DTA measure 1Pb_4 Date: 2024320:143 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1146.28 s Mass = 1386.900 mg data_number = 1426 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2680 -0.7603 245.2836 246.0439 266.0710 2.1225 -0.7600 245.4353 246.1953 266.0885 2.9150 -0.7605 245.5947 246.3552 266.1294 3.7075 -0.7582 245.7413 246.4995 266.1438 4.5295 -0.7539 245.9031 246.6570 266.1719 5.2915 -0.7513 246.0529 246.8042 266.2005 6.1440 -0.7456 246.2141 246.9596 266.2197 6.9060 -0.7401 246.3598 247.0999 266.2446 7.7280 -0.7358 246.5246 247.2605 266.2744 8.5500 -0.7311 246.6930 247.4241 266.3174 9.3115 -0.7266 246.8172 247.5439 266.3641 10.1640 -0.7176 246.9799 247.6975 266.4297 10.9560 -0.7154 247.1376 247.8530 266.4757 11.7475 -0.7089 247.2713 247.9802 266.5295 12.5700 -0.7027 247.4253 248.1280 266.5878 13.3325 -0.7002 247.5720 248.2722 266.6648 14.1848 -0.6929 247.7349 248.4278 266.7511 14.9465 -0.6892 247.8768 248.5660 266.8246 15.7673 -0.6863 248.0384 248.7247 266.9222 16.5855 -0.6855 248.2004 248.8859 267.0133 17.3440 -0.6807 248.3281 249.0088 267.1105 18.1920 -0.6779 248.4817 249.1596 267.2145 18.9500 -0.6744 248.6239 249.2983 267.3155 19.7690 -0.6676 248.7552 249.4228 267.4224 20.5873 -0.6634 248.9133 249.5767 267.5473 21.3460 -0.6617 249.0448 249.7065 267.6561 22.1958 -0.6585 249.1994 249.8578 267.7954 22.9453 -0.6602 249.3457 250.0059 267.9051 23.8018 -0.6590 249.4913 250.1503 268.0388 24.5638 -0.6579 249.6308 250.2887 268.1557 25.3860 -0.6536 249.7791 250.4327 268.2931 26.1780 -0.6519 249.9198 250.5717 268.4151 26.9695 -0.6519 250.0651 250.7169 268.5425 27.8218 -0.6495 250.2087 250.8582 268.6748 28.5835 -0.6479 250.3722 251.0201 268.8091 29.4058 -0.6413 250.5233 251.1646 268.9620 30.1978 -0.6396 250.6630 251.3026 269.0882 30.9895 -0.6361 250.7887 251.4248 269.2082 31.8118 -0.6314 250.9470 251.5784 269.3525 32.6035 -0.6295 251.0754 251.7049 269.4808 33.4258 -0.6257 251.2304 251.8561 269.6116 34.2175 -0.6263 251.3718 251.9980 269.7354 35.0095 -0.6243 251.5135 252.1377 269.8419 35.8618 -0.6219 251.6825 252.3044 269.9652 36.6535 -0.6226 251.8197 252.4423 270.0851 37.4455 -0.6256 251.9452 252.5708 270.2063 38.2675 -0.6237 252.0951 252.7188 270.3250 39.0295 -0.6202 252.2349 252.8551 270.4179 39.8815 -0.6211 252.3754 252.9965 270.5483 40.6735 -0.6211 252.5260 253.1470 270.6632 41.4655 -0.6168 252.6730 253.2899 270.7605 42.2878 -0.6171 252.7996 253.4168 270.8923 43.0505 -0.6170 252.9289 253.5459 270.9972 43.9025 -0.6155 253.0885 253.7040 271.0990 44.6945 -0.6133 253.2327 253.8460 271.2124 45.4865 -0.6116 253.3687 253.9803 271.3232 46.3085 -0.6110 253.5134 254.1244 271.4382 47.0698 -0.6126 253.6407 254.2534 271.5448 47.9213 -0.6112 253.7834 254.3946 271.6624 48.7093 -0.6120 253.9481 254.5601 271.7614 49.4975 -0.6133 254.0761 254.6894 271.8654 50.3160 -0.6140 254.2128 254.8268 271.9676 51.0748 -0.6112 254.3676 254.9787 272.0566 51.9245 -0.6121 254.5094 255.1215 272.1601 52.7140 -0.6116 254.6531 255.2647 272.2542 53.5045 -0.6127 254.7827 255.3955 272.3483 54.3258 -0.6137 254.9152 255.5289 272.4429 55.0870 -0.6117 255.0459 255.6576 272.5286 55.9385 -0.6120 255.1856 255.7976 272.6284 56.7005 -0.6188 255.3303 255.9491 272.7296 57.5215 -0.6170 255.4751 256.0921 272.8055 58.3425 -0.6175 255.6119 256.2294 272.9032 59.1045 -0.6139 255.7558 256.3697 272.9951 59.9565 -0.6139 255.8808 256.4946 273.0925 60.7185 -0.6155 256.0192 256.6347 273.1663 61.5403 -0.6166 256.1611 256.7776 273.2700 62.3625 -0.6201 256.3002 256.9203 273.3797 63.1240 -0.6238 256.4430 257.0669 273.4818 63.9760 -0.6235 256.5814 257.2048 273.5948 64.7380 -0.6247 256.7105 257.3352 273.6826 65.5603 -0.6245 256.8414 257.4659 273.7862 66.3818 -0.6248 256.9905 257.6153 273.8964 67.1435 -0.6261 257.1310 257.7571 273.9990 67.9958 -0.6282 257.2764 257.9046 274.0960 68.7575 -0.6291 257.3909 258.0200 274.1989 69.5805 -0.6256 257.5224 258.1480 274.3059 70.4028 -0.6230 257.6760 258.2991 274.4248 71.1645 -0.6255 257.8021 258.4276 274.5207 72.0173 -0.6266 257.9431 258.5697 274.6169 72.7795 -0.6302 258.0850 258.7152 274.7011 73.6018 -0.6330 258.2341 258.8671 274.8094 74.4240 -0.6329 258.3637 258.9966 274.9231 75.1865 -0.6337 258.4837 259.1174 275.0290 76.0385 -0.6346 258.6458 259.2804 275.1516 76.8005 -0.6373 258.7712 259.4084 275.2319 77.6235 -0.6381 258.9041 259.5422 275.3304 78.4455 -0.6370 259.0312 259.6682 275.4353 79.2075 -0.6374 259.1569 259.7943 275.5288 80.0560 -0.6389 259.3075 259.9465 275.6391 80.8140 -0.6354 259.4398 260.0753 275.7398 81.6310 -0.6299 259.5711 260.2011 275.8483 82.4495 -0.6387 259.7088 260.3474 275.9499 83.2090 -0.6475 259.8360 260.4835 276.0429 84.0570 -0.6507 259.9879 260.6387 276.1578 84.8468 -0.6428 260.1004 260.7432 276.2473 85.6373 -0.6427 260.2477 260.8904 276.3608 86.4865 -0.6510 260.3907 261.0417 276.4660 87.2450 -0.6536 260.5181 261.1717 276.5663 88.0655 -0.6597 260.6505 261.3102 276.6551 88.8565 -0.6588 260.7773 261.4361 276.7703 89.6485 -0.6577 260.9028 261.5604 276.8982 90.5008 -0.6559 261.0438 261.6997 276.9983 91.2625 -0.6571 261.1693 261.8264 277.0842 92.0848 -0.6587 261.3144 261.9731 277.2002 92.8765 -0.6587 261.4468 262.1056 277.3152 93.6685 -0.6669 261.5644 262.2313 277.4292 94.5215 -0.6680 261.7156 262.3836 277.5608 95.3445 -0.6738 261.8510 262.5248 277.6702 96.1365 -0.6767 261.9728 262.6495 277.8008 96.9585 -0.6826 262.1175 262.8001 277.9284 97.7505 -0.6858 262.2490 262.9348 278.0495 98.5425 -0.6917 262.3842 263.0759 278.1720 99.3645 -0.6959 262.5170 263.2129 278.3119 100.2475 -0.6903 262.6492 263.3395 278.4464 101.0095 -0.6887 262.7812 263.4699 278.5609 101.8315 -0.6874 262.9236 263.6110 278.6662 102.6258 -0.6862 263.0581 263.7443 278.7885 103.4190 -0.6828 263.1838 263.8667 278.9045 104.2713 -0.6940 263.3134 264.0074 279.0203 105.0328 -0.6962 263.4343 264.1305 279.1315 105.8550 -0.7012 263.5656 264.2668 279.2324 106.6473 -0.7087 263.6876 264.3963 279.3435 107.4395 -0.7132 263.8244 264.5376 279.4518 108.2923 -0.7110 263.9706 264.6816 279.5615 109.0545 -0.7130 264.0878 264.8009 279.6756 109.8775 -0.7152 264.2064 264.9216 279.7773 110.6698 -0.7132 264.3436 265.0568 279.8729 111.4620 -0.7126 264.4895 265.2021 279.9838 112.2808 -0.7130 264.6201 265.3331 280.0781 113.0693 -0.7162 264.7461 265.4624 280.1849 113.8883 -0.7211 264.8871 265.6082 280.2970 114.6765 -0.7274 265.0099 265.7373 280.4031 115.4650 -0.7309 265.1434 265.8743 280.5004 116.2843 -0.7316 265.2626 265.9941 280.6156 117.0735 -0.7356 265.4008 266.1364 280.7133 117.8945 -0.7409 265.5290 266.2698 280.8169 118.6863 -0.7397 265.6501 266.3898 280.9190 119.4778 -0.7475 265.7904 266.5380 281.0138 120.2985 -0.7498 265.9067 266.6565 281.1153 121.0885 -0.7511 266.0301 266.7812 281.2222 121.9108 -0.7564 266.1793 266.9357 281.3176 122.7030 -0.7612 266.3108 267.0720 281.4402 123.4945 -0.7624 266.4430 267.2054 281.5315 124.3168 -0.7588 266.5670 267.3258 281.6253 125.0890 -0.7672 266.6873 267.4545 281.7215 125.9218 -0.7677 266.8391 267.6067 281.8429 126.7135 -0.7715 266.9465 267.7180 281.9409 127.5358 -0.7717 267.0865 267.8582 282.0296 128.3278 -0.7758 267.2229 267.9987 282.1293 129.1195 -0.7797 267.3534 268.1331 282.2277 129.9418 -0.7812 267.4802 268.2614 282.3222 130.7335 -0.7833 267.5899 268.3733 282.4240 131.5558 -0.7854 267.7312 268.5166 282.5247 132.3478 -0.7895 267.8553 268.6448 282.6230 133.1395 -0.7915 267.9913 268.7827 282.7092 133.9615 -0.7920 268.1191 268.9112 282.8116 134.7235 -0.7931 268.2467 269.0398 282.9168 135.5755 -0.7938 268.3848 269.1786 283.0143 136.3675 -0.7978 268.4959 269.2937 283.1077 137.1595 -0.8001 268.6244 269.4245 283.2034 137.9815 -0.8037 268.7799 269.5836 283.3085 138.7435 -0.8066 268.8822 269.6888 283.3973 139.5955 -0.8083 269.0089 269.8172 283.4960 140.3875 -0.8104 269.1390 269.9494 283.5934 141.1795 -0.8139 269.2641 270.0780 283.7033 142.0018 -0.8175 269.4076 270.2252 283.8164 142.7645 -0.8215 269.5329 270.3543 283.9123 143.6165 -0.8250 269.6476 270.4725 284.0188 144.4090 -0.8292 269.7667 270.5959 284.1290 145.1978 -0.8323 269.9059 270.7382 284.2328 146.0163 -0.8315 270.0441 270.8756 284.3599 146.7758 -0.8309 270.1505 270.9814 284.4635 147.6245 -0.8349 270.2905 271.1254 284.5969 148.4128 -0.8387 270.4081 271.2468 284.7235 149.2018 -0.8440 270.5376 271.3816 284.8385 150.0218 -0.8457 270.6629 271.5086 284.9440 150.7818 -0.8518 270.7814 271.6332 285.0542 151.6305 -0.8534 270.9084 271.7618 285.1900 152.4193 -0.8523 271.0242 271.8765 285.3187 153.2100 -0.8576 271.1492 272.0068 285.4375 154.0305 -0.8627 271.2970 272.1596 285.5637 154.7915 -0.8675 271.4101 272.2776 285.6666 155.6435 -0.8732 271.5447 272.4178 285.7883 156.4075 -0.8770 271.6596 272.5366 285.8904 157.2295 -0.8781 271.7822 272.6604 286.0127 158.0513 -0.8780 271.9184 272.7965 286.1330 158.8135 -0.8808 272.0305 272.9112 286.2266 159.6655 -0.8852 272.1615 273.0467 286.3341 160.4273 -0.8890 272.2953 273.1842 286.4423 161.2490 -0.8892 272.4148 273.3041 286.5516 162.0410 -0.8939 272.5296 273.4236 286.6452 162.8330 -0.8897 272.6712 273.5608 286.7325 163.6848 -0.8957 272.8097 273.7055 286.8376 164.4468 -0.9018 272.9235 273.8252 286.9326 165.2688 -0.9007 273.0360 273.9367 287.0345 166.0705 -0.8996 273.1645 274.0641 287.1411 166.8715 -0.9067 273.2852 274.1919 287.2300 167.6938 -0.9125 273.4125 274.3250 287.3200 168.4555 -0.9154 273.5358 274.4513 287.4153 169.3078 -0.9171 273.6668 274.5839 287.5275 170.0695 -0.9193 273.7892 274.7085 287.6049 170.8915 -0.9154 273.9334 274.8488 287.7121 171.7138 -0.9183 274.0495 274.9678 287.8052 172.4755 -0.9210 274.1609 275.0820 287.8770 173.3283 -0.9304 274.3071 275.2374 287.9932 174.0943 -0.9307 274.4121 275.3428 288.0924 174.9175 -0.9350 274.5293 275.4642 288.1969 175.7105 -0.9359 274.6563 275.5923 288.2965 176.5113 -0.9310 274.7784 275.7094 288.3898 177.3340 -0.9385 274.8987 275.8372 288.5008 178.0920 -0.9429 275.0118 275.9546 288.6002 178.9415 -0.9482 275.1561 276.1043 288.7215 179.7300 -0.9495 275.2863 276.2359 288.8125 180.5180 -0.9537 275.3946 276.3483 288.9428 181.3360 -0.9570 275.5291 276.4861 289.0478 182.1240 -0.9578 275.6474 276.6053 289.1395 182.9430 -0.9632 275.7801 276.7433 289.2802 183.7320 -0.9654 275.9121 276.8775 289.3900 184.5213 -0.9664 276.0214 276.9878 289.4954 185.3420 -0.9697 276.1490 277.1188 289.6164 186.1323 -0.9721 276.2869 277.2590 289.7090 186.9535 -0.9743 276.3972 277.3714 289.8402 187.7445 -0.9778 276.5131 277.4909 289.9520 188.5365 -0.9794 276.6411 277.6204 290.0674 189.3585 -0.9783 276.7687 277.7470 290.1872 190.1505 -0.9875 276.8780 277.8655 290.2942 190.9725 -0.9905 277.0100 278.0004 290.4017 191.7645 -0.9920 277.1329 278.1249 290.5219 192.5565 -0.9943 277.2438 278.2382 290.6424 193.3795 -0.9903 277.3849 278.3753 290.7600 194.1715 -0.9976 277.4964 278.4940 290.8716 194.9935 -1.0044 277.6197 278.6240 290.9988 195.7855 -1.0068 277.7398 278.7466 291.1028 196.5775 -1.0106 277.8661 278.8766 291.2185 197.3995 -1.0140 277.9780 278.9920 291.3425 198.1915 -1.0155 278.0893 279.1048 291.4438 199.0135 -1.0153 278.2194 279.2346 291.5376 199.8053 -1.0169 278.3430 279.3599 291.6304 200.5975 -1.0224 278.4711 279.4935 291.7286 201.4200 -1.0287 278.5941 279.6228 291.8439 202.2128 -1.0329 278.7171 279.7500 291.9421 203.0348 -1.0344 278.8320 279.8664 292.0322 203.8270 -1.0378 278.9636 280.0015 292.1478 204.6198 -1.0414 279.0903 280.1316 292.2435 205.4418 -1.0413 279.2229 280.2641 292.3181 206.2335 -1.0456 279.3250 280.3706 292.3995 207.0558 -1.0506 279.4522 280.5028 292.4717 207.8478 -1.0536 279.5692 280.6228 292.5786 208.6393 -1.0502 279.6806 280.7307 292.6761 209.4583 -1.0464 279.8171 280.8635 292.7533 210.2463 -1.0477 279.9362 280.9839 292.8445 211.0668 -1.0493 280.0566 281.1060 292.9492 211.8555 -1.0542 280.1853 281.2395 293.0453 212.6443 -1.0541 280.3064 281.3604 293.1457 213.4633 -1.0580 280.4332 281.4913 293.2433 214.2520 -1.0601 280.5582 281.6182 293.3415 215.0720 -1.0610 280.6779 281.7389 293.4423 215.8638 -1.0648 280.7979 281.8627 293.5559 216.6550 -1.0665 280.8998 281.9663 293.6721 217.4760 -1.0688 281.0365 282.1053 293.7662 218.2378 -1.0713 281.1593 282.2306 293.8608 219.0900 -1.0712 281.2897 282.3609 293.9724 219.8820 -1.0771 281.3984 282.4755 294.0819 220.6738 -1.0798 281.5223 282.6021 294.1697 221.4960 -1.0809 281.6488 282.7297 294.2835 222.2575 -1.0853 281.7578 282.8431 294.3798 223.1100 -1.0941 281.8784 282.9725 294.4935 223.9018 -1.0994 281.9912 283.0906 294.6088 224.6935 -1.1012 282.1131 283.2143 294.7295 225.5158 -1.1025 282.2331 283.3356 294.8358 226.2775 -1.1058 282.3420 283.4478 294.9306 227.1298 -1.1073 282.4593 283.5666 295.0518 227.8915 -1.1097 282.5989 283.7086 295.1560 228.7138 -1.1117 282.7161 283.8279 295.2764 229.5360 -1.1104 282.8472 283.9576 295.3823 230.2985 -1.1125 282.9765 284.0890 295.4870 231.1508 -1.1126 283.1025 284.2151 295.5886 231.9125 -1.1135 283.2164 284.3299 295.6885 232.7348 -1.1168 283.3181 284.4349 295.8234 233.5570 -1.1185 283.4601 284.5785 295.9214 234.3195 -1.1225 283.5784 284.7009 296.0161 235.1720 -1.1252 283.6827 284.8078 296.1302 235.9345 -1.1352 283.8132 284.9484 296.2430 236.7565 -1.1411 283.9255 285.0666 296.3573 237.5485 -1.1440 284.0318 285.1758 296.4568 238.3405 -1.1482 284.1523 285.3005 296.5562 239.1930 -1.1508 284.2791 285.4299 296.6693 239.9555 -1.1516 284.4045 285.5560 296.7662 240.7765 -1.1530 284.5431 285.6961 296.8804 241.5650 -1.1539 284.6586 285.8125 296.9877 242.3540 -1.1561 284.7727 285.9288 297.1067 243.2038 -1.1578 284.8882 286.0460 297.2206 243.9630 -1.1604 284.9992 286.1596 297.3284 244.7833 -1.1627 285.1204 286.2831 297.4286 245.5723 -1.1683 285.2461 286.4144 297.5362 246.3633 -1.1711 285.3857 286.5568 297.6463 247.1833 -1.1730 285.4946 286.6676 297.7599 247.9735 -1.1770 285.5983 286.7753 297.8783 248.7955 -1.1804 285.7132 286.8936 297.9860 249.5875 -1.1830 285.8404 287.0235 298.0908 250.3795 -1.1844 285.9518 287.1362 298.1906 251.2015 -1.1861 286.0884 287.2745 298.2951 251.9635 -1.1901 286.1963 287.3864 298.4033 252.8155 -1.1924 286.3102 287.5027 298.5241 253.6075 -1.1955 286.4281 287.6236 298.6291 254.3995 -1.1960 286.5500 287.7461 298.7382 255.2215 -1.2023 286.6829 287.8851 298.8337 255.9835 -1.2072 286.7918 287.9990 298.9491 256.8355 -1.2078 286.9214 288.1292 299.0576 257.5985 -1.2047 287.0441 288.2489 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