DTA measure 2Pb_3 Date: 2024320:1332 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.31 s Mass = 1386.900 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4145 -4.7208 425.8623 430.5831 423.8771 4.0285 -4.7179 426.0571 430.7750 423.8788 5.6426 -4.7132 426.2677 430.9810 423.8584 7.2425 -4.7278 426.4637 431.1915 423.8123 8.8570 -4.7272 426.6554 431.3826 423.7362 10.4565 -4.7210 426.8440 431.5649 423.6243 12.0853 -4.7182 427.0200 431.7382 423.5026 13.6824 -4.7181 427.2188 431.9369 423.3682 15.2741 -4.7184 427.4070 432.1254 423.1839 16.8831 -4.7138 427.5806 432.2943 422.9835 18.4761 -4.7175 427.7614 432.4790 422.7767 20.0993 -4.7269 427.9433 432.6702 422.5661 21.6930 -4.7297 428.1198 432.8495 422.3577 23.2895 -4.7243 428.2782 433.0024 422.1440 24.9035 -4.7208 428.4498 433.1706 421.9475 26.5021 -4.7321 428.6019 433.3340 421.7376 28.1311 -4.7273 428.7717 433.4990 421.5043 29.7300 -4.7203 428.9367 433.6571 421.2791 31.3288 -4.7186 429.0688 433.7874 421.0747 32.9426 -4.7317 429.2205 433.9522 420.8297 34.5416 -4.7524 429.3651 434.1176 420.6045 36.1715 -4.7534 429.5073 434.2607 420.3708 37.7718 -4.7443 429.6466 434.3909 420.1343 39.3866 -4.7196 429.7810 434.5006 419.9192 40.9856 -4.7122 429.9171 434.6294 419.7194 42.5996 -4.7125 430.0459 434.7583 419.5094 44.2145 -4.7090 430.1570 434.8660 419.3297 45.8130 -4.7101 430.2655 434.9755 419.1605 47.4044 -4.7105 430.3806 435.0911 418.9875 49.0115 -4.7112 430.5054 435.2166 418.8215 50.6030 -4.7114 430.5993 435.3107 418.6595 52.2256 -4.7103 430.7094 435.4197 418.4789 53.8185 -4.7098 430.8164 435.5263 418.3132 55.4146 -4.7103 430.9154 435.6257 418.1321 57.0135 -4.7154 431.0059 435.7213 417.9571 58.6275 -4.7132 431.1002 435.8134 417.7894 60.2416 -4.7161 431.1827 435.8988 417.6101 61.8405 -4.7154 431.2823 435.9977 417.4294 63.4545 -4.7147 431.3547 436.0694 417.2306 65.0535 -4.7155 431.4301 436.1456 417.0260 66.6525 -4.7161 431.5083 436.2244 416.8524 68.2823 -4.7190 431.5766 436.2956 416.6470 69.8813 -4.7175 431.6455 436.3630 416.4619 71.4948 -4.7216 431.7039 436.4255 416.2729 73.0938 -4.7233 431.7567 436.4800 416.0776 74.6926 -4.7251 431.8282 436.5532 415.8840 76.3216 -4.7255 431.8817 436.6072 415.6818 77.9216 -4.7286 431.9363 436.6649 415.4764 79.5310 -4.7291 431.9795 436.7086 415.2635 81.1220 -4.7305 432.0243 436.7548 415.0544 82.7130 -4.7318 432.0641 436.7959 414.8501 84.3350 -4.7323 432.0826 436.8149 414.6361 85.9300 -4.7362 432.1292 436.8654 414.4254 87.5408 -4.7377 432.1576 436.8953 414.2338 89.1386 -4.7387 432.1932 436.9319 414.0279 90.7386 -4.7409 432.2175 436.9584 413.8318 92.3378 -4.7441 432.2491 436.9932 413.6290 93.9688 -4.7452 432.2572 437.0024 413.4422 95.5676 -4.7426 432.2694 437.0120 413.2456 97.1665 -4.7448 432.2808 437.0256 413.0582 98.7806 -4.7473 432.3082 437.0555 412.8491 100.3796 -4.7479 432.3145 437.0624 412.6615 102.0085 -4.7526 432.3146 437.0672 412.4839 103.6075 -4.7556 432.3176 437.0732 412.2965 105.2065 -4.7567 432.3181 437.0748 412.1109 106.8205 -4.7598 432.3147 437.0746 411.8976 108.4195 -4.7601 432.3267 437.0868 411.6839 110.0481 -4.7604 432.2967 437.0571 411.4818 111.6421 -4.7648 432.2857 437.0505 411.2787 113.2334 -4.7661 432.2716 437.0377 411.0788 114.8396 -4.7666 432.2621 437.0287 410.8720 116.4473 -4.7708 432.2444 437.0151 410.6706 118.0555 -4.7719 432.2154 436.9873 410.4662 119.6525 -4.7722 432.2004 436.9726 410.2676 121.2515 -4.7766 432.1712 436.9478 410.0453 122.8655 -4.7778 432.1323 436.9101 409.8485 124.4645 -4.7803 432.1121 436.8924 409.6618 126.0934 -4.7817 432.0775 436.8592 409.4529 127.6919 -4.7808 432.0201 436.8009 409.2673 129.3060 -4.7836 431.9962 436.7798 409.0655 130.9048 -4.7847 431.9466 436.7313 408.8718 132.5188 -4.7882 431.9186 436.7068 408.6888 134.1336 -4.7877 431.8815 436.6692 408.4966 135.7326 -4.7891 431.8148 436.6039 408.2905 137.3466 -4.7933 431.7766 436.5700 408.0839 138.9456 -4.7926 431.7229 436.5155 407.8746 140.5755 -4.7931 431.6525 436.4456 407.6669 142.1754 -4.7954 431.5925 436.3879 407.4573 143.7840 -4.7968 431.5350 436.3318 407.2542 145.3754 -4.7964 431.4864 436.2828 407.0501 146.9675 -4.7972 431.4191 436.2162 406.8346 148.5904 -4.7997 431.3654 436.1651 406.6341 150.1830 -4.7977 431.3063 436.1040 406.4182 151.7945 -4.7976 431.2274 436.0250 406.2260 153.3926 -4.8006 431.1572 435.9578 406.0247 154.9916 -4.8018 431.0734 435.8752 405.8307 156.5905 -4.8023 431.0025 435.8048 405.6183 158.2195 -4.8027 430.9297 435.7323 405.4304 159.8185 -4.8046 430.8625 435.6671 405.2295 161.4175 -4.8031 430.7681 435.5712 405.0330 163.0315 -4.8071 430.6917 435.4989 404.8502 164.6305 -4.8113 430.6022 435.4135 404.6599 166.2594 -4.8095 430.5140 435.3235 404.4712 167.8585 -4.8086 430.4361 435.2447 404.2778 169.4585 -4.8092 430.3535 435.1628 404.0845 171.0578 -4.8095 430.2595 435.0690 403.8650 172.6723 -4.8102 430.1776 434.9878 403.6788 174.2874 -4.8102 430.0728 434.8830 403.4668 175.8899 -4.8103 429.9738 434.7841 403.2618 177.4863 -4.8123 429.8729 434.6852 403.0614 179.0784 -4.8106 429.7730 434.5836 402.8570 180.6856 -4.8118 429.6753 434.4871 402.6529 182.2788 -4.8132 429.5811 434.3943 402.4635 183.9056 -4.8117 429.4796 434.2912 402.2630 185.5036 -4.8095 429.3770 434.1865 402.0532 187.1026 -4.8123 429.2588 434.0711 401.8496 188.7018 -4.8116 429.1682 433.9798 401.6435 190.3156 -4.8086 429.0636 433.8722 401.4450 191.9296 -4.8111 428.9575 433.7686 401.2410 193.5288 -4.8132 428.8363 433.6495 401.0336 195.1426 -4.8105 428.7340 433.5445 400.8449 196.7416 -4.8092 428.6120 433.4212 400.6420 198.3405 -4.8085 428.4989 433.3074 400.4454 199.9703 -4.8079 428.3976 433.2055 400.2287 201.5846 -4.8088 428.2655 433.0743 400.0224 203.1848 -4.8144 428.1455 432.9598 399.8125 204.7849 -4.8090 428.0283 432.8372 399.5919 206.4000 -4.8024 427.8939 432.6963 399.3806 208.0129 -4.7983 427.7774 432.5757 399.1588 209.6045 -4.7952 427.6537 432.4488 398.9454 211.2116 -4.7937 427.5227 432.3163 398.7170 212.8041 -4.7942 427.4093 432.2034 398.5180 214.3965 -4.7922 427.2712 432.0634 398.3052 216.0211 -4.7881 427.1495 431.9377 398.0913 217.6195 -4.7856 427.0285 431.8141 397.8908 219.2178 -4.7844 426.8946 431.6790 397.6794 220.8321 -4.7813 426.7646 431.5459 397.4778 222.4315 -4.7803 426.6281 431.4085 397.2755 224.0451 -4.7755 426.5011 431.2766 397.0787 225.6589 -4.7742 426.3385 431.1127 396.8829 227.2598 -4.7723 426.2107 430.9829 396.6985 228.8598 -4.7699 426.0923 430.8622 396.4932 230.4736 -4.7673 425.9442 430.7115 396.3182 232.0733 -4.7645 425.7951 430.5595 396.1131 233.7028 -4.7626 425.6604 430.4230 395.9135 235.3026 -4.7604 425.5186 430.2790 395.7217 236.9026 -4.7584 425.3843 430.1427 395.5309 238.5171 -4.7560 425.2485 430.0046 395.3411 240.1146 -4.7538 425.1021 429.8559 395.1453 241.7210 -4.7521 424.9478 429.7000 394.9295 243.3270 -4.7507 424.8047 429.5554 394.7229 244.9188 -4.7473 424.6654 429.4127 394.5118 246.5135 -4.7443 424.5178 429.2621 394.3037 248.1303 -4.7422 424.3679 429.1101 394.0774 249.7293 -4.7407 424.2069 428.9476 393.8581 251.3295 -4.7377 424.0595 428.7971 393.6354 252.9285 -4.7368 423.9134 428.6502 393.4265 254.5576 -4.7319 423.7640 428.4959 393.1912 256.1565 -4.7279 423.6141 428.3421 392.9909 257.7555 -4.7256 423.4729 428.1984 392.7845 259.3695 -4.7234 423.2982 428.0215 392.5554 260.9685 -4.7177 423.1402 427.8579 392.3603 262.5975 -4.7152 422.9842 427.6994 392.1529 264.1963 -4.7135 422.8336 427.5471 391.9441 265.7950 -4.7107 422.6795 427.3901 391.7194 267.3940 -4.7092 422.5222 427.2314 391.5190 269.0083 -4.7033 422.3713 427.0746 391.3114 270.6234 -4.6979 422.2044 426.9023 391.1003 272.2343 -4.6969 422.0471 426.7440 390.8959 273.8258 -4.6939 421.8876 426.5815 390.6963 275.4171 -4.6886 421.7291 426.4177 390.5017 277.0231 -4.6890 421.5619 426.2509 390.2938 278.6456 -4.6850 421.4139 426.0990 390.1056 280.2414 -4.6818 421.2375 425.9193 389.9048 281.8386 -4.6796 421.0623 425.7419 389.6925 283.4378 -4.6745 420.9076 425.5821 389.5217 285.0519 -4.6709 420.7439 425.4149 389.3178 286.6656 -4.6674 420.5651 425.2325 389.1180 288.2594 -4.6640 420.4118 425.0758 388.9393 289.8826 -4.6598 420.2447 424.9046 388.7411 291.4818 -4.6558 420.0883 424.7441 388.5480 293.0956 -4.6538 419.9158 424.5697 388.3574 294.6950 -4.6508 419.7584 424.4092 388.1403 296.2945 -4.6478 419.5752 424.2230 387.9220 297.9235 -4.6448 419.4112 424.0560 387.7167 299.5225 -4.6410 419.2465 423.8875 387.4978 301.1368 -4.6377 419.0712 423.7089 387.2780 302.7369 -4.6331 418.9051 423.5383 387.0558 304.3326 -4.6270 418.7201 423.3471 386.8520 305.9536 -4.6240 418.5532 423.1773 386.6438 307.5601 -4.6209 418.3762 422.9972 386.4113 309.1524 -4.6184 418.2056 422.8241 386.2045 310.7599 -4.6140 418.0261 422.6401 386.0012 312.3546 -4.6078 417.8610 422.4688 385.7836 313.9835 -4.6062 417.6902 422.2964 385.5578 315.5825 -4.6017 417.5130 422.1146 385.3503 317.1815 -4.5986 417.3460 421.9446 385.1540 318.7955 -4.5937 417.1601 421.7537 384.9347 320.3946 -4.5870 416.9826 421.5696 384.7166 322.0255 -4.5831 416.8117 421.3948 384.5132 323.6245 -4.5809 416.6458 421.2267 384.3130 325.2228 -4.5759 416.4603 421.0362 384.0983 326.8368 -4.5699 416.2704 420.8403 383.9021 328.4506 -4.5672 416.0925 420.6597 383.7111 330.0648 -4.5608 415.9148 420.4756 383.4920 331.6646 -4.5549 415.7436 420.2985 383.2904 333.2786 -4.5528 415.5755 420.1283 383.1016 334.8781 -4.5490 415.3753 419.9243 382.9031 336.4918 -4.5433 415.2113 419.7546 382.7081 338.0990 -4.5382 415.0324 419.5706 382.5072 339.6900 -4.5363 414.8492 419.3855 382.3204 341.2810 -4.5280 414.6729 419.2009 382.1266 342.8875 -4.5280 414.4986 419.0266 381.9416 344.4955 -4.5241 414.3104 418.8345 381.7536 346.1078 -4.5191 414.1221 418.6412 381.5437 347.7066 -4.5151 413.9343 418.4493 381.3532 349.3056 -4.5121 413.7531 418.2652 381.1432 350.9046 -4.5073 413.5647 418.0720 380.9211 352.5185 -4.4990 413.3800 417.8790 380.7164 354.1326 -4.4973 413.2164 417.7137 380.4922 355.7465 -4.4989 413.0188 417.5177 380.2845 357.3455 -4.4957 412.8372 417.3329 380.0532 358.9445 -4.4884 412.6564 417.1448 379.8448 360.5455 -4.4780 412.4712 416.9492 379.6220 362.1780 -4.4749 412.2797 416.7547 379.3974 363.7785 -4.4684 412.0993 416.5677 379.1889 365.3918 -4.4652 411.9025 416.3677 378.9589 366.9910 -4.4615 411.7224 416.1839 378.7487 368.5895 -4.4563 411.5346 415.9910 378.5451 370.2110 -4.4519 411.3342 415.7861 378.3276 371.8021 -4.4462 411.1573 415.6034 378.1228 373.4084 -4.4410 410.9571 415.3982 377.8890 375.0006 -4.4359 410.7903 415.2262 377.6933 376.5945 -4.4308 410.6156 415.0463 377.4694 378.2195 -4.4257 410.4166 414.8422 377.2549 379.8184 -4.4211 410.2254 414.6465 377.0511 381.4328 -4.4161 410.0421 414.4581 376.8570 383.0318 -4.4107 409.8363 414.2470 376.6457 384.6308 -4.4060 409.6541 414.0601 376.4432 386.2446 -4.4021 409.4686 413.8707 376.2519 387.8588 -4.3974 409.2808 413.6781 376.0450 389.4576 -4.3922 409.0904 413.4826 375.8577 391.0716 -4.3864 408.8879 413.2743 375.6397 392.6706 -4.3815 408.6999 413.0815 375.4354 394.2849 -4.3776 408.5028 412.8804 375.2531 395.8995 -4.3687 408.3297 412.6984 375.0478 397.5138 -4.3665 408.1443 412.5107 374.8547 399.1139 -4.3621 407.9406 412.3026 374.6544 400.7124 -4.3555 407.7500 412.1056 374.4515 402.3199 -4.3532 407.5551 411.9082 374.2636 403.9260 -4.3501 407.3616 411.7118 374.0679 405.5184 -4.3446 407.1762 411.5208 373.8572 407.1264 -4.3369 406.9831 411.3200 373.6539 408.7196 -4.3315 406.7918 411.1233 373.4653 410.3475 -4.3300 406.6019 410.9319 373.2438 411.9465 -4.3226 406.4191 410.7416 373.0402 413.5455 -4.3195 406.2149 410.5344 372.8182 415.1595 -4.3123 406.0165 410.3288 372.6030 416.7585 -4.3074 405.8214 410.1289 372.3669 418.3875 -4.3032 405.6262 409.9294 372.1631 419.9864 -4.2985 405.4420 409.7405 371.9390 421.5999 -4.2909 405.2407 409.5316 371.7287 423.1990 -4.2886 405.0612 409.3498 371.5370 424.7978 -4.2827 404.8751 409.1578 371.2949 426.4268 -4.2753 404.6737 408.9490 371.0903 428.0409 -4.2732 404.4766 408.7497 370.8915 429.6409 -4.2657 404.2933 408.5589 370.6846 431.2446 -4.2625 404.0926 408.3551 370.4760 432.8553 -4.2565 403.9051 408.1616 370.2492 434.4480 -4.2519 403.7037 407.9555 370.0463 436.0559 -4.2470 403.5085 407.7556 369.8464 437.6633 -4.2398 403.3046 407.5444 369.6357 439.2560 -4.2344 403.1148 407.3492 369.4258 440.8661 -4.2308 402.9380 407.1687 369.2259 442.4628 -4.2259 402.7445 406.9704 369.0129 444.0766 -4.2204 402.5319 406.7524 368.8044 445.6909 -4.2134 402.3241 406.5375 368.6153 447.2896 -4.2090 402.1343 406.3433 368.4247 448.9035 -4.2045 401.9319 406.1364 368.2256 450.5025 -4.2048 401.7381 405.9429 368.0254 452.1765 -4.2158 401.5274 405.7431 367.8006 453.8506 -4.1949 401.3330 405.5279 367.6075 455.4795 -4.1874 401.1251 405.3126 367.4138 457.1085 -4.1775 400.9293 405.1068 367.2106 458.7226 -4.1727 400.7260 404.8986 366.9995 460.3229 -4.1698 400.5374 404.7072 366.8101 461.9219 -4.1652 400.3331 404.4982 366.6221 463.5364 -4.1611 400.1275 404.2885 366.4128 465.1515 -4.1570 399.9341 404.0911 366.2018 466.7611 -4.1504 399.7330 403.8834 365.9921 468.3528 -4.1448 399.5319 403.6767 365.7969 469.9444 -4.1391 399.3439 403.4830 365.5783 471.5509 -4.1349 399.1432 403.2782 365.3734 473.1743 -4.1287 398.9446 403.0734 365.1563 474.7693 -4.1236 398.7496 402.8733 364.9433 476.3680 -4.1192 398.5596 402.6789 364.7235 477.9669 -4.1145 398.3489 402.4635 364.5158 479.5808 -4.1082 398.1596 402.2678 364.3065 481.1950 -4.1018 397.9574 402.0593 364.0678 482.8088 -4.0992 397.7641 401.8633 363.8558 484.4076 -4.0998 397.5679 401.6677 363.6384 486.0066 -4.0974 397.3555 401.4529 363.4205 487.6206 -4.0941 397.1720 401.2660 363.2084 489.2354 -4.0906 396.9710 401.0616 362.9889 490.8499 -4.0898 396.7663 400.8562 362.7643 492.4495 -4.0861 396.5729 400.6590 362.5579 494.0490 -4.0776 396.3740 400.4516 362.3243 495.6635 -4.0685 396.1679 400.2364 362.1143 497.2771 -4.0647 395.9665 400.0312 361.8992 498.8840 -4.0565 395.7673 399.8239 361.6844 500.4761 -4.0535 395.5799 399.6334 361.4750 502.0835 -4.0447 395.3632 399.4079 361.2663 503.6765 -4.0367 395.1653 399.2020 361.0600 505.2996 -4.0325 394.9895 399.0220 360.8518 506.8951 -4.0288 394.7867 398.8154 360.6649 508.4935 -4.0227 394.5873 398.6100 360.4434 510.1075 -4.0186 394.3634 398.3819 360.2361 511.7065 -4.0142 394.1707 398.1849 360.0338 513.3355 -4.0066 393.9636 397.9702 359.8328 514.9345 -3.9992 393.7650 397.7642 359.6352 516.5335 -3.9936 393.5727 397.5663 359.4428 518.1473 -3.9864 393.3577 397.3441 359.2284 519.7460 -3.9806 393.1584 397.1390 359.0266 521.3750 -3.9736 392.9701 396.9437 358.8419 522.9736 -3.9640 392.7600 396.7240 358.6456 524.5876 -3.9563 392.5588 396.5151 358.4463 526.1866 -3.9537 392.3624 396.3161 358.2671 527.8013 -3.9541 392.1495 396.1036 358.0767 529.4161 -3.9500 391.9464 395.8963 357.8716 531.0240 -3.9444 391.7530 395.6974 357.6664 532.6156 -3.9387 391.5518 395.4905 357.4690 534.2075 -3.9334 391.3501 395.2835 357.2660 535.8339 -3.9305 391.1601 395.0906 357.0670 537.4425 -3.9253 390.9522 394.8775 356.8381 539.0380 -3.9227 390.7412 394.6639 356.6316 540.6358 -3.9137 390.5382 394.4519 356.4120 542.2496 -3.9070 390.3488 394.2559 356.2020 543.8636 -3.9039 390.1345 394.0384 355.9851 545.4776 -3.8984 389.9367 393.8352 355.7582 547.0766 -3.8926 389.7345 393.6272 355.5399 548.6756 -3.8856 389.5425 393.4280 355.3348 550.2896 -3.8751 389.3115 393.1866 355.1410 551.9044 -3.8694 389.1111 392.9805 354.9247 553.5186 -3.8625 388.9139 392.7764 354.6990 555.1188 -3.8584 388.7240 392.5824 354.4920 556.7193 -3.8571 388.5185 392.3755 354.2869 558.3341 -3.8513 388.3181 392.1694 354.0788 559.9630 -3.8475 388.1054 391.9529 353.8692 561.5631 -3.8443 387.9022 391.7466 353.6609 563.1559 -3.8416 387.7055 391.5471 353.4575 564.7614 -3.8357 387.5135 391.3493 353.2493 566.3544 -3.8326 387.3039 391.1365 353.0390 567.9788 -3.8258 387.0745 390.9003 352.8355 569.5733 -3.8174 386.8960 390.7134 352.6435 571.1698 -3.8123 386.7039 390.5162 352.4433 572.7835 -3.8078 386.5036 390.3113 352.2427 574.3823 -3.8010 386.2917 390.0926 352.0513 576.0114 -3.7968 386.0934 389.8902 351.8364 577.6099 -3.7904 385.8849 389.6754 351.6356 579.2088 -3.7867 385.6764 389.4631 351.4292 580.8228 -3.7791 385.4979 389.2771 351.2407 582.4368 -3.7710 385.2780 389.0490 351.0476 584.0508 -3.7648 385.0675 388.8323 350.8395 585.6498 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