DTA measure 12_olom Test Date: 202436:1426 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.03 s Mass = 1145.000 mg data_number = 1582 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1923 -1.7349 230.5944 232.3293 261.5821 1.9563 -1.7319 230.7128 232.4447 261.5685 2.8110 -1.7310 230.8334 232.5644 261.5465 3.6030 -1.7263 230.9384 232.6647 261.5043 4.3945 -1.7296 231.0477 232.7774 261.5165 5.2058 -1.7279 231.1711 232.8990 261.5254 5.9965 -1.7219 231.2763 232.9982 261.5225 6.8203 -1.7221 231.4117 233.1339 261.5060 7.5838 -1.7213 231.5216 233.2429 261.5171 8.4373 -1.7196 231.6322 233.3518 261.5266 9.1993 -1.7166 231.7493 233.4659 261.5471 10.0205 -1.7163 231.8902 233.6065 261.5844 10.8125 -1.7156 231.9932 233.7089 261.5821 11.6048 -1.7130 232.0748 233.7878 261.6283 12.4565 -1.7124 232.2187 233.9311 261.6751 13.2193 -1.7094 232.3025 234.0119 261.7202 14.0435 -1.7077 232.4268 234.1346 261.7875 14.8393 -1.7065 232.5331 234.2396 261.8434 15.6415 -1.7056 232.6438 234.3493 261.9152 16.4375 -1.7038 232.7755 234.4793 261.9920 17.2308 -1.7009 232.8876 234.5884 262.0662 18.0535 -1.6999 233.0143 234.7142 262.1411 18.8155 -1.6992 233.1357 234.8349 262.2394 19.6668 -1.7004 233.2468 234.9473 262.3326 20.4600 -1.7020 233.3439 235.0459 262.4247 21.2530 -1.6994 233.4414 235.1407 262.5330 22.0775 -1.6984 233.5736 235.2720 262.6484 22.8398 -1.6994 233.6853 235.3847 262.7452 23.6970 -1.6986 233.8157 235.5143 262.8672 24.4630 -1.6989 233.9088 235.6076 262.9809 25.2853 -1.6942 234.0352 235.7294 263.0992 26.1380 -1.6952 234.1433 235.8385 263.2617 26.8998 -1.6966 234.2543 235.9509 263.3951 27.7218 -1.6944 234.3670 236.0614 263.5285 28.5133 -1.6986 234.4726 236.1713 263.6428 29.3048 -1.7009 234.5696 236.2705 263.7635 30.1605 -1.7011 234.7160 236.4171 263.9230 30.9240 -1.7017 234.8291 236.5308 264.0416 31.7455 -1.6981 234.9560 236.6541 264.1958 32.5373 -1.6965 235.0629 236.7594 264.3363 33.3285 -1.6981 235.1650 236.8630 264.4747 34.1540 -1.6983 235.2711 236.9694 264.6156 34.9198 -1.6982 235.3875 237.0857 264.7627 35.7755 -1.6923 235.5243 237.2166 264.9237 36.5398 -1.6942 235.6014 237.2956 265.0681 37.3613 -1.6947 235.7444 237.4391 265.2388 38.1528 -1.6978 235.8591 237.5569 265.3896 38.9465 -1.6998 235.9615 237.6613 265.5436 39.7713 -1.7005 236.0646 237.7651 265.6846 40.5335 -1.7007 236.1677 237.8684 265.8387 41.3880 -1.7016 236.2467 237.9483 266.0111 42.1540 -1.7010 236.3781 238.0791 266.1470 42.9775 -1.7049 236.4904 238.1952 266.3063 43.7765 -1.7057 236.6206 238.3263 266.4546 44.5718 -1.7025 236.7599 238.4624 266.6178 45.4005 -1.7009 236.8616 238.5625 266.7741 46.1628 -1.7038 236.9686 238.6724 266.9045 47.0210 -1.7020 237.1001 238.8021 267.0346 47.7843 -1.7055 237.1994 238.9049 267.1638 48.6073 -1.7070 237.3231 239.0301 267.3108 49.3990 -1.7072 237.4483 239.1555 267.4518 50.1908 -1.7086 237.5627 239.2714 267.5816 51.0430 -1.7086 237.6686 239.3772 267.7279 51.8050 -1.7110 237.7847 239.4957 267.8492 52.6268 -1.7110 237.8951 239.6062 267.9814 53.4190 -1.7149 238.0085 239.7234 268.1279 54.2105 -1.7122 238.1290 239.8412 268.2612 55.0330 -1.7117 238.2229 239.9347 268.3895 55.7968 -1.7140 238.3470 240.0610 268.5004 56.6568 -1.7169 238.4771 240.1940 268.6245 57.4188 -1.7176 238.5795 240.2971 268.7382 58.2400 -1.7175 238.6908 240.4083 268.8519 59.0345 -1.7202 238.8013 240.5215 268.9748 59.8273 -1.7194 238.9245 240.6439 269.0766 60.6500 -1.7195 239.0358 240.7552 269.1745 61.4413 -1.7176 239.1510 240.8687 269.2817 62.2618 -1.7206 239.2673 240.9879 269.3953 63.0523 -1.7191 239.3609 241.0800 269.4984 63.8438 -1.7222 239.4846 241.2068 269.5960 64.6658 -1.7234 239.6076 241.3310 269.6779 65.4563 -1.7257 239.7247 241.4503 269.7935 66.2775 -1.7272 239.8592 241.5864 269.8901 67.0493 -1.7274 239.9792 241.7066 269.9821 67.8715 -1.7307 240.0874 241.8181 270.1024 68.6633 -1.7328 240.2110 241.9438 270.1880 69.4558 -1.7331 240.3134 242.0465 270.2674 70.3070 -1.7296 240.4168 242.1464 270.3833 71.0703 -1.7316 240.5151 242.2467 270.4534 71.8948 -1.7313 240.6282 242.3595 270.5509 72.6860 -1.7331 240.7428 242.4759 270.6311 73.4803 -1.7317 240.8705 242.6022 270.7136 74.2823 -1.7285 240.9853 242.7138 270.7925 75.0735 -1.7302 241.1063 242.8365 270.8791 75.9248 -1.7326 241.2046 242.9371 270.9825 76.6845 -1.7330 241.3241 243.0572 271.0560 77.5070 -1.7323 241.4341 243.1664 271.1576 78.3263 -1.7320 241.5589 243.2909 271.2517 79.0863 -1.7343 241.6758 243.4101 271.3515 79.9393 -1.7357 241.7780 243.5137 271.4273 80.6998 -1.7370 241.9139 243.6508 271.4954 81.5188 -1.7362 242.0126 243.7488 271.5824 82.3373 -1.7380 242.1167 243.8547 271.6595 83.0968 -1.7390 242.2267 243.9657 271.7285 83.9465 -1.7402 242.3463 244.0865 271.8169 84.7350 -1.7419 242.4567 244.1986 271.9133 85.5240 -1.7434 242.5699 244.3134 271.9843 86.3478 -1.7454 242.6985 244.4439 272.0712 87.1278 -1.7461 242.7947 244.5408 272.1575 87.9498 -1.7466 242.9222 244.6688 272.2433 88.7093 -1.7485 243.0183 244.7668 272.3590 89.5593 -1.7492 243.1377 244.8869 272.4462 90.3488 -1.7485 243.2431 244.9915 272.5294 91.1420 -1.7514 243.3621 245.1135 272.6077 91.9650 -1.7510 243.4922 245.2432 272.7081 92.7250 -1.7525 243.6114 245.3640 272.8052 93.5763 -1.7529 243.7114 245.4643 272.9031 94.3405 -1.7539 243.8217 245.5756 272.9917 95.1635 -1.7562 243.9370 245.6932 273.1031 95.9570 -1.7602 244.0522 245.8124 273.1885 96.7788 -1.7647 244.1584 245.9231 273.2719 97.6000 -1.7590 244.2772 246.0362 273.3828 98.3923 -1.7568 244.3981 246.1549 273.4828 99.1835 -1.7580 244.5063 246.2643 273.5806 100.0040 -1.7599 244.6347 246.3946 273.6764 100.7963 -1.7627 244.7425 246.5052 273.7937 101.6178 -1.7602 244.8620 246.6221 273.8872 102.4093 -1.7641 244.9585 246.7226 274.0047 103.2083 -1.7651 245.0738 246.8389 274.1135 104.0093 -1.7656 245.1757 246.9413 274.2092 104.8025 -1.7680 245.2891 247.0571 274.3536 105.6283 -1.7680 245.3967 247.1648 274.4438 106.3880 -1.7662 245.5036 247.2697 274.5392 107.2450 -1.7702 245.6237 247.3939 274.6740 108.0068 -1.7756 245.7468 247.5224 274.7644 108.8305 -1.7796 245.8444 247.6240 274.8968 109.6225 -1.7801 245.9762 247.7562 275.0036 110.4133 -1.7834 246.0786 247.8619 275.1166 111.2643 -1.7825 246.1819 247.9645 275.2379 112.0250 -1.7844 246.3004 248.0848 275.3631 112.8465 -1.7884 246.4281 248.2165 275.4793 113.6385 -1.7912 246.5196 248.3108 275.5968 114.4298 -1.7903 246.6246 248.4149 275.7363 115.2815 -1.7927 246.7665 248.5592 275.8585 116.0435 -1.7935 246.8630 248.6564 275.9503 116.8655 -1.7969 246.9844 248.7813 276.0763 117.6583 -1.7979 247.0879 248.8858 276.2000 118.4518 -1.8012 247.2039 249.0051 276.3206 119.2750 -1.8016 247.3217 249.1233 276.4380 120.0375 -1.8034 247.4285 249.2320 276.5881 120.8893 -1.8004 247.5478 249.3482 276.6941 121.6805 -1.8043 247.6748 249.4791 276.7875 122.4708 -1.8076 247.8039 249.6115 276.8951 123.2925 -1.8055 247.8834 249.6889 277.0235 124.0523 -1.8051 247.9986 249.8036 277.1445 124.9030 -1.8110 248.1111 249.9221 277.2682 125.6933 -1.8112 248.2202 250.0314 277.3698 126.4845 -1.8121 248.3261 250.1382 277.4965 127.3073 -1.8138 248.4515 250.2653 277.5850 128.0670 -1.8179 248.5487 250.3666 277.6863 128.9188 -1.8148 248.6642 250.4789 277.7955 129.7100 -1.8167 248.7823 250.5991 277.9155 130.5000 -1.8173 248.8809 250.6982 278.0166 131.3225 -1.8187 248.9909 250.8096 278.1232 132.0845 -1.8215 249.1064 250.9280 278.2125 132.9363 -1.8231 249.2236 251.0467 278.3334 133.7308 -1.8243 249.3209 251.1452 278.4334 134.5258 -1.8246 249.4484 251.2730 278.5297 135.3168 -1.8257 249.5488 251.3745 278.6289 136.1073 -1.8246 249.6795 251.5041 278.7409 136.9585 -1.8289 249.7931 251.6220 278.8235 137.7210 -1.8307 249.9040 251.7347 278.9347 138.5460 -1.8319 250.0164 251.8483 279.0459 139.3375 -1.8292 250.1219 251.9511 279.1606 140.1288 -1.8320 250.2312 252.0632 279.2499 140.9505 -1.8343 250.3432 252.1776 279.3501 141.7418 -1.8372 250.4501 252.2873 279.4477 142.5635 -1.8379 250.5666 252.4045 279.5481 143.3555 -1.8396 250.7017 252.5412 279.6397 144.1470 -1.8409 250.8292 252.6701 279.7579 144.9685 -1.8433 250.9246 252.7679 279.8437 145.7588 -1.8423 251.0319 252.8742 279.9242 146.5805 -1.8433 251.1328 252.9761 280.0469 147.3725 -1.8474 251.2489 253.0964 280.1346 148.1628 -1.8462 251.3725 253.2186 280.2304 148.9863 -1.8463 251.4627 253.3089 280.3440 149.7468 -1.8498 251.5729 253.4227 280.4359 150.5990 -1.8562 251.6918 253.5480 280.5087 151.3915 -1.8568 251.8116 253.6684 280.6208 152.1830 -1.8581 251.9318 253.7899 280.7222 153.0060 -1.8566 252.0443 253.9009 280.8039 153.7678 -1.8556 252.1441 253.9997 280.9060 154.6200 -1.8574 252.2671 254.1245 281.0154 155.3808 -1.8587 252.3788 254.2375 281.0956 156.2023 -1.8612 252.4924 254.3537 281.1924 157.0240 -1.8643 252.6053 254.4697 281.3125 157.7845 -1.8649 252.7110 254.5759 281.3931 158.6368 -1.8647 252.8164 254.6811 281.4999 159.3968 -1.8686 252.9399 254.8085 281.6112 160.2185 -1.8686 253.0620 254.9306 281.6946 161.0105 -1.8707 253.1537 255.0244 281.7936 161.8018 -1.8696 253.2735 255.1431 281.8856 162.6525 -1.8724 253.4000 255.2724 281.9954 163.4138 -1.8704 253.5117 255.3821 282.0939 164.2355 -1.8691 253.6195 255.4886 282.2168 165.0275 -1.8732 253.7123 255.5855 282.3211 165.8188 -1.8763 253.8046 255.6809 282.4272 166.6405 -1.8777 253.9185 255.7962 282.5382 167.4025 -1.8764 254.0369 255.9133 282.6264 168.2545 -1.8772 254.1408 256.0179 282.7410 169.0208 -1.8801 254.2609 256.1410 282.8269 169.8425 -1.8818 254.3826 256.2644 282.9290 170.6645 -1.8887 254.4891 256.3778 283.0831 171.4265 -1.9039 254.5980 256.5019 283.1897 172.2800 -1.9046 254.7216 256.6262 283.2983 173.0425 -1.8992 254.8199 256.7191 283.3923 173.8630 -1.8900 254.9315 256.8215 283.5358 174.6863 -1.8933 255.0504 256.9437 283.6509 175.4520 -1.8958 255.1571 257.0529 283.7456 176.3020 -1.8892 255.2876 257.1767 283.8660 177.0638 -1.8833 255.3831 257.2664 283.9771 177.8870 -1.8849 255.5061 257.3910 284.0897 178.6560 -1.8932 255.6408 257.5340 284.2135 179.4915 -1.8959 255.7379 257.6338 284.3175 180.2930 -1.8908 255.8429 257.7337 284.4184 181.0833 -1.8869 255.9561 257.8430 284.5426 181.9100 -1.8982 256.0586 257.9569 284.6487 182.6715 -1.9027 256.1700 258.0727 284.7490 183.5235 -1.9067 256.2818 258.1885 284.8849 184.3148 -1.9082 256.3889 258.2971 285.0046 185.1060 -1.9121 256.5020 258.4141 285.1150 185.9275 -1.9144 256.6256 258.5400 285.2147 186.6895 -1.9169 256.7154 258.6323 285.3132 187.5415 -1.9167 256.8431 258.7597 285.4373 188.3028 -1.9210 256.9458 258.8667 285.5441 189.1245 -1.9212 257.0596 258.9808 285.6619 189.9455 -1.9182 257.1787 259.0969 285.7897 190.7075 -1.9202 257.2883 259.2085 285.8817 191.5595 -1.9222 257.4099 259.3321 286.0085 192.3205 -1.9232 257.5079 259.4311 286.1184 193.1420 -1.9234 257.6296 259.5530 286.2367 193.9333 -1.9224 257.7478 259.6702 286.3301 194.7245 -1.9245 257.8520 259.7765 286.4508 195.5765 -1.9282 257.9535 259.8816 286.5699 196.3375 -1.9293 258.0785 260.0078 286.6701 197.1593 -1.9302 258.2058 260.1360 286.8078 197.9505 -1.9316 258.3110 260.2426 286.9005 198.7415 -1.9337 258.4216 260.3553 287.0052 199.5633 -1.9363 258.5374 260.4737 287.1324 200.3545 -1.9366 258.6280 260.5646 287.2270 201.1758 -1.9409 258.7308 260.6716 287.3560 201.9685 -1.9397 258.8505 260.7902 287.4379 202.7595 -1.9394 258.9636 260.9030 287.5233 203.5823 -1.9418 259.0881 261.0299 287.6524 204.3720 -1.9440 259.1940 261.1379 287.7466 205.1935 -1.9436 259.3069 261.2505 287.8524 205.9840 -1.9451 259.4227 261.3678 287.9533 206.7755 -1.9484 259.5259 261.4743 288.0494 207.5988 -1.9520 259.6389 261.5909 288.1360 208.3588 -1.9523 259.7426 261.6949 288.2240 209.2108 -1.9554 259.8655 261.8209 288.3344 209.9783 -1.9601 259.9780 261.9381 288.4385 210.8005 -1.9623 260.0937 262.0560 288.5437 211.6225 -1.9591 260.2125 262.1716 288.6353 212.3840 -1.9588 260.3372 262.2960 288.7175 213.2355 -1.9645 260.4509 262.4154 288.8118 213.9970 -1.9682 260.5238 262.4920 288.8877 214.8185 -1.9694 260.6516 262.6210 288.9847 215.6105 -1.9699 260.7567 262.7266 289.0685 216.4020 -1.9697 260.8747 262.8444 289.1582 217.2545 -1.9699 260.9970 262.9669 289.2738 218.0155 -1.9703 261.0974 263.0677 289.3707 218.8375 -1.9697 261.2040 263.1737 289.4486 219.6295 -1.9726 261.3061 263.2787 289.5497 220.4208 -1.9767 261.4228 263.3995 289.6190 221.2723 -1.9721 261.5466 263.5187 289.7208 222.0338 -1.9735 261.6642 263.6377 289.8439 222.8550 -1.9740 261.7635 263.7376 289.9705 223.6465 -1.9749 261.8864 263.8614 290.0301 224.4375 -1.9768 262.0063 263.9831 290.1258 225.2888 -1.9799 262.0950 264.0748 290.2369 226.0503 -1.9816 262.2242 264.2057 290.3189 226.8718 -1.9842 262.3424 264.3267 290.4082 227.6678 -1.9851 262.4385 264.4236 290.4998 228.4638 -1.9830 262.5267 264.5097 290.5962 229.2860 -1.9874 262.6426 264.6300 290.7211 230.0558 -1.9914 262.7736 264.7650 290.8283 230.8870 -1.9889 262.8910 264.8799 290.9175 231.6788 -1.9936 262.9818 264.9754 291.0264 232.5008 -1.9946 263.1013 265.0959 291.1189 233.2930 -1.9964 263.2189 265.2153 291.2145 234.0840 -1.9953 263.3136 265.3090 291.3011 234.9055 -1.9985 263.4222 265.4207 291.3868 235.6975 -2.0021 263.5601 265.5622 291.5075 236.5190 -2.0042 263.6655 265.6698 291.6193 237.3105 -2.0060 263.7739 265.7799 291.7138 238.1013 -2.0041 263.8935 265.8976 291.8256 238.9225 -2.0045 264.0144 266.0188 291.9372 239.7138 -2.0046 264.1167 266.1213 292.0234 240.5353 -2.0071 264.2256 266.2326 292.1268 241.3268 -2.0059 264.3317 266.3376 292.2321 242.1178 -2.0078 264.4395 266.4473 292.3277 242.9395 -2.0092 264.5470 266.5562 292.4320 243.7015 -2.0111 264.6506 266.6616 292.5449 244.5533 -2.0120 264.7702 266.7822 292.6587 245.3445 -2.0132 264.8726 266.8858 292.7684 246.1365 -2.0144 264.9808 266.9952 292.8638 246.9358 -2.0174 265.1101 267.1275 292.9525 247.7285 -2.0205 265.2171 267.2376 293.0640 248.5803 -2.0217 265.3288 267.3505 293.1724 249.3415 -2.0230 265.4387 267.4617 293.2770 250.1633 -2.0226 265.5488 267.5715 293.3912 250.9623 -2.0253 265.6551 267.6804 293.5068 251.7555 -2.0299 265.7718 267.8017 293.6161 252.5773 -2.0320 265.8836 267.9156 293.7358 253.3380 -2.0337 265.9868 268.0205 293.8427 254.1898 -2.0318 266.1060 268.1378 293.9725 254.9535 -2.0318 266.2189 268.2507 294.0824 255.7748 -2.0412 266.3373 268.3785 294.2019 256.5970 -2.0534 266.4345 268.4879 294.3147 257.3585 -2.0571 266.5472 268.6043 294.4228 258.2155 -2.0523 266.6680 268.7203 294.5599 258.9503 -2.0571 266.7739 268.8311 294.6785 259.8090 -2.0520 266.8912 268.9432 294.8066 260.5708 -2.0519 266.9917 269.0436 294.9269 261.3925 -2.0605 267.1048 269.1653 295.0520 262.2158 -2.0600 267.2002 269.2602 295.1582 262.9828 -2.0559 267.3210 269.3769 295.2779 263.8045 -2.0554 267.4395 269.4949 295.4098 264.5968 -2.0581 267.5516 269.6098 295.5247 265.4188 -2.0585 267.6562 269.7147 295.6445 266.2105 -2.0635 267.7698 269.8333 295.7522 267.0013 -2.0630 267.8863 269.9493 295.8657 267.8225 -2.0657 267.9942 270.0599 295.9774 268.6145 -2.0684 268.0988 270.1671 296.0991 269.4365 -2.0684 268.2079 270.2763 296.2010 270.2285 -2.0687 268.3145 270.3833 296.3151 271.0200 -2.0718 268.4445 270.5164 296.4190 271.8425 -2.0727 268.5556 270.6283 296.5349 272.6045 -2.0742 268.6467 270.7209 296.6465 273.4565 -2.0749 268.7562 270.8310 296.7577 274.2185 -2.0783 268.8671 270.9454 296.8558 275.0393 -2.0796 268.9933 271.0729 296.9630 275.8613 -2.0837 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