DTA measure 1olom4 Test Date: 20231121:1227 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1274.00 s Mass = 1147 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2325 -0.7608 251.7801 252.5409 258.9691 2.0845 -0.7493 251.8750 252.6243 259.0011 2.8765 -0.7654 251.9483 252.7136 259.0157 3.6695 -0.7694 252.0226 252.7920 259.0192 4.4915 -0.7663 252.1414 252.9078 259.0440 5.2533 -0.7647 252.2799 253.0447 259.0710 6.1050 -0.7675 252.3459 253.1134 259.1051 6.8970 -0.7601 252.4683 253.2283 259.0946 7.6885 -0.7676 252.5403 253.3079 258.9806 8.5110 -0.7712 252.5906 253.3618 259.0944 9.3028 -0.7713 252.6695 253.4408 259.1475 10.1248 -0.7644 252.7983 253.5627 259.0832 10.9170 -0.7639 252.8968 253.6607 259.1358 11.7085 -0.7595 252.8883 253.6478 259.2300 12.5313 -0.7596 253.0465 253.8061 259.2808 13.3235 -0.7541 253.0742 253.8283 259.3333 14.1458 -0.7531 253.2611 254.0142 259.3577 14.9378 -0.7630 253.4433 254.2063 259.3865 15.7295 -0.7566 253.4580 254.2147 259.4697 16.5823 -0.7711 253.5366 254.3077 259.5382 17.3445 -0.7694 253.6501 254.4195 259.6350 18.1665 -0.7634 253.6808 254.4443 259.7086 18.9588 -0.7610 253.8219 254.5829 259.7457 19.7495 -0.7598 254.0596 254.8195 259.8286 20.5990 -0.7711 254.0082 254.7793 259.9282 21.3560 -0.7763 254.1801 254.9564 260.0721 22.1750 -0.7666 254.2001 254.9667 260.1290 22.9618 -0.7734 254.2399 255.0133 260.2612 23.7510 -0.7779 254.3638 255.1417 260.3495 24.5995 -0.7799 254.4781 255.2580 260.4276 25.3580 -0.7760 254.5261 255.3021 260.5443 26.1760 -0.7826 254.5407 255.3233 260.7183 26.9643 -0.7856 254.6233 255.4089 260.7473 27.7633 -0.7762 254.7624 255.5385 260.7778 28.5623 -0.7877 254.8724 255.6601 260.9531 29.3520 -0.7952 254.9704 255.7656 261.0753 30.2013 -0.7994 255.0470 255.8464 261.1378 30.9600 -0.8010 255.0344 255.8354 261.2581 31.7798 -0.7995 255.1361 255.9357 261.4791 32.5698 -0.8097 255.2593 256.0691 261.6133 33.3600 -0.8117 255.3662 256.1780 261.6720 34.2088 -0.8121 255.5272 256.3393 261.7088 34.9698 -0.8201 255.5555 256.3756 261.8337 35.7893 -0.8218 255.6009 256.4228 261.9706 36.5805 -0.8232 255.7259 256.5490 262.0808 37.3710 -0.8281 255.8853 256.7134 262.2593 38.2205 -0.8296 255.9643 256.7939 262.3469 38.9818 -0.8273 256.0153 256.8427 262.4613 39.8038 -0.8281 256.1004 256.9285 262.5491 40.5953 -0.8341 256.1512 256.9852 262.7441 41.3865 -0.8359 256.1682 257.0041 262.7473 42.2090 -0.8361 256.3233 257.1594 262.8642 43.0008 -0.8391 256.3986 257.2377 263.0050 43.8228 -0.8379 256.4755 257.3134 263.1124 44.6150 -0.8432 256.6795 257.5227 263.1890 45.4065 -0.8553 256.7148 257.5702 263.3340 46.2290 -0.8590 256.7989 257.6579 263.4749 46.9905 -0.8546 256.8752 257.7298 263.5281 47.8430 -0.8523 256.9097 257.7620 263.6479 48.6350 -0.8699 257.0078 257.8777 263.7809 49.4265 -0.8550 257.0771 257.9321 263.8333 50.2488 -0.8695 257.2399 258.1094 263.9707 51.0105 -0.8615 257.2949 258.1564 264.0994 51.8625 -0.8760 257.3359 258.2119 264.2241 52.6545 -0.8906 257.4444 258.3350 264.3253 53.4465 -0.8853 257.5833 258.4686 264.4373 54.2685 -0.8907 257.7014 258.5921 264.5319 55.0305 -0.8964 257.7959 258.6923 264.6678 55.8825 -0.8883 257.7383 258.6266 264.7837 56.6745 -0.9081 257.8769 258.7850 264.8984 57.4665 -0.9075 258.0185 258.9260 264.9600 58.2885 -0.9075 258.0383 258.9457 265.0189 59.0505 -0.9004 258.1211 259.0215 265.1205 59.9025 -0.9091 258.1568 259.0659 265.2405 60.6945 -0.9208 258.3005 259.2213 265.3438 61.4863 -0.9232 258.3903 259.3135 265.4924 62.3083 -0.9253 258.4811 259.4064 265.6048 63.0698 -0.9369 258.5444 259.4813 265.6900 63.9220 -0.9432 258.5730 259.5163 265.8765 64.6838 -0.9410 258.7046 259.6456 265.8669 65.5058 -0.9315 258.7691 259.7006 266.0136 66.3280 -0.9321 258.9069 259.8390 266.1386 67.0898 -0.9492 258.9794 259.9286 266.1696 67.9430 -0.9432 259.1668 260.1100 266.2924 68.7058 -0.9489 259.1143 260.0632 266.3937 69.5305 -0.9567 259.1723 260.1290 266.4902 70.3530 -0.9504 259.2955 260.2459 266.5587 71.1155 -0.9598 259.3673 260.3271 266.7712 71.9688 -0.9667 259.3546 260.3212 266.8010 72.7383 -0.9664 259.4783 260.4447 266.7908 73.5605 -0.9639 259.5421 260.5061 266.9510 74.3525 -0.9796 259.6298 260.6095 267.1134 75.1445 -0.9784 259.8309 260.8092 267.1606 75.9970 -0.9702 259.9107 260.8809 267.2830 76.7595 -0.9766 259.9594 260.9360 267.3043 77.5815 -0.9874 260.0328 261.0202 267.4180 78.3735 -0.9975 260.1050 261.1025 267.5694 79.1723 -0.9898 260.2131 261.2029 267.6793 79.9965 -0.9873 260.2302 261.2175 267.7706 80.7883 -0.9969 260.4563 261.4532 267.8288 81.6100 -1.0049 260.4929 261.4978 267.9633 82.4023 -1.0071 260.5725 261.5796 268.0825 83.1935 -1.0050 260.6200 261.6250 268.1493 84.0433 -1.0206 260.6653 261.6858 268.2868 84.8013 -1.0250 260.8001 261.8250 268.4398 85.6193 -1.0286 260.9277 261.9563 268.5577 86.4075 -1.0328 260.9957 262.0286 268.6732 87.1953 -1.0344 261.0248 262.0592 268.7952 88.0140 -1.0405 261.1987 262.2392 268.7871 88.8023 -1.0408 261.2761 262.3169 268.8967 89.6200 -1.0535 261.2335 262.2869 269.1204 90.4083 -1.0505 261.3339 262.3844 269.2307 91.1963 -1.0516 261.5197 262.5714 269.3686 92.0150 -1.0506 261.5440 262.5945 269.4416 92.8035 -1.0585 261.5683 262.6268 269.4722 93.6220 -1.0705 261.6882 262.7587 269.5338 94.4103 -1.0717 261.7576 262.8294 269.6553 95.1980 -1.0815 261.8764 262.9579 269.8014 96.0470 -1.0853 261.8771 262.9624 269.9134 96.8078 -1.0841 262.0094 263.0935 269.9829 97.6295 -1.0844 262.1619 263.2463 270.0898 98.4193 -1.0829 262.2268 263.3097 270.0689 99.2105 -1.0930 262.1981 263.2911 270.2537 100.0370 -1.0976 262.3055 263.4032 270.4185 100.8270 -1.0970 262.4488 263.5458 270.5933 101.6468 -1.1055 262.4414 263.5468 270.6780 102.4390 -1.1040 262.6047 263.7087 270.7090 103.2305 -1.1061 262.6770 263.7831 270.8847 104.0530 -1.1098 262.8474 263.9572 270.9700 104.8445 -1.1142 262.9513 264.0654 271.0343 105.6668 -1.1156 262.9534 264.0689 271.2140 106.4585 -1.1232 263.0890 264.2122 271.2724 107.2505 -1.1161 263.2338 264.3500 271.3428 108.0725 -1.1213 263.2822 264.4034 271.4262 108.8345 -1.1200 263.3412 264.4612 271.6125 109.6865 -1.1330 263.4737 264.6066 271.7509 110.4485 -1.1309 263.4879 264.6188 271.8492 111.2705 -1.1359 263.6264 264.7622 271.8970 112.0925 -1.1363 263.7581 264.8945 272.0328 112.8545 -1.1634 263.7271 264.8905 272.0947 113.7065 -1.1543 263.9217 265.0760 272.2276 114.4685 -1.1554 263.9655 265.1209 272.3209 115.2913 -1.1639 263.9730 265.1369 272.4879 116.1133 -1.1660 264.1762 265.3423 272.5380 116.8755 -1.1663 264.1595 265.3258 272.5728 117.7275 -1.1505 264.3244 265.4749 272.7448 118.4890 -1.1763 264.3557 265.5320 272.8794 119.3108 -1.1717 264.4449 265.6167 272.9041 120.1330 -1.1715 264.5158 265.6873 273.0206 120.8945 -1.1680 264.5282 265.6962 273.1135 121.7475 -1.1859 264.7065 265.8924 273.2106 122.5098 -1.1851 264.8127 265.9979 273.2936 123.3325 -1.1884 264.8748 266.0632 273.5008 124.1250 -1.1797 264.9866 266.1663 273.5817 124.9165 -1.1862 265.1764 266.3626 273.6406 125.7690 -1.1937 265.2060 266.3997 273.7140 126.5305 -1.2031 265.2723 266.4753 273.8308 127.3528 -1.1869 265.3555 266.5423 274.0075 128.1445 -1.1944 265.4614 266.6558 274.1027 128.9365 -1.2024 265.5461 266.7485 274.1716 129.7595 -1.2076 265.5351 266.7426 274.3493 130.5515 -1.2092 265.5961 266.8053 274.4462 131.3735 -1.2059 265.7086 266.9146 274.5331 132.1655 -1.2172 265.8319 267.0491 274.5655 132.9575 -1.2100 265.9492 267.1592 274.6327 133.8100 -1.2161 265.9868 267.2029 274.7762 134.5725 -1.2178 266.0295 267.2474 274.8982 135.3945 -1.2281 266.1313 267.3594 275.0232 136.1875 -1.2144 266.2041 267.4185 275.1570 136.9795 -1.2280 266.3485 267.5765 275.2357 137.8320 -1.2150 266.4909 267.7059 275.3065 138.5943 -1.2249 266.5844 267.8093 275.3371 139.4158 -1.2397 266.6389 267.8786 275.4629 140.2080 -1.2534 266.7077 267.9611 275.5858 140.9995 -1.2488 266.8694 268.1182 275.6719 141.8520 -1.2493 266.9610 268.2103 275.8742 142.6138 -1.2585 267.0101 268.2686 275.9034 143.4358 -1.2565 267.0459 268.3023 275.9333 144.2283 -1.2481 267.0889 268.3370 276.1128 145.0205 -1.2509 267.2252 268.4761 276.1493 145.8728 -1.2606 267.3708 268.6314 276.2295 146.6345 -1.2558 267.5075 268.7634 276.3041 147.4568 -1.2679 267.5380 268.8059 276.5015 148.2450 -1.2660 267.5762 268.8421 276.5827 149.0340 -1.2733 267.7158 268.9891 276.6294 149.8520 -1.2751 267.8319 269.1070 276.7333 150.6400 -1.2772 267.9168 269.1941 276.8932 151.4580 -1.2819 267.9885 269.2703 276.9053 152.2463 -1.2770 268.0528 269.3298 276.9945 153.0355 -1.2809 268.1585 269.4394 277.0684 153.8540 -1.3007 268.2550 269.5557 277.1893 154.6128 -1.2930 268.3356 269.6286 277.1986 155.4620 -1.2919 268.4954 269.7873 277.4498 156.2500 -1.2871 268.5607 269.8479 277.4989 157.0380 -1.2933 268.5717 269.8650 277.5675 157.8563 -1.3072 268.6271 269.9343 277.7402 158.6458 -1.3014 268.7865 270.0879 277.8346 159.4645 -1.2989 268.8877 270.1866 277.9642 160.2545 -1.3054 268.9132 270.2186 278.0417 161.0448 -1.3077 269.0894 270.3972 278.1042 161.8648 -1.3120 269.0964 270.4085 278.3265 162.6558 -1.3184 269.1960 270.5144 278.3901 163.4748 -1.3150 269.3136 270.6286 278.5707 164.2630 -1.3161 269.3565 270.6726 278.6278 165.0520 -1.3282 269.4740 270.8021 278.7775 165.9008 -1.3268 269.5924 270.9192 278.8705 166.6613 -1.3217 269.7343 271.0560 279.0104 167.4825 -1.3360 269.7908 271.1269 279.0887 168.2743 -1.3241 269.9204 271.2446 279.1896 169.0650 -1.3262 270.0068 271.3330 279.3150 169.9158 -1.3239 270.1405 271.4644 279.3957 170.6775 -1.3423 270.1963 271.5386 279.4600 171.4990 -1.3353 270.2659 271.6012 279.5530 172.2913 -1.3494 270.2685 271.6180 279.6795 173.0825 -1.3375 270.2939 271.6313 279.7803 173.9350 -1.3467 270.5296 271.8763 279.9805 174.6968 -1.3552 270.5972 271.9524 280.0659 175.5188 -1.3526 270.7018 272.0544 280.0941 176.3110 -1.3487 270.8301 272.1789 280.1468 177.1025 -1.3572 270.8728 272.2300 280.2547 177.9550 -1.3660 271.0734 272.4394 280.4418 178.7168 -1.3654 271.0397 272.4051 280.5949 179.5388 -1.3645 271.1903 272.5549 280.6753 180.3310 -1.3735 271.2924 272.6659 280.7111 181.1225 -1.3770 271.4105 272.7876 280.8157 181.9753 -1.3671 271.4545 272.8216 280.9176 182.7375 -1.3572 271.5411 272.8984 281.0087 183.5598 -1.3656 271.6271 272.9927 281.1880 184.3518 -1.3600 271.7847 273.1448 281.3156 185.1435 -1.3726 271.8403 273.2129 281.3849 185.9658 -1.3652 271.9105 273.2757 281.5011 186.7575 -1.3778 272.0550 273.4328 281.5940 187.5795 -1.3813 272.1541 273.5354 281.6891 188.3715 -1.3819 272.2334 273.6153 281.8109 189.1635 -1.3932 272.2848 273.6780 281.9973 189.9855 -1.3912 272.4203 273.8116 282.1147 190.7775 -1.3846 272.5106 273.8953 282.2384 191.6003 -1.3791 272.6441 274.0232 282.2337 192.3925 -1.3809 272.7433 274.1242 282.4143 193.1843 -1.3765 272.8042 274.1807 282.5058 194.0070 -1.3980 272.9455 274.3435 282.5809 194.8010 -1.3980 273.0316 274.4297 282.7334 195.6228 -1.4019 273.1582 274.5602 282.8865 196.4150 -1.3926 273.2746 274.6672 282.9411 197.2065 -1.4057 273.2507 274.6564 283.0285 198.0290 -1.4073 273.4583 274.8656 283.1555 198.8208 -1.4007 273.5206 274.9213 283.2132 199.6435 -1.3978 273.4997 274.8975 283.3468 200.4360 -1.4056 273.6932 275.0988 283.4976 201.2275 -1.4133 273.7642 275.1775 283.5444 202.0498 -1.4039 273.8853 275.2892 283.7082 202.8415 -1.4039 274.0202 275.4241 283.8192 203.6635 -1.4201 274.0525 275.4726 283.8889 204.4555 -1.4140 274.1793 275.5933 283.9643 205.2475 -1.4043 274.1834 275.5877 284.0864 206.0695 -1.4225 274.3468 275.7693 284.1443 206.8615 -1.4261 274.4165 275.8426 284.3100 207.6835 -1.4307 274.4785 275.9093 284.3929 208.4755 -1.4271 274.6840 276.1111 284.4507 209.2675 -1.4221 274.7105 276.1326 284.5450 210.1200 -1.4392 274.8394 276.2786 284.6866 210.8825 -1.4378 274.9060 276.3438 284.8283 211.7045 -1.4535 274.9975 276.4510 284.8749 212.4965 -1.4561 275.1293 276.5853 284.9773 213.2833 -1.4445 275.2190 276.6635 285.0779 214.1320 -1.4521 275.2589 276.7110 285.2535 214.8903 -1.4641 275.3429 276.8070 285.3508 215.7083 -1.4643 275.4493 276.9135 285.5014 216.4963 -1.4629 275.6384 277.1013 285.5136 217.2855 -1.4572 275.6943 277.1514 285.6309 218.1063 -1.4545 275.7597 277.2142 285.7396 218.8653 -1.4671 275.8509 277.3180 285.8670 219.7133 -1.4596 275.9264 277.3861 286.0163 220.5015 -1.4729 276.1139 277.5867 286.1353 221.2895 -1.4861 276.3192 277.8053 286.1441 222.1083 -1.4862 276.3065 277.7927 286.2018 222.8968 -1.4791 276.4177 277.8968 286.3425 223.7165 -1.4752 276.5505 278.0257 286.4746 224.5078 -1.4761 276.6156 278.0917 286.5211 225.2973 -1.4765 276.6349 278.1114 286.6999 226.1160 -1.4920 276.7640 278.2560 286.8039 226.9053 -1.4797 276.8171 278.2968 286.9102 227.7238 -1.4811 276.9677 278.4487 286.9539 228.5123 -1.4830 277.1129 278.5959 287.0123 229.3013 -1.4861 277.1437 278.6298 287.1618 230.1213 -1.4992 277.2634 278.7626 287.2602 230.9115 -1.4979 277.3475 278.8454 287.3001 231.7313 -1.4863 277.4735 278.9597 287.4288 232.5220 -1.5053 277.4930 278.9983 287.5795 233.3135 -1.4935 277.6357 279.1292 287.7096 234.1360 -1.5002 277.7114 279.2116 287.8119 234.9278 -1.5003 277.8575 279.3578 287.8728 235.7498 -1.5147 277.9824 279.4971 287.9458 236.5420 -1.5103 278.1095 279.6198 288.1242 237.3335 -1.5037 278.2746 279.7783 288.1929 238.1555 -1.5096 278.3213 279.8309 288.2729 238.9175 -1.5144 278.4355 279.9499 288.3959 239.7700 -1.5114 278.4162 279.9276 288.4559 240.5615 -1.5074 278.4879 279.9952 288.5415 241.3535 -1.5136 278.6280 280.1416 288.6660 242.1755 -1.5067 278.7782 280.2849 288.7063 242.9375 -1.5172 278.7145 280.2317 288.8719 243.7895 -1.5261 278.8333 280.3594 288.9659 244.5818 -1.5321 278.9648 280.4969 289.0117 245.3735 -1.5430 279.1519 280.6949 289.0932 246.1955 -1.5311 279.2667 280.7978 289.1957 246.9575 -1.5322 279.3750 280.9072 289.2727 247.8095 -1.5274 279.5246 281.0520 289.3477 248.6015 -1.5390 279.5664 281.1055 289.5100 249.3930 -1.5484 279.6284 281.1768 289.6448 250.2155 -1.5434 279.7471 281.2905 289.7196 250.9770 -1.5470 279.7706 281.3177 289.7992 251.8290 -1.5433 279.9592 281.5025 289.9088 252.6210 -1.5568 280.0702 281.6269 289.9880 253.4125 -1.5515 280.1084 281.6599 290.1387 254.2350 -1.5351 280.1770 281.7121 290.3083 254.9965 -1.5463 280.3004 281.8467 290.4854 255.8490 -1.5430 280.3697 281.9127 290.5819 256.6410 -1.5562 280.5311 282.0874 290.6507 257.4325 -1.5598 280.6662 282.2260 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