DTA measure 21olom Test Date: 202436:1356 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1649.10 s Mass = 1145.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4543 -4.4068 417.4017 421.8085 420.6494 4.0553 -4.4076 417.4676 421.8753 420.6424 5.6829 -4.4037 417.5440 421.9477 420.6396 7.2818 -4.3991 417.5904 421.9895 420.5995 8.8784 -4.3950 417.6500 422.0450 420.5534 10.4908 -4.3881 417.7294 422.1175 420.4667 12.0898 -4.3804 417.7872 422.1676 420.3904 13.7041 -4.3769 417.8509 422.2277 420.2719 15.3179 -4.3692 417.9112 422.2804 420.1440 16.9168 -4.3815 417.9598 422.3413 420.0025 18.5104 -4.3801 418.0173 422.3974 419.8432 20.1343 -4.3574 418.0598 422.4171 419.6494 21.7376 -4.3388 418.1054 422.4442 419.4631 23.3529 -4.3283 418.1548 422.4831 419.2695 24.9658 -4.3196 418.2012 422.5208 419.0543 26.5753 -4.3085 418.2575 422.5660 418.8540 28.1673 -4.3012 418.2955 422.5967 418.6155 29.7748 -4.2937 418.3262 422.6199 418.3569 31.3841 -4.2851 418.3586 422.6437 418.1222 32.9934 -4.2748 418.3972 422.6720 417.8749 34.5883 -4.2628 418.4278 422.6906 417.6162 36.1965 -4.2480 418.4669 422.7148 417.3509 37.8059 -4.2371 418.4862 422.7233 417.1030 39.4138 -4.2283 418.5267 422.7550 416.8592 41.0243 -4.2184 418.5395 422.7579 416.6083 42.6223 -4.2087 418.5668 422.7754 416.3534 44.2238 -4.1969 418.5883 422.7851 416.1107 45.8215 -4.1869 418.5851 422.7720 415.8746 47.4528 -4.1735 418.6049 422.7784 415.6560 49.0606 -4.1644 418.6320 422.7964 415.4188 50.6585 -4.1540 418.6393 422.7933 415.1934 52.2694 -4.1418 418.6442 422.7860 414.9700 53.8673 -4.1283 418.6425 422.7708 414.7707 55.4790 -4.1154 418.6443 422.7596 414.5726 57.0874 -4.1021 418.6464 422.7485 414.3517 58.6826 -4.0935 418.6653 422.7587 414.1306 60.2931 -4.0820 418.6410 422.7230 413.9369 61.8920 -4.0770 418.6304 422.7074 413.7572 63.5035 -4.0605 418.6372 422.6978 413.5609 65.1194 -4.0461 418.6137 422.6599 413.3611 66.7213 -4.0334 418.5936 422.6270 413.2076 68.3196 -4.0266 418.5527 422.5793 413.0129 70.0165 -4.0153 418.5865 422.6018 412.7896 71.7444 -4.0032 418.5532 422.5564 412.6253 73.3436 -3.9941 418.5314 422.5255 412.4450 74.9603 -3.9839 418.5259 422.5097 412.2625 76.5578 -3.9745 418.4997 422.4741 412.0943 78.1684 -3.9659 418.4552 422.4211 411.9303 79.7778 -3.9518 418.4397 422.3915 411.7625 81.3753 -3.9429 418.3945 422.3374 411.5983 82.9881 -3.9314 418.3822 422.3137 411.4462 84.5859 -3.9249 418.3458 422.2707 411.2528 86.1925 -3.9110 418.3223 422.2333 411.0795 87.8203 -3.9032 418.2797 422.1829 410.8977 89.4146 -3.8931 418.2415 422.1346 410.7152 91.0071 -3.8826 418.2130 422.0956 410.5251 92.6204 -3.8754 418.1622 422.0377 410.3532 94.2176 -3.8643 418.1108 421.9750 410.1709 95.8425 -3.8603 418.0809 421.9412 409.9801 97.4463 -3.8519 418.0374 421.8893 409.7966 99.0449 -3.8408 418.0019 421.8427 409.5991 100.6431 -3.8310 417.9491 421.7800 409.4164 102.2590 -3.8265 417.8981 421.7246 409.2081 103.8574 -3.8161 417.8438 421.6599 409.0362 105.4688 -3.8030 417.7890 421.5920 408.8103 107.0801 -3.7941 417.7310 421.5250 408.6108 108.6758 -3.7853 417.6848 421.4701 408.4239 110.2866 -3.7755 417.6326 421.4081 408.2148 111.8836 -3.7657 417.5512 421.3169 408.0207 113.5105 -3.7553 417.4871 421.2424 407.8064 115.1071 -3.7463 417.4357 421.1820 407.6228 116.7024 -3.7409 417.3664 421.1073 407.4106 118.3114 -3.7478 417.3056 421.0534 407.2172 119.9158 -3.7362 417.2444 420.9805 407.0213 121.5306 -3.7310 417.1771 420.9081 406.8069 123.1306 -3.7136 417.0965 420.8101 406.6094 124.7315 -3.6958 417.0263 420.7221 406.4234 126.3451 -3.6825 416.9397 420.6222 406.2334 127.9403 -3.6768 416.8759 420.5527 406.0355 129.5836 -3.6834 416.8044 420.4877 405.8381 131.2010 -3.6611 416.7213 420.3824 405.6376 132.7894 -3.6519 416.6453 420.2972 405.4537 134.4010 -3.6389 416.5641 420.2030 405.2579 136.0165 -3.6280 416.4868 420.1148 405.0629 137.6306 -3.6187 416.4016 420.0203 404.8519 139.2314 -3.6116 416.3237 419.9353 404.6610 140.8375 -3.6009 416.2280 419.8289 404.4635 142.4364 -3.5935 416.1598 419.7533 404.2551 144.0506 -3.5845 416.0763 419.6608 404.0685 145.6488 -3.5769 415.9784 419.5553 403.8586 147.2458 -3.5658 415.8902 419.4560 403.6668 148.8718 -3.5558 415.7839 419.3397 403.4639 150.4815 -3.5500 415.7194 419.2694 403.2503 152.0808 -3.5410 415.6137 419.1548 403.0570 153.6808 -3.5351 415.5245 419.0596 402.8593 155.2906 -3.5279 415.4211 418.9490 402.6595 156.8963 -3.5187 415.3310 418.8497 402.4794 158.5046 -3.5101 415.2259 418.7361 402.2787 160.1041 -3.5000 415.1264 418.6263 402.0965 161.7155 -3.4923 415.0186 418.5109 401.9049 163.3186 -3.4854 414.9256 418.4110 401.7198 164.9216 -3.4767 414.8257 418.3024 401.5282 166.5336 -3.4664 414.7075 418.1739 401.3262 168.1820 -3.4610 414.6059 418.0669 401.1156 169.7795 -3.4556 414.5030 417.9586 400.9277 171.3750 -3.4490 414.3939 417.8428 400.7242 172.9839 -3.4419 414.2939 417.7359 400.5272 174.5971 -3.4329 414.1640 417.5969 400.3217 176.2068 -3.4216 414.0648 417.4864 400.1155 177.8179 -3.4162 413.9554 417.3715 399.9165 179.4154 -3.4021 413.8456 417.2477 399.7154 181.0124 -3.3935 413.7329 417.1263 399.5182 182.6578 -3.4084 413.6019 417.0104 399.3060 184.3603 -3.3839 413.4783 416.8622 399.1148 185.9544 -3.3688 413.3632 416.7320 398.9144 187.5649 -3.3637 413.2609 416.6246 398.7048 189.1621 -3.3546 413.1480 416.5026 398.4969 190.7739 -3.3447 413.0297 416.3744 398.3206 192.3874 -3.3377 412.9035 416.2411 398.1079 193.9836 -3.3302 412.7798 416.1100 397.9230 195.5946 -3.3204 412.6388 415.9592 397.7212 197.1878 -3.3134 412.5339 415.8473 397.5269 198.8128 -3.3081 412.3931 415.7012 397.3300 200.4141 -3.3059 412.2834 415.5894 397.1413 202.0176 -3.3004 412.1741 415.4745 396.9446 203.6176 -3.2894 412.0342 415.3236 396.7471 205.2195 -3.2796 411.9073 415.1870 396.5514 206.8235 -3.2735 411.7670 415.0405 396.3442 208.4404 -3.2646 411.6279 414.8925 396.1363 210.0564 -3.2572 411.5149 414.7721 395.9306 211.6529 -3.2518 411.3861 414.6378 395.7304 213.2514 -3.2418 411.2574 414.4993 395.5120 214.8644 -3.2358 411.1170 414.3528 395.3234 216.4748 -3.2269 410.9861 414.2130 395.0998 218.0849 -3.2245 410.8558 414.0804 394.8781 219.6821 -3.2165 410.7153 413.9317 394.6776 221.2921 -3.2085 410.5787 413.7872 394.4755 222.8879 -3.1995 410.4471 413.6466 394.2645 224.5019 -3.1912 410.3104 413.5016 394.0533 226.1143 -3.1857 410.1564 413.3421 393.8557 227.7240 -3.1766 410.0248 413.2015 393.6471 229.3145 -3.1678 409.8924 413.0603 393.4317 230.9273 -3.1611 409.7383 412.8994 393.2306 232.5279 -3.1543 409.6047 412.7590 393.0096 234.1408 -3.1504 409.4736 412.6239 392.8091 235.7555 -3.1424 409.3195 412.4619 392.6230 237.3404 -3.1337 409.1816 412.3153 392.4221 238.9563 -3.1273 409.0304 412.1577 392.2101 240.5538 -3.1165 408.9018 412.0183 392.0087 242.1620 -3.1101 408.7427 411.8528 391.8239 243.7779 -3.0999 408.6020 411.7020 391.6049 245.3885 -3.0958 408.4417 411.5375 391.4106 246.9841 -3.0855 408.3201 411.4057 391.2159 248.5796 -3.0778 408.1758 411.2535 391.0188 250.1895 -3.0694 408.0204 411.0898 390.8409 251.8039 -3.0639 407.8796 410.9435 390.6413 253.4148 -3.0587 407.7206 410.7793 390.4405 255.0121 -3.0546 407.5698 410.6244 390.2627 256.6108 -3.0508 407.4208 410.4716 390.0494 258.2145 -3.0410 407.2706 410.3116 389.8554 259.8439 -3.0365 407.1191 410.1555 389.6466 261.4435 -3.0289 406.9730 410.0019 389.4415 263.0400 -3.0230 406.8082 409.8313 389.2363 264.6529 -3.0162 406.6660 409.6821 389.0251 266.2470 -3.0085 406.5251 409.5335 388.8177 267.8719 -3.0024 406.3440 409.3464 388.6181 269.4640 -2.9949 406.2035 409.1984 388.4150 271.0740 -2.9935 406.0417 409.0353 388.2063 272.6721 -2.9896 405.8919 408.8815 388.0003 274.2726 -2.9815 405.7387 408.7202 387.8018 275.9029 -2.9734 405.5795 408.5530 387.5850 277.5015 -2.9651 405.4374 408.4025 387.3746 279.1129 -2.9578 405.2566 408.2143 387.1797 280.7108 -2.9515 405.1103 408.0618 386.9756 282.3123 -2.9477 404.9331 407.8808 386.7873 283.9089 -2.9399 404.7797 407.7196 386.5798 285.5391 -2.9327 404.6307 407.5633 386.3691 287.1386 -2.9259 404.4667 407.3925 386.1751 288.7386 -2.9189 404.2993 407.2183 385.9621 290.3441 -2.9152 404.1428 407.0580 385.7670 291.9506 -2.9070 403.9790 406.8860 385.5536 293.5478 -2.8991 403.8271 406.7262 385.3612 295.1749 -2.8976 403.6479 406.5455 385.1677 296.7693 -2.8890 403.4894 406.3783 384.9713 298.3811 -2.8868 403.3268 406.2136 384.7908 299.9805 -2.8836 403.1746 406.0582 384.5851 301.5934 -2.8760 403.0079 405.8839 384.3912 303.2034 -2.8698 402.8400 405.7098 384.2017 304.8029 -2.8613 402.6894 405.5508 383.9948 306.4056 -2.8586 402.5167 405.3752 383.7952 308.0084 -2.8499 402.3592 405.2091 383.5881 309.6086 -2.8432 402.1845 405.0277 383.3875 311.2203 -2.8383 402.0109 404.8491 383.1838 312.8360 -2.8331 401.8389 404.6720 382.9722 314.4483 -2.8252 401.6737 404.4989 382.7593 316.0481 -2.8188 401.5221 404.3409 382.5682 317.6488 -2.8142 401.3500 404.1642 382.3635 319.2446 -2.8065 401.1877 403.9942 382.1500 320.8585 -2.8012 401.0160 403.8172 381.9363 322.7769 -2.7918 400.8042 403.5960 381.7091 324.5591 -2.7902 400.6084 403.3986 381.4579 326.1665 -2.7825 400.4453 403.2278 381.2535 327.7713 -2.7750 400.2905 403.0655 381.0570 329.3771 -2.7744 400.1278 402.9022 380.8520 330.9756 -2.7678 399.9351 402.7029 380.6499 332.5911 -2.7593 399.7643 402.5236 380.4430 334.2078 -2.7553 399.5856 402.3409 380.2414 335.8476 -2.7476 399.4196 402.1672 380.0267 337.6009 -2.7406 399.2335 401.9742 379.8131 339.2264 -2.7340 399.0602 401.7942 379.6066 340.8238 -2.7267 398.8832 401.6099 379.4284 342.4223 -2.7193 398.7086 401.4279 379.2223 344.0315 -2.7155 398.5510 401.2665 379.0342 345.6395 -2.7088 398.3705 401.0792 378.8335 347.2516 -2.7076 398.1990 400.9067 378.6332 348.8479 -2.7031 398.0413 400.7445 378.4590 350.4586 -2.6994 397.8707 400.5701 378.2475 352.0530 -2.6937 397.7049 400.3987 378.0433 353.6796 -2.6882 397.5145 400.2027 377.8483 355.2770 -2.6837 397.3167 400.0004 377.6275 356.8735 -2.6814 397.1557 399.8371 377.4093 358.4856 -2.6726 397.0011 399.6737 377.2120 360.0855 -2.6691 396.7972 399.4662 376.9893 361.6953 -2.6643 396.6273 399.2916 376.7793 363.3068 -2.6639 396.4425 399.1064 376.5645 364.9180 -2.6548 396.2654 398.9202 376.3511 366.5166 -2.6488 396.0979 398.7467 376.1343 368.1096 -2.6431 395.9271 398.5703 375.9311 369.7251 -2.6385 395.7538 398.3923 375.7064 371.3410 -2.6303 395.5719 398.2023 375.4884 372.9370 -2.6238 395.3921 398.0159 375.2881 374.5499 -2.6161 395.2039 397.8200 375.0901 376.1449 -2.6045 395.0241 397.6287 374.8783 377.7454 -2.6014 394.8616 397.4630 374.6588 379.3605 -2.5996 394.6712 397.2709 374.4409 380.9733 -2.5911 394.4999 397.0910 374.2415 382.5758 -2.5821 394.3095 396.8917 374.0298 384.1885 -2.5786 394.1280 396.7066 373.8313 385.7776 -2.5714 393.9586 396.5301 373.6064 387.3904 -2.5649 393.7793 396.3442 373.4075 388.9885 -2.5629 393.5883 396.1512 373.1864 390.6044 -2.5561 393.4019 395.9580 372.9847 392.2063 -2.5488 393.2295 395.7783 372.8022 393.8046 -2.5416 393.0425 395.5841 372.5845 395.4226 -2.5339 392.8572 395.3911 372.3912 397.0229 -2.5299 392.6876 395.2175 372.1813 398.6225 -2.5244 392.5175 395.0419 371.9740 400.2215 -2.5188 392.3217 394.8405 371.7703 401.8405 -2.5136 392.1194 394.6330 371.5770 403.4435 -2.5075 391.9397 394.4472 371.3849 405.0580 -2.5033 391.7662 394.2695 371.1841 406.6580 -2.4987 391.5802 394.0788 370.9907 408.2620 -2.4904 391.3988 393.8892 370.7996 409.8666 -2.4840 391.2037 393.6877 370.6001 411.4821 -2.4829 391.0228 393.5057 370.4028 413.0846 -2.4756 390.8480 393.3235 370.2123 414.6835 -2.4699 390.6735 393.1434 370.0118 416.2806 -2.4619 390.4906 392.9525 369.8142 417.8911 -2.4535 390.2925 392.7460 369.6145 419.4906 -2.4481 390.1192 392.5673 369.4471 421.0894 -2.4438 389.9277 392.3715 369.2361 422.7181 -2.4396 389.7415 392.1812 369.0173 424.3285 -2.4306 389.5527 391.9833 368.8109 425.9266 -2.4272 389.3641 391.7913 368.6138 427.5231 -2.4214 389.1739 391.5953 368.4081 429.1285 -2.4159 388.9988 391.4148 368.1993 430.7285 -2.4109 388.8206 391.2315 368.0044 432.3598 -2.4026 388.6481 391.0507 367.7951 433.9600 -2.3963 388.4610 390.8573 367.5799 435.5575 -2.3899 388.2762 390.6662 367.3715 437.1546 -2.3872 388.0853 390.4725 367.1570 438.7783 -2.3815 387.8948 390.2763 366.9350 440.3656 -2.3755 387.7123 390.0878 366.7421 441.9798 -2.3709 387.5112 389.8821 366.5401 443.5843 -2.3628 387.3318 389.6946 366.3178 445.1901 -2.3608 387.1401 389.5009 366.1147 446.7883 -2.3554 386.9626 389.3181 365.9083 448.4038 -2.3449 386.7678 389.1127 365.7167 449.9971 -2.3411 386.5789 388.9199 365.5084 451.6105 -2.3360 386.3827 388.7187 365.3084 453.2235 -2.3300 386.2084 388.5384 365.0928 454.8238 -2.3270 386.0268 388.3537 364.8792 456.4360 -2.3181 385.8330 388.1511 364.6788 458.0355 -2.3130 385.6594 387.9724 364.4706 459.6334 -2.3089 385.4747 387.7836 364.2901 461.2603 -2.3050 385.2758 387.5809 364.0816 462.8545 -2.2993 385.0752 387.3745 363.8862 464.4651 -2.2936 384.8965 387.1901 363.7049 466.0623 -2.2894 384.7145 387.0038 363.4967 467.6731 -2.2851 384.5275 386.8126 363.2918 469.2846 -2.2811 384.3289 386.6100 363.0883 470.8828 -2.2736 384.1457 386.4194 362.8919 472.4818 -2.2730 383.9446 386.2175 362.6784 474.0930 -2.2664 383.7531 386.0195 362.4640 475.7026 -2.2603 383.5699 385.8302 362.2754 477.3143 -2.2556 383.3810 385.6366 362.0576 478.9253 -2.2507 383.1988 385.4495 361.8484 480.5249 -2.2435 383.0003 385.2438 361.6407 482.1225 -2.2357 382.8051 385.0408 361.4340 483.7211 -2.2301 382.6372 384.8673 361.2345 485.3348 -2.2274 382.4473 384.6747 361.0279 486.9329 -2.2232 382.2595 384.4827 360.8149 488.5589 -2.2185 382.0558 384.2743 360.5942 490.1544 -2.2122 381.8757 384.0878 360.3873 491.7525 -2.2064 381.6964 383.9028 360.1832 493.3608 -2.2020 381.5008 383.7028 359.9722 494.9545 -2.1987 381.3152 383.5139 359.7783 496.5845 -2.1911 381.1260 383.3170 359.5598 498.1796 -2.1881 380.9213 383.1094 359.3488 499.8680 -2.1815 380.7220 382.9035 359.1329 501.5960 -2.1806 380.5207 382.7013 358.9128 503.1871 -2.1739 380.3403 382.5142 358.7085 504.8049 -2.1681 380.1639 382.3320 358.5101 506.4078 -2.1642 379.9447 382.1090 358.2921 508.0265 -2.1585 379.7472 381.9056 358.0861 509.6259 -2.1572 379.5691 381.7263 357.8825 511.2300 -2.1507 379.3734 381.5241 357.6725 512.8291 -2.1404 379.1945 381.3349 357.4911 514.4246 -2.1386 379.0050 381.1436 357.2805 516.0551 -2.1336 378.8191 380.9527 357.0666 517.6580 -2.1254 378.5996 380.7250 356.8709 519.2614 -2.1176 378.4267 380.5443 356.6726 520.8615 -2.1127 378.2305 380.3431 356.4912 522.4679 -2.1107 378.0308 380.1415 356.2903 524.0668 -2.1093 377.8532 379.9626 356.0829 525.6664 -2.1093 377.6425 379.7517 355.8896 527.2959 -2.1041 377.4604 379.5645 355.6870 528.8943 -2.0952 377.2649 379.3601 355.4908 530.4935 -2.0896 377.0641 379.1536 355.3103 532.0915 -2.0883 376.9022 378.9904 355.1145 533.7064 -2.0831 376.6996 378.7827 354.9014 535.3068 -2.0772 376.4919 378.5691 354.7086 536.9273 -2.0738 376.3171 378.3909 354.4958 538.5184 -2.0698 376.1132 378.1829 354.3081 540.1259 -2.0644 375.9239 377.9883 354.1028 541.7435 -2.0595 375.7485 377.8081 353.8888 543.3435 -2.0529 375.5438 377.5967 353.6951 544.9431 -2.0500 375.3620 377.4120 353.4907 546.5410 -2.0439 375.1589 377.2029 353.3034 548.1700 -2.0398 374.9435 376.9833 353.1085 549.7691 -2.0329 374.7683 376.8012 352.9046 551.3833 -2.0279 374.5972 376.6251 352.7009 552.9838 -2.0248 374.4038 376.4286 352.4875 554.5846 -2.0194 374.2058 376.2252 352.3094 556.2013 -2.0157 374.0069 376.0225 352.0979 557.8038 -2.0098 373.8011 375.8109 351.9083 559.4033 -2.0062 373.6175 375.6237 351.7106 561.0075 -2.0005 373.4209 375.4215 351.5290 562.6279 -1.9977 373.2238 375.2215 351.3200 564.2183 -1.9956 373.0296 375.0251 351.1081 565.8225 -1.9888 372.8356 374.8244 350.9244 567.4530 -1.9850 372.6466 374.6316 350.7239 569.0535 -1.9803 372.4511 374.4315 350.5286 570.6524 -1.9760 372.2576 374.2335 350.3077 572.2511 -1.9693 372.0710 374.0402 350.1252 573.8649 -1.9671 371.8776 373.8447 349.9091 575.4781 -1.9612 371.6887 373.6499 349.6847 577.0769 -1.9551 371.5023 373.4574 349.4752 578.6765 -1.9497 371.2962 373.2459 349.2732 580.2808 -1.9440 371.0905 373.0345 349.0512 581.8953 -1.9381 370.9013 372.8394 348.8336 583.4930 -1.9328 370.7161 372.6489 348.6098 585.1091 -1.9287 370.5157 372.4444 348.4070 586.7139 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