DTA measure 2olom3 Test Date: 20231121:1158 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.67 s Mass = 1147 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3695 -5.2035 430.4492 435.6528 416.0628 3.9615 -5.2069 430.4445 435.6515 415.9412 5.5760 -5.2114 430.4356 435.6470 416.0609 7.1749 -5.2190 430.5207 435.7397 416.0124 8.7889 -5.2206 430.4856 435.7062 415.9047 10.4030 -5.2225 430.5462 435.7687 415.8918 12.0028 -5.2177 430.4817 435.6993 415.7441 13.6166 -5.2228 430.5294 435.7522 415.6947 15.2158 -5.2390 430.5367 435.7757 415.5485 16.8445 -5.2529 430.6748 435.9278 415.4446 18.4409 -5.2604 430.4653 435.7257 415.3273 20.0334 -5.2666 430.4937 435.7603 415.0305 21.6400 -5.2710 430.6175 435.8885 414.8599 23.2310 -5.2696 430.6919 435.9616 414.6643 24.8520 -5.2718 430.6600 435.9318 414.4003 26.4599 -5.2826 430.6678 435.9504 414.3687 28.0576 -5.2845 430.6630 435.9475 414.0851 29.6608 -5.2958 430.6663 435.9621 413.8559 31.2595 -5.3011 430.7158 436.0169 413.6342 32.8735 -5.3228 430.6939 436.0166 413.4475 34.4876 -5.3307 430.6578 435.9884 413.3020 36.0868 -5.3186 430.6146 435.9331 413.0305 37.7015 -5.3065 430.5305 435.8370 412.8728 39.3005 -5.3211 430.6878 436.0089 412.4835 40.8996 -5.3100 430.6695 435.9795 412.3649 42.5298 -5.3172 430.5711 435.8883 412.2231 44.1298 -5.3227 430.6045 435.9272 411.9849 45.7448 -5.3258 430.5345 435.8603 411.7793 47.3443 -5.3244 430.4917 435.8161 411.5326 48.9589 -5.3160 430.5864 435.9024 411.3465 50.5698 -5.3284 430.4760 435.8044 411.1708 52.1610 -5.3193 430.4673 435.7866 410.9756 53.7671 -5.3119 430.4408 435.7528 410.7366 55.3634 -5.3349 430.3903 435.7252 410.5432 56.9551 -5.3484 430.4074 435.7558 410.4542 58.5801 -5.3454 430.3227 435.6681 410.1387 60.1759 -5.3360 430.3323 435.6684 409.8573 61.7899 -5.3388 430.3282 435.6670 409.6534 63.3888 -5.3339 430.3020 435.6359 409.5119 64.9925 -5.3450 430.1419 435.4869 409.1650 66.6099 -5.3421 430.0577 435.3997 409.1193 68.2238 -5.3550 430.1295 435.4844 409.0802 69.8229 -5.3468 429.9812 435.3279 408.8236 71.4366 -5.3402 429.9019 435.2420 408.6300 73.0356 -5.3575 429.8490 435.2065 408.3845 74.6359 -5.3592 429.8709 435.2301 408.1991 76.2585 -5.3550 429.9001 435.2551 408.0370 77.8725 -5.3595 429.7753 435.1348 407.9182 79.4718 -5.3572 429.7612 435.1184 407.5740 81.0718 -5.3646 429.6972 435.0618 407.3679 82.6693 -5.3582 429.6216 434.9799 407.2499 84.2908 -5.3678 429.3890 434.7569 407.0558 85.8820 -5.3701 429.3612 434.7313 406.8818 87.4889 -5.3644 429.4781 434.8424 406.6876 89.0833 -5.3692 429.3864 434.7556 406.5058 90.6793 -5.3766 429.2982 434.6748 406.2946 92.3075 -5.3747 429.2417 434.6165 406.0421 93.9065 -5.3741 429.1877 434.5618 405.8463 95.5055 -5.3701 429.0819 434.4520 405.7294 97.1195 -5.3699 429.0057 434.3755 405.4837 98.7184 -5.3766 428.8397 434.2162 405.2820 100.3206 -5.3649 428.7634 434.1282 405.1998 101.9491 -5.3647 428.6029 433.9676 404.8124 103.5478 -5.3665 428.6141 433.9805 404.6389 105.1474 -5.3795 428.5602 433.9397 404.4286 106.7644 -5.3862 428.4490 433.8352 404.3396 108.3638 -5.3670 428.3648 433.7318 403.9582 109.9928 -5.3760 428.2156 433.5916 403.7556 111.5928 -5.3684 428.1486 433.5170 403.6363 113.1925 -5.3615 428.0836 433.4451 403.3828 114.8064 -5.3874 427.9383 433.3257 403.3680 116.4095 -5.3731 427.8200 433.1931 403.1725 118.0190 -5.3790 427.6856 433.0645 403.0145 119.6269 -5.3765 427.6406 433.0171 402.7398 121.2184 -5.3919 427.5014 432.8933 402.6333 122.8256 -5.3768 427.4323 432.8091 402.3188 124.4215 -5.3810 427.4344 432.8153 402.0314 126.0371 -5.3737 427.3103 432.6839 401.7999 127.6558 -5.3707 427.2842 432.6549 401.5695 129.2545 -5.3873 427.1260 432.5133 401.4864 130.8535 -5.3715 426.9184 432.2899 401.2468 132.4675 -5.4013 426.8409 432.2422 401.0688 134.0965 -5.3890 426.6747 432.0637 400.9241 135.6955 -5.3909 426.4366 431.8275 400.7872 137.2945 -5.3698 426.3519 431.7217 400.4728 138.9085 -5.3907 426.2806 431.6713 400.3253 140.5070 -5.3780 426.2733 431.6513 400.1414 142.1360 -5.3738 426.1333 431.5071 399.8430 143.7358 -5.3705 425.9680 431.3385 399.6897 145.3501 -5.3756 425.9385 431.3142 399.6070 146.9500 -5.3708 425.7827 431.1534 399.4141 148.5434 -5.3833 425.6222 431.0055 399.2165 150.1653 -5.3649 425.4883 430.8533 399.0023 151.7571 -5.3744 425.2543 430.6287 398.8306 153.3506 -5.3675 425.2322 430.5996 398.5269 154.9593 -5.3768 425.1871 430.5639 398.2413 156.5621 -5.3741 425.0110 430.3851 398.0811 158.1634 -5.3844 424.8750 430.2595 397.8898 159.7769 -5.3707 424.7097 430.0804 397.6634 161.3759 -5.3679 424.6027 429.9706 397.5431 162.9748 -5.3535 424.6260 429.9795 397.2254 164.5886 -5.3754 424.3603 429.7357 397.1524 166.1876 -5.3683 424.2846 429.6529 396.8849 167.8016 -5.3604 424.1125 429.4729 396.5989 169.4165 -5.3641 424.0808 429.4450 396.3920 171.0155 -5.3701 423.8099 429.1800 396.2905 172.6299 -5.3579 423.7040 429.0619 396.0696 174.2295 -5.3650 423.5318 428.8969 395.8767 175.8285 -5.3514 423.3758 428.7272 395.7132 177.4583 -5.3583 423.2820 428.6403 395.4363 179.0568 -5.3710 423.1858 428.5569 395.2132 180.6560 -5.3592 423.0544 428.4136 395.0360 182.2713 -5.3522 422.7871 428.1393 394.8712 183.8714 -5.3444 422.7205 428.0649 394.5857 185.5008 -5.3497 422.5482 427.8979 394.4591 187.1008 -5.3369 422.4074 427.7443 394.1825 188.7009 -5.3415 422.3631 427.7046 393.8540 190.3161 -5.3326 422.1366 427.4693 393.7609 191.9161 -5.3426 421.9547 427.2972 393.5630 193.5455 -5.3357 421.7290 427.0647 393.3733 195.1369 -5.3489 421.5776 426.9265 393.2024 196.7273 -5.3273 421.4931 426.8205 393.0307 198.3189 -5.3370 421.2999 426.6369 392.8712 199.9258 -5.3321 421.1770 426.5091 392.5451 201.5478 -5.3394 421.0650 426.4044 392.4003 203.1418 -5.3334 420.9683 426.3017 392.1712 204.7353 -5.3128 420.7802 426.0930 391.9748 206.3478 -5.3279 420.6453 425.9731 391.8416 207.9534 -5.3350 420.4442 425.7792 391.6050 209.5624 -5.3319 420.1860 425.5179 391.3838 211.1765 -5.3020 420.0561 425.3581 391.1833 212.7759 -5.3096 419.9794 425.2891 391.1059 214.3771 -5.3088 419.7848 425.0937 390.8293 215.9918 -5.3158 419.5595 424.8753 390.6696 217.6059 -5.3124 419.5103 424.8227 390.4147 219.2199 -5.3025 419.3569 424.6594 390.2121 220.8188 -5.2990 419.1378 424.4368 389.8989 222.4326 -5.2888 418.9513 424.2402 389.7242 224.0321 -5.2973 418.7936 424.0908 389.6243 225.6473 -5.3097 418.6571 423.9668 389.4403 227.2613 -5.2907 418.4838 423.7746 389.1368 228.8541 -5.2890 418.4583 423.7474 388.9208 230.4475 -5.2970 418.2028 423.4998 388.6339 232.0545 -5.2958 418.0065 423.3023 388.4806 233.6619 -5.2795 417.9370 423.2165 388.3526 235.2694 -5.2774 417.7050 422.9824 388.1530 236.8666 -5.2820 417.4982 422.7802 387.9079 238.4805 -5.2815 417.4197 422.7011 387.7307 240.0796 -5.2811 417.1816 422.4626 387.5855 241.6935 -5.2729 416.9395 422.2124 387.3521 243.3075 -5.2754 416.8131 422.0885 387.1553 244.9065 -5.2608 416.7082 421.9690 386.9852 246.5055 -5.2539 416.5071 421.7610 386.8139 248.1195 -5.2632 416.4319 421.6951 386.6280 249.7185 -5.2614 416.0047 421.2661 386.3916 251.3475 -5.2614 415.9759 421.2374 386.0761 252.9463 -5.2598 415.7680 421.0279 385.8826 254.5451 -5.2583 415.5326 420.7909 385.7627 256.1599 -5.2481 415.4485 420.6966 385.5349 257.7588 -5.2361 415.2874 420.5235 385.3075 259.3865 -5.2466 415.1041 420.3507 385.1375 260.9781 -5.2354 415.0119 420.2473 385.0018 262.5695 -5.2266 414.8046 420.0312 384.7093 264.1621 -5.2277 414.5496 419.7773 384.6346 265.7705 -5.2473 414.3693 419.6166 384.4716 267.3806 -5.2401 414.1480 419.3881 384.0897 268.9939 -5.2339 414.0055 419.2394 383.9249 270.5928 -5.2341 413.9190 419.1531 383.5205 272.1918 -5.2307 413.6849 418.9156 383.4211 273.7908 -5.2272 413.6425 418.8697 383.2368 275.4063 -5.2287 413.2952 418.5239 383.1426 277.0209 -5.2300 413.1405 418.3705 382.9080 278.6196 -5.2316 412.9398 418.1714 382.7204 280.2233 -5.2249 412.7265 417.9515 382.5430 281.8256 -5.2183 412.5656 417.7839 382.1956 283.4403 -5.2164 412.4476 417.6639 382.0455 285.0555 -5.2113 412.3746 417.5859 381.8826 286.6695 -5.2068 412.1542 417.3610 381.6055 288.2688 -5.2002 411.9334 417.1336 381.3721 289.8743 -5.2093 411.7947 417.0040 381.2271 291.4809 -5.2035 411.5171 416.7206 381.0019 293.0725 -5.1952 411.3078 416.5030 380.7721 294.6948 -5.1891 411.1650 416.3540 380.6104 296.2889 -5.1875 411.1041 416.2915 380.4512 297.8838 -5.1763 410.8191 415.9955 380.1383 299.4949 -5.1848 410.5760 415.7608 379.9962 301.0943 -5.1837 410.4962 415.6799 379.7263 302.6945 -5.1773 410.2968 415.4741 379.5706 304.3235 -5.1766 410.0722 415.2488 379.4132 305.9225 -5.1799 409.9152 415.0952 379.1535 307.5221 -5.1777 409.8016 414.9792 378.9035 309.1371 -5.1732 409.6648 414.8380 378.7686 310.7360 -5.1630 409.4045 414.5676 378.5658 312.3650 -5.1474 409.0708 414.2181 378.4384 313.9639 -5.1548 408.9608 414.1156 378.1489 315.5638 -5.1523 408.8056 413.9579 377.9136 317.1781 -5.1443 408.7577 413.9020 377.7455 318.7926 -5.1242 408.5263 413.6505 377.5831 320.4068 -5.1369 408.3098 413.4467 377.4977 322.0209 -5.1291 408.1063 413.2354 377.2307 323.6186 -5.1453 407.8501 412.9955 377.1081 325.2108 -5.1320 407.6408 412.7727 376.8186 326.8328 -5.1214 407.4451 412.5666 376.5965 328.4399 -5.1007 407.3396 412.4403 376.2016 330.0318 -5.1005 407.1523 412.2528 376.0394 331.6299 -5.0956 406.9482 412.0438 375.9359 333.2296 -5.0934 406.7558 411.8492 375.7075 334.8586 -5.0983 406.4916 411.5899 375.5369 336.4575 -5.0926 406.3720 411.4646 375.3404 338.0715 -5.0796 406.2248 411.3044 375.1935 339.6705 -5.0873 405.8914 410.9787 374.9520 341.2695 -5.0811 405.8479 410.9290 374.7557 342.8985 -5.0773 405.5990 410.6763 374.4704 344.4983 -5.0519 405.4436 410.4955 374.3326 346.1135 -5.0596 405.2739 410.3335 374.1680 347.7131 -5.0601 404.9428 410.0029 373.9559 349.3130 -5.0488 404.8831 409.9319 373.7684 350.9269 -5.0463 404.7084 409.7547 373.5495 352.5409 -5.0275 404.5223 409.5497 373.3257 354.1550 -5.0233 404.3912 409.4145 373.0524 355.7549 -5.0204 404.0632 409.0835 372.8442 357.3493 -5.0182 403.9003 408.9185 372.7199 358.9553 -5.0005 403.8159 408.8164 372.3587 360.5610 -4.9925 403.5395 408.5321 372.2518 362.1536 -4.9820 403.4094 408.3913 372.1188 363.7626 -5.0018 403.0200 408.0218 372.0623 365.3575 -4.9851 402.9494 407.9346 371.7791 366.9558 -4.9926 402.7830 407.7756 371.5984 368.5850 -4.9973 402.5723 407.5697 371.4538 370.1838 -4.9941 402.4095 407.4036 371.2144 371.7828 -5.0007 402.2291 407.2299 371.0424 373.3816 -4.9996 401.9012 406.9008 370.7786 374.9958 -4.9856 401.6759 406.6615 370.4510 376.6096 -4.9829 401.6188 406.6016 370.2024 378.2236 -4.9674 401.5022 406.4696 369.9151 379.8225 -4.9584 401.3315 406.2899 369.7628 381.4215 -4.9442 401.1526 406.0968 369.5139 383.0355 -4.9305 400.8056 405.7361 369.2074 384.6503 -4.9235 400.5959 405.5193 369.1120 386.2653 -4.9221 400.3984 405.3205 369.0107 387.8640 -4.9331 400.2065 405.1396 368.8225 389.4563 -4.9156 400.0046 404.9202 368.6158 391.0638 -4.9158 399.8569 404.7727 368.2852 392.6705 -4.9226 399.6237 404.5463 368.0503 394.2780 -4.9063 399.5458 404.4521 367.8112 395.8718 -4.9046 399.2468 404.1514 367.5794 397.4686 -4.8950 399.0437 403.9387 367.4307 399.0825 -4.8932 398.9600 403.8532 367.2069 400.6964 -4.8815 398.7658 403.6473 367.0110 402.2976 -4.8881 398.5760 403.4642 366.8307 403.9030 -4.8711 398.2700 403.1411 366.6378 405.5168 -4.8741 398.2324 403.1065 366.4845 407.1158 -4.8638 397.8366 402.7005 366.1866 408.7148 -4.8656 397.6081 402.4737 366.0353 410.3440 -4.8405 397.4568 402.2972 365.8578 411.9428 -4.8458 397.2173 402.0631 365.5510 413.5416 -4.8390 397.0386 401.8775 365.3607 415.1556 -4.8371 396.9512 401.7883 365.1923 416.7553 -4.8429 396.6982 401.5412 365.0002 418.3845 -4.8342 396.5512 401.3854 364.8328 419.9841 -4.8290 396.3384 401.1674 364.6397 421.5770 -4.8274 396.2265 401.0539 364.4095 423.1830 -4.8290 395.9121 400.7410 364.2076 424.7905 -4.8113 395.7037 400.5151 363.9271 426.3989 -4.8045 395.5917 400.3961 363.7785 427.9944 -4.8124 395.4310 400.2435 363.5137 429.5920 -4.8024 395.1974 399.9998 363.3203 431.2056 -4.7959 394.9794 399.7752 363.1517 432.8045 -4.7988 394.7214 399.5202 362.9408 434.4185 -4.7830 394.5670 399.3500 362.6758 436.0325 -4.7803 394.4054 399.1857 362.4931 437.6315 -4.7842 394.1696 398.9538 362.3102 439.2305 -4.7702 393.9003 398.6705 362.1174 440.8445 -4.7689 393.7686 398.5375 361.9089 442.4585 -4.7707 393.5690 398.3397 361.7550 444.0724 -4.7638 393.3501 398.1139 361.5731 445.6718 -4.7472 393.1919 397.9391 361.3011 447.2708 -4.7316 393.0263 397.7579 361.1071 448.8854 -4.7367 392.8993 397.6361 360.8695 450.4998 -4.7293 392.6271 397.3564 360.6762 452.1133 -4.7159 392.3140 397.0299 360.4725 453.7064 -4.7126 392.1523 396.8649 360.2538 455.2986 -4.7095 392.0037 396.7132 360.0855 456.8908 -4.6934 391.8762 396.5696 359.9200 458.5138 -4.7003 391.5894 396.2898 359.6953 460.1086 -4.6821 391.3539 396.0360 359.4933 461.7218 -4.6835 391.2279 395.9114 359.2628 463.3208 -4.6763 391.0959 395.7722 359.0191 464.9249 -4.6643 390.7587 395.4230 358.8117 466.5246 -4.6693 390.6153 395.2846 358.7106 468.1539 -4.6597 390.4686 395.1284 358.4051 469.7528 -4.6416 390.1947 394.8363 358.2103 471.3526 -4.6374 390.1440 394.7814 358.0171 472.9666 -4.6298 389.8599 394.4897 357.7631 474.5655 -4.6248 389.5419 394.1667 357.5568 476.1945 -4.6290 389.3721 394.0011 357.3415 477.7945 -4.6165 389.1062 393.7227 357.1410 479.3935 -4.6170 388.9489 393.5659 356.9334 481.0079 -4.6059 388.7451 393.3510 356.7279 482.6075 -4.6029 388.7183 393.3211 356.4942 484.2378 -4.5933 388.3668 392.9601 356.2637 485.8344 -4.5876 388.2026 392.7902 356.0574 487.4248 -4.5915 388.0302 392.6218 355.8986 489.0164 -4.5923 387.8011 392.3934 355.7050 490.6236 -4.5753 387.5613 392.1366 355.5282 492.2336 -4.5676 387.3938 391.9614 355.2982 493.8465 -4.5713 387.1952 391.7664 355.0736 495.4439 -4.5616 386.9999 391.5615 354.8085 497.0424 -4.5563 386.7776 391.3338 354.6985 498.6409 -4.5509 386.6489 391.1998 354.4557 500.2703 -4.5389 386.3751 390.9140 354.2531 501.8699 -4.5462 386.2013 390.7475 353.9952 503.4689 -4.5403 386.0053 390.5456 353.8669 505.0845 -4.5300 385.7275 390.2575 353.6112 506.6838 -4.5187 385.6060 390.1247 353.4943 508.2976 -4.5074 385.2983 389.8057 353.2364 509.9121 -4.5121 385.2986 389.8107 352.9933 511.5125 -4.5090 385.0524 389.5614 352.8846 513.1270 -4.5026 384.8643 389.3669 352.6341 514.7265 -4.4955 384.5973 389.0928 352.4111 516.3261 -4.4944 384.4021 388.8966 352.1786 517.9528 -4.4888 384.3010 388.7898 352.1271 519.5451 -4.4903 384.0478 388.5380 351.8557 521.1386 -4.4744 383.7638 388.2382 351.7580 522.7320 -4.4771 383.5267 388.0039 351.5498 524.3413 -4.4664 383.3147 387.7811 351.2903 525.9596 -4.4670 383.0896 387.5565 351.1345 527.5595 -4.4684 383.0593 387.5277 350.9007 529.1585 -4.4612 382.8869 387.3481 350.6919 530.7579 -4.4491 382.6424 387.0916 350.5152 532.3595 -4.4460 382.4277 386.8737 350.3126 533.9735 -4.4410 382.3173 386.7583 350.0897 535.5874 -4.4407 382.0837 386.5244 349.8798 537.1863 -4.4392 381.8063 386.2455 349.6864 538.7998 -4.4332 381.6945 386.1278 349.4526 540.3991 -4.4164 381.4145 385.8309 349.2344 541.9988 -4.4183 381.2050 385.6234 349.0251 543.6279 -4.4086 381.0160 385.4246 348.7072 545.2268 -4.4029 380.8027 385.2056 348.5864 546.8266 -4.3983 380.6698 385.0681 348.4765 548.4410 -4.3888 380.4011 384.7899 348.1671 550.0370 -4.3837 380.1532 384.5368 347.9289 551.6289 -4.3880 379.9741 384.3622 347.6930 553.2511 -4.3823 379.8942 384.2765 347.5680 554.8433 -4.3659 379.6765 384.0424 347.4115 556.4515 -4.3666 379.5309 383.8975 347.1138 558.0469 -4.3633 379.2580 383.6214 346.8891 559.6458 -4.3489 378.9614 383.3103 346.6771 561.2749 -4.3551 378.7733 383.1284 346.4625 562.8736 -4.3437 378.6079 382.9515 346.3455 564.4726 -4.3457 378.4121 382.7578 346.2260 566.0715 -4.3398 378.2163 382.5562 345.9044 567.6856 -4.3243 378.0348 382.3591 345.7854 569.2996 -4.3139 377.7160 382.0299 345.5538 570.9145 -4.3005 377.6061 381.9066 345.3865 572.5145 -4.3034 377.4015 381.7049 345.1602 574.1135 -4.2948 377.1051 381.3999 344.9406 575.7125 -4.2934 376.9530 381.2464 344.6878 577.3410 -4.2924 376.8087 381.1011 344.4717 578.9550 -4.2895 376.6022 380.8917 344.2929 580.5550 -4.2803 376.3120 380.5922 344.0454 582.1503 -4.2785 376.1160 380.3945 343.8592 583.7419 -4.2688 375.9404 380.2091 343.7521 585.3650 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