1.8003 278.8787 280.6790 287.4253 188.3340 -1.7849 279.0146 280.7994 287.5417 189.0958 -1.7893 279.0194 280.8088 287.5997 189.9178 -1.7843 279.0653 280.8496 287.7108 190.7100 -1.7837 279.2358 281.0195 287.8262 191.5018 -1.7815 279.2628 281.0443 288.0515 192.3540 -1.7806 279.2207 281.0013 288.1389 193.1158 -1.7845 279.3607 281.1452 288.2157 193.9378 -1.7773 279.5602 281.3375 288.2450 194.7300 -1.7866 279.5177 281.3043 288.4078 195.5215 -1.7841 279.6181 281.4021 288.5498 196.3738 -1.7841 279.7559 281.5400 288.7209 197.1355 -1.7854 279.9103 281.6956 288.9057 197.9578 -1.7796 279.9488 281.7285 289.0769 198.7498 -1.7774 280.0264 281.8038 289.0623 199.5415 -1.7937 280.1630 281.9567 289.2010 200.3635 -1.7839 280.2309 282.0148 289.2403 201.1558 -1.7771 280.2845 282.0616 289.4044 201.9785 -1.7823 280.3606 282.1428 289.5502 202.7705 -1.7904 280.3991 282.1895 289.7561 203.5625 -1.7859 280.5484 282.3344 289.9261 204.3848 -1.7738 280.5336 282.3075 290.0992 205.1775 -1.7727 280.7017 282.4743 290.1986 206.0003 -1.7762 280.7678 282.5440 290.3247 206.7898 -1.7807 280.8495 282.6302 290.3895 207.5778 -1.7792 281.0201 282.7993 290.5747 208.3958 -1.7801 281.1224 282.9026 290.7949 209.1540 -1.7759 281.2356 283.0115 290.9663 210.0030 -1.7674 281.2349 283.0023 291.0085 210.7910 -1.7633 281.3343 283.0976 291.1207 211.5805 -1.7877 281.3900 283.1777 291.3125 212.4000 -1.7901 281.4920 283.2821 291.4618 213.1608 -1.7825 281.5477 283.3302 291.5956 214.0103 -1.7850 281.6209 283.4059 291.6590 214.7998 -1.7715 281.7675 283.5390 291.8700 215.5915 -1.7894 281.8482 283.6376 291.9448 216.4130 -1.7883 281.8843 283.6726 292.1143 217.1745 -1.7903 282.0132 283.8034 292.2725 218.0265 -1.7937 282.1127 283.9064 292.5090 218.7885 -1.7911 282.1287 283.9198 292.5628 219.6105 -1.7869 282.3259 284.1128 292.6657 220.4325 -1.7880 282.4037 284.1917 292.7950 221.1945 -1.7847 282.4966 284.2814 293.0007 222.0465 -1.7947 282.5677 284.3624 293.1336 222.8085 -1.8000 282.6280 284.4279 293.2549 223.6305 -1.7901 282.6763 284.4664 293.4036 224.4225 -1.7979 282.8285 284.6264 293.4566 225.2143 -1.7881 283.0622 284.8503 293.5817 226.0663 -1.8047 283.0529 284.8576 293.5581 226.8280 -1.7860 283.0642 284.8502 293.6819 227.6498 -1.7792 283.1518 284.9310 293.9285 228.4420 -1.7935 283.2670 285.0605 294.1219 229.2335 -1.7879 283.3821 285.1700 294.2326 230.0860 -1.7888 283.4491 285.2380 294.2959 230.8478 -1.7872 283.5612 285.3484 294.3384 231.6698 -1.7803 283.6715 285.4518 294.4831 232.4620 -1.7959 283.8170 285.6129 294.6214 233.2545 -1.7936 283.8653 285.6590 294.6890 234.1075 -1.7892 284.0264 285.8157 294.8693 234.8695 -1.7930 284.0966 285.8896 294.9955 235.6918 -1.7899 284.1260 285.9159 295.1051 236.4838 -1.8146 284.3061 286.1207 295.1188 237.2755 -1.8040 284.4108 286.2148 295.3293 238.1275 -1.8092 284.4978 286.3070 295.5310 238.8863 -1.7980 284.6118 286.4098 295.6515 239.7040 -1.7881 284.6738 286.4619 295.7450 240.4923 -1.7885 284.7130 286.5016 295.8326 241.2810 -1.7919 284.8477 286.6396 296.0254 242.1290 -1.7837 284.9527 286.7363 296.2571 242.8870 -1.7882 285.0428 286.8310 296.3130 243.7058 -1.7964 285.2222 287.0186 296.4344 244.4948 -1.8033 285.3016 287.1049 296.6263 245.2845 -1.7908 285.3989 287.1897 296.6777 246.1335 -1.7752 285.4533 287.2285 296.8430 246.8948 -1.7870 285.5894 287.3764 296.9329 247.7168 -1.7918 285.6560 287.4478 297.1004 248.5388 -1.7753 285.8604 287.6357 297.3320 249.3005 -1.7884 285.8665 287.6549 297.4749 250.1530 -1.7937 285.9425 287.7361 297.5342 250.9145 -1.7878 286.0954 287.8832 297.6455 251.7368 -1.7777 286.1798 287.9575 297.8028 252.5285 -1.7910 286.2880 288.0790 298.0137 253.3205 -1.7912 286.4636 288.2549 298.1283 254.1728 -1.7849 286.4969 288.2818 298.2212 254.9345 -1.7700 286.5229 288.2929 298.2685 255.7568 -1.7706 286.5937 288.3643 298.4768 256.5485 -1.7836 286.7626 288.5462 298.5627 257.3405 -1.7918 286.8888 288.6806 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