DTA measure 1olom3 Test Date: 20231121:1124 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.19 s Mass = 1450 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2370 -4.4843 241.6421 246.1264 266.9510 2.0258 -4.4804 241.8637 246.3441 266.8660 2.8748 -4.4587 241.9726 246.4313 266.9335 3.6335 -4.4507 242.1725 246.6232 266.9824 4.4530 -4.4618 242.2766 246.7385 267.0055 5.2738 -4.4655 242.3876 246.8531 266.9653 6.0335 -4.4602 242.4824 246.9426 266.9795 6.8828 -4.4376 242.6557 247.0933 267.1915 7.6723 -4.4447 242.6980 247.1426 266.9292 8.4620 -4.4447 242.8521 247.2968 266.8343 9.2813 -4.4366 243.0099 247.4465 266.9632 10.0705 -4.4221 243.0396 247.4617 266.9882 10.8898 -4.4185 243.1981 247.6166 266.9969 11.6783 -4.4103 243.2886 247.6989 267.0048 12.4670 -4.4029 243.3299 247.7329 267.1636 13.3165 -4.4210 243.4151 247.8361 267.2162 14.0753 -4.4087 243.4600 247.8687 267.2438 14.8948 -4.3919 243.6262 248.0181 267.2374 15.7133 -4.3807 243.7684 248.1491 267.3081 16.4720 -4.3778 243.8301 248.2079 267.3581 17.3205 -4.3815 243.9487 248.3302 267.3722 18.1090 -4.3569 244.1648 248.5218 267.5289 18.8980 -4.3628 244.2862 248.6491 267.6083 19.7465 -4.3551 244.3291 248.6843 267.7416 20.5050 -4.3425 244.3692 248.7117 267.8792 21.3258 -4.3432 244.4718 248.8150 268.0038 22.1145 -4.3365 244.5093 248.8458 268.0732 22.9040 -4.3399 244.6424 248.9823 268.1844 23.7535 -4.3335 244.7893 249.1228 268.3549 24.5123 -4.3055 244.8470 249.1525 268.5210 25.3318 -4.2999 244.9017 249.2015 268.6948 26.1503 -4.3022 244.9375 249.2397 268.8215 26.9090 -4.2971 245.0647 249.3618 268.8330 27.7575 -4.2949 245.2391 249.5340 269.0072 28.5460 -4.2900 245.2770 249.5669 269.2043 29.3345 -4.2807 245.3391 249.6198 269.3940 30.1850 -4.2780 245.4164 249.6944 269.5397 30.9435 -4.2632 245.6277 249.8909 269.7855 31.7620 -4.2786 245.6218 249.9004 269.9385 32.5808 -4.2645 245.7684 250.0329 270.0303 33.3390 -4.2547 245.8439 250.0986 270.1322 34.1878 -4.2470 246.0120 250.2589 270.3606 34.9763 -4.2521 246.1030 250.3551 270.5340 35.7650 -4.2539 246.1687 250.4227 270.5693 36.5835 -4.2410 246.3156 250.5566 270.7747 37.3723 -4.2341 246.4005 250.6346 270.7841 38.1920 -4.2385 246.4729 250.7114 271.0205 39.0103 -4.2521 246.5728 250.8249 271.3041 39.7690 -4.2512 246.6886 250.9398 271.5860 40.6190 -4.2482 246.7975 251.0457 271.7452 41.3783 -4.2425 246.9654 251.2079 271.9397 42.1998 -4.2452 247.0659 251.3111 272.0203 43.0208 -4.2634 247.1308 251.3942 272.2534 43.7800 -4.2820 247.3219 251.6039 272.3296 44.6285 -4.2551 247.4446 251.6997 272.4946 45.4170 -4.2515 247.5494 251.8010 272.6091 46.2068 -4.2476 247.7092 251.9568 272.8073 47.0263 -4.2409 247.5560 251.7969 273.1487 47.8150 -4.2330 247.7170 251.9500 273.2674 48.6615 -4.2383 247.8117 252.0500 273.3673 49.4210 -4.2420 247.8904 252.1324 273.5206 50.2418 -4.2240 248.0201 252.2441 273.7784 51.0303 -4.2257 248.0397 252.2654 273.8767 51.8200 -4.2165 248.1336 252.3501 274.0917 52.6693 -4.2151 248.0309 252.2459 274.2888 53.4280 -4.2279 248.3706 252.5985 274.4400 54.2468 -4.2324 248.4378 252.6702 274.6153 55.0658 -4.2156 248.5772 252.7928 274.7113 55.8253 -4.2295 248.7573 252.9868 274.8318 56.6760 -4.2265 248.8415 253.0680 275.1104 57.4645 -4.2087 248.9635 253.1722 275.1258 58.2533 -4.2121 249.0737 253.2858 275.3175 59.0745 -4.2177 249.2150 253.4326 275.3711 59.8633 -4.2181 249.3362 253.5543 275.3585 60.6820 -4.2231 249.4865 253.7096 275.5688 61.4705 -4.2187 249.4615 253.6802 275.5765 62.2590 -4.1994 249.5279 253.7273 275.7444 63.1098 -4.1916 249.6870 253.8786 275.9649 63.8680 -4.2034 249.6970 253.9004 275.9884 64.6870 -4.2140 249.8972 254.1112 276.1986 65.5053 -4.2295 249.9917 254.2212 276.3395 66.2640 -4.2053 250.2819 254.4872 276.4495 67.1125 -4.1995 250.3624 254.5619 276.6354 67.9015 -4.1909 250.4031 254.5940 276.7021 68.6910 -4.2001 250.4859 254.6860 276.8491 69.5395 -4.2003 250.5801 254.7804 276.9108 70.2980 -4.2034 250.6456 254.8490 277.0381 71.1168 -4.2113 250.7960 255.0073 277.1318 71.9355 -4.2294 250.9232 255.1526 277.3089 72.6940 -4.2045 250.9921 255.1966 277.3470 73.5425 -4.2111 251.0771 255.2882 277.4168 74.3310 -4.2100 251.2153 255.4253 277.5643 75.1200 -4.2190 251.2479 255.4669 277.7087 75.9383 -4.2243 251.4141 255.6384 277.6990 76.7273 -4.2057 251.5531 255.7587 277.6639 77.5478 -4.1970 251.7438 255.9408 277.7920 78.3360 -4.2226 251.8404 256.0630 277.9409 79.1250 -4.2103 251.8842 256.0944 278.0073 79.9743 -4.2071 251.9861 256.1931 278.1272 80.7630 -4.2145 252.0763 256.2909 278.2588 81.5520 -4.2227 252.3079 256.5305 278.4175 82.3708 -4.2101 252.4577 256.6678 278.3211 83.1598 -4.1927 252.5349 256.7276 278.4459 83.9783 -4.2105 252.7405 256.9509 278.6252 84.7668 -4.2203 252.8359 257.0562 278.7676 85.5550 -4.2214 252.9381 257.1595 278.9298 86.4040 -4.2338 253.0077 257.2416 279.1864 87.1620 -4.2205 253.1835 257.4040 279.2949 87.9810 -4.2215 253.2821 257.5037 279.4045 88.7995 -4.2263 253.3652 257.5916 279.5109 89.5580 -4.2252 253.5262 257.7514 279.7277 90.4068 -4.2343 253.5930 257.8274 279.7398 91.1958 -4.2446 253.5687 257.8133 279.8919 91.9850 -4.2365 253.7840 258.0205 280.0262 92.8033 -4.2322 253.9075 258.1397 280.0624 93.5923 -4.2398 254.0420 258.2818 280.3845 94.4120 -4.2480 254.0420 258.2900 280.4572 95.2005 -4.2504 254.1329 258.3833 280.5260 95.9900 -4.2595 254.3027 258.5622 280.6985 96.8403 -4.2672 254.3319 258.5992 280.8606 97.5990 -4.2529 254.4026 258.6555 280.8562 98.4178 -4.2535 254.5089 258.7624 281.0440 99.2378 -4.2721 254.6737 258.9458 281.1964 99.9970 -4.2732 254.7223 258.9955 281.3794 100.8468 -4.2668 254.8882 259.1551 281.4850 101.6365 -4.2621 254.9354 259.1975 281.6914 102.4260 -4.2716 255.0003 259.2718 281.9111 103.2443 -4.2862 255.1420 259.4282 281.9858 104.0335 -4.2716 255.1506 259.4221 282.1763 104.8538 -4.2684 255.2758 259.5442 282.2469 105.6420 -4.2794 255.3480 259.6274 282.4649 106.4310 -4.2982 255.4399 259.7381 282.7104 107.2795 -4.2884 255.5290 259.8174 282.7922 108.0380 -4.2871 255.5947 259.8818 282.8032 108.8568 -4.2851 255.6785 259.9637 282.8601 109.7498 -4.2852 255.7912 260.0764 283.0882 110.6753 -4.2918 255.8332 260.1249 283.1442 111.4633 -4.3093 255.8397 260.1490 283.3340 112.2820 -4.3119 255.9938 260.3057 283.6237 113.0710 -4.3082 256.1225 260.4307 283.7531 113.8610 -4.3132 256.2391 260.5523 283.9293 114.7108 -4.3005 256.3476 260.6481 284.0635 115.4690 -4.3229 256.4235 260.7464 284.2669 116.2880 -4.3374 256.5130 260.8504 284.3414 117.1080 -4.3335 256.6277 260.9612 284.4317 117.8670 -4.3298 256.7106 261.0404 284.5754 118.7165 -4.3180 256.7539 261.0719 284.6557 119.5055 -4.3369 256.8234 261.1603 284.8368 120.2950 -4.3468 256.8530 261.1998 285.0206 121.1133 -4.3503 257.0479 261.3982 285.0485 121.9020 -4.3661 257.0487 261.4148 285.2654 122.7208 -4.3841 257.1293 261.5134 285.4584 123.5090 -4.3786 257.2628 261.6414 285.6003 124.2980 -4.3760 257.3631 261.7391 285.6416 125.1473 -4.3961 257.5605 261.9566 285.7898 125.9060 -4.3905 257.6266 262.0171 285.9826 126.7248 -4.3880 257.7942 262.1822 286.0583 127.5440 -4.4016 257.8293 262.2309 286.3839 128.3030 -4.3967 257.8787 262.2754 286.5529 129.1515 -4.3982 258.0890 262.4872 286.7320 129.9453 -4.4115 258.1425 262.5540 286.8925 130.7510 -4.4195 258.2599 262.6794 287.1819 131.5693 -4.4117 258.4103 262.8220 287.3045 132.3280 -4.4071 258.4082 262.8153 287.4648 133.1765 -4.3876 258.4987 262.8863 287.5631 133.9650 -4.4119 258.5321 262.9440 287.7036 134.7540 -4.4236 258.6811 263.1047 287.8477 135.5723 -4.4236 258.8530 263.2766 287.9539 136.3610 -4.4208 258.8867 263.3075 288.0648 137.1798 -4.4205 259.1007 263.5212 288.0689 137.9680 -4.4370 259.2365 263.6735 288.0544 138.7568 -4.4343 259.3087 263.7430 288.1797 139.6050 -4.4339 259.3523 263.7862 288.3987 140.3408 -4.4389 259.6225 264.0613 288.4993 141.2053 -4.4402 259.5757 264.0158 288.4856 141.9943 -4.4462 259.6711 264.1173 288.4948 142.7830 -4.4579 259.7997 264.2576 288.5693 143.6015 -4.4600 259.8874 264.3474 288.8028 144.3900 -4.4418 260.0066 264.4484 288.7776 145.2090 -4.4613 260.0690 264.5303 289.0121 145.9973 -4.4494 260.1854 264.6348 288.9246 146.7860 -4.4442 260.3609 264.8051 289.0668 147.6348 -4.4528 260.4747 264.9275 289.0631 148.3930 -4.4607 260.5150 264.9757 289.1885 149.2118 -4.4700 260.7029 265.1729 289.2924 150.0303 -4.4639 260.7871 265.2511 289.4663 150.8190 -4.4763 260.8383 265.3146 289.5961 151.6378 -4.4711 261.0269 265.4980 289.7260 152.4260 -4.4714 261.0946 265.5659 289.7602 153.2150 -4.4719 261.2507 265.7226 289.8231 154.0635 -4.4833 261.3879 265.8712 289.8752 154.8220 -4.4891 261.4176 265.9067 290.0545 155.6408 -4.4842 261.6128 266.0970 290.2064 156.4593 -4.4930 261.6258 266.1188 290.1945 157.2180 -4.5082 261.6118 266.1200 290.3962 158.0665 -4.5027 261.7483 266.2510 290.4380 158.8553 -4.4973 261.9117 266.4090 290.6285 159.6450 -4.5110 262.0249 266.5359 290.6869 160.4633 -4.5183 262.0980 266.6163 290.7218 161.2520 -4.5160 262.2331 266.7491 290.9350 162.0708 -4.5217 262.3339 266.8556 291.0392 162.8893 -4.5408 262.3710 266.9119 291.2616 163.6480 -4.5392 262.4287 266.9679 291.4169 164.5008 -4.5389 262.6783 267.2172 291.5540 165.2595 -4.5371 262.8054 267.3425 291.5613 166.0795 -4.5420 262.7957 267.3377 291.7765 166.8985 -4.5274 263.0106 267.5380 291.7669 167.6570 -4.5434 263.0871 267.6305 292.0367 168.5060 -4.5546 263.2492 267.8038 292.1906 169.2948 -4.5528 263.3998 267.9526 292.3552 170.0840 -4.5453 263.3960 267.9412 292.5047 170.9025 -4.5611 263.4209 267.9819 292.6810 171.6910 -4.5571 263.5584 268.1155 292.9611 172.5100 -4.5555 263.7100 268.2655 292.9982 173.3283 -4.5516 263.8757 268.4273 293.0302 174.0870 -4.5484 264.0453 268.5937 293.2683 174.9355 -4.5578 264.0926 268.6504 293.3304 175.7240 -4.5642 264.1470 268.7112 293.4996 176.5130 -4.5758 264.2346 268.8104 293.7826 177.3313 -4.5750 264.4024 268.9774 294.0483 178.1200 -4.5890 264.4383 269.0272 294.1497 178.9398 -4.6017 264.4683 269.0701 294.3729 179.7280 -4.6087 264.5538 269.1625 294.6170 180.5170 -4.5894 264.6398 269.2292 294.7648 181.3675 -4.5976 264.8381 269.4357 294.9331 182.1260 -4.5956 264.9441 269.5397 295.0862 182.9448 -4.6030 265.1136 269.7166 295.3740 183.7638 -4.6092 265.2170 269.8262 295.5185 184.5230 -4.6168 265.2740 269.8908 295.6725 185.3735 -4.6281 265.3896 270.0177 295.7219 186.1633 -4.6194 265.5087 270.1281 295.8922 186.9540 -4.6233 265.5617 270.1849 295.9870 187.7723 -4.6449 265.7137 270.3587 296.2431 188.5613 -4.6404 265.7528 270.3932 296.2945 189.3808 -4.6346 265.8464 270.4810 296.4478 190.1693 -4.6361 266.0699 270.7060 296.5338 190.9590 -4.6618 266.2282 270.8899 296.7155 191.8275 -4.6724 266.2788 270.9513 296.8000 192.5630 -4.6548 266.3666 271.0214 296.9727 193.4120 -4.6645 266.5174 271.1819 297.0723 194.1708 -4.6711 266.6343 271.3054 297.2333 194.9913 -4.6779 266.7512 271.4291 297.4178 195.8105 -4.6857 266.8610 271.5467 297.4670 196.5700 -4.6943 266.8940 271.5882 297.6287 197.4188 -4.7064 267.0314 271.7379 297.7925 198.2085 -4.6963 267.1114 271.8077 297.8995 198.9980 -4.7103 267.2693 271.9796 298.0566 199.8173 -4.7012 267.3564 272.0576 298.0733 200.6065 -4.7125 267.4795 272.1920 298.1597 201.4270 -4.7190 267.6725 272.3915 298.2657 202.2163 -4.7092 267.7503 272.4595 298.3842 203.0080 -4.7196 267.8794 272.5991 298.4801 203.8568 -4.7186 267.8485 272.5671 298.5579 204.6150 -4.7280 268.0998 272.8278 298.6547 205.4338 -4.7444 268.2662 273.0106 298.8591 206.2545 -4.7368 268.3467 273.0836 298.8425 207.0140 -4.7505 268.3878 273.1382 299.1331 207.8625 -4.7585 268.4934 273.2519 299.2035 208.6510 -4.7613 268.5484 273.3098 299.2452 209.4400 -4.7589 268.6353 273.3941 299.3617 210.2588 -4.7450 268.7488 273.4938 299.5042 211.0183 -4.7599 268.9971 273.7569 299.5660 211.8713 -4.7567 269.0032 273.7599 299.6852 212.6600 -4.7593 269.0093 273.7686 299.7138 213.4490 -4.7616 269.2204 273.9821 299.8242 214.2975 -4.7616 269.2725 274.0341 299.9356 215.0560 -4.7835 269.4690 274.2525 300.1651 215.8758 -4.7825 269.5447 274.3272 300.2975 216.6955 -4.7886 269.5904 274.3790 300.3712 217.4575 -4.7970 269.7013 274.4984 300.5362 218.3110 -4.7884 269.9605 274.7489 300.6290 219.0700 -4.7895 270.0133 274.8028 300.7384 219.8885 -4.7904 270.1984 274.9888 300.8283 220.7088 -4.8018 270.2520 275.0538 301.0268 221.4673 -4.7942 270.3582 275.1524 301.1085 222.3168 -4.7836 270.4771 275.2608 301.2091 223.1055 -4.7931 270.5037 275.2967 301.2918 223.8940 -4.8119 270.7024 275.5143 301.5044 224.7430 -4.8133 270.8621 275.6755 301.6201 225.5010 -4.8115 270.9729 275.7843 301.6830 226.3200 -4.8293 271.1637 275.9930 301.8260 227.1423 -4.8369 271.2040 276.0409 301.9501 227.9020 -4.8176 271.2698 276.0874 302.1230 228.7518 -4.8373 271.3987 276.2359 302.3409 229.5100 -4.8429 271.5074 276.3503 302.3832 230.3298 -4.8459 271.5610 276.4068 302.5281 231.1483 -4.8344 271.6195 276.4539 302.6193 231.9070 -4.8394 271.7166 276.5560 302.8619 232.7755 -4.8566 271.8117 276.6683 303.0603 233.5410 -4.8622 271.8714 276.7336 303.2170 234.3598 -4.8630 271.9461 276.8091 303.2988 235.1480 -4.8473 272.2212 277.0685 303.4930 235.9370 -4.8674 272.3563 277.2238 303.6908 236.7855 -4.8669 272.4052 277.2721 303.6939 237.5440 -4.8571 272.4612 277.3183 303.9111 238.3628 -4.8767 272.5176 277.3943 304.0440 239.1813 -4.8730 272.5104 277.3834 304.2284 239.9400 -4.8761 272.6271 277.5032 304.4361 240.7885 -4.8687 272.8122 277.6809 304.4957 241.5770 -4.8718 272.9213 277.7930 304.6258 242.3660 -4.8558 273.1499 278.0057 304.7678 243.1725 -4.8643 273.3116 278.1759 304.8825 243.9660 -4.8781 273.3056 278.1837 305.0099 244.8145 -4.8871 273.3923 278.2794 305.0631 245.5730 -4.8982 273.6053 278.5034 305.1932 246.3918 -4.8918 273.7346 278.6264 305.3496 247.2105 -4.9004 273.7661 278.6665 305.6193 247.9698 -4.8992 273.8827 278.7820 305.7840 248.8190 -4.9129 274.0698 278.9827 305.8847 249.6078 -4.9139 274.1952 279.1091 306.0386 250.3970 -4.9076 274.3535 279.2612 306.1860 251.2155 -4.9168 274.2888 279.2056 306.3321 252.0045 -4.9303 274.4653 279.3956 306.5554 252.8250 -4.9333 274.6931 279.6264 306.6690 253.6435 -4.9386 274.6729 279.6114 306.7077 254.4020 -4.9455 274.6793 279.6248 306.8536 255.2508 -4.9398 274.7734 279.7132 306.8590 256.0393 -4.9524 274.9773 279.9297 307.0281 256.8280 -4.9723 275.0937 280.0660 307.0367 257.6463 -4.9631 275.2122 280.1753 307.2394 258.4360 -4.9657 275.2228 280.1886 307.4402 259.2548 -4.9783 275.3603 280.3386 307.5766 260.0430 -4.9747 275.3995 280.3741 307.7934 260.8320 -4.9755 275.6233 280.5988 307.8183 261.6805 -4.9878 275.7027 280.6905 307.8847 262.4390 -5.0042 275.9002 280.9044 307.9930 263.2578 -4.9985 276.0823 281.0808 308.1685 264.0770 -5.0024 276.2800 281.2824 308.1976 264.8360 -5.0130 276.3913 281.4043 308.3436 265.6855 -5.0287 276.4541 281.4828 308.4361 266.4743 -5.0139 276.6432 281.6571 308.4831 267.2630 -5.0237 276.6899 281.7136 308.6671 268.1115 -5.0230 276.8865 281.9095 308.8187 268.8723 -5.0267 277.0865 282.1132 308.8324 269.6938 -5.0286 277.1469 282.1755 308.9999 270.4820 -5.0336 277.1986 282.2322 309.2131 271.2710 -5.0348 277.4315 282.4663 309.2587 272.1213 -5.0394 277.6737 282.7131 309.4151 272.8800 -5.0408 277.7485 282.7892 309.6302 273.6988 -5.0445 277.8105 282.8549 309.7751 274.5185 -5.0475 277.9159 282.9634 309.8410 275.2778 -5.0611 277.9870 283.0481 309.9337 276.1268 -5.0551 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