DTA measure 1Pb_3 Date: 2024320:132 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 889.12 s Mass = 1386.900 mg data_number = 1106 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0830 0.5881 228.1176 227.5295 265.8884 1.9023 0.5895 228.3739 227.7843 265.8857 2.7220 0.5890 228.6445 228.0555 265.8839 3.4820 0.5864 228.9030 228.3165 265.8891 4.3318 0.5891 229.1462 228.5571 265.8900 5.0928 0.5889 229.3777 228.7889 265.9012 5.9140 0.5888 229.6430 229.0542 265.9111 6.7355 0.5873 229.9079 229.3206 265.9340 7.4975 0.5864 230.1360 229.5496 265.9612 8.3495 0.5834 230.3869 229.8036 266.0033 9.1115 0.5802 230.6363 230.0561 266.0449 9.9333 0.5834 230.8928 230.3094 266.0832 10.7555 0.5850 231.1411 230.5561 266.1587 11.5170 0.5834 231.3784 230.7950 266.2244 12.3690 0.5826 231.6221 231.0395 266.2987 13.1310 0.5809 231.8725 231.2916 266.3784 13.9528 0.5810 232.1278 231.5468 266.4913 14.7753 0.5796 232.3707 231.7911 266.6032 15.5375 0.5787 232.6012 232.0225 266.7011 16.3903 0.5756 232.8515 232.2759 266.8296 17.1525 0.5759 233.0835 232.5076 266.9604 17.9748 0.5750 233.3073 232.7322 267.0882 18.7970 0.5729 233.5507 232.9778 267.2550 19.5595 0.5698 233.7833 233.2136 267.3859 20.4118 0.5670 234.0277 233.4606 267.5409 21.1735 0.5668 234.2606 233.6938 267.7063 21.9958 0.5633 234.4970 233.9337 267.8708 22.8178 0.5594 234.7471 234.1876 268.0458 23.5910 0.5578 234.9613 234.4035 268.2237 24.4138 0.5542 235.2189 234.6647 268.4086 25.2055 0.5537 235.4476 234.8939 268.5920 26.0275 0.5499 235.6848 235.1349 268.7425 26.8195 0.5482 235.9279 235.3797 268.9075 27.6100 0.5451 236.1497 235.6047 269.0892 28.4280 0.5433 236.3709 235.8275 269.2727 29.2160 0.5379 236.5940 236.0561 269.4423 30.0340 0.5339 236.8215 236.2875 269.6146 30.8223 0.5317 237.0449 236.5132 269.7787 31.6120 0.5279 237.2829 236.7549 269.9391 32.4303 0.5225 237.5082 236.9857 270.1031 33.2190 0.5188 237.7354 237.2167 270.2592 34.0388 0.5144 237.9773 237.4630 270.4255 34.8280 0.5084 238.1937 237.6853 270.5699 35.6195 0.5048 238.4038 237.8990 270.7172 36.4710 0.4998 238.6362 238.1364 270.8725 37.2325 0.4963 238.8323 238.3360 271.0111 38.0545 0.4911 239.0571 238.5661 271.1599 38.8465 0.4842 239.2758 238.7916 271.2822 39.6385 0.4824 239.4923 239.0099 271.4127 40.4608 0.4783 239.7422 239.2639 271.5448 41.2528 0.4739 239.9634 239.4895 271.6791 42.0748 0.4648 240.1899 239.7250 271.7953 42.8665 0.4585 240.4040 239.9455 271.9272 43.6608 0.4567 240.6237 240.1670 272.0511 44.4845 0.4501 240.8522 240.4021 272.1669 45.2765 0.4444 241.0525 240.6081 272.2803 46.0985 0.4402 241.2781 240.8379 272.4014 46.8905 0.4339 241.4817 241.0478 272.5145 47.6825 0.4323 241.7021 241.2698 272.6383 48.5045 0.4258 241.9290 241.5032 272.7571 49.2965 0.4192 242.1281 241.7089 272.8547 50.1185 0.4141 242.3568 241.9427 272.9779 50.9105 0.4113 242.5587 242.1474 273.1032 51.7025 0.4061 242.7684 242.3624 273.2140 52.5248 0.3966 242.9918 242.5953 273.3360 53.3175 0.3941 243.2139 242.8198 273.4534 54.1398 0.3883 243.4260 243.0377 273.5964 54.9325 0.3839 243.6358 243.2519 273.7093 55.7235 0.3779 243.8335 243.4556 273.8274 56.5765 0.3726 244.0541 243.6815 273.9757 57.3385 0.3657 244.2534 243.8877 274.1170 58.1608 0.3596 244.4846 244.1250 274.2395 58.9528 0.3537 244.6994 244.3457 274.3546 59.7420 0.3496 244.8984 244.5488 274.4861 60.5900 0.3457 245.1081 244.7624 274.6347 61.3480 0.3391 245.3136 244.9746 274.7461 62.1660 0.3316 245.5086 245.1770 274.8887 62.9850 0.3283 245.7372 245.4089 275.0299 63.7433 0.3209 245.9381 245.6171 275.1535 64.5918 0.3134 246.1437 245.8303 275.2930 65.3803 0.3091 246.3466 246.0375 275.4282 66.1690 0.3041 246.5508 246.2467 275.5483 66.9878 0.2982 246.7690 246.4709 275.6931 67.7485 0.2911 246.9588 246.6678 275.8260 68.6000 0.2830 247.1720 246.8890 275.9809 69.3913 0.2784 247.3637 247.0852 276.1031 70.1825 0.2692 247.5535 247.2843 276.2140 71.0053 0.2640 247.7661 247.5021 276.3474 71.7668 0.2590 247.9724 247.7134 276.4855 72.6190 0.2531 248.1914 247.9383 276.6289 73.4108 0.2455 248.3857 248.1402 276.7542 74.2040 0.2395 248.5709 248.3314 276.8856 75.0313 0.2334 248.7788 248.5455 277.0221 75.7925 0.2264 248.9720 248.7456 277.1571 76.6448 0.2216 249.1749 248.9533 277.2829 77.4065 0.2128 249.3752 249.1624 277.4114 78.2288 0.2023 249.5899 249.3876 277.5364 79.0508 0.1926 249.7767 249.5841 277.6742 79.8125 0.1950 249.9683 249.7733 277.8149 80.6648 0.1811 250.1885 250.0074 277.9595 81.4265 0.1547 250.3665 250.2118 278.0886 82.2488 0.1298 250.5559 250.4262 278.2073 83.0705 0.1203 250.7756 250.6554 278.3461 83.8325 0.1198 250.9525 250.8326 278.4468 84.6848 0.1142 251.1601 251.0460 278.6051 85.4773 0.1057 251.3601 251.2544 278.7417 86.2715 0.0996 251.5509 251.4513 278.8565 87.0935 0.0906 251.7427 251.6521 278.9919 87.8555 0.0815 251.9378 251.8563 279.1192 88.7080 0.0781 252.1332 252.0551 279.2678 89.4705 0.0700 252.3257 252.2557 279.3921 90.2933 0.0655 252.5176 252.4520 279.5176 91.1155 0.0583 252.7116 252.6533 279.6331 91.8775 0.0511 252.9087 252.8576 279.7630 92.7278 0.0427 253.1137 253.0709 279.9050 93.4858 0.0441 253.3032 253.2591 280.0338 94.3048 0.0402 253.4894 253.4492 280.1733 95.1243 0.0401 253.6827 253.6426 280.3080 95.8828 0.0568 253.8525 253.7957 280.4393 96.7310 0.0530 254.0820 254.0290 280.5789 97.4890 0.0460 254.2475 254.2015 280.7106 98.3085 0.0388 254.4286 254.3898 280.8294 99.1273 0.0312 254.6224 254.5912 280.9582 99.8865 0.0305 254.7993 254.7689 281.0804 100.7355 0.0305 255.0109 254.9803 281.2087 101.4990 0.0212 255.1943 255.1731 281.3444 102.3265 0.0154 255.3946 255.3791 281.4866 103.1185 0.0062 255.5726 255.5663 281.6104 103.9105 -0.0011 255.7538 255.7549 281.7233 104.7325 -0.0064 255.9409 255.9473 281.8553 105.5245 -0.0086 256.1338 256.1424 281.9773 106.3465 -0.0176 256.3186 256.3362 282.1208 107.1385 -0.0258 256.4891 256.5150 282.2683 107.9305 -0.0306 256.6651 256.6957 282.3748 108.7525 -0.0341 256.8838 256.9180 282.5146 109.5145 -0.0431 257.0649 257.1079 282.6448 110.3663 -0.0491 257.2644 257.3135 282.7768 111.1583 -0.0554 257.4267 257.4821 282.9027 111.9503 -0.0597 257.6124 257.6721 283.0366 112.7723 -0.0658 257.8194 257.8852 283.1780 113.5338 -0.0733 257.9824 258.0556 283.3085 114.3860 -0.0786 258.1958 258.2744 283.4716 115.1780 -0.0845 258.3491 258.4335 283.6001 115.9695 -0.0906 258.5355 258.6261 283.7316 116.7918 -0.0979 258.7275 258.8254 283.8788 117.5535 -0.1049 258.9019 259.0068 284.0390 118.4058 -0.1120 259.1151 259.2271 284.2001 119.1675 -0.1177 259.2773 259.3950 284.3291 119.9898 -0.1236 259.4636 259.5872 284.4808 120.8118 -0.1317 259.6423 259.7740 284.6509 121.5735 -0.1370 259.8187 259.9557 284.7855 122.4258 -0.1434 259.9962 260.1395 284.9436 123.1875 -0.1496 260.1722 260.3218 285.0836 124.0098 -0.1562 260.3464 260.5026 285.2268 124.8285 -0.1657 260.5506 260.7162 285.3808 125.5968 -0.1692 260.7116 260.8808 285.4990 126.4280 -0.1766 260.8885 261.0651 285.6368 127.1860 -0.1816 261.0613 261.2429 285.7678 128.0340 -0.1917 261.2446 261.4363 285.9035 128.7920 -0.1958 261.4290 261.6249 286.0152 129.6100 -0.2022 261.6000 261.8022 286.1498 130.4285 -0.2073 261.7849 261.9923 286.2730 131.1888 -0.2148 261.9650 262.1798 286.3849 132.0388 -0.2246 262.1684 262.3929 286.5150 132.7980 -0.2304 262.3243 262.5546 286.6324 133.6195 -0.2347 262.4929 262.7276 286.7645 134.4418 -0.2400 262.6640 262.9040 286.8939 135.2035 -0.2454 262.8607 263.1061 287.0146 136.0555 -0.2517 263.0398 263.2915 287.1431 136.8175 -0.2575 263.2169 263.4744 287.2654 137.6398 -0.2659 263.4102 263.6760 287.3983 138.4318 -0.2727 263.5663 263.8390 287.5075 139.2235 -0.2768 263.7258 264.0026 287.6228 140.0458 -0.2829 263.9073 264.1902 287.7516 140.8375 -0.2871 264.0824 264.3695 287.8645 141.6595 -0.2982 264.2705 264.5687 287.9903 142.4515 -0.3036 264.4615 264.7652 288.1108 143.2435 -0.3082 264.6336 264.9418 288.2399 144.0655 -0.3141 264.7905 265.1045 288.3367 144.8575 -0.3189 264.9757 265.2947 288.4649 145.6795 -0.3251 265.1519 265.4770 288.5932 146.4715 -0.3303 265.3306 265.6609 288.7484 147.2635 -0.3389 265.4955 265.8344 288.8888 148.0855 -0.3426 265.6793 266.0218 289.0142 148.8775 -0.3492 265.8372 266.1864 289.1465 149.6995 -0.3554 266.0149 266.3703 289.2777 150.4915 -0.3595 266.1947 266.5542 289.4168 151.2845 -0.3638 266.3780 266.7418 289.5411 152.1068 -0.3723 266.5552 266.9275 289.6882 152.8993 -0.3783 266.7264 267.1048 289.8281 153.7215 -0.3850 266.9052 267.2902 289.9722 154.5138 -0.3928 267.0618 267.4546 290.1262 155.3065 -0.3977 267.2354 267.6331 290.2533 156.1288 -0.4045 267.4018 267.8063 290.4032 156.9170 -0.4075 267.5878 267.9952 290.5494 157.7353 -0.4133 267.7655 268.1788 290.6770 158.5230 -0.4182 267.9191 268.3372 290.8163 159.3110 -0.4246 268.0776 268.5022 290.9695 160.1298 -0.4308 268.2653 268.6961 291.1052 160.9180 -0.4343 268.4266 268.8609 291.2505 161.7373 -0.4420 268.6056 269.0476 291.3868 162.5260 -0.4463 268.7712 269.2174 291.5203 163.3145 -0.4509 268.9390 269.3900 291.6479 164.1635 -0.4585 269.1146 269.5731 291.7959 164.9228 -0.4668 269.2779 269.7447 291.9348 165.7443 -0.4706 269.4593 269.9299 292.0860 166.5365 -0.4755 269.6230 270.0985 292.2240 167.3280 -0.4826 269.7936 270.2763 292.3501 168.1515 -0.4896 269.9551 270.4448 292.5025 168.9425 -0.4950 270.1270 270.6221 292.6384 169.7650 -0.4981 270.2916 270.7898 292.7805 170.5570 -0.5046 270.4618 270.9664 292.9040 171.3488 -0.5131 270.6473 271.1604 293.0346 172.1710 -0.5159 270.8028 271.3188 293.1557 172.9628 -0.5226 270.9645 271.4871 293.2757 173.7848 -0.5282 271.1474 271.6757 293.4132 174.5768 -0.5331 271.3290 271.8620 293.5219 175.3685 -0.5398 271.4825 272.0223 293.6244 176.2208 -0.5464 271.6720 272.2184 293.7568 176.9825 -0.5524 271.8301 272.3824 293.8672 177.8055 -0.5572 272.0132 272.5704 293.9948 178.5978 -0.5623 272.1530 272.7153 294.1178 179.3895 -0.5682 272.3220 272.8902 294.2249 180.2423 -0.5748 272.5097 273.0845 294.3651 181.0045 -0.5796 272.6524 273.2320 294.4843 181.8268 -0.5843 272.8306 273.4149 294.6021 182.6188 -0.5904 273.0010 273.5914 294.7316 183.4105 -0.5943 273.1722 273.7666 294.8577 184.2633 -0.5974 273.3415 273.9388 294.9958 185.0255 -0.6037 273.5009 274.1046 295.1083 185.8475 -0.6083 273.6658 274.2741 295.2442 186.6395 -0.6130 273.8255 274.4385 295.3659 187.4315 -0.6186 274.0019 274.6205 295.5108 188.2828 -0.6240 274.1671 274.7911 295.6606 189.0408 -0.6289 274.3295 274.9584 295.7976 189.8588 -0.6350 274.5033 275.1382 295.9252 190.6770 -0.6408 274.6743 275.3150 296.0521 191.4350 -0.6446 274.8257 275.4703 296.1808 192.2830 -0.6507 275.0033 275.6540 296.3040 193.0710 -0.6544 275.1609 275.8154 296.4536 193.8600 -0.6609 275.3131 275.9740 296.5987 194.6783 -0.6681 275.4845 276.1525 296.7314 195.4370 -0.6713 275.6450 276.3163 296.8701 196.2865 -0.6761 275.8238 276.4999 297.0004 197.0780 -0.6807 275.9737 276.6544 297.1312 197.8688 -0.6856 276.1380 276.8236 297.2751 198.6905 -0.6929 276.3136 277.0065 297.4142 199.4525 -0.6956 276.4688 277.1644 297.5494 200.3045 -0.7047 276.6398 277.3446 297.6760 201.0965 -0.7088 276.8018 277.5105 297.7991 201.8885 -0.7128 276.9565 277.6693 297.9304 202.7105 -0.7203 277.1315 277.8517 298.0607 203.4728 -0.7259 277.2852 278.0111 298.2023 204.3245 -0.7307 277.4642 278.1949 298.3649 205.1165 -0.7328 277.6219 278.3546 298.4957 205.9085 -0.7402 277.7840 278.5243 298.6358 206.7305 -0.7465 277.9564 278.7029 298.7505 207.4950 -0.7500 278.1000 278.8500 298.8791 208.3505 -0.7532 278.2666 279.0198 299.0177 209.1425 -0.7618 278.4441 279.2059 299.1664 209.9345 -0.7642 278.5832 279.3475 299.2893 210.7563 -0.7670 278.7507 279.5177 299.4289 211.5185 -0.7749 278.9025 279.6774 299.5582 212.3703 -0.7795 279.0754 279.8548 299.7000 213.1620 -0.7881 279.2516 280.0398 299.8237 213.9535 -0.7937 279.4096 280.2033 299.9484 214.7763 -0.7964 279.5718 280.3682 300.0918 215.5685 -0.8008 279.7217 280.5225 300.2247 216.3915 -0.8042 279.8962 280.7004 300.3702 217.1838 -0.8103 280.0400 280.8503 300.4883 217.9755 -0.8144 280.2021 281.0165 300.6135 218.7980 -0.8178 280.3708 281.1885 300.7441 219.5905 -0.8222 280.5431 281.3652 300.8726 220.4128 -0.8271 280.6942 281.5213 301.0209 221.2043 -0.8325 280.8603 281.6927 301.1523 221.9930 -0.8367 281.0063 281.8430 301.2905 222.8113 -0.8415 281.1809 282.0224 301.4305 223.5990 -0.8493 281.3368 282.1861 301.5473 224.4170 -0.8520 281.5171 282.3690 301.6906 225.2050 -0.8571 281.6591 282.5162 301.8149 225.9930 -0.8600 281.7997 282.6597 301.9495 226.8120 -0.8651 281.9815 282.8466 302.0744 227.6010 -0.8699 282.1483 283.0182 302.2024 228.4203 -0.8771 282.3164 283.1935 302.3367 229.2100 -0.8834 282.4661 283.3495 302.4725 230.0003 -0.8849 282.6061 283.4910 302.5915 230.8218 -0.8885 282.7694 283.6579 302.7441 231.6138 -0.8928 282.9275 283.8203 302.8671 232.4358 -0.8987 283.0909 283.9895 302.9927 233.2278 -0.9035 283.2571 284.1606 303.1193 234.0195 -0.9078 283.3981 284.3060 303.2803 234.8418 -0.9120 283.5767 284.4887 303.4061 235.6035 -0.9191 283.7265 284.6456 303.5253 236.4558 -0.9226 283.8923 284.8149 303.6774 237.2478 -0.9271 284.0424 284.9695 303.7986 238.0395 -0.9308 284.1996 285.1304 303.9331 238.8618 -0.9338 284.3634 285.2972 304.0608 239.6235 -0.9393 284.5122 285.4516 304.1767 240.4758 -0.9461 284.6793 285.6254 304.3007 241.2678 -0.9474 284.8402 285.7875 304.4398 242.0595 -0.9559 284.9923 285.9482 304.5615 242.8815 -0.9589 285.1463 286.1052 304.6841 243.6435 -0.9614 285.3023 286.2636 304.7982 244.4955 -0.9650 285.4582 286.4232 304.9635 245.2875 -0.9722 285.6290 286.6012 305.0585 246.0805 -0.9791 285.7939 286.7730 305.1852 246.9025 -0.9814 285.9361 286.9175 305.3153 247.6645 -0.9857 286.0855 287.0712 305.4392 248.5165 -0.9914 286.2544 287.2458 305.5851 249.2785 -0.9951 286.4007 287.3958 305.6801 250.1005 -0.9985 286.5741 287.5726 305.7991 250.9223 -1.0007 286.7503 287.7511 305.9398 251.6843 -1.0054 286.8874 287.8928 306.0530 252.5365 -1.0083 287.0209 288.0291 306.1891 253.2988 -1.0142 287.1814 288.1956 306.3069 254.1163 -1.0194 287.3696 288.3890 306.4460 254.9345 -1.0226 287.5135 288.5361 306.5915 255.6923 -1.0325 287.6658 288.6983 306.7241 256.5410 -1.0378 287.8263 288.8641 306.8585 257.2998 -1.0423 287.9661 289.0084 306.9906 258.1190 -1.0483 288.1203 289.1687 307.1480 258.9368 -1.0530 288.2682 289.3212 307.2861 259.6948 -1.0597 288.4330 289.4927 307.4269 260.5438 -1.0649 288.5994 289.6642 307.5829 261.3033 -1.0616 288.7597 289.8213 307.7207 262.1240 -1.0651 288.8908 289.9559 307.8786 262.9445 -1.0743 289.0630 290.1373 308.0241 263.7065 -1.0876 289.2083 290.2959 308.1568 264.5585 -1.0936 289.3831 290.4767 308.3013 265.3205 -1.0978 289.5299 290.6277 308.4438 266.1420 -1.1031 289.6879 290.7910 308.6029 266.9345 -1.1072 289.8553 290.9625 308.7439 267.7265 -1.1120 290.0090 291.1210 308.8750 268.5785 -1.1157 290.1602 291.2759 309.0133 269.3445 -1.1196 290.3103 291.4299 309.1447 270.1660 -1.1228 290.4652 291.5880 309.2894 270.9580 -1.1282 290.6206 291.7488 309.4135 271.7498 -1.1339 290.7672 291.9012 309.5381 272.5720 -1.1379 290.9154 292.0534 309.6637 273.3335 -1.1419 291.0688 292.2107 309.7714 274.1858 -1.1449 291.2242 292.3691 309.9039 274.9778 -1.1472 291.3881 292.5353 310.0422 275.7695 -1.1487 291.5483 292.6970 310.1636 276.5918 -1.1515 291.7061 292.8576 310.2773 277.3535 -1.1559 291.8404 292.9964 310.3948 278.2058 -1.1573 292.0128 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